CN111419762A - Tea bran silicone oil-free shampoo and preparation method thereof - Google Patents
Tea bran silicone oil-free shampoo and preparation method thereof Download PDFInfo
- Publication number
- CN111419762A CN111419762A CN202010490673.5A CN202010490673A CN111419762A CN 111419762 A CN111419762 A CN 111419762A CN 202010490673 A CN202010490673 A CN 202010490673A CN 111419762 A CN111419762 A CN 111419762A
- Authority
- CN
- China
- Prior art keywords
- parts
- oil
- essential oil
- temperature
- tea bran
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/899—Poaceae or Gramineae (Grass family), e.g. bamboo, corn or sugar cane
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/04—Antipruritics
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/002—Preparations for repairing the hair, e.g. hair cure
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/008—Preparations for oily hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
- A61K2800/34—Free of silicones
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Epidemiology (AREA)
- Medicinal Chemistry (AREA)
- Pharmacology & Pharmacy (AREA)
- Botany (AREA)
- Dermatology (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Biotechnology (AREA)
- Organic Chemistry (AREA)
- Birds (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Alternative & Traditional Medicine (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Medical Informatics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to a tea bran silicone oil-free shampoo and a preparation method thereof. The shampoo has the advantages that the loose skin after losing weight is firmer, the shampoo has very good effects of resisting depression, bacteria, sterilization, dispelling flatulence, deodorizing, helping digestion, killing mold, preventing diseases, stimulating, tonifying body and the like by adopting the lemon grass essential oil, and is helpful for relieving itching, and the shampoo has the effects of removing hair oil, treating scalp itch, removing dandruff, stopping alopecia, growing hair and blackening and brightening hair by adopting the tea bran extract.
Description
Technical Field
The invention relates to shampoo, and particularly relates to tea bran silicone oil-free shampoo and a preparation method thereof.
Background
The shampoo is a necessary daily necessity in the life of people. With the improvement of living standard and the acceleration of life rhythm of people, factors such as environmental pollution, increased working pressure, irregular diet, hair dyeing and perming, the use of electronic products and the like bring great influence on the health of the hair quality of people, and the problems of vigorous hair grease secretion, little white hair, dandruff, alopecia and the like bring serious troubles to the daily life of people. How to have bright, smooth and elastic hair, and one head of the hair is beautiful and easy to comb becomes the identification standard of people for the quality requirement of the shampoo. Therefore, the shampoo is required to have the effects of removing dirt and dandruff, and also has the effects of environmental protection, alopecia prevention, itching relief, allergy resistance, deep conditioning and the like.
At present, shampoos with various functions sold in the market are generally produced by mixing chemical substances, the decontamination effect is obvious, but after long-term use, the side effects of the chemical substances are easy to cause hair nutrition loss, hair quality damage, hair becoming more and more rough, dry and withered and even alopecia, so that the development of the shampoo without silicone oil is necessary.
Disclosure of Invention
Aiming at the situation and overcoming the defects of the prior art, the invention provides the tea bran silicone-free shampoo and the preparation method thereof, the rosemary essential oil is adopted to have the effects of strong convergence, crease resistance and cortex regulation, conditioning greasy and dirty skin, promoting blood circulation, stimulating hair regeneration and enabling the loose skin after losing weight to be firmer, the lemon grass essential oil is adopted to enable the shampoo to have the effects of resisting depression, resisting bacteria, sterilizing, dispelling flatulence, deodorizing, helping digestion, killing mildew, preventing diseases, stimulating, tonifying body and the like, and the shampoo is helpful for relieving itching, and the tea bran extract is adopted to enable the shampoo to have the effects of removing hair oil, treating head itch, removing dandruff, stopping alopecia, growing hair and blackening and brightening hair.
In order to achieve the purpose, the invention provides the following technical scheme: the shampoo is mainly prepared from the following raw materials in parts by weight: 2-4 parts of ethyl benzoate, 1-2 parts of citral, 2-4 parts of amino acid, 1-3 parts of vitamin E, 2-4 parts of tea tree oil, 3-6 parts of oil-soluble tea polyphenol, 2-5 parts of tea bran extract, 6-8 parts of potassium sodium tartrate, 1-3 parts of alkyl acid phosphate, 10-15 parts of soapberry extract, 4-5 parts of saponin, 2-4 parts of alkyl glycoside, 4-7 parts of lemon grass essential oil, 4-9 parts of rosemary essential oil, 2-4 parts of euphorbia hirta extract and 30-40 parts of pure water.
The lemon grass essential oil is prepared by the following method: fresh leaves, flowers of lemon grass; II, tools used: a cutting machine, a distillation tower, a steam conveying pipe, a cooling tank and a filling bottle; thirdly, cleaning the cut lemongrass, and drying in the sun; fourthly, cutting the lemon grass into segments with the length of less than or equal to 2cm by using a cutting and crushing machine; fifthly, putting the cut lemon grass into a distillation tower for steam distillation, wherein the distillation temperature is more than or equal to 100 ℃ at 120 ℃, the bottom of a distillation pot needs to keep moisture, the raw materials cannot touch the bottom of the pot so as to avoid scorching, and the middle part needs to be loose, so that the airflow at the bottom can rise conveniently; sixthly, directly conveying the distilled mixed gas to a cooling tank through a gas conveying pipe, pressurizing and liquefying at a cooling temperature of-5 ℃ or more and less than 0 ℃, and separating ice blocks from the liquid to obtain the lemongrass essential oil; seventhly, filling the lemon grass essential oil into a bottle sealing cover at low temperature, wherein the temperature of the filling bottle is more than or equal to 5 ℃ below zero and is less than 0 ℃.
The rosemary essential oil is prepared by the following method: cleaning herba Rosmarini officinalis, cutting, and air drying with cold air; mixing vegetable white oil, coconut oil and olive oil, heating to 67 deg.C and keeping the temperature for 1 hr to obtain mixed essential oil; cutting radix Angelicae Dahuricae, folium Menthae, Aloe, fructus Lycii and herba Leonuri, adding into the mixed essential oil, heating to 89 deg.C under stirring, keeping the temperature for 3 hr, and cooling to room temperature; adding herba Rosmarini officinalis for standby, and performing ultrasonic high-speed dispersion at ultrasonic frequency of 12KHz at dispersion speed of 3560r/min for 45 min; filtering the obtained essential oil, and removing filter residue to obtain the final product.
The tea bran extract is prepared by the following method: 1) pulverizing tea bran; 2) then continuing the high-pressure micro-jet superfine grinding treatment to obtain paste slurry; 3) performing microwave extraction on the paste slurry to obtain a microwave extracting solution; 4) passing the microwave extract through macroporous resin chromatographic column, eluting with ethanol solution, and collecting eluate; 5) concentrating, and drying to obtain the desired tea bran extract.
The preparation method of the ethyl benzoate comprises the following steps: adding benzoic acid, absolute ethyl alcohol, modified clay and a water-carrying agent into a reaction container with a water separator, installing the water separator, a reflux condenser pipe and a thermometer on the reaction container, heating for reflux water separation, reacting until no water drops appear, discharging a water layer after cooling for 25min at normal temperature, washing the reaction liquid with water, drying, distilling the previous fraction, and collecting the fraction at 101-103 ℃ as a product.
The preparation method comprises the following steps: (1) humidifying raw materials of 1 part of citral, 2 parts of amino acid, 1 parts of vitamin E, 3 parts of oil-soluble tea polyphenol, 2 parts of tea bran extract, 6 parts of sodium potassium tartrate, 1 part of alkyl acid phosphate, 4 parts of saponin, 2 parts of alkyl glycoside, 4 parts of rosemary essential oil and 2 parts of euphorbia hirta extract, and then passing through a colloid mill to enable the raw materials to be in a relatively stable colloid state;
(2) adding 10-20 parts of pure water into an emulsifying pot, adding 2 parts of tea tree oil, heating to 100-115 ℃, decocting at 100-115 ℃ for 1-2.1 h, cooling and standing for 12-16 h;
(3) re-heating to 90-100 ℃, adding 2 parts of ethyl benzoate in the first step, homogenizing for 15-20 min, adding 10 parts of homogenized soapberry extract in the second step, and homogenizing for 10-30 min after adding; thirdly, adding 4 parts of lemongrass essential oil; the temperature is maintained at 78-83 ℃ during feeding;
(4) adding 2 parts of homogenized euphorbia hirta extract into an emulsifying pot at the temperature of 90-95 ℃, and stirring and homogenizing for 25-35 min;
(5) adding 20 parts of pure water into the emulsifying pot at the temperature of 90-95 ℃, stirring and homogenizing for 1.5-2.5 h, and then cooling; and finally, supplementing the rest water, and stirring and homogenizing for 1.5-2.5 h to obtain a finished product.
Has the advantages that: the shampoo has the effects of strongly astringing, preventing wrinkles and regulating cortex by adopting the rosemary essential oil, conditioning greasy and dirty skin, promoting blood circulation, stimulating hair regeneration and enabling the loose skin after losing weight to be firmer, has the effects of resisting depression, resisting bacteria, sterilizing, removing flatulence, deodorizing, helping digestion, killing mold, preventing diseases, exciting, tonifying body and the like by adopting the lemon grass essential oil, is favorable for relieving itching, and has the effects of removing hair oil, treating scalp itching, removing dandruff, stopping alopecia, growing hair and blackening and brightening hair by adopting the tea bran extract.
Detailed Description
The following provides a more detailed description of the embodiments of the present invention.
The invention provides a tea bran silicone oil-free shampoo and a preparation method thereof, wherein the shampoo is mainly prepared from the following raw materials in parts by weight: 2-4 parts of ethyl benzoate, 1-2 parts of citral, 2-4 parts of amino acid, 1-3 parts of vitamin E, 2-4 parts of tea tree oil, 3-6 parts of oil-soluble tea polyphenol, 2-5 parts of tea bran extract, 6-8 parts of potassium sodium tartrate, 1-3 parts of alkyl acid phosphate, 10-15 parts of soapberry extract, 4-5 parts of saponin, 2-4 parts of alkyl glycoside, 4-7 parts of lemon grass essential oil, 4-9 parts of rosemary essential oil, 2-4 parts of euphorbia hirta extract and 30-40 parts of pure water.
According to the technical scheme: the lemon grass essential oil is prepared by the following method: fresh leaves, flowers of lemon grass; II, tools used: a cutting machine, a distillation tower, a steam conveying pipe, a cooling tank and a filling bottle; thirdly, cleaning the cut lemongrass, and drying in the sun; fourthly, cutting the lemon grass into segments with the length of less than or equal to 2cm by using a cutting and crushing machine; fifthly, putting the cut lemon grass into a distillation tower for steam distillation, wherein the distillation temperature is more than or equal to 100 ℃ at 120 ℃, the bottom of a distillation pot needs to keep moisture, the raw materials cannot touch the bottom of the pot so as to avoid scorching, and the middle part needs to be loose, so that the airflow at the bottom can rise conveniently; sixthly, directly conveying the distilled mixed gas to a cooling tank through a gas conveying pipe, pressurizing and liquefying at a cooling temperature of-5 ℃ or more and less than 0 ℃, and separating ice blocks from the liquid to obtain the lemongrass essential oil; seventhly, filling the lemon grass essential oil into a bottle sealing cover at low temperature, wherein the temperature of the filling bottle is more than or equal to 5 ℃ below zero and is less than 0 ℃.
According to the technical scheme: the rosemary essential oil is prepared by the following method: cleaning herba Rosmarini officinalis, cutting, and air drying with cold air; mixing vegetable white oil, coconut oil and olive oil, heating to 67 deg.C and keeping the temperature for 1 hr to obtain mixed essential oil; cutting radix Angelicae Dahuricae, folium Menthae, Aloe, fructus Lycii and herba Leonuri, adding into the mixed essential oil, heating to 89 deg.C under stirring, keeping the temperature for 3 hr, and cooling to room temperature; adding herba Rosmarini officinalis for standby, and performing ultrasonic high-speed dispersion at ultrasonic frequency of 12KHz at dispersion speed of 3560r/min for 45 min; filtering the obtained essential oil, and removing filter residue to obtain the final product.
According to the technical scheme: the tea bran extract is prepared by the following method: 1) pulverizing tea bran; 2) then continuing the high-pressure micro-jet superfine grinding treatment to obtain paste slurry; 3) performing microwave extraction on the paste slurry to obtain a microwave extracting solution; 4) passing the microwave extract through macroporous resin chromatographic column, eluting with ethanol solution, and collecting eluate; 5) concentrating, and drying to obtain the desired tea bran extract.
According to the technical scheme: the preparation method of the ethyl benzoate comprises the following steps: adding benzoic acid, absolute ethyl alcohol, modified clay and a water-carrying agent into a reaction container with a water separator, installing the water separator, a reflux condenser pipe and a thermometer on the reaction container, heating for reflux water separation, reacting until no water drops appear, discharging a water layer after cooling for 25min at normal temperature, washing the reaction liquid with water, drying, distilling the previous fraction, and collecting the fraction at 101-103 ℃ as a product.
The preparation method comprises the following steps: (1) humidifying raw materials of 1 part of citral, 2 parts of amino acid, 1 parts of vitamin E, 3 parts of oil-soluble tea polyphenol, 2 parts of tea bran extract, 6 parts of sodium potassium tartrate, 1 part of alkyl acid phosphate, 4 parts of saponin, 2 parts of alkyl glycoside, 4 parts of rosemary essential oil and 2 parts of euphorbia hirta extract, and then passing through a colloid mill to enable the raw materials to be in a relatively stable colloid state;
(2) adding 10-20 parts of pure water into an emulsifying pot, adding 2 parts of tea tree oil, heating to 100-115 ℃, decocting at 100-115 ℃ for 1-2.1 h, cooling and standing for 12-16 h;
(3) re-heating to 90-100 ℃, adding 2 parts of ethyl benzoate in the first step, homogenizing for 15-20 min, adding 10 parts of homogenized soapberry extract in the second step, and homogenizing for 10-30 min after adding; thirdly, adding 4 parts of lemongrass essential oil; the temperature is maintained at 78-83 ℃ during feeding;
(4) adding 2 parts of homogenized euphorbia hirta extract into an emulsifying pot at the temperature of 90-95 ℃, and stirring and homogenizing for 25-35 min;
(5) adding 20 parts of pure water into the emulsifying pot at the temperature of 90-95 ℃, stirring and homogenizing for 1.5-2.5 h, and then cooling; and finally, supplementing the rest water, and stirring and homogenizing for 1.5-2.5 h to obtain a finished product.
The second embodiment of the invention provides a tea bran silicone oil-free shampoo and a preparation method thereof, wherein the shampoo is mainly prepared from the following raw materials in parts by weight: 2-4 parts of ethyl benzoate, 1-2 parts of citral, 2-4 parts of amino acid, 1-3 parts of vitamin E, 2-4 parts of tea tree oil, 3-6 parts of oil-soluble tea polyphenol, 2-5 parts of tea bran extract, 6-8 parts of potassium sodium tartrate, 1-3 parts of alkyl acid phosphate, 10-15 parts of soapberry extract, 4-5 parts of saponin, 2-4 parts of alkyl glycoside, 4-7 parts of lemon grass essential oil, 4-9 parts of rosemary essential oil, 2-4 parts of euphorbia hirta extract and 30-40 parts of pure water.
According to the technical scheme: the lemon grass essential oil is prepared by the following method: fresh leaves, flowers of lemon grass; II, tools used: a cutting machine, a distillation tower, a steam conveying pipe, a cooling tank and a filling bottle; thirdly, cleaning the cut lemongrass, and drying in the sun; fourthly, cutting the lemon grass into segments with the length of less than or equal to 2cm by using a cutting and crushing machine; fifthly, putting the cut lemon grass into a distillation tower for steam distillation, wherein the distillation temperature is more than or equal to 100 ℃ at 120 ℃, the bottom of a distillation pot needs to keep moisture, the raw materials cannot touch the bottom of the pot so as to avoid scorching, and the middle part needs to be loose, so that the airflow at the bottom can rise conveniently; sixthly, directly conveying the distilled mixed gas to a cooling tank through a gas conveying pipe, pressurizing and liquefying at a cooling temperature of-5 ℃ or more and less than 0 ℃, and separating ice blocks from the liquid to obtain the lemongrass essential oil; seventhly, filling the lemon grass essential oil into a bottle sealing cover at low temperature, wherein the temperature of the filling bottle is more than or equal to 5 ℃ below zero and is less than 0 ℃.
According to the technical scheme: the rosemary essential oil is prepared by the following method: cleaning herba Rosmarini officinalis, cutting, and air drying with cold air; mixing vegetable white oil, coconut oil and olive oil, heating to 67 deg.C and keeping the temperature for 1 hr to obtain mixed essential oil; cutting radix Angelicae Dahuricae, folium Menthae, Aloe, fructus Lycii and herba Leonuri, adding into the mixed essential oil, heating to 89 deg.C under stirring, keeping the temperature for 3 hr, and cooling to room temperature; adding herba Rosmarini officinalis for standby, and performing ultrasonic high-speed dispersion at ultrasonic frequency of 12KHz at dispersion speed of 3560r/min for 45 min; filtering the obtained essential oil, and removing filter residue to obtain the final product.
The tea bran extract is prepared by the following method: 1) pulverizing tea bran; 2) then continuing the high-pressure micro-jet superfine grinding treatment to obtain paste slurry; 3) performing microwave extraction on the paste slurry to obtain a microwave extracting solution; 4) passing the microwave extract through macroporous resin chromatographic column, eluting with ethanol solution, and collecting eluate; 5) concentrating, and drying to obtain the desired tea bran extract.
According to the technical scheme: the preparation method of the ethyl benzoate comprises the following steps: adding benzoic acid, absolute ethyl alcohol, modified clay and a water-carrying agent into a reaction container with a water separator, installing the water separator, a reflux condenser pipe and a thermometer on the reaction container, heating for reflux water separation, reacting until no water drops appear, discharging a water layer after cooling for 25min at normal temperature, washing the reaction liquid with water, drying, distilling the previous fraction, and collecting the fraction at 101-103 ℃ as a product.
The preparation method comprises the following steps: (1) humidifying raw materials of 2 parts of citral, 4 parts of amino acid, 3 parts of vitamin E, 6 parts of oil-soluble tea polyphenol, 5 parts of tea bran extract, 8 parts of sodium potassium tartrate, 3 parts of alkyl acid phosphate, 5 parts of saponin, 4 parts of alkyl glycoside, 9 parts of rosemary essential oil and 4 parts of euphorbia hirta extract, and then passing through a colloid mill to enable the raw materials to be in a relatively stable colloid state;
(2) adding 20 parts of pure water into an emulsifying pot, adding 4 parts of tea tree oil, heating to 100-115 ℃, decocting at 100-115 ℃ for 1-2.1 h, cooling and standing for 12-16 h;
(3) re-heating to 90-100 ℃, adding 4 parts of ethyl benzoate in the first step, homogenizing for 15-20 min, adding 15 parts of homogenized soapberry extract in the second step, and homogenizing for 10-30 min after adding; thirdly, adding 7 parts of lemongrass essential oil; the temperature is maintained at 78-83 ℃ during feeding;
(4) adding 4 parts of homogenized euphorbia hirta extract into an emulsifying pot at the temperature of 90-95 ℃, and stirring and homogenizing for 25-35 min;
(5) adding 35 parts of pure water into the emulsifying pot at the temperature of 90-95 ℃, stirring and homogenizing for 1.5-2.5 h, and then cooling; and finally, supplementing the rest water, and stirring and homogenizing for 1.5-2.5 h to obtain a finished product.
Has the advantages that: the shampoo has the effects of strongly astringing, preventing wrinkles and regulating cortex by adopting the rosemary essential oil, conditioning greasy and dirty skin, promoting blood circulation, stimulating hair regeneration and enabling the loose skin after losing weight to be firmer, has the effects of resisting depression, resisting bacteria, sterilizing, removing flatulence, deodorizing, helping digestion, killing mold, preventing diseases, exciting, tonifying body and the like by adopting the lemon grass essential oil, is favorable for relieving itching, and has the effects of removing hair oil, treating scalp itching, removing dandruff, stopping alopecia, growing hair and blackening and brightening hair by adopting the tea bran extract.
Has the advantages that: the packing box is novel in structure, ingenious in conception, high in drying efficiency of the packing box body 1, good in drying effect and convenient to carry the packing box body 1, and meanwhile, the packing belt can penetrate through the groove 8 to be packed, so that the packing belt is prevented from shaking.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that changes may be made in the embodiments and/or equivalents thereof without departing from the spirit and scope of the invention. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (6)
1. The silicone oil-free tea bran shampoo is characterized in that: the shampoo is mainly prepared from the following raw materials in parts by weight: 2-4 parts of ethyl benzoate, 1-2 parts of citral, 2-4 parts of amino acid, 1-3 parts of vitamin E, 2-4 parts of tea tree oil, 3-6 parts of oil-soluble tea polyphenol, 2-5 parts of tea bran extract, 6-8 parts of potassium sodium tartrate, 1-3 parts of alkyl acid phosphate, 10-15 parts of soapberry extract, 4-5 parts of saponin, 2-4 parts of alkyl glycoside, 4-7 parts of lemon grass essential oil, 4-9 parts of rosemary essential oil, 2-4 parts of euphorbia hirta extract and 30-40 parts of pure water.
2. The tea bran silicone oil-free shampoo as claimed in claim 1, wherein the lemon grass essential oil is prepared by the following method: fresh leaves, flowers of lemon grass; II, tools used: a cutting machine, a distillation tower, a steam conveying pipe, a cooling tank and a filling bottle; thirdly, cleaning the cut lemongrass, and drying in the sun; fourthly, cutting the lemon grass into segments with the length of less than or equal to 2cm by using a cutting and crushing machine; fifthly, putting the cut lemon grass into a distillation tower for steam distillation, wherein the distillation temperature is more than or equal to 100 ℃ at 120 ℃, the bottom of a distillation pot needs to keep moisture, the raw materials cannot touch the bottom of the pot so as to avoid scorching, and the middle part needs to be loose, so that the airflow at the bottom can rise conveniently; sixthly, directly conveying the distilled mixed gas to a cooling tank through a gas conveying pipe, pressurizing and liquefying at a cooling temperature of-5 ℃ or more and less than 0 ℃, and separating ice blocks from the liquid to obtain the lemongrass essential oil; seventhly, filling the lemon grass essential oil into a bottle sealing cover at low temperature, wherein the temperature of the filling bottle is more than or equal to 5 ℃ below zero and is less than 0 ℃.
3. The tea bran silicone oil-free shampoo as claimed in claim 1, wherein the rosemary essential oil is prepared by the following method: cleaning herba Rosmarini officinalis, cutting, and air drying with cold air; mixing vegetable white oil, coconut oil and olive oil, heating to 67 deg.C and keeping the temperature for 1 hr to obtain mixed essential oil; cutting radix Angelicae Dahuricae, folium Menthae, Aloe, fructus Lycii and herba Leonuri, adding into the mixed essential oil, heating to 89 deg.C under stirring, keeping the temperature for 3 hr, and cooling to room temperature; adding herba Rosmarini officinalis for standby, and performing ultrasonic high-speed dispersion at ultrasonic frequency of 12KHz at dispersion speed of 3560r/min for 45 min; filtering the obtained essential oil, and removing filter residue to obtain the final product.
4. The tea bran silicone oil-free shampoo as claimed in claim 1, wherein the tea bran extract is prepared by the following method: 1) pulverizing tea bran; 2) then continuing the high-pressure micro-jet superfine grinding treatment to obtain paste slurry; 3) performing microwave extraction on the paste slurry to obtain a microwave extracting solution; 4) passing the microwave extract through macroporous resin chromatographic column, eluting with ethanol solution, and collecting eluate; 5) concentrating, and drying to obtain the desired tea bran extract.
5. The tea bran silicone oil-free shampoo as claimed in claim 1, wherein the preparation method of the ethyl benzoate comprises the following steps: adding benzoic acid, absolute ethyl alcohol, modified clay and a water-carrying agent into a reaction container with a water separator, installing the water separator, a reflux condenser pipe and a thermometer on the reaction container, heating for reflux water separation, reacting until no water drops appear, discharging a water layer after cooling for 25min at normal temperature, washing the reaction liquid with water, drying, distilling the previous fraction, and collecting the fraction at 101-103 ℃ as a product.
6. The preparation method of the tea bran silicone oil-free shampoo is characterized by comprising the following steps:
(1) humidifying raw materials of 1-2 parts of citral, 2-4 parts of amino acid, 1-3 parts of vitamin E, 3-6 parts of oil-soluble tea polyphenol, 2-5 parts of tea bran extract, 6-8 parts of sodium potassium tartrate, 1-3 parts of alkyl acid phosphate, 4-5 parts of saponin, 2-4 parts of alkyl glycoside, 4-9 parts of rosemary essential oil and 2-4 parts of euphorbia hirta extract, and then passing through a colloid mill to enable the raw materials to be in a relatively stable colloid state;
(2) adding 10-20 parts of pure water into an emulsifying pot, adding 2-4 parts of tea tree oil, heating to 100-115 ℃, decocting at 100-115 ℃ for 1-2.1 h, cooling and standing for 12-16 h;
(3) re-heating to 90-100 ℃, adding 2-4 parts of ethyl benzoate in the first step, homogenizing for 15-20 min, adding 10-15 parts of homogenized soapberry extract in the second step, and homogenizing for 10-30 min after adding; thirdly, adding 4-7 parts of lemon grass essential oil; the temperature is maintained at 78-83 ℃ during feeding;
(4) adding 2-4 parts of homogenized euphorbia hirta extract into an emulsifying pot at the temperature of 90-95 ℃, and stirring and homogenizing for 25-35 min;
(5) adding 20-35 parts of pure water into the emulsifying pot at the temperature of 90-95 ℃, stirring and homogenizing for 1.5-2.5 h, and then cooling; and finally, supplementing the rest water, and stirring and homogenizing for 1.5-2.5 h to obtain a finished product.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202010490673.5A CN111419762A (en) | 2020-06-02 | 2020-06-02 | Tea bran silicone oil-free shampoo and preparation method thereof |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202010490673.5A CN111419762A (en) | 2020-06-02 | 2020-06-02 | Tea bran silicone oil-free shampoo and preparation method thereof |
Publications (1)
Publication Number | Publication Date |
---|---|
CN111419762A true CN111419762A (en) | 2020-07-17 |
Family
ID=71553192
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN202010490673.5A Pending CN111419762A (en) | 2020-06-02 | 2020-06-02 | Tea bran silicone oil-free shampoo and preparation method thereof |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN111419762A (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111991261A (en) * | 2020-08-21 | 2020-11-27 | 广州德谷个人护理用品有限公司 | Mild oil control shampoo composition suitable for sensitive scalp and preparation method thereof |
CN111991303A (en) * | 2020-09-27 | 2020-11-27 | 广州德谷个人护理用品有限公司 | Plant extract composition with multi-target scalp oil control and dandruff removal effects, preparation method thereof and scalp care composition |
CN113425636A (en) * | 2021-05-21 | 2021-09-24 | 广州德谷个人护理用品有限公司 | Preparation method of tea bran flavone and application of tea bran flavone in anti-hair loss product |
Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104311414A (en) * | 2014-09-16 | 2015-01-28 | 常州市松盛香料有限公司 | Preparation method of ethyl benzoate |
CN104490644A (en) * | 2014-11-22 | 2015-04-08 | 青岛海芬海洋生物科技有限公司 | Plant composition for hair care |
CN106491403A (en) * | 2016-12-07 | 2017-03-15 | 王领娣 | A kind of rosemary ethereal oil |
CN106806176A (en) * | 2017-03-28 | 2017-06-09 | 钦州市桂耘贸易有限公司 | Tea bran extract and preparation method thereof |
CN109181880A (en) * | 2018-10-18 | 2019-01-11 | 吕小萍 | The extracting method of lemon grass (Cymbopogon citratus) essential oil |
CN109316396A (en) * | 2017-07-31 | 2019-02-12 | 何学军 | A kind of no silicone oil shampoo |
-
2020
- 2020-06-02 CN CN202010490673.5A patent/CN111419762A/en active Pending
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104311414A (en) * | 2014-09-16 | 2015-01-28 | 常州市松盛香料有限公司 | Preparation method of ethyl benzoate |
CN104490644A (en) * | 2014-11-22 | 2015-04-08 | 青岛海芬海洋生物科技有限公司 | Plant composition for hair care |
CN106491403A (en) * | 2016-12-07 | 2017-03-15 | 王领娣 | A kind of rosemary ethereal oil |
CN106806176A (en) * | 2017-03-28 | 2017-06-09 | 钦州市桂耘贸易有限公司 | Tea bran extract and preparation method thereof |
CN109316396A (en) * | 2017-07-31 | 2019-02-12 | 何学军 | A kind of no silicone oil shampoo |
CN109181880A (en) * | 2018-10-18 | 2019-01-11 | 吕小萍 | The extracting method of lemon grass (Cymbopogon citratus) essential oil |
Non-Patent Citations (3)
Title |
---|
国家药品监督管理局: "《《化妆品安全技术规范(2015年版)》2021年修订版》", 26 May 2021 * |
崔钟雷: "《魅力女人》", 31 January 2015, 黑龙江美术出版社 * |
王亮: "《精油的科学》", 31 December 2018, 东南大学出版社 * |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111991261A (en) * | 2020-08-21 | 2020-11-27 | 广州德谷个人护理用品有限公司 | Mild oil control shampoo composition suitable for sensitive scalp and preparation method thereof |
CN111991261B (en) * | 2020-08-21 | 2021-10-08 | 广州德谷个人护理用品有限公司 | Mild oil control shampoo composition suitable for sensitive scalp and preparation method thereof |
CN111991303A (en) * | 2020-09-27 | 2020-11-27 | 广州德谷个人护理用品有限公司 | Plant extract composition with multi-target scalp oil control and dandruff removal effects, preparation method thereof and scalp care composition |
CN111991303B (en) * | 2020-09-27 | 2022-11-04 | 广州德谷个人护理用品有限公司 | Plant extract composition with multi-target scalp oil control and dandruff removal effects, preparation method thereof and scalp care composition |
CN113425636A (en) * | 2021-05-21 | 2021-09-24 | 广州德谷个人护理用品有限公司 | Preparation method of tea bran flavone and application of tea bran flavone in anti-hair loss product |
CN113425636B (en) * | 2021-05-21 | 2023-01-31 | 广州德谷个人护理用品有限公司 | Preparation method of tea bran flavone and application of tea bran flavone in anti-hair loss product |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN111419762A (en) | Tea bran silicone oil-free shampoo and preparation method thereof | |
KR102017187B1 (en) | Composition for preventing hair loss and promoting hair growth and manufacturing method thereof | |
CN107157861B (en) | Chrysanthemum hydrolat and beauty fluid prepared from same | |
CN107281020A (en) | A kind of preparation method of maca whitening and skin-protecting emulsion | |
CN110354031A (en) | A kind of toner and preparation method thereof adjusting skin water and oil balance | |
KR20130123626A (en) | Sea cucumber composition capable of preventing alopecia and skin-aging and environment-friendly cosmetic products using the same | |
CN106038464A (en) | Composite anti-wrinkle skin care product and preparation method thereof | |
CN107095820A (en) | A kind of preparation method of saururus chinensis whitening emulsion | |
KR101281059B1 (en) | Shampoo composition and the manufacturing method thereof | |
CN108524336A (en) | A kind of Fatsia japonica natural activity face cream and preparation method thereof | |
CN102711527A (en) | Preparation method of tea water, and tea water obtained thereby | |
CN105726363A (en) | Plant care composition and preparation method thereof | |
CN109157475A (en) | Dendrobium candidum facial mask and preparation method thereof | |
CN105434264B (en) | A kind of motherwort toothpaste | |
CN104013565B (en) | A kind of hair protecting shampoo | |
CN112870141A (en) | Edible natural plant skin-care mask lotion and preparation method thereof | |
KR101281060B1 (en) | Composition for accelerating hair groth and the manufacturing method thereof | |
CN110897971A (en) | Hair care cleaning composition containing selaginella tamariscina and preparation method thereof | |
CN105596281A (en) | Sleep mask with functions of acne treatment and beautifying and preparation method of sleep mask | |
CN105902481B (en) | A kind of cosmetics and its preparation process containing traditional Chinese medicinal components | |
CN107714551A (en) | A kind of shampoo | |
CN109528616A (en) | A kind of preparation method of rose facial mask | |
CN104116649A (en) | Jasminum sambac oil with whitening function and preparation technology thereof | |
CN109010211A (en) | It is a kind of for preventing and treating the facial cleanser of subcutaneous fat tumor | |
CN1031861C (en) | Composite cosmetics containing natural rhodiola root and preparation method thereof |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
RJ01 | Rejection of invention patent application after publication |
Application publication date: 20200717 |
|
RJ01 | Rejection of invention patent application after publication |