CN110288894A - A kind of preparation method of plant specimen - Google Patents

A kind of preparation method of plant specimen Download PDF

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Publication number
CN110288894A
CN110288894A CN201910593838.9A CN201910593838A CN110288894A CN 110288894 A CN110288894 A CN 110288894A CN 201910593838 A CN201910593838 A CN 201910593838A CN 110288894 A CN110288894 A CN 110288894A
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China
Prior art keywords
plant
preparation
resin
sample
mold
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Pending
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CN201910593838.9A
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Chinese (zh)
Inventor
林什全
艾彩霞
刘吉善
石敏鸿
洪梦颖
刘万山
蔡文杰
匡标
程彬
吴亚楠
李林
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Guangdong Sen Lin Green Co Ltd
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Guangdong Sen Lin Green Co Ltd
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Priority to CN201910593838.9A priority Critical patent/CN110288894A/en
Publication of CN110288894A publication Critical patent/CN110288894A/en
Pending legal-status Critical Current

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    • GPHYSICS
    • G09EDUCATION; CRYPTOGRAPHY; DISPLAY; ADVERTISING; SEALS
    • G09BEDUCATIONAL OR DEMONSTRATION APPLIANCES; APPLIANCES FOR TEACHING, OR COMMUNICATING WITH, THE BLIND, DEAF OR MUTE; MODELS; PLANETARIA; GLOBES; MAPS; DIAGRAMS
    • G09B23/00Models for scientific, medical, or mathematical purposes, e.g. full-sized devices for demonstration purposes
    • G09B23/38Models for scientific, medical, or mathematical purposes, e.g. full-sized devices for demonstration purposes for botany

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  • Physics & Mathematics (AREA)
  • Engineering & Computer Science (AREA)
  • General Physics & Mathematics (AREA)
  • Mathematical Analysis (AREA)
  • Mathematical Physics (AREA)
  • Algebra (AREA)
  • Computational Mathematics (AREA)
  • Botany (AREA)
  • Health & Medical Sciences (AREA)
  • Mathematical Optimization (AREA)
  • General Health & Medical Sciences (AREA)
  • Pure & Applied Mathematics (AREA)
  • Business, Economics & Management (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Educational Administration (AREA)
  • Educational Technology (AREA)
  • Theoretical Computer Science (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)

Abstract

The invention discloses a kind of preparation methods of plant specimen, comprising the following steps: S1. first prepares plant pretreatment fluid, and the pretreatment fluid by ferrous salt and with the ferrous salt there is the acid of identical acid group to be formulated;S2. plant sample is immersed in plant pretreatment fluid and is heated reaction, until translucent appearance is presented in plant sample;S3. drying and processing is carried out to plant sample;S4. plant sample tiling is put into transparent polybag, then polybag vacuumize being bonded plant sample with polybag;S5. the plant sample of packaging plastic bags is put into mold and mold is vacuumized after injecting resin into mold to eliminate bubble, then demoulding obtains finished product after hardening of resin.

Description

A kind of preparation method of plant specimen
Technical field
The invention patent relates to sample technical field more particularly to a kind of preparation methods of plant specimen.
Background technique
Making plant specimen is one of the powerful measure for solving the problems, such as botany teaching aid.If classroom teaching has the work of plant Body is more favorable for student and deepens understanding.Using plant specimen, can be avoided Activities of Some Plants has regional, seasonal limitation. Plant specimen saves the shape and color of plant simultaneously, so as to observation again and research in the future.A small number of plant specimens also have There is the value of collection.Common plant specimen is exsiccata and resin sample, and usually fresh vegetable material absorbs water Bookbinding sample made of (this paper is known as platform paper) on white hard paper after letterweight system is allowed to dry.However due in wax page sample Plant be directly exposed in external environment, influenced the problems such as being easy to appear mildew, moth by humidity and air oxidation. Resin sample is packaged plant specimen using resin, can completely cut off the influence of air and humidity to plant specimen, however resin Need to inject resin fluid in-mold molding in the manufacturing process of sample, plant specimen be easy to be fluid affected appearance fold or The deformation such as bending, are unfavorable for showing;Furthermore also with plant specimen physical and chemical reaction, which can occur, for certain resin materials goes out plant specimen Situations such as now decolourizing.
Summary of the invention
The invention patent aims to overcome that the deficiencies in the prior art, provides beautiful and generous can be reserved for of one kind and works well Plant specimen manufacture craft.
In order to achieve the goal above, the technical scheme adopted by the invention is that:
A kind of preparation method of plant specimen, comprising the following steps:
S1. plant pretreatment fluid is first prepared, the pretreatment fluid has identical acid group by ferrous salt and with the ferrous salt Acid is formulated;
S2. plant sample is immersed in plant pretreatment fluid and is heated reaction, until translucent appearance is presented in plant sample;
S3. drying and processing is carried out to plant sample;
S4. plant sample tiling is put into transparent polybag, then vacuumize to polybag makes plant sample and modeling Material bag fitting;
S5. the plant sample of packaging plastic bags is put into mold and mold is vacuumized to eliminate after injecting resin into mold Bubble, then demoulding obtains finished product after hardening of resin.
Further, the plant pretreatment fluid includes ferrous sulfate and dilute sulfuric acid mixed liquor or hydrochloric acid ferrous iron and dilute hydrochloric acid Mixed liquor or ferrous nitrate and dust technology mixed liquor.
Further, the molar concentration rate of ferrous salt in the plant pretreatment fluid and acid is 1:1, and the two is rubbed Your concentration is 1 ~ 3.5mol/L.
Further, in the step S2, heating temperature is 65 ~ 70 DEG C, and heating time is 2 ~ 3 hours.
Further, the material of the polybag is in polyethylene terephthalate, polyethylene, polyamide or polypropylene It is one or more of.
Further, the resin includes the raw material of following parts by weight: 90 ~ 99 parts of polymethyl methacrylate, fourth cyanogen 1 ~ 2 Part.
Further, in the step S5, polymethyl methacrylate pours into mold after mixing with fourth cyanogen vacuumize after, it is right Resin carries out heating water bath until hardening of resin, wherein bath temperature is 45 DEG C 80 DEG C.
The beneficial effects of the present invention are: plant specimen of the invention is before being made as artificial specimen first with polybag pair Plant specimen carries out Vacuum Package to carry out being protected from the ambroids such as resin material and directly connects with plant specimen to plant specimen Touching causes resin and plant to generate physical and chemical reaction, while can also be conducive to plant specimen and keep preferably showing that form prevents resin The bending of fluid driven plant specimen or folded deformation when pouring into mold.
Detailed description of the invention
Fig. 1 is the side sectional view of plant specimen of the invention.
Wherein, 1- resin layer, 2- polybag, 3- plant specimen.
Specific embodiment
De-protected technical solution is wanted to be described in further detail the present invention now in conjunction with specific embodiment.
A kind of preparation method of plant specimen in the present embodiment, comprising the following steps:
S1. plant pretreatment fluid is first prepared, the plant pretreatment fluid has same acids by ferrous salt and with the ferrous salt The acid of root is formulated, and specifically in the present embodiment, the plant pretreatment fluid includes that molar concentration is 1.5mol/L sulphur Sour ferrous and molar concentration is 1mol/L dilute sulfuric acid mixed liquor, and plant pretreatment fluid can be sub- for hydrochloric acid in other embodiments Iron and dilute hydrochloric acid mixed liquor or ferrous nitrate and dust technology mixed liquor.
S2. plant sample is immersed in plant pretreatment fluid and is heated reaction, until plant sample is presented outside translucent It sees;In the present embodiment, heating temperature is 65 ~ 70 DEG C, and heating time is 2 ~ 3 hours.Due in chlorophyll in acid condition Magnesium elements just gradually replaced hydrogen ion, make the de-magnesium pheophytin of brown, therefore dilute sulphur can be used in the present embodiment Acid replaces the magnesium in chlorophyll, then reacts the hydrogen for replacing its ferrous ion in chlorophyll with chlorophyll by ferrous sulfate The metastable metal of chemical property is obtained for chlorophyll, so that plant specimen be made to keep green, there is sample good outer It sees.
S3. drying and processing is carried out to plant sample, drying temperature is 60 ~ 80 DEG C, drying time about 2 ~ 3 hours, passes through drop The rate and mildew of low inside plants hydrolysis.
S4. plant sample tiling is put into transparent polybag, then polybag vacuumize making plant sample It is bonded with polybag;In the present embodiment, the material of polybag is polyethylene terephthalate, is gathered in other embodiments One or more of ethylene, polyamide or polypropylene.Plant specimen after drying is put into polybag and is vacuumized Sealing makes plant specimen and air exclusion that plant specimen be prevented to be mixed into oxygen during subsequent technique to cause to aoxidize, furthermore Since the compactness of polyethylene terephthalate polybag is good, chemical stability height can by polybag to plant specimen into Row protection, prevents resin and the direct haptoreaction of sample, while being easier in next work using the plant sample of packaging plastic bags Sequence resin keeps original posture when pouring into, prevent plant sample from being deformed by resin fluid Foldable.
S5. the plant sample of packaging plastic bags is put into mold and injected into mold after resin to mold vacuumize with Bubble is eliminated, in the present embodiment, the resin includes the raw material of following parts by weight: 90 ~ 99 parts of polymethyl methacrylate, fourth 1 ~ 2 part of cyanogen, polymethyl methacrylate pours into mold after mixing with fourth cyanogen vacuumize after, to resin carry out heating water bath until Hardening of resin, wherein bath temperature is 45 DEG C 80 DEG C.Plant specimen shown in FIG. 1 is finally obtained, wherein sample is from outside to inside It successively include resin layer 1, polybag 2 and plant specimen 3.
The embodiment of the above is only presently preferred embodiments of the present invention, not does limit in any form to the present invention System.Anyone skilled in the art, without departing from the scope of the technical proposal of the invention, all using the disclosure above Technology contents more possible variations and retouching are made to technical solution of the present invention, or be revised as the equivalence enforcement of equivalent variations Example.Therefore all contents without departing from technical solution of the present invention, equivalent equivalence changes, should all cover made by thinking according to the present invention In in protection scope of the present invention.

Claims (7)

1. a kind of preparation method of plant specimen, which comprises the following steps:
S1. plant pretreatment fluid is first prepared, the pretreatment fluid has identical acid group by ferrous salt and with the ferrous salt Acid is formulated;
S2. plant sample is immersed in plant pretreatment fluid and is heated reaction, until translucent appearance is presented in plant sample;
S3. drying and processing is carried out to plant sample;
S4. plant sample tiling is put into transparent polybag, then vacuumize to polybag makes plant sample and modeling Material bag fitting;
S5. the plant sample of packaging plastic bags is put into mold and mold is vacuumized to eliminate after injecting resin into mold Bubble, then demoulding obtains finished product after hardening of resin.
2. a kind of preparation method of plant specimen according to claim 1, it is characterised in that: the plant pretreatment fluid Including ferrous sulfate and dilute sulfuric acid mixed liquor or hydrochloric acid ferrous iron and dilute hydrochloric acid mixed liquor or ferrous nitrate and dust technology mixed liquor.
3. a kind of preparation method of plant specimen according to claim 1 or 2, it is characterised in that: the plant pretreatment The molar concentration rate of ferrous salt and acid in liquid is 1.5:1, and the molar concentration of acid is 1 ~ 3.5mol/L.
4. a kind of preparation method of plant specimen according to claim 1, it is characterised in that: in the step S2, heating Temperature is 65 ~ 70 DEG C, and heating time is 2 ~ 3 hours.
5. a kind of preparation method of plant specimen according to claim 1, it is characterised in that: the material of the polybag is One or more of polyethylene terephthalate, polyethylene, polyamide or polypropylene.
6. a kind of preparation method of plant specimen according to claim 1, it is characterised in that: the resin includes following heavy The raw material of amount part: 90 ~ 99 parts of polymethyl methacrylate, 1 ~ 2 part of fourth cyanogen.
7. a kind of preparation method of plant specimen according to claim 6, it is characterised in that: in the step S5, poly- first Base methyl acrylate pours into mold after mixing with fourth cyanogen vacuumize after, heating water bath is carried out until hardening of resin to resin, Middle bath temperature is 45 DEG C 80 DEG C.
CN201910593838.9A 2019-07-03 2019-07-03 A kind of preparation method of plant specimen Pending CN110288894A (en)

Priority Applications (1)

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CN201910593838.9A CN110288894A (en) 2019-07-03 2019-07-03 A kind of preparation method of plant specimen

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Application Number Priority Date Filing Date Title
CN201910593838.9A CN110288894A (en) 2019-07-03 2019-07-03 A kind of preparation method of plant specimen

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CN110288894A true CN110288894A (en) 2019-09-27

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Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1058131A (en) * 1991-02-12 1992-01-29 张家口市植物标本站 The colour-keeping treatment method of transparent plant specimens
CN101341868A (en) * 2008-08-20 2009-01-14 杜静磊 Process for preparing biological specimen
CN102499234A (en) * 2011-10-27 2012-06-20 云南省烟草农业科学研究院 Manufacturing method for liquid film closed type plant primary-color herbarium specimens
JP5634346B2 (en) * 2011-08-08 2014-12-03 市村 清 Plant leaf processing method
CN106173816A (en) * 2015-05-28 2016-12-07 株式会社佐藤运送 Restore green plant or the method keeping green
CN107476529A (en) * 2017-08-08 2017-12-15 江门市江海区金昇咨询有限公司 A kind of resin decorative sheet and preparation method thereof
CN108077248A (en) * 2017-11-27 2018-05-29 阜阳师范学院 Red Chinese rose dries color-protection technique
CN109085028A (en) * 2018-06-07 2018-12-25 西南大学 The production method that citrus leaves disease solidifies sample

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1058131A (en) * 1991-02-12 1992-01-29 张家口市植物标本站 The colour-keeping treatment method of transparent plant specimens
CN101341868A (en) * 2008-08-20 2009-01-14 杜静磊 Process for preparing biological specimen
JP5634346B2 (en) * 2011-08-08 2014-12-03 市村 清 Plant leaf processing method
CN102499234A (en) * 2011-10-27 2012-06-20 云南省烟草农业科学研究院 Manufacturing method for liquid film closed type plant primary-color herbarium specimens
CN106173816A (en) * 2015-05-28 2016-12-07 株式会社佐藤运送 Restore green plant or the method keeping green
CN107476529A (en) * 2017-08-08 2017-12-15 江门市江海区金昇咨询有限公司 A kind of resin decorative sheet and preparation method thereof
CN108077248A (en) * 2017-11-27 2018-05-29 阜阳师范学院 Red Chinese rose dries color-protection technique
CN109085028A (en) * 2018-06-07 2018-12-25 西南大学 The production method that citrus leaves disease solidifies sample

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Application publication date: 20190927