CN110317678A - A kind of tea tree ethereal oil extracting method and the skin care item using tea tree ethereal oil preparation - Google Patents
A kind of tea tree ethereal oil extracting method and the skin care item using tea tree ethereal oil preparation Download PDFInfo
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- CN110317678A CN110317678A CN201910658785.4A CN201910658785A CN110317678A CN 110317678 A CN110317678 A CN 110317678A CN 201910658785 A CN201910658785 A CN 201910658785A CN 110317678 A CN110317678 A CN 110317678A
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- tree ethereal
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- 239000000341 volatile oil Substances 0.000 title claims abstract description 45
- 235000009024 Ceanothus sanguineus Nutrition 0.000 title claims abstract description 41
- 240000003553 Leptospermum scoparium Species 0.000 title claims abstract description 41
- 235000015459 Lycium barbarum Nutrition 0.000 title claims abstract description 41
- 238000000034 method Methods 0.000 title claims abstract description 14
- 238000002360 preparation method Methods 0.000 title claims abstract description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 29
- 238000001914 filtration Methods 0.000 claims abstract description 13
- 238000003756 stirring Methods 0.000 claims abstract description 9
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 claims abstract description 7
- 238000010438 heat treatment Methods 0.000 claims abstract description 7
- 238000000605 extraction Methods 0.000 claims abstract description 4
- 238000000874 microwave-assisted extraction Methods 0.000 claims abstract description 4
- 239000003921 oil Substances 0.000 claims abstract description 4
- 239000002904 solvent Substances 0.000 claims abstract description 4
- 235000003325 Ilex Nutrition 0.000 claims description 15
- 241000209035 Ilex Species 0.000 claims description 15
- 240000000851 Vaccinium corymbosum Species 0.000 claims description 15
- 235000003095 Vaccinium corymbosum Nutrition 0.000 claims description 15
- 235000017537 Vaccinium myrtillus Nutrition 0.000 claims description 15
- 235000021014 blueberries Nutrition 0.000 claims description 15
- 229960004756 ethanol Drugs 0.000 claims description 11
- 239000000706 filtrate Substances 0.000 claims description 10
- 239000012467 final product Substances 0.000 claims description 10
- 235000021028 berry Nutrition 0.000 claims description 9
- 235000009051 Ambrosia paniculata var. peruviana Nutrition 0.000 claims description 5
- 235000003097 Artemisia absinthium Nutrition 0.000 claims description 5
- 240000001851 Artemisia dracunculus Species 0.000 claims description 5
- 235000017731 Artemisia dracunculus ssp. dracunculus Nutrition 0.000 claims description 5
- 235000003261 Artemisia vulgaris Nutrition 0.000 claims description 5
- 239000001138 artemisia absinthium Substances 0.000 claims description 5
- 239000001224 daucus carota l. seed absolute Substances 0.000 claims description 5
- 229960000935 dehydrated alcohol Drugs 0.000 claims description 5
- 239000002002 slurry Substances 0.000 claims description 5
- KDYFGRWQOYBRFD-UHFFFAOYSA-N succinic acid Chemical compound OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 claims description 5
- 238000002137 ultrasound extraction Methods 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 239000006228 supernatant Substances 0.000 claims description 4
- 239000000047 product Substances 0.000 claims description 3
- 238000003303 reheating Methods 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 2
- 206010013786 Dry skin Diseases 0.000 abstract description 3
- 208000003251 Pruritus Diseases 0.000 abstract description 3
- 230000037336 dry skin Effects 0.000 abstract description 3
- 230000000694 effects Effects 0.000 abstract description 3
- 208000024891 symptom Diseases 0.000 abstract description 2
- 206010025482 malaise Diseases 0.000 abstract 1
- 210000002374 sebum Anatomy 0.000 description 2
- 230000028327 secretion Effects 0.000 description 2
- 208000002874 Acne Vulgaris Diseases 0.000 description 1
- 206010011224 Cough Diseases 0.000 description 1
- 208000001840 Dandruff Diseases 0.000 description 1
- 208000005171 Dysmenorrhea Diseases 0.000 description 1
- 206010013935 Dysmenorrhoea Diseases 0.000 description 1
- 206010048461 Genital infection Diseases 0.000 description 1
- 208000037093 Menstruation Disturbances Diseases 0.000 description 1
- 206010027339 Menstruation irregular Diseases 0.000 description 1
- 244000131316 Panax pseudoginseng Species 0.000 description 1
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 description 1
- 235000003140 Panax quinquefolius Nutrition 0.000 description 1
- 206010000496 acne Diseases 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 239000002260 anti-inflammatory agent Substances 0.000 description 1
- 230000001741 anti-phlogistic effect Effects 0.000 description 1
- 208000006673 asthma Diseases 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 235000008434 ginseng Nutrition 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000001151 other effect Effects 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 206010039083 rhinitis Diseases 0.000 description 1
- 210000001732 sebaceous gland Anatomy 0.000 description 1
- 210000004243 sweat Anatomy 0.000 description 1
- 210000000106 sweat gland Anatomy 0.000 description 1
- BWMISRWJRUSYEX-SZKNIZGXSA-N terbinafine hydrochloride Chemical compound Cl.C1=CC=C2C(CN(C\C=C\C#CC(C)(C)C)C)=CC=CC2=C1 BWMISRWJRUSYEX-SZKNIZGXSA-N 0.000 description 1
- 201000004647 tinea pedis Diseases 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/04—Antipruritics
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/84—Products or compounds obtained by lyophilisation, freeze-drying
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Birds (AREA)
- Dermatology (AREA)
- Epidemiology (AREA)
- Wood Science & Technology (AREA)
- Bioinformatics & Cheminformatics (AREA)
- General Chemical & Material Sciences (AREA)
- Medicinal Chemistry (AREA)
- Pharmacology & Pharmacy (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
A kind of extracting method of tea tree ethereal oil and skin care item using tea tree ethereal oil preparation, the initial tea tree ethereal oil that selection is just squeezed;Tea tree ethereal oil is put into percolator, using ethanol water as solvent, heating and stirring, after extraction, filtering obtains extracting solution;It adds the ethanol solution that volume fraction is 80~90% and carries out Microwave Extraction;Extracting solution is put into 5 degree of space environment and is refrigerated 2-3 hours, then carry out water-oil separating, then carry out mocromembrane filtering, is concentrated under reduced pressure, obtain the tea tree ethereal oil of finished product.The present invention has good massage effect, the malaise symptoms such as itch, chap caused by being effectively relieved because of dry skin.
Description
Technical field
The present invention relates to a kind of tea tree ethereal oil, specifically a kind of tea tree ethereal oil extracting method and use the tea tree ethereal oil
The skin care item of preparation.
Background technique
Tea tree ethereal oil originates in Australia, is the extract of tea tree.With bactericidal antiphlogistic, convergence pore, treatment cold,
Cough, rhinitis, asthma improve dysmenorrhea, irregular menstruation and genital infection and other effects.Suitable for oiliness and acne-prone skin, treatment
It suppurative wound and burns, tan severely, athlete's foot and dandruff.It clears the head, rejuvenates, anti-depression.
Sebaceous glands and sweat gland are dispersed in human skin, the sebum and sweat of secretion can form one layer thin on the skin
Film makes skin holding lubricate, is flexible to reduce moisture of skin evaporation.Autumn and winter due to temperature reduction, is air-dried, can make
Human skin lacks moisture, sebum secretion reduces, and then the symptoms such as itch, chap occurs;And with advancing age, skin generation
It thanks to slowing down for function, skin moisture-keeping effect and barrier function can also weakened, dry skin is caused to crack.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of extracting method of tea tree ethereal oil and use the tea tree ethereal oil system
Standby skin care item.
In order to solve the above-mentioned technical problem, the present invention takes following technical scheme:
A kind of extracting method of tea tree ethereal oil, comprising the following steps:
The initial tea tree ethereal oil that selection is just squeezed;
Tea tree ethereal oil is put into percolator, using ethanol water as solvent, heating and stirring, after extraction, filtering is obtained
Obtain extracting solution;
It adds the ethanol solution that volume fraction is 80~90% and carries out Microwave Extraction;
Extracting solution is put into 5 degree of space environment and is refrigerated 2-3 hours, then carried out water-oil separating, then carry out mocromembrane filtering, subtract
Pressure concentration, obtains the tea tree ethereal oil of finished product.
The weight of the ethanol solution of the addition is 3-5 times of tea tree ethereal oil.
In the heating process, it is evenly heated simultaneously using side and bottom, is heated to 65-85 DEG C.
After the addition ethanol water, 3 hours are stood also under 18-20 degrees Celsius, then reheating is handled.
A kind of skin care item, including 40-50 parts of tea tree ethereal oil, 20-25 parts of carrot seed oil, 12-18 parts of Chinese ilex leaf extract,
6-8 parts of wormwood essential oil, 5-7 parts of blueberry berry extract.
The Chinese ilex leaf extract is the ethanol solution that 1.5 times of its weight, 70-80wt% are added in the leaf of Chinese ilex of picking,
It is filtered after 60-70 DEG C of ultrasonic extraction 30-50min, filtrate crushes after being concentrated to dryness to obtain the final product.
The blueberry berry extract is that the water of 1.5 times of its weight is added in blueberries to be beaten, the filtering of gained slurries
Afterwards, the dehydrated alcohol of its volume 20-30% is added in filtrate, stands 3-5h after stirring and evenly mixing, is then centrifuged for handling, on gained
Clear liquid is freeze-dried to obtain the final product.
The present invention has good massage effect, the uncomfortable diseases such as itch, chap caused by being effectively relieved because of dry skin
Shape.
Specific embodiment
To further understand the features of the present invention, technological means and specific purposes achieved, function, below with reference to
Present invention is further described in detail for specific embodiment.
Present invention discloses a kind of extracting methods of tea tree ethereal oil, comprising the following steps:
A kind of extracting method of tea tree ethereal oil, comprising the following steps:
The initial tea tree ethereal oil that selection is just squeezed;
Tea tree ethereal oil is put into percolator, using ethanol water as solvent, heating and stirring, after extraction, filtering is obtained
Obtain extracting solution;
It adds the ethanol solution that volume fraction is 80~90% and carries out Microwave Extraction;
Extracting solution is put into 5 degree of space environment and is refrigerated 2-3 hours, then carried out water-oil separating, then carry out mocromembrane filtering, subtract
Pressure concentration, obtains the tea tree ethereal oil of finished product.
The weight of the ethanol solution of the addition is 3-5 times of tea tree ethereal oil.
In the heating process, it is evenly heated simultaneously using side and bottom, is heated to 65-85 DEG C.
After the addition ethanol water, 3 hours are stood also under 18-20 degrees Celsius, then reheating is handled.
Embodiment one
A kind of skin care item, including 40 parts of tea tree ethereal oil, 20 parts of carrot seed oil, 12 parts of Chinese ilex leaf extract, 6 parts of wormwood essential oil,
5 parts of blueberry berry extract.
The Chinese ilex leaf extract is the ethanol solution that 1.5 times of its weight, 70wt% are added in the leaf of Chinese ilex of picking, 60
It is filtered after DEG C ultrasonic extraction 30min, filtrate crushes after being concentrated to dryness to obtain the final product.The blueberry berry extract is added in blueberries
The water of 1.5 times of its weight is beaten, and after the filtering of gained slurries, the dehydrated alcohol of its volume 20% is added in filtrate, stirring is mixed
It stands 3h after even, is then centrifuged for handling, gained supernatant is freeze-dried to obtain the final product.
Embodiment two
A kind of skin care item, including 45 parts of tea tree ethereal oil, 22 parts of carrot seed oil, 16 parts of Chinese ilex leaf extract, 7 parts of wormwood essential oil,
6 parts of blueberry berry extract.
The Chinese ilex leaf extract is the ethanol solution that 1.5 times of its weight, 75wt% are added in the leaf of Chinese ilex of picking, 65
It is filtered after DEG C ultrasonic extraction 40min, filtrate crushes after being concentrated to dryness to obtain the final product.The blueberry berry extract is added in blueberries
The water of 1.5 times of its weight is beaten, and after the filtering of gained slurries, the dehydrated alcohol of its volume 25% is added in filtrate, stirring is mixed
It stands 4h after even, is then centrifuged for handling, gained supernatant is freeze-dried to obtain the final product.
Embodiment three
A kind of skin care item, including 50 parts of tea tree ethereal oil, 25 parts of carrot seed oil, 18 parts of Chinese ilex leaf extract, 8 parts of wormwood essential oil,
7 parts of blueberry berry extract.
The Chinese ilex leaf extract is the ethanol solution that 1.5 times of its weight, 80wt% are added in the leaf of Chinese ilex of picking, 70
It is filtered after DEG C ultrasonic extraction 50min, filtrate crushes after being concentrated to dryness to obtain the final product.The blueberry berry extract is added in blueberries
The water of 1.5 times of its weight is beaten, and after the filtering of gained slurries, the dehydrated alcohol of its volume 30% is added in filtrate, stirring is mixed
It stands 5h after even, is then centrifuged for handling, gained supernatant is freeze-dried to obtain the final product.
It should be noted that these are only the preferred embodiment of the present invention, it is not intended to restrict the invention, although ginseng
According to embodiment, invention is explained in detail, for those skilled in the art, still can be to aforementioned reality
Technical solution documented by example is applied to modify or equivalent replacement of some of the technical features, but it is all in this hair
Within bright spirit and principle, any modification, equivalent replacement, improvement and so on should be included in protection scope of the present invention
Within.
Claims (7)
1. a kind of extracting method of tea tree ethereal oil, comprising the following steps:
The initial tea tree ethereal oil that selection is just squeezed;
Tea tree ethereal oil is put into percolator, using ethanol water as solvent, heating and stirring, after extraction, filtering is obtained
Obtain extracting solution;
It adds the ethanol solution that volume fraction is 80~90% and carries out Microwave Extraction;
Extracting solution is put into 5 degree of space environment and is refrigerated 2-3 hours, then carried out water-oil separating, then carry out mocromembrane filtering, subtract
Pressure concentration, obtains the tea tree ethereal oil of finished product.
2. the extracting method of tea tree ethereal oil according to claim 1, which is characterized in that the weight of the ethanol solution of the addition
Amount is 3-5 times of tea tree ethereal oil.
3. the extracting method of tea tree ethereal oil according to claim 2, which is characterized in that in the heating process, using side
Portion and bottom are evenly heated simultaneously, are heated to 65-85 DEG C.
4. the extracting method of tea tree ethereal oil according to claim 3, which is characterized in that after the addition ethanol water,
3 hours are stood also under 18-20 degrees Celsius, then reheating is handled.
5. a kind of skin care item for the tea tree ethereal oil preparation extracted using extracting method described in claim 1, which is characterized in that packet
40-50 parts of tea tree ethereal oil are included, 20-25 parts of carrot seed oil, 12-18 parts of Chinese ilex leaf extract, 6-8 parts of wormwood essential oil, blueberries
5-7 parts of extract.
6. skin care item according to claim 5, which is characterized in that the Chinese ilex leaf extract is in the leaf of Chinese ilex of picking
The ethanol solution of 1.5 times of its weight, 70-80wt% is added, is filtered after 60-70 DEG C of ultrasonic extraction 30-50min, filtrate is concentrated to dryness
After crush to obtain the final product.
7. skin care item according to claim 6, which is characterized in that the blueberry berry extract is that it is added in blueberries
The water that 1.5 times of weight is beaten, and after the filtering of gained slurries, the dehydrated alcohol of its volume 20-30% is added in filtrate, stirs
It stands 3-5h after mixing, is then centrifuged for handling, gained supernatant is freeze-dried to obtain the final product.
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CN201910658785.4A CN110317678A (en) | 2019-07-22 | 2019-07-22 | A kind of tea tree ethereal oil extracting method and the skin care item using tea tree ethereal oil preparation |
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CN201910658785.4A CN110317678A (en) | 2019-07-22 | 2019-07-22 | A kind of tea tree ethereal oil extracting method and the skin care item using tea tree ethereal oil preparation |
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Citations (6)
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---|---|---|---|---|
CN104830538A (en) * | 2015-05-25 | 2015-08-12 | 江苏耐雀生物工程技术有限公司 | Method of extracting tea tree essential oil from tea trees |
CN106010792A (en) * | 2016-06-27 | 2016-10-12 | 福建澳树佳生物科技有限公司 | Method for extracting melaleuca alternifolia and tea tree essence oil |
CN106221922A (en) * | 2016-08-26 | 2016-12-14 | 广西灏源盛世生物科技有限公司 | A kind of tea tree ethereal oil extracts processing technique |
CN106420991A (en) * | 2016-12-19 | 2017-02-22 | 福建万亿店中店电子商务有限责任公司 | Skin care massage oil containing tea tree essential oil |
CN106929159A (en) * | 2017-05-05 | 2017-07-07 | 黎显军 | A kind of extracting method of recovery rate tea tree ethereal oil high |
CN108721478A (en) * | 2018-09-11 | 2018-11-02 | 广州旭升化工科技有限公司 | A kind of plant multi-effect compound agent of mosquito-proof sting |
-
2019
- 2019-07-22 CN CN201910658785.4A patent/CN110317678A/en active Pending
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104830538A (en) * | 2015-05-25 | 2015-08-12 | 江苏耐雀生物工程技术有限公司 | Method of extracting tea tree essential oil from tea trees |
CN106010792A (en) * | 2016-06-27 | 2016-10-12 | 福建澳树佳生物科技有限公司 | Method for extracting melaleuca alternifolia and tea tree essence oil |
CN106221922A (en) * | 2016-08-26 | 2016-12-14 | 广西灏源盛世生物科技有限公司 | A kind of tea tree ethereal oil extracts processing technique |
CN106420991A (en) * | 2016-12-19 | 2017-02-22 | 福建万亿店中店电子商务有限责任公司 | Skin care massage oil containing tea tree essential oil |
CN106929159A (en) * | 2017-05-05 | 2017-07-07 | 黎显军 | A kind of extracting method of recovery rate tea tree ethereal oil high |
CN108721478A (en) * | 2018-09-11 | 2018-11-02 | 广州旭升化工科技有限公司 | A kind of plant multi-effect compound agent of mosquito-proof sting |
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