CN111419762A - Tea bran silicone oil-free shampoo and preparation method thereof - Google Patents

Tea bran silicone oil-free shampoo and preparation method thereof Download PDF

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CN111419762A
CN111419762A CN202010490673.5A CN202010490673A CN111419762A CN 111419762 A CN111419762 A CN 111419762A CN 202010490673 A CN202010490673 A CN 202010490673A CN 111419762 A CN111419762 A CN 111419762A
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oil
essential oil
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tea bran
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陈殿松
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Guangzhou Gude Personal Nursing Products Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
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    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/002Preparations for repairing the hair, e.g. hair cure
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/006Antidandruff preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/008Preparations for oily hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/02Preparations for cleaning the hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/20Chemical, physico-chemical or functional or structural properties of the composition as a whole
    • A61K2800/30Characterized by the absence of a particular group of ingredients
    • A61K2800/34Free of silicones
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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Abstract

The invention relates to a tea bran silicone oil-free shampoo and a preparation method thereof. The shampoo has the advantages that the loose skin after losing weight is firmer, the shampoo has very good effects of resisting depression, bacteria, sterilization, dispelling flatulence, deodorizing, helping digestion, killing mold, preventing diseases, stimulating, tonifying body and the like by adopting the lemon grass essential oil, and is helpful for relieving itching, and the shampoo has the effects of removing hair oil, treating scalp itch, removing dandruff, stopping alopecia, growing hair and blackening and brightening hair by adopting the tea bran extract.

Description

Tea bran silicone oil-free shampoo and preparation method thereof
Technical Field
The invention relates to shampoo, and particularly relates to tea bran silicone oil-free shampoo and a preparation method thereof.
Background
The shampoo is a necessary daily necessity in the life of people. With the improvement of living standard and the acceleration of life rhythm of people, factors such as environmental pollution, increased working pressure, irregular diet, hair dyeing and perming, the use of electronic products and the like bring great influence on the health of the hair quality of people, and the problems of vigorous hair grease secretion, little white hair, dandruff, alopecia and the like bring serious troubles to the daily life of people. How to have bright, smooth and elastic hair, and one head of the hair is beautiful and easy to comb becomes the identification standard of people for the quality requirement of the shampoo. Therefore, the shampoo is required to have the effects of removing dirt and dandruff, and also has the effects of environmental protection, alopecia prevention, itching relief, allergy resistance, deep conditioning and the like.
At present, shampoos with various functions sold in the market are generally produced by mixing chemical substances, the decontamination effect is obvious, but after long-term use, the side effects of the chemical substances are easy to cause hair nutrition loss, hair quality damage, hair becoming more and more rough, dry and withered and even alopecia, so that the development of the shampoo without silicone oil is necessary.
Disclosure of Invention
Aiming at the situation and overcoming the defects of the prior art, the invention provides the tea bran silicone-free shampoo and the preparation method thereof, the rosemary essential oil is adopted to have the effects of strong convergence, crease resistance and cortex regulation, conditioning greasy and dirty skin, promoting blood circulation, stimulating hair regeneration and enabling the loose skin after losing weight to be firmer, the lemon grass essential oil is adopted to enable the shampoo to have the effects of resisting depression, resisting bacteria, sterilizing, dispelling flatulence, deodorizing, helping digestion, killing mildew, preventing diseases, stimulating, tonifying body and the like, and the shampoo is helpful for relieving itching, and the tea bran extract is adopted to enable the shampoo to have the effects of removing hair oil, treating head itch, removing dandruff, stopping alopecia, growing hair and blackening and brightening hair.
In order to achieve the purpose, the invention provides the following technical scheme: the shampoo is mainly prepared from the following raw materials in parts by weight: 2-4 parts of ethyl benzoate, 1-2 parts of citral, 2-4 parts of amino acid, 1-3 parts of vitamin E, 2-4 parts of tea tree oil, 3-6 parts of oil-soluble tea polyphenol, 2-5 parts of tea bran extract, 6-8 parts of potassium sodium tartrate, 1-3 parts of alkyl acid phosphate, 10-15 parts of soapberry extract, 4-5 parts of saponin, 2-4 parts of alkyl glycoside, 4-7 parts of lemon grass essential oil, 4-9 parts of rosemary essential oil, 2-4 parts of euphorbia hirta extract and 30-40 parts of pure water.
The lemon grass essential oil is prepared by the following method: fresh leaves, flowers of lemon grass; II, tools used: a cutting machine, a distillation tower, a steam conveying pipe, a cooling tank and a filling bottle; thirdly, cleaning the cut lemongrass, and drying in the sun; fourthly, cutting the lemon grass into segments with the length of less than or equal to 2cm by using a cutting and crushing machine; fifthly, putting the cut lemon grass into a distillation tower for steam distillation, wherein the distillation temperature is more than or equal to 100 ℃ at 120 ℃, the bottom of a distillation pot needs to keep moisture, the raw materials cannot touch the bottom of the pot so as to avoid scorching, and the middle part needs to be loose, so that the airflow at the bottom can rise conveniently; sixthly, directly conveying the distilled mixed gas to a cooling tank through a gas conveying pipe, pressurizing and liquefying at a cooling temperature of-5 ℃ or more and less than 0 ℃, and separating ice blocks from the liquid to obtain the lemongrass essential oil; seventhly, filling the lemon grass essential oil into a bottle sealing cover at low temperature, wherein the temperature of the filling bottle is more than or equal to 5 ℃ below zero and is less than 0 ℃.
The rosemary essential oil is prepared by the following method: cleaning herba Rosmarini officinalis, cutting, and air drying with cold air; mixing vegetable white oil, coconut oil and olive oil, heating to 67 deg.C and keeping the temperature for 1 hr to obtain mixed essential oil; cutting radix Angelicae Dahuricae, folium Menthae, Aloe, fructus Lycii and herba Leonuri, adding into the mixed essential oil, heating to 89 deg.C under stirring, keeping the temperature for 3 hr, and cooling to room temperature; adding herba Rosmarini officinalis for standby, and performing ultrasonic high-speed dispersion at ultrasonic frequency of 12KHz at dispersion speed of 3560r/min for 45 min; filtering the obtained essential oil, and removing filter residue to obtain the final product.
The tea bran extract is prepared by the following method: 1) pulverizing tea bran; 2) then continuing the high-pressure micro-jet superfine grinding treatment to obtain paste slurry; 3) performing microwave extraction on the paste slurry to obtain a microwave extracting solution; 4) passing the microwave extract through macroporous resin chromatographic column, eluting with ethanol solution, and collecting eluate; 5) concentrating, and drying to obtain the desired tea bran extract.
The preparation method of the ethyl benzoate comprises the following steps: adding benzoic acid, absolute ethyl alcohol, modified clay and a water-carrying agent into a reaction container with a water separator, installing the water separator, a reflux condenser pipe and a thermometer on the reaction container, heating for reflux water separation, reacting until no water drops appear, discharging a water layer after cooling for 25min at normal temperature, washing the reaction liquid with water, drying, distilling the previous fraction, and collecting the fraction at 101-103 ℃ as a product.
The preparation method comprises the following steps: (1) humidifying raw materials of 1 part of citral, 2 parts of amino acid, 1 parts of vitamin E, 3 parts of oil-soluble tea polyphenol, 2 parts of tea bran extract, 6 parts of sodium potassium tartrate, 1 part of alkyl acid phosphate, 4 parts of saponin, 2 parts of alkyl glycoside, 4 parts of rosemary essential oil and 2 parts of euphorbia hirta extract, and then passing through a colloid mill to enable the raw materials to be in a relatively stable colloid state;
(2) adding 10-20 parts of pure water into an emulsifying pot, adding 2 parts of tea tree oil, heating to 100-115 ℃, decocting at 100-115 ℃ for 1-2.1 h, cooling and standing for 12-16 h;
(3) re-heating to 90-100 ℃, adding 2 parts of ethyl benzoate in the first step, homogenizing for 15-20 min, adding 10 parts of homogenized soapberry extract in the second step, and homogenizing for 10-30 min after adding; thirdly, adding 4 parts of lemongrass essential oil; the temperature is maintained at 78-83 ℃ during feeding;
(4) adding 2 parts of homogenized euphorbia hirta extract into an emulsifying pot at the temperature of 90-95 ℃, and stirring and homogenizing for 25-35 min;
(5) adding 20 parts of pure water into the emulsifying pot at the temperature of 90-95 ℃, stirring and homogenizing for 1.5-2.5 h, and then cooling; and finally, supplementing the rest water, and stirring and homogenizing for 1.5-2.5 h to obtain a finished product.
Has the advantages that: the shampoo has the effects of strongly astringing, preventing wrinkles and regulating cortex by adopting the rosemary essential oil, conditioning greasy and dirty skin, promoting blood circulation, stimulating hair regeneration and enabling the loose skin after losing weight to be firmer, has the effects of resisting depression, resisting bacteria, sterilizing, removing flatulence, deodorizing, helping digestion, killing mold, preventing diseases, exciting, tonifying body and the like by adopting the lemon grass essential oil, is favorable for relieving itching, and has the effects of removing hair oil, treating scalp itching, removing dandruff, stopping alopecia, growing hair and blackening and brightening hair by adopting the tea bran extract.
Detailed Description
The following provides a more detailed description of the embodiments of the present invention.
The invention provides a tea bran silicone oil-free shampoo and a preparation method thereof, wherein the shampoo is mainly prepared from the following raw materials in parts by weight: 2-4 parts of ethyl benzoate, 1-2 parts of citral, 2-4 parts of amino acid, 1-3 parts of vitamin E, 2-4 parts of tea tree oil, 3-6 parts of oil-soluble tea polyphenol, 2-5 parts of tea bran extract, 6-8 parts of potassium sodium tartrate, 1-3 parts of alkyl acid phosphate, 10-15 parts of soapberry extract, 4-5 parts of saponin, 2-4 parts of alkyl glycoside, 4-7 parts of lemon grass essential oil, 4-9 parts of rosemary essential oil, 2-4 parts of euphorbia hirta extract and 30-40 parts of pure water.
According to the technical scheme: the lemon grass essential oil is prepared by the following method: fresh leaves, flowers of lemon grass; II, tools used: a cutting machine, a distillation tower, a steam conveying pipe, a cooling tank and a filling bottle; thirdly, cleaning the cut lemongrass, and drying in the sun; fourthly, cutting the lemon grass into segments with the length of less than or equal to 2cm by using a cutting and crushing machine; fifthly, putting the cut lemon grass into a distillation tower for steam distillation, wherein the distillation temperature is more than or equal to 100 ℃ at 120 ℃, the bottom of a distillation pot needs to keep moisture, the raw materials cannot touch the bottom of the pot so as to avoid scorching, and the middle part needs to be loose, so that the airflow at the bottom can rise conveniently; sixthly, directly conveying the distilled mixed gas to a cooling tank through a gas conveying pipe, pressurizing and liquefying at a cooling temperature of-5 ℃ or more and less than 0 ℃, and separating ice blocks from the liquid to obtain the lemongrass essential oil; seventhly, filling the lemon grass essential oil into a bottle sealing cover at low temperature, wherein the temperature of the filling bottle is more than or equal to 5 ℃ below zero and is less than 0 ℃.
According to the technical scheme: the rosemary essential oil is prepared by the following method: cleaning herba Rosmarini officinalis, cutting, and air drying with cold air; mixing vegetable white oil, coconut oil and olive oil, heating to 67 deg.C and keeping the temperature for 1 hr to obtain mixed essential oil; cutting radix Angelicae Dahuricae, folium Menthae, Aloe, fructus Lycii and herba Leonuri, adding into the mixed essential oil, heating to 89 deg.C under stirring, keeping the temperature for 3 hr, and cooling to room temperature; adding herba Rosmarini officinalis for standby, and performing ultrasonic high-speed dispersion at ultrasonic frequency of 12KHz at dispersion speed of 3560r/min for 45 min; filtering the obtained essential oil, and removing filter residue to obtain the final product.
According to the technical scheme: the tea bran extract is prepared by the following method: 1) pulverizing tea bran; 2) then continuing the high-pressure micro-jet superfine grinding treatment to obtain paste slurry; 3) performing microwave extraction on the paste slurry to obtain a microwave extracting solution; 4) passing the microwave extract through macroporous resin chromatographic column, eluting with ethanol solution, and collecting eluate; 5) concentrating, and drying to obtain the desired tea bran extract.
According to the technical scheme: the preparation method of the ethyl benzoate comprises the following steps: adding benzoic acid, absolute ethyl alcohol, modified clay and a water-carrying agent into a reaction container with a water separator, installing the water separator, a reflux condenser pipe and a thermometer on the reaction container, heating for reflux water separation, reacting until no water drops appear, discharging a water layer after cooling for 25min at normal temperature, washing the reaction liquid with water, drying, distilling the previous fraction, and collecting the fraction at 101-103 ℃ as a product.
The preparation method comprises the following steps: (1) humidifying raw materials of 1 part of citral, 2 parts of amino acid, 1 parts of vitamin E, 3 parts of oil-soluble tea polyphenol, 2 parts of tea bran extract, 6 parts of sodium potassium tartrate, 1 part of alkyl acid phosphate, 4 parts of saponin, 2 parts of alkyl glycoside, 4 parts of rosemary essential oil and 2 parts of euphorbia hirta extract, and then passing through a colloid mill to enable the raw materials to be in a relatively stable colloid state;
(2) adding 10-20 parts of pure water into an emulsifying pot, adding 2 parts of tea tree oil, heating to 100-115 ℃, decocting at 100-115 ℃ for 1-2.1 h, cooling and standing for 12-16 h;
(3) re-heating to 90-100 ℃, adding 2 parts of ethyl benzoate in the first step, homogenizing for 15-20 min, adding 10 parts of homogenized soapberry extract in the second step, and homogenizing for 10-30 min after adding; thirdly, adding 4 parts of lemongrass essential oil; the temperature is maintained at 78-83 ℃ during feeding;
(4) adding 2 parts of homogenized euphorbia hirta extract into an emulsifying pot at the temperature of 90-95 ℃, and stirring and homogenizing for 25-35 min;
(5) adding 20 parts of pure water into the emulsifying pot at the temperature of 90-95 ℃, stirring and homogenizing for 1.5-2.5 h, and then cooling; and finally, supplementing the rest water, and stirring and homogenizing for 1.5-2.5 h to obtain a finished product.
The second embodiment of the invention provides a tea bran silicone oil-free shampoo and a preparation method thereof, wherein the shampoo is mainly prepared from the following raw materials in parts by weight: 2-4 parts of ethyl benzoate, 1-2 parts of citral, 2-4 parts of amino acid, 1-3 parts of vitamin E, 2-4 parts of tea tree oil, 3-6 parts of oil-soluble tea polyphenol, 2-5 parts of tea bran extract, 6-8 parts of potassium sodium tartrate, 1-3 parts of alkyl acid phosphate, 10-15 parts of soapberry extract, 4-5 parts of saponin, 2-4 parts of alkyl glycoside, 4-7 parts of lemon grass essential oil, 4-9 parts of rosemary essential oil, 2-4 parts of euphorbia hirta extract and 30-40 parts of pure water.
According to the technical scheme: the lemon grass essential oil is prepared by the following method: fresh leaves, flowers of lemon grass; II, tools used: a cutting machine, a distillation tower, a steam conveying pipe, a cooling tank and a filling bottle; thirdly, cleaning the cut lemongrass, and drying in the sun; fourthly, cutting the lemon grass into segments with the length of less than or equal to 2cm by using a cutting and crushing machine; fifthly, putting the cut lemon grass into a distillation tower for steam distillation, wherein the distillation temperature is more than or equal to 100 ℃ at 120 ℃, the bottom of a distillation pot needs to keep moisture, the raw materials cannot touch the bottom of the pot so as to avoid scorching, and the middle part needs to be loose, so that the airflow at the bottom can rise conveniently; sixthly, directly conveying the distilled mixed gas to a cooling tank through a gas conveying pipe, pressurizing and liquefying at a cooling temperature of-5 ℃ or more and less than 0 ℃, and separating ice blocks from the liquid to obtain the lemongrass essential oil; seventhly, filling the lemon grass essential oil into a bottle sealing cover at low temperature, wherein the temperature of the filling bottle is more than or equal to 5 ℃ below zero and is less than 0 ℃.
According to the technical scheme: the rosemary essential oil is prepared by the following method: cleaning herba Rosmarini officinalis, cutting, and air drying with cold air; mixing vegetable white oil, coconut oil and olive oil, heating to 67 deg.C and keeping the temperature for 1 hr to obtain mixed essential oil; cutting radix Angelicae Dahuricae, folium Menthae, Aloe, fructus Lycii and herba Leonuri, adding into the mixed essential oil, heating to 89 deg.C under stirring, keeping the temperature for 3 hr, and cooling to room temperature; adding herba Rosmarini officinalis for standby, and performing ultrasonic high-speed dispersion at ultrasonic frequency of 12KHz at dispersion speed of 3560r/min for 45 min; filtering the obtained essential oil, and removing filter residue to obtain the final product.
The tea bran extract is prepared by the following method: 1) pulverizing tea bran; 2) then continuing the high-pressure micro-jet superfine grinding treatment to obtain paste slurry; 3) performing microwave extraction on the paste slurry to obtain a microwave extracting solution; 4) passing the microwave extract through macroporous resin chromatographic column, eluting with ethanol solution, and collecting eluate; 5) concentrating, and drying to obtain the desired tea bran extract.
According to the technical scheme: the preparation method of the ethyl benzoate comprises the following steps: adding benzoic acid, absolute ethyl alcohol, modified clay and a water-carrying agent into a reaction container with a water separator, installing the water separator, a reflux condenser pipe and a thermometer on the reaction container, heating for reflux water separation, reacting until no water drops appear, discharging a water layer after cooling for 25min at normal temperature, washing the reaction liquid with water, drying, distilling the previous fraction, and collecting the fraction at 101-103 ℃ as a product.
The preparation method comprises the following steps: (1) humidifying raw materials of 2 parts of citral, 4 parts of amino acid, 3 parts of vitamin E, 6 parts of oil-soluble tea polyphenol, 5 parts of tea bran extract, 8 parts of sodium potassium tartrate, 3 parts of alkyl acid phosphate, 5 parts of saponin, 4 parts of alkyl glycoside, 9 parts of rosemary essential oil and 4 parts of euphorbia hirta extract, and then passing through a colloid mill to enable the raw materials to be in a relatively stable colloid state;
(2) adding 20 parts of pure water into an emulsifying pot, adding 4 parts of tea tree oil, heating to 100-115 ℃, decocting at 100-115 ℃ for 1-2.1 h, cooling and standing for 12-16 h;
(3) re-heating to 90-100 ℃, adding 4 parts of ethyl benzoate in the first step, homogenizing for 15-20 min, adding 15 parts of homogenized soapberry extract in the second step, and homogenizing for 10-30 min after adding; thirdly, adding 7 parts of lemongrass essential oil; the temperature is maintained at 78-83 ℃ during feeding;
(4) adding 4 parts of homogenized euphorbia hirta extract into an emulsifying pot at the temperature of 90-95 ℃, and stirring and homogenizing for 25-35 min;
(5) adding 35 parts of pure water into the emulsifying pot at the temperature of 90-95 ℃, stirring and homogenizing for 1.5-2.5 h, and then cooling; and finally, supplementing the rest water, and stirring and homogenizing for 1.5-2.5 h to obtain a finished product.
Has the advantages that: the shampoo has the effects of strongly astringing, preventing wrinkles and regulating cortex by adopting the rosemary essential oil, conditioning greasy and dirty skin, promoting blood circulation, stimulating hair regeneration and enabling the loose skin after losing weight to be firmer, has the effects of resisting depression, resisting bacteria, sterilizing, removing flatulence, deodorizing, helping digestion, killing mold, preventing diseases, exciting, tonifying body and the like by adopting the lemon grass essential oil, is favorable for relieving itching, and has the effects of removing hair oil, treating scalp itching, removing dandruff, stopping alopecia, growing hair and blackening and brightening hair by adopting the tea bran extract.
Has the advantages that: the packing box is novel in structure, ingenious in conception, high in drying efficiency of the packing box body 1, good in drying effect and convenient to carry the packing box body 1, and meanwhile, the packing belt can penetrate through the groove 8 to be packed, so that the packing belt is prevented from shaking.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that changes may be made in the embodiments and/or equivalents thereof without departing from the spirit and scope of the invention. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.

Claims (6)

1. The silicone oil-free tea bran shampoo is characterized in that: the shampoo is mainly prepared from the following raw materials in parts by weight: 2-4 parts of ethyl benzoate, 1-2 parts of citral, 2-4 parts of amino acid, 1-3 parts of vitamin E, 2-4 parts of tea tree oil, 3-6 parts of oil-soluble tea polyphenol, 2-5 parts of tea bran extract, 6-8 parts of potassium sodium tartrate, 1-3 parts of alkyl acid phosphate, 10-15 parts of soapberry extract, 4-5 parts of saponin, 2-4 parts of alkyl glycoside, 4-7 parts of lemon grass essential oil, 4-9 parts of rosemary essential oil, 2-4 parts of euphorbia hirta extract and 30-40 parts of pure water.
2. The tea bran silicone oil-free shampoo as claimed in claim 1, wherein the lemon grass essential oil is prepared by the following method: fresh leaves, flowers of lemon grass; II, tools used: a cutting machine, a distillation tower, a steam conveying pipe, a cooling tank and a filling bottle; thirdly, cleaning the cut lemongrass, and drying in the sun; fourthly, cutting the lemon grass into segments with the length of less than or equal to 2cm by using a cutting and crushing machine; fifthly, putting the cut lemon grass into a distillation tower for steam distillation, wherein the distillation temperature is more than or equal to 100 ℃ at 120 ℃, the bottom of a distillation pot needs to keep moisture, the raw materials cannot touch the bottom of the pot so as to avoid scorching, and the middle part needs to be loose, so that the airflow at the bottom can rise conveniently; sixthly, directly conveying the distilled mixed gas to a cooling tank through a gas conveying pipe, pressurizing and liquefying at a cooling temperature of-5 ℃ or more and less than 0 ℃, and separating ice blocks from the liquid to obtain the lemongrass essential oil; seventhly, filling the lemon grass essential oil into a bottle sealing cover at low temperature, wherein the temperature of the filling bottle is more than or equal to 5 ℃ below zero and is less than 0 ℃.
3. The tea bran silicone oil-free shampoo as claimed in claim 1, wherein the rosemary essential oil is prepared by the following method: cleaning herba Rosmarini officinalis, cutting, and air drying with cold air; mixing vegetable white oil, coconut oil and olive oil, heating to 67 deg.C and keeping the temperature for 1 hr to obtain mixed essential oil; cutting radix Angelicae Dahuricae, folium Menthae, Aloe, fructus Lycii and herba Leonuri, adding into the mixed essential oil, heating to 89 deg.C under stirring, keeping the temperature for 3 hr, and cooling to room temperature; adding herba Rosmarini officinalis for standby, and performing ultrasonic high-speed dispersion at ultrasonic frequency of 12KHz at dispersion speed of 3560r/min for 45 min; filtering the obtained essential oil, and removing filter residue to obtain the final product.
4. The tea bran silicone oil-free shampoo as claimed in claim 1, wherein the tea bran extract is prepared by the following method: 1) pulverizing tea bran; 2) then continuing the high-pressure micro-jet superfine grinding treatment to obtain paste slurry; 3) performing microwave extraction on the paste slurry to obtain a microwave extracting solution; 4) passing the microwave extract through macroporous resin chromatographic column, eluting with ethanol solution, and collecting eluate; 5) concentrating, and drying to obtain the desired tea bran extract.
5. The tea bran silicone oil-free shampoo as claimed in claim 1, wherein the preparation method of the ethyl benzoate comprises the following steps: adding benzoic acid, absolute ethyl alcohol, modified clay and a water-carrying agent into a reaction container with a water separator, installing the water separator, a reflux condenser pipe and a thermometer on the reaction container, heating for reflux water separation, reacting until no water drops appear, discharging a water layer after cooling for 25min at normal temperature, washing the reaction liquid with water, drying, distilling the previous fraction, and collecting the fraction at 101-103 ℃ as a product.
6. The preparation method of the tea bran silicone oil-free shampoo is characterized by comprising the following steps:
(1) humidifying raw materials of 1-2 parts of citral, 2-4 parts of amino acid, 1-3 parts of vitamin E, 3-6 parts of oil-soluble tea polyphenol, 2-5 parts of tea bran extract, 6-8 parts of sodium potassium tartrate, 1-3 parts of alkyl acid phosphate, 4-5 parts of saponin, 2-4 parts of alkyl glycoside, 4-9 parts of rosemary essential oil and 2-4 parts of euphorbia hirta extract, and then passing through a colloid mill to enable the raw materials to be in a relatively stable colloid state;
(2) adding 10-20 parts of pure water into an emulsifying pot, adding 2-4 parts of tea tree oil, heating to 100-115 ℃, decocting at 100-115 ℃ for 1-2.1 h, cooling and standing for 12-16 h;
(3) re-heating to 90-100 ℃, adding 2-4 parts of ethyl benzoate in the first step, homogenizing for 15-20 min, adding 10-15 parts of homogenized soapberry extract in the second step, and homogenizing for 10-30 min after adding; thirdly, adding 4-7 parts of lemon grass essential oil; the temperature is maintained at 78-83 ℃ during feeding;
(4) adding 2-4 parts of homogenized euphorbia hirta extract into an emulsifying pot at the temperature of 90-95 ℃, and stirring and homogenizing for 25-35 min;
(5) adding 20-35 parts of pure water into the emulsifying pot at the temperature of 90-95 ℃, stirring and homogenizing for 1.5-2.5 h, and then cooling; and finally, supplementing the rest water, and stirring and homogenizing for 1.5-2.5 h to obtain a finished product.
CN202010490673.5A 2020-06-02 2020-06-02 Tea bran silicone oil-free shampoo and preparation method thereof Pending CN111419762A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111991261A (en) * 2020-08-21 2020-11-27 广州德谷个人护理用品有限公司 Mild oil control shampoo composition suitable for sensitive scalp and preparation method thereof
CN111991303A (en) * 2020-09-27 2020-11-27 广州德谷个人护理用品有限公司 Plant extract composition with multi-target scalp oil control and dandruff removal effects, preparation method thereof and scalp care composition
CN113425636A (en) * 2021-05-21 2021-09-24 广州德谷个人护理用品有限公司 Preparation method of tea bran flavone and application of tea bran flavone in anti-hair loss product

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104311414A (en) * 2014-09-16 2015-01-28 常州市松盛香料有限公司 Preparation method of ethyl benzoate
CN104490644A (en) * 2014-11-22 2015-04-08 青岛海芬海洋生物科技有限公司 Plant composition for hair care
CN106491403A (en) * 2016-12-07 2017-03-15 王领娣 A kind of rosemary ethereal oil
CN106806176A (en) * 2017-03-28 2017-06-09 钦州市桂耘贸易有限公司 Tea bran extract and preparation method thereof
CN109181880A (en) * 2018-10-18 2019-01-11 吕小萍 The extracting method of lemon grass (Cymbopogon citratus) essential oil
CN109316396A (en) * 2017-07-31 2019-02-12 何学军 A kind of no silicone oil shampoo

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104311414A (en) * 2014-09-16 2015-01-28 常州市松盛香料有限公司 Preparation method of ethyl benzoate
CN104490644A (en) * 2014-11-22 2015-04-08 青岛海芬海洋生物科技有限公司 Plant composition for hair care
CN106491403A (en) * 2016-12-07 2017-03-15 王领娣 A kind of rosemary ethereal oil
CN106806176A (en) * 2017-03-28 2017-06-09 钦州市桂耘贸易有限公司 Tea bran extract and preparation method thereof
CN109316396A (en) * 2017-07-31 2019-02-12 何学军 A kind of no silicone oil shampoo
CN109181880A (en) * 2018-10-18 2019-01-11 吕小萍 The extracting method of lemon grass (Cymbopogon citratus) essential oil

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
国家药品监督管理局: "《《化妆品安全技术规范(2015年版)》2021年修订版》", 26 May 2021 *
崔钟雷: "《魅力女人》", 31 January 2015, 黑龙江美术出版社 *
王亮: "《精油的科学》", 31 December 2018, 东南大学出版社 *

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111991261A (en) * 2020-08-21 2020-11-27 广州德谷个人护理用品有限公司 Mild oil control shampoo composition suitable for sensitive scalp and preparation method thereof
CN111991261B (en) * 2020-08-21 2021-10-08 广州德谷个人护理用品有限公司 Mild oil control shampoo composition suitable for sensitive scalp and preparation method thereof
CN111991303A (en) * 2020-09-27 2020-11-27 广州德谷个人护理用品有限公司 Plant extract composition with multi-target scalp oil control and dandruff removal effects, preparation method thereof and scalp care composition
CN111991303B (en) * 2020-09-27 2022-11-04 广州德谷个人护理用品有限公司 Plant extract composition with multi-target scalp oil control and dandruff removal effects, preparation method thereof and scalp care composition
CN113425636A (en) * 2021-05-21 2021-09-24 广州德谷个人护理用品有限公司 Preparation method of tea bran flavone and application of tea bran flavone in anti-hair loss product
CN113425636B (en) * 2021-05-21 2023-01-31 广州德谷个人护理用品有限公司 Preparation method of tea bran flavone and application of tea bran flavone in anti-hair loss product

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