CN110327255A - A kind of mildy wash and preparation method thereof containing fiery numb essential oil - Google Patents
A kind of mildy wash and preparation method thereof containing fiery numb essential oil Download PDFInfo
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- CN110327255A CN110327255A CN201910737483.6A CN201910737483A CN110327255A CN 110327255 A CN110327255 A CN 110327255A CN 201910737483 A CN201910737483 A CN 201910737483A CN 110327255 A CN110327255 A CN 110327255A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/347—Phenols
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/10—Anti-acne agents
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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Abstract
The invention discloses a kind of mildy wash and preparation method thereof containing fiery numb essential oil.The mildy wash includes following raw material: fire fiber crops essential oil, amino acid surfactant, moisturizer, conditioner, pearling agent, chelating agent, preservative, deionized water.The numb essential oil of fire of the present invention is formulated by cannabidiol and fiery sesame oil, fiery sesame oil is the oil plant for being uniquely dissolved in water, it not only has the function of moist moisturizing, the cannabidiol for being practically insoluble in water can also be made sufficiently to dissolve wherein, to generating synergistic effect, make product that there is antibacterial anti-inflammatory, anti-acne to releive, is anti-oxidant and other effects.The present invention uses amino acid surfactant, and cleaning force is moderate, mild non-stimulated, and fire fiber crops essential oil platymiscium source activity ingredient is safe and effective, without side-effects.
Description
Technical field
The invention belongs to skin care fields, and in particular to a kind of mildy wash and preparation method thereof containing fiery numb essential oil.
Background technique
Mildy wash for removing facial excess oil, dirt, cosmetics residue etc., be daily skin care necessary article it
One.Good mildy wash should have both the effect of the protection skin such as cleaning, nutrition, maintenance.It is wound or acne for face to make
The auxiliaring effect that should also have antibacterial anti-inflammatory, anti-acne to releive with crowd, mildy wash.
Hemp also known as fiber crops, Chinese fiber crops, fire fiber crops, mountain silk seedling, jute, have important agricultural, military and medical value.In hemp
Main active cannboid has valuable pharmacological and physiological activity, has separated more than 100 kinds plant source cannboids so far.And
There is antibacterial, anti-inflammatory, anti-acne to releive, is anti-oxidant and to damaging cells for the cannabidiol (abbreviation CBD) of rich content in cannboid
Repair.
Fiery sesame oil is the oily mixture that fructus cannabis is extracted by techniques such as low-temperature cold pressing, subcritical low-temperature extractions, is
The oil plant of water can be uniquely dissolved in.Fiery flaxseed oil is full of nutrition, containing antioxidant, protein, carrotene, phytosterol,
Phosphatide and several mineral materials and a high proportion of essential fatty acid, have anti-inflammatory, anti-agings, moisten moisturizing, handle skin infection,
Skin injury and anti-oxidation efficacy are cured in help.
Patent CN107802530A discloses a kind of composition containing Cannador and its application in cosmetics, should
Invention will be formulated by a certain percentage after hemp plant different parts extract combination with cosmetic, be had obviously to bacterium
It kills, inhibiting effect, the active constituent to play a major role is phenolic substances；Patent CN10919851A discloses Cannador
Or Cannador is added directly to different cosmetics and matched by application of the cannabidiol in removal cicatrix of skin, the invention
Fang Zhong.But the more phenolic substances of content such as cannabidiol belongs to fat-soluble compound in hemp, is practically insoluble in water, and face cleaning
It is mostly water in newborn or other cosmetic formulations, directly addition Cannador or cannabidiol can be reduced into auxiliary material
The solubility of effective component, or even effective component CBD is precipitated, to be not easy to be absorbed by the skin, bioavilability is caused to drop
It is low, its effect cannot be given full play to；Patent CN109276491A discloses a kind of clear acne oil-control of foaming certainly containing Cannador
Face cleaning foam and preparation method thereof, the invention in order to improve the solubility of Cannador in formula, using dipropylene glycol and
Decyl glucoside as solubilizer, but chemicals be excessively used it is unfavorable to skin.
In order to solve the solubility problem of CBD, to reduce use of the chemicals solubilizer in mildy wash formula, the present invention
Fire fiber crops essential oil obtained by being prepared using plant extract cannabidiol and fiery sesame oil, can improve cannabidiol solubility and
The effect of energy collaboration plays fiery sesame oil and many physiological effects of cannabidiol, and really performance antibacterial anti-inflammatory, anti-acne are releived.
Summary of the invention
In view of the above problems and consumer demand, big by improving in conjunction with the unique physiological function of cannabidiol
The solubility of numb diphenol, and then its bioavailability is improved, the present invention provides a kind of mildy wash and its system containing fiery numb essential oil
Preparation Method, product of the present invention can be effectively suppressed various pathogens, anti-inflammatory anti-acne, releive, be anti-oxidant, and cleaning force is moderate, safety
It is without side-effects.
To achieve the above object, the invention adopts the following technical scheme:
(1) a kind of mildy wash containing fiery numb essential oil, be made of the raw material of following weight percent: 0.1%-5% is rich in cannabidiol
(CBD) fire numb essential oil, 10%-30% amino acid surfactant, 1%-10% moisturizer, 0.1%-3% conditioner, 0.1%-3% moisturizing
Grease, 0.1%-2% pearling agent, 0.01%-1% chelating agent, 0.001%-0.1%pH regulator, 0.001%-0.1% preservative, surplus
For deionized water.
Further, the amino acid surfactant is sodium lauroyl sarcosine, sodium lauroyl glutamate, methyl cocoyl
One or more mixtures in acyl taurines sodium, cocaminopropionic acid sodium.
Further, the moisturizer is at least one of glycerol, allantoin, Sodium Hyaluronate.
Further, the conditioner is one of Polyquaternium-10, polyquaternium -52, cation guar gum or more
Kind mixture.
Further, the moisturizing grease is one of olive oil, tea-seed oil, saualane or a variety of mixtures.
Further, the pearling agent is one or both of ethylene glycol monostearate, ethylene glycol double stearate
Mixture.
Further, the chelating agent is disodium ethylene diamine tetraacetate, one or two are mixed in tetrasodium ethylenediamine tetraacetate
Close object.
Further, the preservative is one of sodium benzoate, Phenoxyethanol, potassium sorbate or a variety of mixtures.
Further, the pH adjusting agent can be one or both of citric acid, lactic acid mixture.
(2) method using above-mentioned composition preparation containing fiery numb essential oil mildy wash, comprising the following steps:
S1: dry by required disinfecting utensils.
S2: into reaction kettle plus deionized water, chelating agent, conditioner, stirring obtain solution A to being completely dissolved.
S3: being heated to 70-90 DEG C for solution A, sequentially adds amino acid surfactant, moisturizer, pearling agent, stirring is extremely
It is completely dissolved, obtains solution B.
S4: being cooled to 30-50 DEG C to solution B, fire numb essential oil, moisturizing grease, preservative, pH adjusting agent is added, stirring is extremely
It is completely dissolved, is cooled to 25 DEG C, adjust pH value to 5.5-7.0, filtering and discharging is up to mildy wash.
(3) preparation method of the numb essential oil of the fire, by cannabidiol crystal (99% or more purity) with fiery sesame oil according to certain
Ratio be mixed, be completely dissolved to cannabidiol to get fiery numb essential oil.
(4) content of cannabidiol is 5~60% in the numb essential oil of the fire.
Compared with prior art, beneficial effects of the present invention:
1, cannabidiol and fiery sesame oil belong to industrial hemp converted products, and the two is applied in combination, and does not add any other composition, accord with
Close natural green theory.
2, cannabidiol is practically insoluble in water, and direct use can reduce its bioavilability, is unfavorable for absorption of human body.This hair
It is bright that cannabidiol is dissolved in fiery sesame oil, so that cannabidiol molecule is dispersed in fiery sesame oil, human body is substantially increased to hemp two
The absorption of phenol avoids carrying out solubilising using a large amount of chemicals in formula.
3, the numb essential oil of fire, can improve hemp obtained by the present invention is prepared using plant extract cannabidiol and fiery sesame oil
The solubility of diphenol, and the fiery sesame oil of performance and many physiological effects of cannabidiol can be cooperateed with, really play antibacterial anti-inflammatory, anti-acne is relaxed
Slow effect.
4, the numb essential oil mildy wash of fire of the present invention can effectively inhibit pathogen, have preferable anti-inflammatory anti-acne, improved
The multi-efficiencies such as moisturizing are moistened in quick reaction, and the present invention uses amino acid surfactant, and cleaning force is moderate, mild non-stimulated, fire
Numb essential oil platymiscium source activity ingredient, it is safe and effective, without side-effects.
Specific embodiment
Embodiments of the present invention are described in further detail below with reference to embodiment, following embodiment is merely to illustrate
The present invention, but cannot be used to limit the scope of the invention.
Embodiment 1
(1) preparation of the numb essential oil of fire
5 grams of cannabidiol solid powders are added in 95 grams of fiery sesame oil, are sufficiently stirred, dissolve solid sufficiently to get containing hemp
The numb essential oil of the fire of diphenol 5%.
(2) a kind of mildy wash containing fiery numb essential oil is prepared, steps are as follows:
100 grams of products are prepared, 30 grams of deionized waters, 0.01 gram of EDTA-2Na, 0.1 gram of Polyquaternium-10 is weighed and is added to reaction
In kettle, stirs to being completely dissolved, be then heated to 70 DEG C, 10 grams of sodium lauroyl sarcosines, 1 gram of Sodium Hyaluronate, 0.1 gram are added
Ethylene glycol double stearate, stirring is to being completely dissolved；50 DEG C are cooled to solution, sequentially adds 0.1 gram of fire numb essential oil, 0.1 gram
Olive oil, 0.001 gram of Phenoxyethanol, 0.001 gram of citric acid, stir evenly after being completely dissolved, and surplus adds deionized water to supply, to
Solution is cooled to 25 DEG C, adjusts pH value to 5.5, filtering and discharging is up to mildy wash.
Embodiment 2
(1) preparation of the numb essential oil of fire
15 grams of cannabidiol solid powders are added in 85 grams of fiery sesame oil, are sufficiently stirred, dissolve solid sufficiently to get containing hemp
The numb essential oil of the fire of diphenol 15%.
(2) a kind of mildy wash containing fiery numb essential oil is prepared, steps are as follows:
100 grams of products are prepared, 30 grams of deionized waters, 0.1 gram of EDTA-2Na, 0.5 gram of Polyquaternium-10,0.5 gram of cation are weighed
Guar gum is added in reaction kettle, is stirred to being completely dissolved, is then heated to 75 DEG C, 10 grams of sodium lauroyl glutamates, 5 grams are added
Cocaminopropionic acid sodium, 3 grams of glycerol, 2 grams of allantoins, 0.5 gram of ethylene glycol monostearate, stirring is to being completely dissolved；To molten
Liquid is cooled to 45 DEG C, sequentially adds 1 gram of fire numb essential oil, 0.5 gram of olive oil, 0.5 gram of saualane, 0.01 Keshan potassium sorbate, 0.01
Gram lactic acid, stirs evenly after being completely dissolved, and surplus adds deionized water to supply, and is cooled to 25 DEG C to solution, adjusts pH value to 6.0, mistake
It filters out and expects up to mildy wash.
Embodiment 3
(1) preparation of the numb essential oil of fire
35 grams of cannabidiol solid powders are added in 65 grams of fiery sesame oil, are sufficiently stirred, dissolve solid sufficiently to get containing hemp
The numb essential oil of the fire of diphenol 35%.
(2) a kind of mildy wash containing fiery numb essential oil is prepared, steps are as follows:
100 grams of products are prepared, 30 grams of deionized waters, 0.5 gram of EDTA-4Na, 1 gram of polyquaternium -52,0.5 gram of cationic melon are weighed
You are added in reaction kettle glue, stir to being completely dissolved, are then heated to 80 DEG C, 10 grams of sodium lauroyl glutamates, 10 grams are added
Sodium methyl cocoyl taurate, 3 grams of allantoins, 3 grams of Sodium Hyaluronates, 1 gram of ethylene glycol monostearate are stirred to completely molten
Solution；Be cooled to 45 DEG C to solution, sequentially add the numb essential oils of 2.5 grams of fire, 1 gram of tea-seed oil, 1 gram of saualane, 0.05 gram of sodium benzoate,
0.05 gram of citric acid, stirs evenly after being completely dissolved, and surplus adds deionized water to supply, and is cooled to 25 DEG C to solution, adjusts pH value extremely
6.0, filtering and discharging is up to mildy wash.
Embodiment 4
(1) preparation of the numb essential oil of fire
45 grams of cannabidiol solid powders are added in 55 grams of fiery sesame oil, are sufficiently stirred, dissolve solid sufficiently to get containing hemp
The numb essential oil of the fire of diphenol 45%.
(2) a kind of mildy wash containing fiery numb essential oil is prepared, steps are as follows:
100 grams of products are prepared, 30 grams of deionized waters, 0.5 gram of EDTA-4Na, 1 gram of polyquaternium -52,0.5 gram of cationic melon are weighed
You are added in reaction kettle glue, stir to being completely dissolved, are then heated to 85 DEG C, 15 grams of sodium lauroyl sarcosines, 15 grams are added
Sodium methyl cocoyl taurate, 5 grams of glycerol, 5 grams of Sodium Hyaluronates, 1 gram of ethylene glycol double stearate are stirred to completely molten
Solution；35 DEG C are cooled to solution, sequentially adds 4 grams of fire numb essential oil, 1.5 grams of tea-seed oils, 1.5 grams of olive oil, 0.1 gram of benzoic acid
Sodium, 0.1 gram of lactic acid, stir evenly after being completely dissolved, and surplus adds deionized water to supply, and are cooled to 25 DEG C to solution, adjust pH value extremely
6.5, filtering and discharging is up to mildy wash.
Embodiment 5
(1) preparation of the numb essential oil of fire
60 grams of cannabidiol solid powders are added in 40 grams of fiery sesame oil, are sufficiently stirred, dissolve solid sufficiently to get containing hemp
The numb essential oil of the fire of diphenol 60%.
(2) a kind of mildy wash containing fiery numb essential oil is prepared, steps are as follows:
100 grams of products are prepared, 30 grams of deionized waters, 1 gram of EDTA-2Na, 3 grams of Polyquaternium-10s is weighed and is added in reaction kettle,
Stirring is then heated to 90 DEG C, it is hard that 30 grams of cocaminopropionic acid sodium, 10 grams of glycerol, 2 grams of ethylene glycol lists is added to being completely dissolved
Resin acid ester, stirring is to being completely dissolved；35 DEG C are cooled to solution, sequentially adds 5 grams of fire numb essential oil, 3 grams of saualanes, 0.1 Keshan
Potassium sorbate, 0.1 gram of citric acid, stir evenly after being completely dissolved, and surplus adds deionized water to supply, and are cooled to 25 DEG C to solution, adjust
PH value is to 7.0, and filtering and discharging is up to mildy wash.
The antibacterial effect test of the numb essential oil mildy wash of 6 fire of embodiment
One, experimental material
1, bacterial strain: staphylococcus aureus, Candida albicans, escherichia coli, propionibacterium acnes.
2, test specimen: the product that embodiment 3 is prepared.
Two, experimental method
1, test is by QB/T2738-2012 " evaluation method of daily chemical products antibacterial bacteriostatic effect " 7 .2 antibacterial type daily chemical products
The antibacterial effect method of inspection (suspension quantitative method).
2, in 1:1 (v/v) ratio sterile water dilution test sample, sample after dilution is then taken to act on test organisms
5min, test are repeated 3 times under the conditions of 20 ± 1 DEG C, are averaged.
Three, effect assessment
Sterilizing rate >=90%, product have bactericidal effect；Sterilizing rate >=50%~90%, product have bacteriostasis.
Four, test result
The antibacterial effect of formulation product described in 1 embodiment 3 of table is evaluated
Test result shows that the product has preferable antibacterial effect, the especially antibacterial to the propionibacterium acnes for causing acne
Effect is most obvious.
The anti-acne effect test of the numb essential oil mildy wash of 7 fire of embodiment
1, study subject: clinical manifestation is that a variety of damages such as papule, warts, tubercle, tumour and scar are presented in face, with face
Skin oil soapy feeling person chooses 100 teenagers with above-mentioned symptom and middle aged men and women as study subject.
2, test specimen: product, the commercially available mildy wash of the preparation of 1 ~ embodiment of embodiment 5.
3, application method: warm water cooperates mildy wash face cleaning, daily each 1 time of morning and evening.
4, anti-acne effect evaluation criteria:
Recovery from illness: symptom completely disappears；
Effective: symptom has clear improvement or improves；
Invalid: symptom is without improvement.
5, according to above-mentioned evaluation criterion, the mildy wash for using embodiment 1 ~ 5 to prepare 100 subjects respectively, 4 months
After count curative effect, statistical result is shown in Table 2.
2 anti-acne curative effect statistical result of table
From table 2 it can be seen that product prepared by the embodiment of the present invention 1 ~ 5 has preferable anti-acne effect.
The foregoing is merely the schematical specific embodiments of the present invention, are not intended to limit the scope of the present invention.
To those skilled in the art, it is all without departing from same embodiment made by the technology of the present invention spirit or change in this hair
Within bright protection scope.
Claims (6)
1. a kind of mildy wash and preparation method thereof containing fiery numb essential oil, the mildy wash by following weight percent raw material group
At: 0.1%-5% rich in the numb essential oil of cannabidiol (CBD) fire, 10%-30% amino acid surfactant, 1%-10% moisturizer,
0.1%-3% conditioner, 0.1%-3% moisturizing grease, 0.1%-2% pearling agent, 0.01%-1% chelating agent, 0.001%-0.1%pH are adjusted
Agent, 0.001%-0.1% preservative, surplus are deionized water.
2. a kind of mildy wash and preparation method thereof containing fiery numb essential oil according to claim 1, which is characterized in that the table
Face activating agent is sodium lauroyl sarcosine, sodium lauroyl glutamate, sodium methyl cocoyl taurate, cocaminopropionic acid sodium
In one or more mixtures；The moisturizer is one of glycerol, allantoin, Sodium Hyaluronate or a variety of mixtures；Institute
Stating conditioner is one of Polyquaternium-10, polyquaternium -52, cation guar gum or a variety of mixtures；The soothing oil
Rouge is one of olive oil, tea-seed oil, saualane or a variety of mixtures；The pearling agent is ethylene glycol monostearate, second
One or both of the double stearates of glycol mixture；The chelating agent is disodium ethylene diamine tetraacetate, ethylenediamine tetra-acetic acid
One or both of four sodium mixture；The preservative is one of sodium benzoate, Phenoxyethanol, potassium sorbate or a variety of
Mixture；The pH adjusting agent can be one or both of citric acid, lactic acid mixture.
3. a kind of mildy wash and preparation method thereof containing fiery numb essential oil according to claim 1 or 2, which is characterized in that institute
The method of stating includes the following steps:
S1: dry by required disinfecting utensils；
S2: into reaction kettle plus deionized water, chelating agent, conditioner, stirring obtain solution A to being completely dissolved；
S3: being heated to 70-90 DEG C for solution A, sequentially adds amino acid surfactant, moisturizer, pearling agent, stirs to complete
Dissolution, obtains solution B；
S4: being cooled to 30-50 DEG C to solution B, and fire numb essential oil, moisturizing grease, preservative, pH adjusting agent is added, stirs to complete
Dissolution is cooled to 25 DEG C, adjusts pH value to 5.5-7.0, filtering and discharging is up to mildy wash.
4. a kind of mildy wash and preparation method thereof containing fiery numb essential oil according to claim 1, which is characterized in that the fire
The preparation method of numb essential oil: cannabidiol crystal and fiery sesame oil are mixed according to a certain percentage, complete to cannabidiol
Dissolution is to get fiery numb essential oil.
5. the preparation method of the numb essential oil of fire according to claim 4, which is characterized in that the cannabidiol crystal purity is wanted
Ask 99% or more.
6. the preparation method of the numb essential oil of fire according to claim 4, which is characterized in that cannabidiol in the numb essential oil of fire
Content be 5~60%.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110917053A (en) * | 2019-12-06 | 2020-03-27 | 辉达生物医药（苏州）有限公司 | Anti-inflammatory composition |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110917053A (en) * | 2019-12-06 | 2020-03-27 | 辉达生物医药（苏州）有限公司 | Anti-inflammatory composition |
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Application publication date: 20191015 |
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