CN110327248A - A kind of composition and manufacture craft of no silicone oil conditioning hair - Google Patents
A kind of composition and manufacture craft of no silicone oil conditioning hair Download PDFInfo
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- CN110327248A CN110327248A CN201910717451.XA CN201910717451A CN110327248A CN 110327248 A CN110327248 A CN 110327248A CN 201910717451 A CN201910717451 A CN 201910717451A CN 110327248 A CN110327248 A CN 110327248A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/463—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfuric acid derivatives, e.g. sodium lauryl sulfate
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
- A61K8/4913—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having five membered rings, e.g. pyrrolidone carboxylic acid
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
- A61K2800/34—Free of silicones
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
A kind of composition and manufacture craft of no silicone oil conditioning hair, formula include: quaternary ammonium salt -91, the bent ammonium methyl sulphate in west, cetostearyl alcohol, PEG-60 almond glyceride type, hydroxypropyl-trimethyl ammonium chloride hydrolytic collagen, water, butanediol, lysine, histidine, arginine, aspartic acid, threonine, serine, glutamic acid, proline, glycine, alanine, valine, isoleucine, leucine, tyrosine and phenylalanine；It will not cause scalp itch, the generation of alopecia because of silicon；The wherein addition of amino acid various in formula, provides required nutrition for hair, is beneficial to prevent alopecia, and wherein compound can improve the pliability of hair and prevent hair scale pad wear；Wherein hydroxypropyl-trimethyl ammonium chloride hydrolytic collagen improves hair various aspects of performance；Compounding subassembly of the invention has good moisturizing, anti-dandruff, nutrition and black hair effect, and mild, non-stimulated, has no adverse effects to scalp and hair.
Description
Technical field
The present invention relates to shampoo technical field, the specially a kind of composition and manufacture craft of no silicone oil conditioning hair.
Background technique
Shampoo also known as shampoo, shampoo or hair cream are the hair shampoo articles being most widely used at present, and
One of most common hair cosmetic, for cleaning the grease of human secretory being attached on scalp and hair, sweat mixed with dirt, on scalp
Cell and external dust, microorganism, the residue of approved product and bad smell for falling off etc. keep scalp and hair clear
Clean and hair is beautiful；All it is called the ingredient of " dimethyl silicone polymer " in ninety percent shampoo containing one kind on the market at present, this
Kind substance is exactly smooth dose of so-called silicone oil.Due to the chemical substance of this silicon or dimethyl siloxane, between hair scale piece
Gap fill up, so it is very smooth for washing hair after head, but due to the impermeability and inertia of silicon, can block pores, hold
Scalp itch or even alopecia, hair loss etc. easily are made one, and shampoo moisturizing on existing market, anti-dandruff, nutrition and other effects are general,
The manufacture craft of shampoo is not standardized, so that the active principle in shampoo is more easily damaged, therefore designs one kind
The composition and manufacture craft of no silicone oil conditioning hair are meaningful.
Summary of the invention
The purpose of the present invention is to provide the compositions and manufacture craft of a kind of no silicone oil conditioning hair, to solve above-mentioned back
The problem of being proposed in scape technology.
In order to solve the above technical problem, the present invention provides following technical solutions: a kind of combination of no silicone oil conditioning hair
Object, formula include: quaternary ammonium salt -91, west bent ammonium methyl sulphate, cetostearyl alcohol, PEG-60 almond glyceride type, hydroxypropyl three
Ammonio methacrylate hydrolytic collagen, water, butanediol, lysine, histidine, arginine, aspartic acid, threonine, serine, paddy ammonia
Acid, proline, glycine, alanine, valine, isoleucine, leucine, tyrosine and phenylalanine, the quality of each component
Percentage composition is respectively: 0.1%-5% quaternary ammonium salt -91, the west 0.1%-5% bent ammonium methyl sulphate, 0.1%-5% cetearyl alcohol
Alcohol, 0.1%-10%PEG-60 almond glyceride type, 0.1%-10% hydroxypropyl-trimethyl ammonium chloride hydrolytic collagen, 0.1%-
10% water, 0.1%-10% butanediol, 0.1%-10% lysine, 0.1%-10% histidine, 0.1%-10% arginine,
0.1%-10% aspartic acid, 0.1%-10% threonine, 0.1%-10% serine, 0.1%-10% glutamic acid, 0.1%-
10% proline, 0.1%-10% glycine, 0.1%-10% alanine, 0.1%-10% valine, 0.1%-10% are different bright
Propylhomoserin, 0.1%-10% leucine, 0.1%-10% tyrosine and 0.1%-10% phenylalanine.
A kind of manufacture craft of the composition of no silicone oil conditioning hair, includes the following steps, step 1, raw material weighs；
Step 2, the preparation of A phase solution；Step 3, the preparation of B phase solution；Step 4, finished product mixing；Step 5, finished product detection packaging；
Wherein in above-mentioned steps one, the mass percentage according to each component be respectively 0.1%-5% quaternary ammonium salt -91,
The bent ammonium methyl sulphate in the west 0.1%-5%, 0.1%-5% cetostearyl alcohol, 0.1%-10%PEG-60 almond glyceride type,
0.1%-10% hydroxypropyl-trimethyl ammonium chloride hydrolytic collagen, 0.1%-10% water, 0.1%-10% butanediol, 0.1%-10%
Lysine, 0.1%-10% histidine, 0.1%-10% arginine, 0.1%-10% aspartic acid, 0.1%-10% threonine,
0.1%-10% serine, 0.1%-10% glutamic acid, 0.1%-10% proline, 0.1%-10% glycine, 0.1%-
10% alanine, 0.1%-10% valine, 0.1%-10% isoleucine, 0.1%-10% leucine, 0.1%-10% junket
Propylhomoserin and 0.1%-10% phenylalanine, and weighed according to the sum of weight percent for 1；
Wherein in above-mentioned steps two, agitated kettle is taken, step 1 is weighed and is weighed in 15% and step 1 of water total weight
The bent ammonium methyl sulphate of quaternary ammonium salt and west be added to agitated kettle, A phase solution is uniformly obtained by agitated kettle stirring and dissolving, is collected
It is spare；
Wherein in above-mentioned steps three, remaining water is added in agitated kettle and is pre-heated to 60 DEG C, then by cetearyl alcohol
Alcohol, almond glyceride type and butanediol are added in agitated kettle together, uniformly obtain B phase solution by agitated kettle stirring and dissolving；
Wherein in above-mentioned steps four, the B phase solution in step 3 is cooled to 50 DEG C, A obtained in step 2 is mixed
Liquid is added in B phase solution, uniformly obtains mixed solution by agitated kettle stirring and dissolving；Mixed solution is cooled to 40 DEG C again,
Weighed hydroxypropyl-trimethyl ammonium chloride hydrolytic collagen in step 1, lysine, histidine, smart ammonia are sequentially added into solution
Acid, aspartic acid, threonine, serine, glutamic acid, proline, glycine, alanine, valine, isoleucine, leucine
Tyrosine and phenylalanine, by agitated kettle stirring and dissolving uniformly and be cooled to room temperature, obtain final mean annual increment solution；
Wherein in above-mentioned steps five, final mean annual increment solution obtained in step 4 is detected, the progress of physical and chemical index qualification
Bottling packing.
According to the above technical scheme, the water in the formula is a kind of deionized water.
According to the above technical scheme, taken in the step 2 agitated kettle using preceding by 100-120 DEG C of condition
Under carry out disinfection sterilization processing, after the completion, dry cooling, spare in the environment of sealing.
According to the above technical scheme, the mixing speed in the step 2 and step 3 be 100r/min, and stir when
Between be 3min.
According to the above technical scheme, it is stirred during formula material sequentially adds using when being added in the step 4
The mode mixed.
According to the above technical scheme, mixing speed is 120r/min in the step 4, and the time stirred is 5min.
According to the above technical scheme, in the step 4 after obtaining final mean annual increment solution, the tune by way of citric acid is added
The Ph to 5.5-6.5 of whole solution.
According to the above technical scheme, the capacity that canned bottle is carried out in the step 5 is 250ml, and canned preceding to bottle
Carry out sterilizing.
Compared with prior art, the beneficial effects obtained by the present invention are as follows being: the invention, it is opposite to be free of with traditional shampoo
Silicon will not cause scalp itch, alopecia, the generation of hair loss because of silicon；The wherein addition of amino acid various in formula, mentions for hair
For required nutrition, it is beneficial to prevent alopecia, wherein compound (quaternary ammonium salt -91, west bent ammonium methyl sulphate, cetearyl alcohol
Alcohol) pliability of hair can be substantially improved；In addition, it also has hair color protection, the protection of hair scale piece, lipophilic active object
Deposition and improvement dry and wet comb the advantage of performance etc.；The pliability of hair can be improved and prevent hair scale pad wear；Wherein hydroxypropyl three
The high performance cation opsonizing agent of ammonio methacrylate hydrolytic collagen, improves hair various aspects of performance；Wherein PEG-60 apricot
Benevolence glyceride type greatly reduces the irritation of ion and amphoteric ion table living body system, maintains the lubricity of grease itself, while easily
In dispersing in water；Compounding subassembly of the invention has good moisturizing, anti-dandruff, nutrition and black hair effect, and mild, nothing
Stimulation, has no adverse effects to scalp and hair, and standardize to manufacture craft preparation process, is strictly controlled to temperature etc.
System, avoids active principle from being destroyed.
Detailed description of the invention
Attached drawing is used to provide further understanding of the present invention, and constitutes part of specification, with reality of the invention
It applies example to be used to explain the present invention together, not be construed as limiting the invention.In the accompanying drawings:
Fig. 1 is the flow chart of manufacture craft of the present invention.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other
Embodiment shall fall within the protection scope of the present invention.
Referring to Fig. 1, the present invention provides a kind of technical solution: a kind of composition and production work of no silicone oil conditioning hair
Skill:
Embodiment 1:
A kind of composition of no silicone oil conditioning hair, formula include: that quaternary ammonium salt -91, the bent ammonium methyl sulphate in west, spermaceti are hard
Lipidol, PEG-60 almond glyceride type, hydroxypropyl-trimethyl ammonium chloride hydrolytic collagen, water, butanediol, lysine, histidine, essence
Propylhomoserin, aspartic acid, threonine, serine, glutamic acid, proline, glycine, alanine, valine, isoleucine, bright ammonia
Acid, tyrosine and phenylalanine, the mass percentage of each component is respectively: 0.1%-5% quaternary ammonium salt -91, the west 0.1%-5%
Bent ammonium methyl sulphate, 0.1%-5% cetostearyl alcohol, 0.1%-10%PEG-60 almond glyceride type, 0.1%-10% hydroxyl
Hydroxypropyltrimonium chloride hydrolytic collagen, 0.1%-10% water, 0.1%-10% butanediol, 0.1%-10% lysine,
0.1%-10% histidine, 0.1%-10% arginine, 0.1%-10% aspartic acid, 0.1%-10% threonine, 0.1%-
10% serine, 0.1%-10% glutamic acid, 0.1%-10% proline, 0.1%-10% glycine, the third ammonia of 0.1%-10%
Acid, 0.1%-10% valine, 0.1%-10% isoleucine, 0.1%-10% leucine, 0.1%-10% tyrosine and
0.1%-10% phenylalanine.
A kind of manufacture craft of the composition of no silicone oil conditioning hair, includes the following steps, step 1, raw material weighs；
Step 2, the preparation of A phase solution；Step 3, the preparation of B phase solution；Step 4, finished product mixing；Step 5, finished product detection packaging；
Wherein in above-mentioned steps one, the mass percentage according to each component is 3% quaternary ammonium salt -91, the bent ammonium in 3% west respectively
Methylsulfate, 3% cetostearyl alcohol, 5%PEG-60 almond glyceride type, 8% hydroxypropyl-trimethyl ammonium chloride hydrolytic collagen,
10% water, 8% butanediol, 4% lysine, 4% histidine, 4% arginine, 4% aspartic acid, 4% threonine, 4% ammonia
Acid, 4% glutamic acid, 4% proline, 4% glycine, 4% alanine, 4% valine, 4% isoleucine, 4% leucine,
4% tyrosine and 4% phenylalanine, and weighed according to the sum of weight percent for 1；
Wherein in above-mentioned steps two, agitated kettle is taken, step 1 is weighed and is weighed in 15% and step 1 of water total weight
The bent ammonium methyl sulphate of quaternary ammonium salt and west be added to agitated kettle, A phase solution is uniformly obtained by agitated kettle stirring and dissolving, is collected
It is spare；
Wherein in above-mentioned steps three, remaining water is added in agitated kettle and is pre-heated to 60 DEG C, then by cetearyl alcohol
Alcohol, almond glyceride type and butanediol are added in agitated kettle together, uniformly obtain B phase solution by agitated kettle stirring and dissolving；
Wherein in above-mentioned steps four, the B phase solution in step 3 is cooled to 50 DEG C, A obtained in step 2 is mixed
Liquid is added in B phase solution, uniformly obtains mixed solution by agitated kettle stirring and dissolving；Mixed solution is cooled to 40 DEG C again,
Weighed hydroxypropyl-trimethyl ammonium chloride hydrolytic collagen in step 1, lysine, histidine, smart ammonia are sequentially added into solution
Acid, aspartic acid, threonine, serine, glutamic acid, proline, glycine, alanine, valine, isoleucine, leucine
Tyrosine and phenylalanine, by agitated kettle stirring and dissolving uniformly and be cooled to room temperature, obtain final mean annual increment solution；
Wherein in above-mentioned steps five, final mean annual increment solution obtained in step 4 is detected, the progress of physical and chemical index qualification
Bottling packing.
Wherein, the water in formula is a kind of deionized water.
Wherein, taken in step 2 agitated kettle using it is preceding by 100-120 DEG C under conditions of carry out disinfection at sterilization
Reason, after the completion, dry cooling, spare in the environment of sealing.
Wherein, the mixing speed in step 2 and step 3 is 100r/min, and the time stirred is 3min.
Wherein, in step 4 during formula material sequentially adds by the way of stirring while adding.
Wherein, mixing speed is 120r/min in step 4, and the time stirred is 5min.
Wherein, in step 4 after obtaining final mean annual increment solution, the Ph to 5.5- of solution is adjusted by way of citric acid is added
6.5。
Wherein, the capacity that canned bottle is carried out in step 5 is 250ml, and canned preceding to bottle progress sterilizing.
Embodiment 2:
A kind of composition of no silicone oil conditioning hair, formula include: that quaternary ammonium salt -91, the bent ammonium methyl sulphate in west, spermaceti are hard
Lipidol, PEG-60 almond glyceride type, hydroxypropyl-trimethyl ammonium chloride hydrolytic collagen, water, butanediol, lysine, histidine, essence
Propylhomoserin, aspartic acid, threonine, serine, glutamic acid, proline, glycine, alanine, valine, isoleucine, bright ammonia
Acid, tyrosine and phenylalanine, the mass percentage of each component is respectively: 0.1%-5% quaternary ammonium salt -91, the west 0.1%-5%
Bent ammonium methyl sulphate, 0.1%-5% cetostearyl alcohol, 0.1%-10%PEG-60 almond glyceride type, 0.1%-10% hydroxyl
Hydroxypropyltrimonium chloride hydrolytic collagen, 0.1%-10% water, 0.1%-10% butanediol, 0.1%-10% lysine,
0.1%-10% histidine, 0.1%-10% arginine, 0.1%-10% aspartic acid, 0.1%-10% threonine, 0.1%-
10% serine, 0.1%-10% glutamic acid, 0.1%-10% proline, 0.1%-10% glycine, the third ammonia of 0.1%-10%
Acid, 0.1%-10% valine, 0.1%-10% isoleucine, 0.1%-10% leucine, 0.1%-10% tyrosine and
0.1%-10% phenylalanine.
A kind of manufacture craft of the composition of no silicone oil conditioning hair, includes the following steps, step 1, raw material weighs；
Step 2, the preparation of A phase solution；Step 3, the preparation of B phase solution；Step 4, finished product mixing；Step 5, finished product detection packaging；
Wherein in above-mentioned steps one, the mass percentage according to each component is 3% quaternary ammonium salt -91, the bent ammonium in 3% west respectively
Methylsulfate, 3% cetostearyl alcohol, 5%PEG-60 almond glyceride type, 8% hydroxypropyl-trimethyl ammonium chloride hydrolytic collagen,
10% water, 8% butanediol, 4% lysine, 4% histidine, 4% arginine, 4% aspartic acid, 4% threonine, 4% ammonia
Acid, 4% glutamic acid, 4% proline, 4% glycine, 4% alanine, 4% valine, 4% isoleucine, 4% leucine,
4% tyrosine and 4% phenylalanine, and weighed according to the sum of weight percent for 1；
Wherein in above-mentioned steps two, agitated kettle is taken, step 1 is weighed and is weighed in 15% and step 1 of water total weight
The bent ammonium methyl sulphate of quaternary ammonium salt and west be added to agitated kettle, A phase solution is uniformly obtained by agitated kettle stirring and dissolving, is collected
It is spare；
Wherein in above-mentioned steps three, remaining water is added in agitated kettle and is pre-heated to 60 DEG C, then by cetearyl alcohol
Alcohol, almond glyceride type and butanediol are added in agitated kettle together, uniformly obtain B phase solution by agitated kettle stirring and dissolving；
Wherein in above-mentioned steps four, the B phase solution in step 3 is cooled to 50 DEG C, A obtained in step 2 is mixed
Liquid is added in B phase solution, uniformly obtains mixed solution by agitated kettle stirring and dissolving；Mixed solution is cooled to 40 DEG C again,
Weighed hydroxypropyl-trimethyl ammonium chloride hydrolytic collagen in step 1, lysine, histidine, smart ammonia are sequentially added into solution
Acid, aspartic acid, threonine, serine, glutamic acid, proline, glycine, alanine, valine, isoleucine, leucine
Tyrosine and phenylalanine, by agitated kettle stirring and dissolving uniformly and be cooled to room temperature, obtain final mean annual increment solution；
Wherein in above-mentioned steps five, final mean annual increment solution obtained in step 4 is detected, the progress of physical and chemical index qualification
Bottling packing.
Wherein, the water in formula is a kind of deionized water.
Wherein, taken in step 2 agitated kettle using it is preceding by 100-120 DEG C under conditions of carry out disinfection at sterilization
Reason, after the completion, dry cooling, spare in the environment of sealing.
Wherein, the mixing speed in step 2 and step 3 is 100r/min, and the time stirred is 3min.
Wherein, in step 4 during formula material sequentially adds by the way of stirring while adding.
Wherein, mixing speed is 120r/min in step 4, and the time stirred is 5min.
Wherein, in step 4 after obtaining final mean annual increment solution, the Ph to 5.5- of solution is adjusted by way of citric acid is added
6.5。
Wherein, the capacity that canned bottle is carried out in step 5 is 250ml, and canned preceding to bottle progress sterilizing.
Embodiment 3:
A kind of composition of no silicone oil conditioning hair, formula include: that quaternary ammonium salt -91, the bent ammonium methyl sulphate in west, spermaceti are hard
Lipidol, PEG-60 almond glyceride type, hydroxypropyl-trimethyl ammonium chloride hydrolytic collagen, water, butanediol, lysine, histidine, essence
Propylhomoserin, aspartic acid, threonine, serine, glutamic acid, proline, glycine, alanine, valine, isoleucine, bright ammonia
Acid, tyrosine and phenylalanine, the mass percentage of each component is respectively: 0.1%-5% quaternary ammonium salt -91, the west 0.1%-5%
Bent ammonium methyl sulphate, 0.1%-5% cetostearyl alcohol, 0.1%-10%PEG-60 almond glyceride type, 0.1%-10% hydroxyl
Hydroxypropyltrimonium chloride hydrolytic collagen, 0.1%-10% water, 0.1%-10% butanediol, 0.1%-10% lysine,
0.1%-10% histidine, 0.1%-10% arginine, 0.1%-10% aspartic acid, 0.1%-10% threonine, 0.1%-
10% serine, 0.1%-10% glutamic acid, 0.1%-10% proline, 0.1%-10% glycine, the third ammonia of 0.1%-10%
Acid, 0.1%-10% valine, 0.1%-10% isoleucine, 0.1%-10% leucine, 0.1%-10% tyrosine and
0.1%-10% phenylalanine.
A kind of manufacture craft of the composition of no silicone oil conditioning hair, includes the following steps, step 1, raw material weighs；
Step 2, the preparation of A phase solution；Step 3, the preparation of B phase solution；Step 4, finished product mixing；Step 5, finished product detection packaging；
Wherein in above-mentioned steps one, the mass percentage according to each component is 4% quaternary ammonium salt -91, the bent ammonium in 4% west respectively
Methylsulfate, 4% cetostearyl alcohol, 6%PEG-60 almond glyceride type, 6% hydroxypropyl-trimethyl ammonium chloride hydrolytic collagen,
10% water, 6% butanediol, 4% lysine, 4% histidine, 4% arginine, 4% aspartic acid, 4% threonine, 4% ammonia
Acid, 4% glutamic acid, 4% proline, 4% glycine, 4% alanine, 4% valine, 4% isoleucine, 4% leucine,
4% tyrosine and 4% phenylalanine, and weighed according to the sum of weight percent for 1；
Wherein in above-mentioned steps two, agitated kettle is taken, step 1 is weighed and is weighed in 15% and step 1 of water total weight
The bent ammonium methyl sulphate of quaternary ammonium salt and west be added to agitated kettle, A phase solution is uniformly obtained by agitated kettle stirring and dissolving, is collected
It is spare；
Wherein in above-mentioned steps three, remaining water is added in agitated kettle and is pre-heated to 60 DEG C, then by cetearyl alcohol
Alcohol, almond glyceride type and butanediol are added in agitated kettle together, uniformly obtain B phase solution by agitated kettle stirring and dissolving；
Wherein in above-mentioned steps four, the B phase solution in step 3 is cooled to 50 DEG C, A obtained in step 2 is mixed
Liquid is added in B phase solution, uniformly obtains mixed solution by agitated kettle stirring and dissolving；Mixed solution is cooled to 40 DEG C again,
Weighed hydroxypropyl-trimethyl ammonium chloride hydrolytic collagen in step 1, lysine, histidine, smart ammonia are sequentially added into solution
Acid, aspartic acid, threonine, serine, glutamic acid, proline, glycine, alanine, valine, isoleucine, leucine
Tyrosine and phenylalanine, by agitated kettle stirring and dissolving uniformly and be cooled to room temperature, obtain final mean annual increment solution；
Wherein in above-mentioned steps five, final mean annual increment solution obtained in step 4 is detected, the progress of physical and chemical index qualification
Bottling packing.
Wherein, the water in formula is a kind of deionized water.
Wherein, taken in step 2 agitated kettle using it is preceding by 100-120 DEG C under conditions of carry out disinfection at sterilization
Reason, after the completion, dry cooling, spare in the environment of sealing.
Wherein, the mixing speed in step 2 and step 3 is 100r/min, and the time stirred is 3min.
Wherein, in step 4 during formula material sequentially adds by the way of stirring while adding.
Wherein, mixing speed is 120r/min in step 4, and the time stirred is 5min.
Wherein, in step 4 after obtaining final mean annual increment solution, the Ph to 5.5- of solution is adjusted by way of citric acid is added
6.5。
Wherein, the capacity that canned bottle is carried out in step 5 is 250ml, and canned preceding to bottle progress sterilizing.
Each embodiment property comparison is as follows:
| Silicone content (%) | Moistening effect | Anti-dandruff effect | Have non-stimulated | |
| Embodiment 1 | 0 | Well | Well | Nothing |
| Embodiment 2 | 0 | Well | Well | Nothing |
| Embodiment 3 | 0 | Well | Well | Nothing |
| Existing shampoo | 12% | Generally | Generally | It is faint |
In conclusion the shampoo of the embodiment of the present invention is not opposite siliceous with traditional shampoo, it is not in scalp hair
Itch, alopecia, the generation of hair loss；Relatively traditional shampoo has good moistening effect and anti-dandruff effect, and does not have stimulation
Property.
It should be noted that, in this document, relational terms such as first and second and the like are used merely to a reality
Body or operation are distinguished with another entity or operation, are deposited without necessarily requiring or implying between these entities or operation
In any actual relationship or order or sequence.Moreover, the terms "include", "comprise" or its any other variant are intended to
Non-exclusive inclusion, so that the process, method, article or equipment including a series of elements is not only wanted including those
Element, but also including other elements that are not explicitly listed, or further include for this process, method, article or equipment
Intrinsic element.Finally, it should be noted that the foregoing is only a preferred embodiment of the present invention, it is not limited to this
Invention, although the present invention is described in detail referring to the foregoing embodiments, for those skilled in the art, according to
It is so possible to modify the technical solutions described in the foregoing embodiments, or part of technical characteristic is equally replaced
It changes.All within the spirits and principles of the present invention, any modification, equivalent replacement, improvement and so on should be included in the present invention
Protection scope within.
Claims (9)
1. a kind of composition of no silicone oil conditioning hair, it is characterised in that: formula includes: quaternary ammonium salt -91, the bent ammonium methylsulfuric acid in west
Salt, cetostearyl alcohol, PEG-60 almond glyceride type, hydroxypropyl-trimethyl ammonium chloride hydrolytic collagen, water, butanediol, lysine,
It is histidine, arginine, aspartic acid, threonine, serine, glutamic acid, proline, glycine, alanine, valine, different bright
The mass percentage of propylhomoserin, leucine, tyrosine and phenylalanine, each component is respectively: 0.1%-5% quaternary ammonium salt -91,
The bent ammonium methyl sulphate in the west 0.1%-5%, 0.1%-5% cetostearyl alcohol, 0.1%-10%PEG-60 almond glyceride type,
0.1%-10% hydroxypropyl-trimethyl ammonium chloride hydrolytic collagen, 0.1%-10% water, 0.1%-10% butanediol, 0.1%-10%
Lysine, 0.1%-10% histidine, 0.1%-10% arginine, 0.1%-10% aspartic acid, 0.1%-10% threonine,
0.1%-10% serine, 0.1%-10% glutamic acid, 0.1%-10% proline, 0.1%-10% glycine, 0.1%-
10% alanine, 0.1%-10% valine, 0.1%-10% isoleucine, 0.1%-10% leucine, 0.1%-10% junket
Propylhomoserin and 0.1%-10% phenylalanine.
2. a kind of manufacture craft of the composition of no silicone oil conditioning hair, includes the following steps, step 1, raw material weighs；Step
Rapid two, A phase solution preparation；Step 3, the preparation of B phase solution；Step 4, finished product mixing；Step 5, finished product detection packaging；It is special
Sign is:
Wherein in above-mentioned steps one, the mass percentage according to each component is 0.1%-5% quaternary ammonium salt -91,0.1%- respectively
5% west bent ammonium methyl sulphate, 0.1%-5% cetostearyl alcohol, 0.1%-10%PEG-60 almond glyceride type, 0.1%-
10% hydroxypropyl-trimethyl ammonium chloride hydrolytic collagen, 0.1%-10% water, 0.1%-10% butanediol, 0.1%-10% rely ammonia
Acid, 0.1%-10% histidine, 0.1%-10% arginine, 0.1%-10% aspartic acid, 0.1%-10% threonine,
0.1%-10% serine, 0.1%-10% glutamic acid, 0.1%-10% proline, 0.1%-10% glycine, 0.1%-
10% alanine, 0.1%-10% valine, 0.1%-10% isoleucine, 0.1%-10% leucine, 0.1%-10% junket
Propylhomoserin and 0.1%-10% phenylalanine, and weighed according to the sum of weight percent for 1；
Wherein in above-mentioned steps two, agitated kettle is taken, step 1 is weighed into weighed season in 15% and step 1 of water total weight
The bent ammonium methyl sulphate of ammonium salt and west is added to agitated kettle, uniformly obtains A phase solution by agitated kettle stirring and dissolving, collects standby
With；
Wherein in above-mentioned steps three, remaining water is added in agitated kettle and is pre-heated to 60 DEG C, then by cetostearyl alcohol, apricot
Benevolence glyceride type and butanediol are added in agitated kettle together, uniformly obtain B phase solution by agitated kettle stirring and dissolving；
Wherein in above-mentioned steps four, the B phase solution in step 3 is cooled to 50 DEG C, A phase solution obtained in step 2 is added
Enter into B phase solution, mixed solution is uniformly obtained by agitated kettle stirring and dissolving；Mixed solution is cooled to 40 DEG C again, Xiang Rong
Weighed hydroxypropyl-trimethyl ammonium chloride hydrolytic collagen, lysine, histidine, arginine, day in step 1 are sequentially added in liquid
Aspartic acid, threonine, serine, glutamic acid, proline, glycine, alanine, valine, isoleucine, leucine tyrosine
And phenylalanine, by agitated kettle stirring and dissolving uniformly and be cooled to room temperature, obtain final mean annual increment solution；
Wherein in above-mentioned steps five, final mean annual increment solution obtained in step 4 is detected, physical and chemical index qualification bottle
Packaging.
3. a kind of composition of no silicone oil conditioning hair according to claim 1, it is characterised in that: the water in the formula
For a kind of deionized water.
4. a kind of manufacture craft of the composition of no silicone oil conditioning hair according to claim 2, it is characterised in that: described
Taken in step 2 agitated kettle using it is preceding by 100-120 DEG C under conditions of carry out disinfection sterilization processing, after the completion, close
Dry cooling, spare in the environment of envelope.
5. a kind of manufacture craft of the composition of no silicone oil conditioning hair according to claim 2, it is characterised in that: described
Mixing speed in step 2 and step 3 is 100r/min, and the time stirred is 3min.
6. a kind of manufacture craft of the composition of no silicone oil conditioning hair according to claim 2, it is characterised in that: described
In step 4 during formula material sequentially adds by the way of stirring while adding.
7. a kind of manufacture craft of the composition of no silicone oil conditioning hair according to claim 2, it is characterised in that: described
Mixing speed is 120r/min in step 4, and the time stirred is 5min.
8. a kind of manufacture craft of the composition of no silicone oil conditioning hair according to claim 2, it is characterised in that: described
In step 4 after obtaining final mean annual increment solution, the Ph to 5.5-6.5 of solution is adjusted by way of citric acid is added.
9. a kind of manufacture craft of the composition of no silicone oil conditioning hair according to claim 2, it is characterised in that: described
The capacity that canned bottle is carried out in step 5 is 250ml, and canned preceding to bottle progress sterilizing.
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| CN201910717451.XA CN110327248A (en) | 2019-08-05 | 2019-08-05 | A kind of composition and manufacture craft of no silicone oil conditioning hair |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115887276A (en) * | 2022-11-30 | 2023-04-04 | 广州澳博生物科技有限公司 | Fibroin washing and protecting article and preparation process thereof |
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|---|---|---|---|---|
| CN107349117A (en) * | 2017-06-15 | 2017-11-17 | 郑鹏 | A kind of compound amino acid composition and without silicone oil conditioner shampoo |
| CN107913227A (en) * | 2017-11-15 | 2018-04-17 | 广州无与伦比企业集团有限公司 | Containing small yellow ginger without silicone oil hair conditioner and its preparation process |
| CN109464294A (en) * | 2018-12-26 | 2019-03-15 | 广州蜜妆生物科技有限公司 | A kind of hydrolysis of keratin hair conditioner and preparation method thereof |
| CN109602639A (en) * | 2019-01-31 | 2019-04-12 | 广州艾蓓生物科技有限公司 | A kind of amino pickling shield shampoo and preparation method thereof |
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2019
- 2019-08-05 CN CN201910717451.XA patent/CN110327248A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107349117A (en) * | 2017-06-15 | 2017-11-17 | 郑鹏 | A kind of compound amino acid composition and without silicone oil conditioner shampoo |
| CN107913227A (en) * | 2017-11-15 | 2018-04-17 | 广州无与伦比企业集团有限公司 | Containing small yellow ginger without silicone oil hair conditioner and its preparation process |
| CN109464294A (en) * | 2018-12-26 | 2019-03-15 | 广州蜜妆生物科技有限公司 | A kind of hydrolysis of keratin hair conditioner and preparation method thereof |
| CN109602639A (en) * | 2019-01-31 | 2019-04-12 | 广州艾蓓生物科技有限公司 | A kind of amino pickling shield shampoo and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN115887276A (en) * | 2022-11-30 | 2023-04-04 | 广州澳博生物科技有限公司 | Fibroin washing and protecting article and preparation process thereof |
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