CN1737095A - Black slime soap and its manufacturing method - Google Patents
Black slime soap and its manufacturing method Download PDFInfo
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- CN1737095A CN1737095A CN 200510012804 CN200510012804A CN1737095A CN 1737095 A CN1737095 A CN 1737095A CN 200510012804 CN200510012804 CN 200510012804 CN 200510012804 A CN200510012804 A CN 200510012804A CN 1737095 A CN1737095 A CN 1737095A
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Abstract
The proportion by weight of mineral black mud perfumed soap is that aliphatic acid natrium: 2, 6- butylated hydroxytoluene: ethylene diamine tetraacetic acid, perfume compounds: adeps lanae: isooctanoic acid octyl: glycerin: black mud: water is 75-80:0.05-0.1:0.2-0.4:1-2.5:1-3:1-3:1-3:0.5-6: 13-14. The invention adopts the method of adding the black mud in the granulating procedure or blend procedure. The invention has the advantages of making the perfumed soap skin-protecting and making the skin metabolism positive cycle.
Description
Affiliated field
The invention belongs to a kind of perfumed soap and production method, relate in particular to a kind of production formula and production method that black slime is added perfumed soap.
Background technology
Traditional perfumed soap production formula, how to clean with washing is purpose, lays particular stress in the prescription and uses sanitising agent, and be equipped with softener commonly used to reach the purpose of skin care.Require to use pure water in process of production, and with some metal ions of sequestrant complexing.Tradition perfumed soap production formula is that major ingredient is sodium soap or lipid acid potassium; Auxiliary material is antioxidant BHT, sequestrant EDTA, essence, pigment, sterilant, glycerine, titanium dioxide etc.
Add the black slime soap that black slime is produced, the human consumer uses this kind of perfumed soap, in cleaning skin, can also reach the purpose of the secretion of balance skin oil and fat, skin nutrition.Appear in the newspapers in the end by retrieval.
Summary of the invention
The purpose of this invention is to provide a kind of can be in cleaning skin, can also reach the purpose black slime soap and the production method of the secretion of balance skin oil and fat, skin nutrition.
1. the weight ratio of black slime soap of the present invention consists of:
Sodium soap: BHT (2,6 ditertiary butyl p cresol): EDTA (ethylenediamine tetraacetic acid (EDTA)): essence: lanolin: EH (the different monooctyl ester of isocaprylic acid): glycerine: black mud: water=75-80: 0.05-0.1: 0.2-0.4: 1-2.5: 1-3: 1-3: 1-3: 0.5-6: 13-14.Aforesaid black mud is the Yuncheng black mud.
Production method of the present invention comprises following two kinds of technologies:
First kind of production method: black mud adds in granulating working procedure
(1), the weight ratio of pressing black slime soap forms, and black mud is ground to below the 44 μ m, adding temperature is in the sodium soap of 85-90 ℃ of liquid state, after stirring, advances the prilling tower vacuum granulation, must contain the perfumed soap grain of black mud;
(2), the weight ratio of pressing black slime soap forms, BHT is dissolved in the essence;
(3), the weight ratio of pressing black slime soap forms, and EDTA is soluble in water;
(4), the weight ratio of pressing black slime soap forms, and lanolin, EH (the different monooctyl ester of isocaprylic acid), glycerine are mixed at normal temperatures and pressures with step (1), (2) and (3) gained raw material, is stirred to even;
(5), three-roll grinder grinds, and in the process of lapping, soap bar should be returned three-roll grinder and grind, grind 3-4 time;
(6), printing shaping.
Second kind: black mud adds in compounding process
(1), the weight ratio of pressing black slime soap forms, and black mud is ground to below the 44 μ m, mix with glycerine;
(2), the weight ratio of pressing black slime soap forms, BHT is dissolved in the essence;
(3), the weight ratio of pressing black slime soap forms, EDTA is soluble in water;
(4), the weight ratio of pressing black slime soap forms, and the perfumed soap grain of fatty acids sodium at 85%-86% mixed at normal temperatures and pressures with lanolin, EH (the different monooctyl ester of isocaprylic acid) and step (1), (2) and (3) gained raw material, is stirred to even;
(5), three-roll grinder grinds, and in the process of lapping, soap bar should be returned three-roll grinder and grind, grind 3-4 time;
(6), printing shaping.
The present invention compared with prior art has following meaning:
1, provides a kind of novel toilet soap, for perfumed soap family increases new member;
2, make perfumed soap cross over the cleaning skin-protection type by clean, this skin care is not traditional skin care, but provides mineral substance to skin, and the secretion of balance skin oil and fat makes skin metabolism move towards benign cycle.
3, make Chinese perfumed soap product structure that variation take place.China's perfumed soap not only has common perfumed soap, and the mineral substance perfumed soap has been arranged.
Embodiment
Embodiment 1 prepares burden various raw materials in following ratio:
Sodium soap: BHT: EDTA: essence: lanolin: EH: glycerine: black mud: water=77: 0.05: 0.2: 1: 1: 1: 3: 3: 13.75.
(1), black mud is ground to below the 44 μ m, add in the liquid sodium soap (88 ℃ of temperature), after stirring, advance the prilling tower vacuum granulation, must contain the perfumed soap grain of black mud;
(2), BHT is dissolved in the essence;
(3), EDTA is soluble in water;
(4), lanolin, EH (the different monooctyl ester of isocaprylic acid), glycerine are mixed at normal temperatures and pressures with above-mentioned (1), (2), (3), gained raw material, be stirred to evenly;
(5), three-roll grinder grinds. and in the process of lapping, soap bar is returned three-roll grinder grind 3 times;
(6), printing shaping.Make black mud content and be 3% black mud perfumed soap.The quality examination of black mud perfumed soap the results are shown in Table 1
Embodiment 2 prepares burden various raw materials in following ratio:
Sodium soap: BHT: EDTA: essence: lanolin: EH: glycerine: black mud=80: 0.05: 0.2: 1: 1: 1: 3: 0.5: 13.25.
(1), black mud is ground to below the 44 μ m, mix with glycerine;
(2), BHT is dissolved in the essence;
(3), EDTA is soluble in water;
(4), perfumed soap grain and lanolin with fatty acids sodium 86%, EH (the different monooctyl ester of isocaprylic acid) and above-mentioned (1), (2), (3), gained raw material mix at normal temperatures and pressures, be stirred to evenly;
(5), three-roll grinder grinds. in the process of lapping, soap bar is returned grinding 4 times;
(6), printing shaping.Make black mud content and be 0.5% black mud perfumed soap.The quality examination of black mud perfumed soap the results are shown in Table 1
Embodiment 3 prepares burden various raw materials in following ratio:
Sodium soap: BHT: EDTA: essence: lanolin: EH: glycerine: black mud: water=75.6: 0.05: 0.4: 1: 1: 1: 2: 5: 13.95.System
(1), black mud is ground to below the 44 μ m, add in the liquid sodium soap (90 ℃ of temperature), after stirring, advance the prilling tower vacuum granulation, must contain the perfumed soap grain of black mud 5%;
(2), BHT is dissolved in the essence;
(3), EDTA is soluble in water;
(4), lanolin, EH (the different monooctyl ester of isocaprylic acid), glycerine are mixed at normal temperatures and pressures with above-mentioned (1), (2), (3), gained raw material, be stirred to evenly;
(5), three-roll grinder grinds. and in the process of lapping, soap bar is returned three-roll grinder grind 4 times;
(6), printing shaping.One-tenth black mud content is 5% black mud perfumed soap.The quality examination of black mud perfumed soap the results are shown in Table 1
Embodiment 4 prepares burden various raw materials in following ratio:
Sodium soap: BHT: EDTA: essence: lanolin: EH: glycerine: black mud: water=77: 0.05: 0.2: 1: 2: 1: 3: 2: 13.75.
(1), black mud is ground to below the 44 μ m, mix with glycerine;
(2), BHT is dissolved in the essence;
(3), EDTA is soluble in water;
(4), perfumed soap grain and lanolin with fatty acids sodium 85.5%, EH (the different monooctyl ester of isocaprylic acid) and above-mentioned (1), (2), (3), gained raw material mix at normal temperatures and pressures, be stirred to evenly;
(5), three-roll grinder grinds. in the process of lapping, soap bar is returned grinding 3 times;
(6), printing shaping.Make black mud content and be 2% black mud perfumed soap.The quality examination of black mud perfumed soap the results are shown in Table 1
Embodiment 5 prepares burden various raw materials in following ratio:
Sodium soap: BHT: EDTA: essence: lanolin: EH: glycerine: black mud: water=75: 0.05: 0.3: 1: 1.5: 1: 2: 6: 13.15.
(1), black mud is ground to below the 44 μ m, mix with glycerine;
(2), BHT is dissolved in the essence;
(3), EDTA is soluble in water;
(4), perfumed soap grain and lanolin with fatty acids sodium 86%, EH (the different monooctyl ester of isocaprylic acid) and above-mentioned (1), (2), (3), gained raw material mix at normal temperatures and pressures, be stirred to evenly;
(5), three-roll grinder grinds. in the process of lapping, soap bar is returned grinding 4 times;
(6), printing shaping.Make black mud content and be 6% black mud perfumed soap.The quality examination of black mud perfumed soap the results are shown in Table 1
Table one black mud perfumed soap quality examination result
| Sequence number | Dry soap content (%) | Cracking | Stick with paste mashed |
| 1 | 77.9 | 3 grades | 2.9mm |
| 2 | 75.8 | 3 grades | 2.8mm |
| 3 | 81.6 | 3 grades | 3.0mm |
| 4 | 77.4 | 3 grades | 3.0mm |
| 5 | 75.0 | 3 grades | 2.9mm |
Claims (4)
1, a kind of black slime soap, the weight ratio that it is characterized in that black slime soap consists of: sodium soap: 2,6 ditertiary butyl p cresol: ethylenediamine tetraacetic acid (EDTA): essence: lanolin: the different monooctyl ester of isocaprylic acid: glycerine: black mud: water=75-80: 0.05-0.1: 0.2-0.4: 1-2.5: 1-3: 1-3: 1-3: 0.5-6: 13-14.
2, a kind of black slime soap as claimed in claim 1 is characterized in that described black mud is the Yuncheng black mud.
3, the production method of a kind of black slime soap as claimed in claim 1 or 2 is characterized in that comprising the steps:
(1), the weight ratio of pressing black slime soap forms, and black mud is ground to below the 44 μ m, adding temperature is in the sodium soap of 85-90 ℃ of liquid state, after stirring, advances the prilling tower vacuum granulation, must contain the perfumed soap grain of black mud;
(2), the weight ratio of pressing black slime soap forms, BHT is dissolved in the essence;
(3), the weight ratio of pressing black slime soap forms, and EDTA is soluble in water;
(4), the weight ratio of pressing black slime soap forms, and lanolin, the different monooctyl ester of isocaprylic acid, glycerine are mixed at normal temperatures and pressures with step (1), (2) and (3) gained raw material, is stirred to even;
(5), three-roll grinder grinds, and in the process of lapping, soap bar should be returned three-roll grinder and grind, grind 3-4 time;
(6), printing shaping.
4,, the production method of a kind of black slime soap as claimed in claim 1 or 2, it is characterized in that comprising the steps:
(1), the weight ratio of pressing black slime soap forms, and black mud is ground to below the 44 μ m, mix with glycerine;
(2), the weight ratio of pressing black slime soap forms, BHT is dissolved in the essence;
(3), the weight ratio of pressing black slime soap forms, EDTA is soluble in water;
(4), the weight ratio of pressing black slime soap forms, and the perfumed soap grain of fatty acids sodium at 85%-86% mixed at normal temperatures and pressures with lanolin, the different monooctyl ester of isocaprylic acid and step (1), (2) and (3) gained raw material, is stirred to even;
(5), three-roll grinder grinds, and in the process of lapping, soap bar should be returned three-roll grinder and grind, grind 3-4 time;
(6), printing shaping.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2005100128044A CN1333060C (en) | 2005-09-08 | 2005-09-08 | Black slime soap and its manufacturing method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2005100128044A CN1333060C (en) | 2005-09-08 | 2005-09-08 | Black slime soap and its manufacturing method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1737095A true CN1737095A (en) | 2006-02-22 |
| CN1333060C CN1333060C (en) | 2007-08-22 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2005100128044A Active CN1333060C (en) | 2005-09-08 | 2005-09-08 | Black slime soap and its manufacturing method |
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| CN (1) | CN1333060C (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101023911B (en) * | 2007-04-09 | 2010-05-19 | 王梦飞 | Mineral black-mud dry powder for skin care and health-care and preparing method |
| CN102579284A (en) * | 2012-03-13 | 2012-07-18 | 南风化工集团股份有限公司 | Rock salt moisturizing and whitening fancy soap and production method thereof |
| CN102579311A (en) * | 2012-03-13 | 2012-07-18 | 南风化工集团股份有限公司 | Dunaliella beauty soap and production method thereof |
| CN104087450A (en) * | 2014-06-27 | 2014-10-08 | 安庆一枝梅化工有限责任公司 | Beauty-treatment toilet medicinal soap and preparation method thereof |
| CN110305745A (en) * | 2019-07-30 | 2019-10-08 | 北京周整无为健康管理有限责任公司 | A kind of elongation rock soap and preparation method thereof |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1219506C (en) * | 2003-09-16 | 2005-09-21 | 邵鲁安 | Skin protection product containing refined bittern or black soil from salt lake |
| CN1528264A (en) * | 2003-10-16 | 2004-09-15 | 邵鲁安 | Black mud for producing beauty, thinning and skin-care articles |
| KR20040108375A (en) * | 2004-11-25 | 2004-12-23 | 서성욱 | manufacture process of black mud powder is contain soap |
-
2005
- 2005-09-08 CN CNB2005100128044A patent/CN1333060C/en active Active
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101023911B (en) * | 2007-04-09 | 2010-05-19 | 王梦飞 | Mineral black-mud dry powder for skin care and health-care and preparing method |
| CN102579284A (en) * | 2012-03-13 | 2012-07-18 | 南风化工集团股份有限公司 | Rock salt moisturizing and whitening fancy soap and production method thereof |
| CN102579311A (en) * | 2012-03-13 | 2012-07-18 | 南风化工集团股份有限公司 | Dunaliella beauty soap and production method thereof |
| CN104087450A (en) * | 2014-06-27 | 2014-10-08 | 安庆一枝梅化工有限责任公司 | Beauty-treatment toilet medicinal soap and preparation method thereof |
| CN110305745A (en) * | 2019-07-30 | 2019-10-08 | 北京周整无为健康管理有限责任公司 | A kind of elongation rock soap and preparation method thereof |
| CN110305745B (en) * | 2019-07-30 | 2021-05-11 | 北京周整无为健康管理有限责任公司 | Elongated stone soap and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1333060C (en) | 2007-08-22 |
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| TR01 | Transfer of patent right |
Effective date of registration: 20190104 Address after: No. 376 Hongqi East Street, Yanhu District, Yuncheng City, Shanxi Province, 044000 Patentee after: Shanxi Coking Coal Yuncheng Salinization Group Co.,Ltd. Address before: 044000 No. 294 Jiefang Middle Road, Yuncheng City, Shanxi Province Patentee before: China Nafine Group Intenational Co.,Ltd. |
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| TR01 | Transfer of patent right |
Effective date of registration: 20230207 Address after: Room 1006, No. 376, Hongqi East Street, Yanhu District, Yuncheng City, Shanxi Province 044000 Patentee after: Nanfeng Chemical (Yuncheng) Group Co.,Ltd. Address before: No. 376 Hongqi East Street, Yanhu District, Yuncheng City, Shanxi Province, 044000 Patentee before: Shanxi Coking Coal Yuncheng Salinization Group Co.,Ltd. |
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| TR01 | Transfer of patent right |