CN110305745A - A kind of elongation rock soap and preparation method thereof - Google Patents
A kind of elongation rock soap and preparation method thereof Download PDFInfo
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- CN110305745A CN110305745A CN201910691907.XA CN201910691907A CN110305745A CN 110305745 A CN110305745 A CN 110305745A CN 201910691907 A CN201910691907 A CN 201910691907A CN 110305745 A CN110305745 A CN 110305745A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
- C11D10/042—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap based on anionic surface-active compounds and soap
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Abstract
The present invention provides a kind of elongation rock soap, the raw material for preparing the elongation rock soap includes elongating mountain flour and soap base matter, and the partial size for elongating mountain flour is 1.5 μm -2 μm, and the mountain flour and the mass ratio of soap base matter of elongating is 5-10: 60-80；Elongation rock soap provided by the invention has effects that significantly to improve cock skin skin, and it is less to elongate precipitating of the mountain flour in soap.
Description
Technical field
The invention belongs to cosmetic field, in particular to a kind of elongation rock soap and preparation method thereof.
Background technique
Perfumed soap is by extensive received personal cleanliness's articles, and cleaning capacity is stronger, and price is relatively inexpensive, is in people's life
Necessity is mainly grouped as, generally solid block by fat, grease and salt group, but also has paste and liquid product, in order to increase
The cleaning action or other effects of strong perfumed soap；Labradorite is one kind of plagioclase, the class matter being made of albite and anorthite
With as series, common to make ornaments, labradorite, which acts on, has effects that sedate, firm, long wavelength, relieving fatigue, helps to add
Strong vitality promotes physical strength, endurance, and it is scorching to remove human body, is very beneficial to human body, the prior art often in perfumed soap plus
Enter traditional Chinese medicine ingredients or other ingredients to skin beneficiating, but yet there are no the research being applied to labradorite in perfumed soap.
Summary of the invention
In order to fill up the blank of the prior art, the present invention provides a kind of elongation rock soaps and preparation method thereof, and the present invention is also
Providing a kind of elongation rock soap has effects that improve cock skin skin.
Specific technical solution of the present invention is as follows:
The present invention provides a kind of elongation rock soap, the raw material for preparing the elongation rock soap includes elongating mountain flour and soap base matter, is drawn
The partial size of feldspar powder is 1.5 μm -2 μm, and the mass ratio for elongating mountain flour and soap base matter is 5-10: 60-80.
Further, raw material further includes tremella powder, active carbon, elongates stone powder, tremella powder, active carbon and labradorite soap base
The mass ratio of matter is 5-10: 5-10: 10-20: 60-80.
Wherein, soap base matter includes that can be prepared into the combination for the auxiliary material for elongating rock soap；The present invention by numerous studies find,
Skin can be infiltrated through by chafing against skin and on a small quantity by elongating mountain flour, served both functions to the treatment of cock skin skin, worked as elongation
When the partial size of stone is less than 1.5 μm, the effect for improving cock skin skin will be greatly lowered, but when its partial size is greater than 1 μm, preparation
A large amount of labradorite powder precipitation will be generated in elongate rock soap bottom the phenomenon that by elongating rock soap, in order to overcome the technical problem,
Tremella powder and active carbon is added in the present invention in the preparation process for elongating rock soap, makes 1.5 μm -2 μm of partial size of elongation stone powder
It can be distributed evenly in and elongate in rock soap, reduce the amount that mountain flour precipitates in elongating rock soap of elongating.
Further, the mass ratio for elongating stone powder, tremella powder, active carbon and soap base matter is 5: 8: 15: 72.
The present invention uses the elongation stone powder of the above ratio, tremella powder, active carbon and soap base by the way that largely research confirms
Matter can reduce the amount that mountain flour precipitates in elongating rock soap of elongating to the maximum extent.
Further, the partial size of tremella powder is 80 μm -100 μm.
The research of the invention finds that elongating mountain flour when the partial size of tremella powder is 80 μm -100 μm and being precipitated in elongating rock soap
Amount it is less.
Further, the partial size of active carbon is 30 μm -40 μm.
The study find that can further decrease when the partial size of active carbon is 30 μm -40 μm and elongate mountain flour in labradorite
The amount precipitated in soap.
Further, soap base matter includes sodium citrate, water, neat soap, glucono-δ-lactone, plants essential oil and dodecane
Base benzene sulfonic acid sodium salt, the quality of sodium citrate, water, neat soap, glucono-δ-lactone, plants essential oil and neopelex
Than being 0.4-0.6: 20-30: 60-70: 1-2: 0.1-0.5: 10-15.
The present invention passes through the ingredient for specifically limiting soap base matter, and the above ingredient is made with mountain flour, tremella powder and active carbon is elongated
Elongation rock soap be not easy to paste it is rotten, it is more durable.
Further, sodium citrate, water, neat soap, glucono-δ-lactone, plants essential oil and neopelex
Mass ratio be 0.5: 25: 65: 1.5: 0.3: 12.
Wherein, neat soap of the invention refers to the complex mixture of fatty acid sodium salt；Wherein, plants essential oil includes rhodamine toner
The harmless essential oil that oil, Lavender etc. are gone out with plant extract；The research of the invention finds that passing through the above mass ratio
The rotten degree of paste of the elongation rock soap of soap base matter preparation is minimum, after the paste column degree in the present invention refers to that elongating rock soap part ducks in drink
The degree being soaked in water refers specifically to be the thickness for elongating the rotten layer of paste that rock soap was flooded after profit a period of time, when by labradorite
When being prepared into common perfumed soap, labradorite used be powdery, preferably 5000-6000 mesh.
Preferably, soap base matter further includes that glycyrrhiza glabra extract, Artemisia capillaris flower extract, mulberry root extract and scutellariae,radix mention
Take object.
The present invention can play the role of skin whitening, when will elongate by four kinds of ingredients more than adding in soap base matter
When stone is prepared into the perfumed soap with whitening function, labradorite used be powdery, preferably 6000-7000 mesh.
Preferably, soap base matter includes plant ass, animal and plant fat and salt.
Wherein, plant ass includes but is not limited to ashes made from the burning plants such as Chenopodiaceae chenopodium ambrosiodies, thorn Chenopodiaceae, fragrant Chenopodiaceae, can also be with
The above soap base matter is replaced with other soap base matter for being used to prepare soap labradorite soap is made；The present invention is by specifically limiting soap
Labradorite is applied to soap, can be used for cleaning clothing etc., improve the cleaning effect of soap, be prepared into when by labradorite by matrix
When soap, labradorite used be powdery, preferably 3000-4000 mesh.
Further, mountain flour is elongated to be prepared from the following steps:
(1) it pre-processes: taking labradorite, clean；
(2) boiling: pretreated labradorite pearl is placed in reaction kettle, boiling is added to boil, wherein labradorite pearl and water
Volume ratio is 1: 8-10, and adjustment pressure is 600-800KPa, primary every 6-8min stirring, stirs 3-5min, stirring speed every time
Degree is 50-70prm, altogether boiling 8-10h, is down to room temperature, takes out labradorite；
(3) crush: it is 1.5 μm -2 μm that the labradorite pearl after boiling, which is handled to partial size,.
Wherein, then the present invention crushes by carrying out boiling to labradorite, can remove the foul in labradorite and surface
Bacterium.
Further, step (3) crush specifically includes the following steps:
(31) it prepares labradorite coarse powder: the labradorite after boiling being dried, 1000 meshes were crushed to, it is thick that labradorite is made
Powder；
(32) it prepares labradorite mixed liquor: labradorite coarse powder is placed in grinding device, add first time water with 200-
The mass ratio of the speed grinding 5-10min of 300prm, labradorite coarse powder and first time water is 10-12: 5-10, then in grinding device
Middle that second of water is added with the speed grinding 20-40min of 800-1000prm, the mass ratio of second of water and labradorite coarse powder is
10-12: 100-150, labradorite mixed liquor is made；
(33) stone powder is elongated in preparation: standing 2min-3min, incline supernatant, and gained is precipitated as the first precipitating, by first
Step (32) are repeated after precipitating drying, supernatant is stood into -36h for 24 hours, incline supernatant, and gained is precipitated as the second precipitating, by the
Two precipitating drying, being ground to partial size is 1.5 μm -2 μm to get elongation stone powder.
The present invention crushes labradorite by above method, and can filter out in labradorite more has improvement cock skin skin
The substance of effect gives up the substance of effect difference in labradorite, further increases the therapeutic effect for elongating rock soap to cock skin skin.
The present invention also provides it is a kind of elongate rock soap preparation method, which is characterized in that method the following steps are included:
S1: the sodium citrate of definite quality ratio is added in the water of definite quality ratio, stirring while adding to sodium citrate
It completely dissolves in water, is cooled to 40 DEG C -45 DEG C, sodium citrate solution is made；
S2: by the neat soap of definite quality ratio, plants essential oil, glucono-δ-lactone, plants essential oil and detergent alkylate sulphur
Sour sodium is placed in heating container and is heated to 80 DEG C -95 DEG C, stirs evenly, and the first mixed solution is made；
S3: the tremella powder of definite quality ratio and active carbon are added in mixed solution and stirred under conditions of temperature-resistant
The second mixed solution is made in 15min-20min；
S4: the elongation stone powder of definite quality ratio is added in the second mixed solution, is stirred with the speed of 60prm-80prm
30min-50min is mixed, third mixed solution is made；
S5: sodium citrate solution is poured into third mixed solution, stirs 10min- under the speed of 500prm-600prm
20min pours into grinding tool, is covered grinding tool with plastic film, places 2-3 days under the conditions of 30-38 DEG C to get rock soap is elongated.
The rotten degree of paste that rock soap is elongated as made from above method is lower.
The present invention also provides elongate rock soap to have the application in the cosmetics for improving chicken skin effects in preparation.
Elongation rock soap provided by the invention has effects that significantly to improve cock skin skin, and elongates mountain flour in elongating rock soap
Precipitating it is less.
Specific embodiment
Embodiment 1
A kind of elongation rock soap, the elongation rock soap include elongating stone powder, tremella powder, active carbon and soap base matter, elongate mountain flour
End is prepared by labradorite, and the partial size for elongating stone powder is 1.5 μm, elongates stone powder, tremella powder, active carbon and soap base matter
Quality is respectively 80g, 50g, 100g, 600g；
Wherein, soap base matter includes the sodium citrate that mass ratio is 0.5: 25: 65: 1.5: 0.3: 12, water, neat soap, white oil, olive
Olive oil and neopelex；
The partial size of tremella powder is 150 μm；
The partial size of active carbon is 50 μm；
Elongating mountain flour is that labradorite is directly crushed to 1.5 μm to be made；
The preparation method of the elongation rock soap the following steps are included:
S1: the sodium citrate of definite quality ratio being added in the water of definite quality ratio, stirs evenly, is cooled to room temperature,
Sodium citrate solution is made；
S2: the neat soap of definite quality ratio, white oil, olive oil, tremella powder and active carbon are placed in heating container and heated
It to 60 DEG C, stirs evenly, total mixed solution is made；
S4: the elongation stone powder of definite quality ratio is added in total mixed solution, stirs 30min with the speed of 60prm,
Labradorite mixed solution is made；
S5: sodium citrate solution being poured into labradorite mixed solution, is stirred evenly, grinding tool is poured into, will with plastic film
Grinding tool covers, and places 2 days under the conditions of 30 DEG C, is equably cut into blocky to get elongation rock soap；
All neat soaps in the embodiment of the present invention are purchased from Qingdao Taurus oil technology Co., Ltd.
Embodiment 2
A kind of elongation rock soap, the elongation rock soap include elongating stone powder, tremella powder, active carbon and soap base matter, elongate mountain flour
End is prepared by labradorite, and the partial size for elongating stone powder is 1.5 μm, elongates stone powder, tremella powder, active carbon and soap base matter
Quality is respectively 50g, 80g, 150g, 720g；
Soap base matter includes the sodium citrate that mass ratio is 0.5: 25: 65: 1.5: 0.3: 12, water, neat soap, sunflower oil, mustard
Oil and neopelex；
The partial size of tremella powder is 50 μm；
The partial size of active carbon is 20 μm；
Elongating mountain flour is that labradorite is directly crushed to 1.5 μm to be made；
The preparation method is the same as that of Example 1 for the elongation rock soap.
Embodiment 3
A kind of elongation rock soap, the elongation rock soap include elongating stone powder, tremella powder, active carbon and soap base matter, elongate mountain flour
End is prepared by labradorite, and the partial size for elongating stone powder is 2 μm, elongates the matter of stone powder, tremella powder, active carbon and soap base matter
Amount is respectively 100g, 100g, 200g, 800g；
Soap base matter includes the sodium citrate that mass ratio is 0.5: 25: 65: 1.5: 0.3: 12, water, neat soap, cocoa butter, beeswax
And neopelex；
The partial size of tremella powder is 200 μm；
The partial size of active carbon is 100 μm；
Elongating mountain flour is that labradorite is directly crushed to 1.5 μm to be made；
The preparation method is the same as that of Example 1 for the elongation rock soap.
Embodiment 4
A kind of elongation rock soap, the elongation rock soap include elongating stone powder, tremella powder, active carbon and soap base matter, elongate mountain flour
End is prepared by labradorite, and the partial size for elongating stone powder is 1.5 μm, elongates stone powder, tremella powder, active carbon and soap base matter
Quality is respectively 80g, 50g, 100g, 600g；
Wherein, soap base matter include mass ratio be 0.5: 25: 65: 1.5: 0.3: 12 sodium citrate, water, neat soap, cocoa butter,
Beeswax and neopelex；
The partial size of tremella powder is 80 μm；
The partial size of active carbon is 50 μm；
Elongating mountain flour is that labradorite is directly crushed to 1.5 μm to be made；
The preparation method is the same as that of Example 1 for the elongation rock soap.
Embodiment 5
A kind of elongation rock soap, the elongation rock soap include elongating stone powder, tremella powder, active carbon and soap base matter, elongate mountain flour
End is prepared by labradorite, and the partial size for elongating stone powder is 1.5 μm, elongates stone powder, tremella powder, active carbon and soap base matter
Quality is respectively 50g, 80g, 150g, 720g；
Wherein, soap base matter include mass ratio be 0.5: 25: 65: 1.5: 0.3: 12 sodium citrate, water, neat soap, cocoa butter,
Beeswax and neopelex；
The partial size of tremella powder is 50 μm；
The partial size of active carbon is 40 μm；
Elongating mountain flour is that labradorite is directly crushed to 1.5 μm to be made；
The preparation method is the same as that of Example 1 for the elongation rock soap.
Embodiment 6
A kind of elongation rock soap, the elongation rock soap include elongating stone powder, tremella powder, active carbon and soap base matter, elongate mountain flour
End is prepared by labradorite, and the partial size for elongating stone powder is 2 μm, elongates the matter of stone powder, tremella powder, active carbon and soap base matter
Amount is respectively 100g, 100g, 200g, 800g；
Wherein, soap base matter include mass ratio be 0.5: 25: 65: 1.5: 0.3: 12 sodium citrate, water, neat soap, cocoa butter,
Beeswax and neopelex；
The partial size of tremella powder is 90 μm；
The partial size of active carbon is 35 μm；
Elongating mountain flour is that labradorite is directly crushed to 1.5 μm to be made；
The preparation method is the same as that of Example 1 for the elongation rock soap.
Embodiment 7
A kind of elongation rock soap, the elongation rock soap include elongating stone powder, tremella powder, active carbon and soap base matter, elongate mountain flour
End is prepared by labradorite, and the partial size for elongating stone powder is 1.5 μm, elongates stone powder, tremella powder, active carbon and soap base matter
Quality is respectively 50g, 80g, 105g, 720g；
Wherein, soap base matter include mass ratio be 0.5: 25: 65: 1.5: 0.3: 12 sodium citrate, water, neat soap, cocoa butter,
Beeswax and neopelex；
The partial size of tremella powder is 50 μm；
The partial size of active carbon is 40 μm；
Elongating mountain flour is that labradorite is directly crushed to 1.5 μm to be made.
Wherein, mountain flour is elongated to be prepared from the following steps:
(1) it pre-processes: taking labradorite, clean；
(2) boiling: pretreated labradorite pearl is placed in reaction kettle, boiling is added to boil, wherein labradorite pearl and water
Volume ratio is 1: 8, and adjustment pressure is 600KPa, primary every 6min stirring, stirs 3min, mixing speed 50prm every time, altogether
Boiling 8h is down to room temperature, takes out labradorite；
(3) crush: it is 1.5 μm that the labradorite pearl after boiling, which is handled to partial size,；
The preparation method is the same as that of Example 1 for the elongation rock soap.
Embodiment 8
A kind of elongation rock soap, the elongation rock soap include elongating stone powder, tremella powder, active carbon and soap base matter, elongate mountain flour
End is prepared by labradorite, and the partial size for elongating stone powder is 1.5 μm, elongates stone powder, tremella powder, active carbon and soap base matter
Quality is respectively 50g, 80g, 150g, 720g；
Wherein, soap base matter include mass ratio be 0.5: 25: 65: 1.5: 0.3: 12 sodium citrate, water, neat soap, cocoa butter,
Beeswax and neopelex；
The partial size of tremella powder is 50 μm；
The partial size of active carbon is 40 μm；
Elongating mountain flour is that labradorite is directly crushed to 1.5 μm to be made.
Wherein, mountain flour is elongated to be prepared from the following steps:
(1) it pre-processes: taking labradorite, clean；
(2) boiling: pretreated labradorite pearl is placed in reaction kettle, boiling is added to boil, wherein labradorite pearl and water
Volume ratio is 1: 10, and adjustment pressure is 800KPa, primary every 8min stirring, stirs 5min, mixing speed 570prm every time,
Boiling 10h altogether is down to room temperature, takes out labradorite；
(3) crush: it is 1.5 μm that the labradorite pearl after boiling, which is handled to partial size,；
Wherein, step (3) crush specifically includes the following steps:
(31) it prepares labradorite coarse powder: the labradorite after boiling being dried, 1000 meshes were crushed to, it is thick that labradorite is made
Powder；
(32) it prepares labradorite mixed liquor: labradorite coarse powder is placed in grinding device, add first time water with 200prm
Speed grind 5min, the mass ratio of labradorite coarse powder and first time water is 1: 1, then be added in grinding device second of water with
The mass ratio of the speed grinding 20min of 800prm, second of water and labradorite coarse powder is 1: 15, and labradorite mixed liquor is made；
Stone powder is elongated in preparation: standing 2min, incline supernatant, and gained is precipitated as the first precipitating, and the first precipitating is dried
Step (32) are repeated afterwards, supernatant is stood for 24 hours, incline supernatant, and gained is precipitated as the second precipitating, the second precipitating is dried,
Being ground to partial size is 1.5 μm to get elongation stone powder；
The preparation method is the same as that of Example 1 for the elongation rock soap.
Embodiment 9
A kind of elongation rock soap, the elongation rock soap include elongating stone powder, tremella powder, active carbon and soap base matter, elongate mountain flour
End is prepared by labradorite, and the partial size for elongating stone powder is 1.5 μm, elongates stone powder, tremella powder, active carbon and soap base matter
Mass ratio is 50g, 80g, 150g, 720g；
Wherein, soap base matter include mass ratio be 0.5: 25: 65: 1.5: 0.3: 12 sodium citrate, water, neat soap, cocoa butter,
Beeswax and neopelex；
The partial size of tremella powder is 50 μm；
The partial size of active carbon is 40 μm；
Elongating mountain flour is that labradorite is directly crushed to 1.5 μm to be made.
Wherein, mountain flour is elongated to be prepared from the following steps:
(1) it pre-processes: taking labradorite, clean；
(2) boiling: pretreated labradorite pearl is placed in reaction kettle, boiling is added to boil, wherein labradorite pearl and water
Volume ratio is 1: 10, and adjustment pressure is 800KPa, primary every 8min stirring, stirs 5min, mixing speed 570prm every time,
Boiling 10h altogether is down to room temperature, takes out labradorite；
(3) crush: it is 1.5 μm that the labradorite pearl after boiling, which is handled to partial size,；
Wherein, step (3) crush specifically includes the following steps:
(31) it prepares labradorite coarse powder: the labradorite after boiling being dried, 1000 meshes were crushed to, it is thick that labradorite is made
Powder；
(32) it prepares labradorite mixed liquor: labradorite coarse powder is placed in grinding device, add first time water with 300prm
Speed grind 10min, the mass ratio of labradorite coarse powder and first time water is 12: 5, then second of water is added in grinding device
With the speed grinding 40min of 1000prm, the mass ratio of second of water and labradorite coarse powder is 3: 25, and labradorite mixed liquor is made；
Stone powder is elongated in preparation: standing 3min, incline supernatant, and gained is precipitated as the first precipitating, and the first precipitating is dried
Step (32) are repeated afterwards, supernatant is stood into 36h, incline supernatant, and gained is precipitated as the second precipitating, the second precipitating is dried,
Being ground to partial size is 1.5 μm to get elongation stone powder；
The preparation method is the same as that of Example 1 for the elongation rock soap.
Embodiment 10
A kind of elongation rock soap, elongating rock soap includes elongating stone powder, tremella powder, active carbon and soap base matter, elongates stone powder
It is prepared by labradorite, the partial size for elongating stone powder is 1.5 μm, elongates the matter of stone powder, tremella powder, active carbon and soap base matter
Amount is respectively 80g, 50g, 100g, 600g；
Wherein, soap base matter includes sodium citrate, water, neat soap, glucono-δ-lactone, Rosa Damascana and detergent alkylate
Sodium sulfonate, sodium citrate, water, neat soap, glucono-δ-lactone, Rosa Damascana and neopelex mass ratio be
0.4:20:60:1:0.1:10；
The partial size of tremella powder is 150 μm；
The partial size of active carbon is 50 μm；
Elongating mountain flour is that labradorite is directly crushed to 1.5 μm to be made；
The preparation method is the same as that of Example 1 for the elongation rock soap, and the glucono-δ-lactone in the embodiment of the present invention is purchased from river
Nan Ruiren bioengineering Co., Ltd, the Rosa Damascana in all embodiments of the invention, which is purchased from Heilongjiang Province's Jin Fuyuan liquefaction, to be had
Limit company, the neopelex in all embodiments of the invention are purchased from Shandong Guang Kun Biotechnology Co., Ltd.
Embodiment 11
Elongating rock soap includes elongating stone powder, tremella powder, active carbon and soap base matter, elongate stone powder prepared by labradorite and
At, the partial size for elongating stone powder is 1.5 μm, elongate stone powder, tremella powder, active carbon and soap base matter quality be respectively 50g,
80g,150g,720g；
Soap base matter includes sodium citrate, water, neat soap, glucono-δ-lactone, Rosa Damascana and dodecyl benzene sulfonic acid
Sodium, sodium citrate, water, neat soap, glucono-δ-lactone, Rosa Damascana and neopelex mass ratio be 0.5:
25:65:1.5:0.3:12；
The partial size of tremella powder is 50 μm；
The partial size of active carbon is 20 μm；
Elongating mountain flour is that labradorite is directly crushed to 1.5 μm to be made；
It elongates rock soap to be prepared by following methods: the sodium citrate of definite quality ratio S1: being added to definite quality ratio
Water in, it is stirring while adding to be completely dissolved in water to sodium citrate, be cooled to 40 DEG C, be made sodium citrate solution；
S2: by the neat soap of definite quality ratio, Rosa Damascana, glucono-δ-lactone, Rosa Damascana and detergent alkylate sulphur
Sour sodium is placed in heating container and is heated to 80 DEG C, stirs evenly, and the first mixed solution is made；
S3: the tremella powder of definite quality ratio and active carbon are added in mixed solution and stirred under conditions of temperature-resistant
The second mixed solution is made in 15min；
S4: the elongation stone powder of definite quality ratio is added in the second mixed solution, is stirred with the speed of 60prm
Third mixed solution is made in 30min；
S5: sodium citrate solution is poured into third mixed solution, stirs 10min under the speed of 500prm, pours into mill
Tool, is covered grinding tool with plastic film, places 2 days under the conditions of 30 DEG C to get rock soap is elongated.
Embodiment 12
Elongating rock soap includes elongating stone powder, tremella powder, active carbon and soap base matter, elongate stone powder prepared by labradorite and
At, the partial size for elongating stone powder is 2 μm, elongate stone powder, tremella powder, active carbon and soap base matter quality be respectively 100g,
100g,200g,800g；
Soap base matter includes sodium citrate, water, neat soap, glucono-δ-lactone, Rosa Damascana and dodecyl benzene sulfonic acid
Sodium, sodium citrate, water, neat soap, glucono-δ-lactone, Rosa Damascana and neopelex mass ratio be 0.6:
30:70:2:0.5:15；
The partial size of tremella powder is 200 μm；
The partial size of active carbon is 100 μm；
Elongating mountain flour is that labradorite is directly crushed to 1.5 μm to be made；
It elongates rock soap to be prepared by following methods: the sodium citrate of definite quality ratio S1: being added to definite quality ratio
Water in, it is stirring while adding to be completely dissolved in water to sodium citrate, be cooled to 45 DEG C, be made sodium citrate solution；
S2: by the neat soap of definite quality ratio, Rosa Damascana, glucono-δ-lactone, Rosa Damascana and detergent alkylate sulphur
Sour sodium is placed in heating container and is heated to 95 DEG C, stirs evenly, and the first mixed solution is made；
S3: the tremella powder of definite quality ratio and active carbon are added in mixed solution and stirred under conditions of temperature-resistant
The second mixed solution is made in 20min；
S4: the elongation stone powder of definite quality ratio is added in the second mixed solution, is stirred with the speed of 80prm
Third mixed solution is made in 50min；
S5: sodium citrate solution is poured into third mixed solution, stirs 20min under the speed of 600prm, pours into mill
Tool, is covered grinding tool with plastic film, places 3 days under the conditions of 38 DEG C to get rock soap is elongated.
Reference examples 1
Elongating rock soap includes elongating stone powder, tremella powder, active carbon and soap base matter, elongate stone powder prepared by labradorite and
At, the partial size for elongating stone powder is 1 μm, elongate stone powder, tremella powder, active carbon and soap base matter quality be respectively 50g, 80g,
150g,720g；
Soap base matter includes the sodium citrate that mass ratio is 0.5: 25: 65: 1.5: 0.3: 12, water, neat soap, sunflower oil, mustard
Oil and neopelex；
The partial size of tremella powder is 50 μm；
The partial size of active carbon is 20 μm；
Elongating mountain flour is that labradorite is directly crushed to 1 μm to be made；
The preparation method is the same as that of Example 1 for the elongation rock soap.
Reference examples 2
A kind of elongation rock soap, elongating rock soap includes elongating stone powder, tremella powder and soap base matter, elongates stone powder by labradorite
Be prepared, the partial size for elongating stone powder is 1.5 μm, elongate stone powder, the quality of tremella powder and soap base matter be respectively 80g,
50g,600g；
Soap base matter includes the sodium citrate that mass ratio is 0.5: 25: 65: 1.5: 0.3: 12, water, neat soap, sunflower oil, mustard
Oil and neopelex；
The partial size of tremella powder is 150 μm；
Elongating mountain flour is that labradorite is directly crushed to 1.5 μm to be made；
The preparation method is the same as that of Example 1 for the elongation rock soap.
Reference examples 3
A kind of elongation rock soap, elongating rock soap includes elongating stone powder, active carbon and soap base matter, elongates stone powder by labradorite
Be prepared, the partial size for elongating stone powder is 1.5 μm, elongate stone powder, the quality of active carbon and soap base matter be respectively 80g,
100g,600g；
Soap base matter includes the sodium citrate that mass ratio is 0.5: 25: 65: 1.5: 0.3: 12, water, neat soap, sunflower oil, mustard
Oil and neopelex；
The partial size of active carbon is 50 μm；
Elongating mountain flour is that labradorite is directly crushed to 1.5 μm to be made；
The preparation method is the same as that of Example 1 for the elongation rock soap.
Reference examples 4
A kind of elongation rock soap, elongating rock soap includes elongating stone powder and soap base matter, elongate stone powder prepared by labradorite and
At the partial size for elongating stone powder is 1.5 μm, and the quality for elongating stone powder and soap base matter is respectively 80g, 600g；
Soap base matter includes the sodium citrate that mass ratio is 0.5: 25: 65: 1.5: 0.3: 12, water, neat soap, sunflower oil, mustard
Oil and neopelex；
Elongating mountain flour is that labradorite is directly crushed to 1.5 μm to be made；
The preparation method is the same as that of Example 1 for the elongation rock soap.
Reference examples 5
Elongating rock soap includes elongating stone powder, tremella powder, active carbon and soap base matter, elongate stone powder prepared by labradorite and
At, the partial size for elongating stone powder is 1.5 μm, elongate stone powder, tremella powder, active carbon and soap base matter quality be respectively 80g,
140g,300g,720g；
Soap base matter includes the sodium citrate that mass ratio is 0.5: 25: 65: 1.5: 0.3: 12, water, neat soap, sunflower oil, mustard
Oil and neopelex；
The partial size of tremella powder is 50 μm；
The partial size of active carbon is 20 μm；
Elongating mountain flour is that labradorite is directly crushed to 1.5 μm to be made；
The preparation method is the same as that of Example 1 for the elongation rock soap.
Reference examples 6
A kind of elongation rock soap, elongating rock soap includes elongating stone powder, tremella powder, active carbon and soap base matter, elongates stone powder
It is prepared by labradorite, the partial size for elongating stone powder is 1.5 μm, elongates the matter of stone powder, tremella powder, active carbon and soap base matter
Amount is respectively 80g, 50g, 100g, 600g；
Wherein, soap base matter includes sodium citrate, water, neat soap, Rosa Damascana and neopelex, sodium citrate,
Water, neat soap, Rosa Damascana and neopelex mass ratio be 0.4: 20: 60: 0.1: 10；
The partial size of tremella powder is 150 μm；
The partial size of active carbon is 50 μm；
Elongating mountain flour is that labradorite is directly crushed to 1.5 μm to be made；
The preparation method is the same as that of Example 1 for the elongation rock soap.
Reference examples 7
A kind of elongation rock soap, elongating rock soap includes elongating stone powder, tremella powder, active carbon and soap base matter, elongates stone powder
It is prepared by labradorite, the partial size for elongating stone powder is 1.5 μm, elongates the matter of stone powder, tremella powder, active carbon and soap base matter
Amount is respectively 80g, 50g, 100g, 600g；
Wherein, soap base matter includes sodium citrate, water, neat soap, glucono-δ-lactone, Rosa Damascana, sodium citrate, water,
Neat soap, glucono-δ-lactone, Rosa Damascana mass ratio be 0.4: 20: 60: 0.5: 15；
The partial size of tremella powder is 150 μm；
The partial size of active carbon is 50 μm；
Elongating mountain flour is that labradorite is directly crushed to 1.5 μm to be made；
The preparation method is the same as that of Example 1 for the elongation rock soap.
Reference examples 8
A kind of elongation rock soap, elongating rock soap includes elongating stone powder, tremella powder, active carbon and soap base matter, elongates stone powder
It is prepared by labradorite, the partial size for elongating stone powder is 1.5 μm, elongates the matter of stone powder, tremella powder, active carbon and soap base matter
Amount is respectively 80g, 50g, 100g, 600g；
Wherein, soap base matter includes sodium citrate, water, neat soap, glucono-δ-lactone, Rosa Damascana and detergent alkylate
Sodium sulfonate, sodium citrate, water, neat soap, glucono-δ-lactone, coconut oil and neopelex mass ratio be 0.4
:20:60:1:0.1:10；
The partial size of tremella powder is 150 μm；
The partial size of active carbon is 50 μm；
Elongating mountain flour is that labradorite is directly crushed to 1.5 μm to be made；
The preparation method is the same as that of Example 1 for the elongation rock soap.
Test example 1, which elongates rock soap, improves the effect of cock skin skin
Randomly select 70 cock skin skin patients and carry out clinical tests, the cock skin skin degree of 70 patients is suitable, by patient with
Machine is divided into test 1-5 group and control 1-2 group, and every group 10, test 1-2 group uses the elongation rock soap of embodiment 1-2, test respectively
3-5 group uses the elongation rock soap of embodiment 7-9 respectively, and 1 group of control is gone cock skin to elongate rock soap using commercially available, commercially available that cock skin is gone to elongate
The brand of rock soap is that Duo Laduoshang removes cock skin soap with abrasive, 2 groups of the control elongation rock soaps for using reference examples 1, each test group and right
Affected part is cleaned using corresponding product according to group, twice a day, is used continuously 2 months, during which, the affected part of patient is clear without using other
Clean articles evaluate the curative effect of each set product, the standard of curative effect evaluation are as follows: granular protrusion is whole at healing-patient affected part skin
It disappears, without pigmentation；Granular convex portion disappears at improvement-illing skin, and pigment deposits on a small quantity；In vain-affected part
The protrusion of skin particles shape has no reduction or increases, and the results are shown in Table 1.
1. each group of table, which elongates rock soap, improves the effect of cock skin skin
As shown in Table 1, the elongation rock soap that various embodiments of the present invention provide is higher than control group to the cure rate of cock skin skin,
In, embodiment 1-2 is up to 80% to the cure rate of cock skin skin, and the cure rate for compareing 2 groups only has 30%, it was demonstrated that when elongation rock soap
When the middle partial size for elongating stone powder is less than 1.5 μm, the cure rate of cock skin skin will be greatly lowered, embodiment 7 is drawn in preparation
Boiling has been carried out to labradorite when feldspar powder, has removed foul and the bacterium on labradorite surface, on the basis of embodiment 1-2,
Further improve and elongate rock soap to the cure rate of cock skin skin, and embodiment 8-9 with method provided by the invention to boiling after
Labradorite is crushed, and so that elongation rock soap is reached 100% to the cure rate of cock skin skin, it was demonstrated that use elongation provided by the invention
The preparation method of mountain flour can further increase and elongate rock soap to the therapeutic effect of cock skin skin.
2 each group of test example elongates the rate of deposition measurement test that mountain flour is elongated in rock soap
The embodiment 1-6 and reference examples 2-5 elongation rock soap prepared is cut into side length for the square of 3cm, in square
The total weight of the elongation stone powder contained be G2 from each group elongate the above 0.5cm in rock soap lower surface be horizontally cut into above and below two
The part that each group is elongated below rock soap is dissolved in part, and the weight G1 of the elongation mountain flour weighed elongates rock soap lower part
The weight for elongating mountain flour is G2/6, and is calculated by the following formula each group and elongates the rate of deposition for elongating mountain flour in rock soap, and every group is done 5
A Duplicate Samples, results are averaged, the results are shown in Table 2；
Wherein, P is rate of deposition, and G1 is to elongate labradorite in rock soap lower part
The weight of powder, G2 are the total weight for elongating the elongation stone powder contained in rock soap.
2. each group of table elongates the rate of deposition test result that mountain flour is elongated in rock soap
As shown in Table 2, the size of rate of deposition is as follows: 5 groups of < embodiments of embodiment, 4,6 groups of < embodiments, 2 groups of < embodiments
1,3 groups of < reference examples 2-5 groups, illustrate, when elongating rock soap using tremella powder, active carbon and soap base matter and elongation mountain flour preparation,
The rate of deposition for elongating mountain flour in elongation rock soap can be reduced significantly, and ought specifically limit the partial size of tremella powder and active carbon
When, can further reduce elongate mountain flour elongate rock soap in rate of deposition, when delete formula in tremella powder, active carbon or
When both the above, the rate of deposition for elongating and elongating mountain flour in rock soap can be increased substantially, when change tremella powder, active carbon, soap base
Matter and elongate mountain flour proportion when, will also result in elongate mountain flour elongate rock soap in rate of deposition increase, and when elongate stone powder,
When the mass ratio of tremella powder, active carbon and soap base matter is 5: 8: 15: 72, it can further decrease and elongate stone powder in elongation rock soap
In rate of deposition.
3 each group of test example elongates the rotten degree test of paste of rock soap
The elongation rock soap of Example 9-12 and reference examples 6-8 elongates one end of rock soap with iron wire insertion each group, is suspended on
In wide-mouth bottle with heat insulation function, the water that 200ml temperature is 20 DEG C is added in wide-mouth bottle, each group elongates the 2/ of rock soap bottom
3 are soaked in water, elongate rock soap and are not in contact with bottle wall, and each group is taken out after five hours and elongates rock soap, wait elongate on rock soap
Water droplet drip off after, rock soap will be elongated and be placed on smooth desktop, each group is elongated into rock soap from the side perpendicular to desktop with knife
To incision, the thickness of the section three rotten layers of paste being measured with a yardstick, pasting the average value that rotten degree is three thickness, every group of elongation rock soap does 5
A Duplicate Samples, results are averaged, the results are shown in Table 3.
3. each group of table elongates the rate of deposition test result that mountain flour is elongated in rock soap
As shown in Table 3, the rotten degree of paste that embodiment 10-12 group elongates rock soap is substantially less than embodiment 9, it was demonstrated that when this hair of use
After the soap base matter of bright offer, the rotten degree of paste for elongating rock soap can be reduced significantly, and reference examples 6-8 replaces or deletes respectively this
Individual components in invention soap base matter significantly improve the results show that it pastes rotten degree, and the rotten degree of paste of the elongation rock soap of embodiment 11
Substantially less than embodiment 10 and embodiment 12, it was demonstrated that when sodium citrate, water, neat soap, glucono-δ-lactone, plants essential oil and
When the mass ratio of neopelex is 5: 25: 65: 1.5: 18: 12, the rotten degree of paste for elongating rock soap is minimum.
To sum up, only the preferred embodiments of the invention, is not limited the scope of protection of the present invention with this, all according to the invention patent
Equivalent changes and modifications made by range and description are all within the scope of the invention patent covers.
Claims (10)
1. a kind of elongation rock soap, which is characterized in that preparing the raw material for elongating rock soap includes elongating mountain flour and soap base matter, described
The partial size for elongating mountain flour is 1.5 μm -2 μm, and the mountain flour and the mass ratio of soap base matter of elongating is 5-10: 60-80.
2. elongating rock soap as described in claim 1, which is characterized in that the raw material further includes tremella powder, active carbon, the drawing
Feldspar powder, tremella powder, active carbon and perfumed soap matrix mass ratio be 5-10: 5-10: 10-20: 60-80.
3. elongating rock soap as claimed in claim 2, which is characterized in that the elongation stone powder, tremella powder, active carbon and soap base
The mass ratio of matter is 5: 8: 15: 72.
4. elongating rock soap as claimed in claim 2, which is characterized in that the partial size of the tremella powder is 80 μm -100 μm；It is described
The partial size of active carbon is 30 μm -40 μm.
5. elongating rock soap as described in claim 1, which is characterized in that the soap base matter includes sodium citrate, water, neat soap, Portugal
Saccharic acid glucono-δ-lactone, plants essential oil and neopelex, the sodium citrate, water, neat soap, gluconic acid-
The mass ratio of delta-lactone, plants essential oil and neopelex is 0.4-0.6: 20-30: 60-70: 1-2: 0.1-0.5:
10-15。
6. elongating rock soap as claimed in claim 5, which is characterized in that the sodium citrate, water, neat soap, gluconic acid-δ-interior
The mass ratio of ester, plants essential oil and neopelex is 0.5: 25: 65: 1.5: 0.3: 12.
7. elongating rock soap as described in claim 1, which is characterized in that the elongation mountain flour is prepared from the following steps:
1) it pre-processes: taking labradorite pearl, clean；
2) boiling: pretreated labradorite pearl is placed in reaction kettle, boiling is added to boil, wherein labradorite pearl and water volume
Than being 1: 8-10, adjustment pressure is 600-800KPa, primary every 6-8min stirring, stirs 3-5min every time, mixing speed is
50-70prm, boiling 8-10h, is down to room temperature altogether, takes out labradorite pearl；
3) crush: it is 1.5 μm -2 μm that the labradorite pearl after boiling, which is handled to partial size,.
8. as claimed in claim 7 elongate rock soap, which is characterized in that step 3) it is described crush specifically includes the following steps:
It prepares labradorite coarse powder: the labradorite after boiling being dried, 1000 meshes were crushed to, labradorite coarse powder is made；
(31) it prepares labradorite mixed liquor: labradorite coarse powder is placed in grinding device, add first time water with 200-300prm
Speed grind 5-10min, the mass ratio of labradorite coarse powder and first time water is 10-12: 5-10, then is added in grinding device
Second of water grinds 20-40min with the speed of 800-1000prm, and the mass ratio of second of water and labradorite coarse powder is 10-12:
Labradorite mixed liquor is made in 100-150；
(32) stone powder is elongated in preparation: standing 2min-3min, incline supernatant, and gained is precipitated as the first precipitating, by described first
Step (32) are repeated after precipitating drying, supernatant are stood into -36h for 24 hours, incline supernatant, and gained is precipitated as the second precipitating, by institute
The drying of the second precipitating is stated, being ground to partial size is 1.5 μm -2 μm to get elongation stone powder.
9. a kind of preparation method as claimed in claim 5 for elongating rock soap, which is characterized in that the method includes following steps
It is rapid:
S1: the sodium citrate of definite quality ratio is added in the water of definite quality ratio, stirring while adding complete to sodium citrate
It is dissolved in the water, is cooled to 40 DEG C -45 DEG C, sodium citrate solution is made；
S2: by the neat soap of definite quality ratio, plants essential oil, glucono-δ-lactone, plants essential oil and neopelex
It is placed in heating container and is heated to 80 DEG C -95 DEG C, stir evenly, the first mixed solution is made；
S3: the tremella powder of definite quality ratio and active carbon are added in mixed solution and stirred under conditions of temperature-resistant
The second mixed solution is made in 15min-20min；
S4: the elongation stone powder of definite quality ratio is added in the second mixed solution, is stirred with the speed of 60prm-80prm
Third mixed solution is made in 30min-50min；
S5: sodium citrate solution is poured into third mixed solution, stirs 10min- under the speed of 500prm-600prm
20min pours into grinding tool, is covered grinding tool with plastic film, places 2-3 days under the conditions of 30-38 DEG C to get rock soap is elongated.
10. the application of any of claims 1 or 2 for elongating rock soap in the cosmetics that preparation has improvement chicken skin effects.
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