CN110279625B - Preparation method, application and application method of toothbrush tree powder - Google Patents

Preparation method, application and application method of toothbrush tree powder Download PDF

Info

Publication number
CN110279625B
CN110279625B CN201910629192.5A CN201910629192A CN110279625B CN 110279625 B CN110279625 B CN 110279625B CN 201910629192 A CN201910629192 A CN 201910629192A CN 110279625 B CN110279625 B CN 110279625B
Authority
CN
China
Prior art keywords
toothbrush
powder
percent
tree powder
application
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201910629192.5A
Other languages
Chinese (zh)
Other versions
CN110279625A (en
Inventor
李愔杰
宋珂
李铮
丁亚伟
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Xinlu Biotechnology Guangzhou Co ltd
Original Assignee
Xinlu Biotechnology Guangzhou Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Xinlu Biotechnology Guangzhou Co ltd filed Critical Xinlu Biotechnology Guangzhou Co ltd
Priority to CN201910629192.5A priority Critical patent/CN110279625B/en
Publication of CN110279625A publication Critical patent/CN110279625A/en
Application granted granted Critical
Publication of CN110279625B publication Critical patent/CN110279625B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q11/00Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses

Abstract

The invention discloses a preparation method of toothbrush tree powder and application and an application method thereof. A preparation method of toothbrush tree powder comprises the following steps: removing impurities and leaves from fresh toothbrush branches without diseases and insect pests, preliminarily cleaning, disinfecting, cleaning with purified water, draining and drying; crushing the dried toothbrush branches to form fine powder with the fineness of 120-500 meshes; and (3) carrying out magnetic separation on the fine powder by a magnetic separator, detecting by a metal detector, and obtaining the toothbrush tree powder after the detection is qualified. The application of the toothbrush tree powder is the application of the toothbrush tree powder in oral care products. The application of the tooth brush dust in the toothpaste or tooth powder comprises an abrasive agent, a humectant, a foaming agent, a stable thickening agent, a flavoring agent, a freshener, a sweetening agent and a preservative, wherein the abrasive agent comprises the tooth brush dust. The invention also discloses an application method of the toothbrush tree powder.

Description

Preparation method, application and application method of toothbrush tree powder
Technical Field
The invention relates to the field of oral care products, in particular to a preparation method of toothbrush tree powder and application and an application method thereof.
Background
Prior to the invention of modern toothpaste and dentifrice, in Africa and Arabic tropical areas, local people used toothbrush branches directly to brush their teeth, which had a long history as a natural oral care tool. The toothbrush branches are used for brushing teeth and cleaning the oral cavity, so that the toothbrush has the effects of protecting and protecting the teeth, preventing decayed teeth and whitening, is fresh, clean and comfortable in the oral cavity after being used, is natural and environment-friendly, and has the advantages that a plurality of modern toothpaste abrasives cannot achieve.
Disclosure of Invention
Based on the above, the invention aims to provide a preparation method of the toothbrush tree powder, and application methods thereof.
The preparation method of the toothbrush tree powder comprises the following steps:
removing impurities and leaves from fresh toothbrush branches without diseases and insect pests, preliminarily cleaning, disinfecting, cleaning with purified water, draining and drying;
crushing the dried toothbrush branches to form fine powder with the fineness of 120-500 meshes;
and (4) carrying out magnetic separation on the fine powder by a magnetic separator, detecting by a metal detector, and obtaining the toothbrush tree powder after the detection is qualified.
The preparation method of the toothbrush tree powder can completely or partially replace an abrasive in modern toothpaste by making the toothbrush tree powder with special functions and effects into pure plant fine powder, can better meet the pursuit of modern people advocating nature and enjoying the traditional functions of natural plants, can be applied to oral care products, and achieves the effects of strengthening and protecting teeth, preventing caries and whitening.
Further preferably, the preliminary cleaning includes: putting the toothbrush branches into a cleaning pool for primary cleaning and secondary cleaning;
the disinfecting, comprising: putting the preliminarily cleaned toothbrush branches into a disinfection tank, adding disinfectant, and performing soaking disinfection and sterilization treatment;
the draining and drying process comprises the following steps: draining the cleaned toothbrush branches, and drying in a drying box or a tunnel dryer.
Further preferably, the crushing of the dried toothbrush branches to form fine powder with fineness of 120-500 meshes comprises: firstly, putting the dried toothbrush branches into a universal pulverizer to pulverize into particles with the size of 2-10mm, and then putting the particles into an ultrafine pulverizer to form 120-mesh 500-mesh fine powder.
The invention also provides an application of the toothbrush tree powder prepared by the preparation method of the toothbrush tree powder in an oral care product.
The application of the toothbrush tree powder disclosed by the invention in an oral care product can make the oral cavity fresh and comfortable after use and obviously eliminate foreign odor.
Further preferably, the application is the application of the toothbrush tree powder in toothpaste or tooth powder;
the toothpaste or dentifrice comprises an abrasive agent, a humectant, a foaming agent, a stable thickening agent, a flavoring agent, a freshener, a sweetening agent and a preservative;
the abrasive comprises the toothbrush tree powder and one or more of calcium carbonate, calcium hydrophosphate dihydrate and silicon dioxide;
the humectant comprises glycerin and/or sorbitol;
the foaming agent comprises sodium dodecyl sulfate and/or sodium lauroyl sarcosinate;
the stabilizing thickener comprises sodium carboxymethylcellulose and/or xanthan gum;
the flavoring agent comprises edible essence;
the cooling agent comprises menthol;
the sweetener comprises saccharin and/or xylitol;
the preservative comprises sodium benzoate.
The application of the tooth brush tree powder is applied to toothpaste or tooth powder, the tooth brush tree powder is added into an abrasive, the prepared toothpaste or tooth powder has the effects of tooth care, tooth protection, caries prevention and whitening, the oral cavity is fresh and comfortable after use, and foreign odor can be obviously eliminated.
Further preferably, the toothpaste or dentifrice further comprises a buffering agent comprising monocalcium phosphate and/or tetrasodium pyrophosphate.
Further preferably, the toothpaste or the tooth powder comprises the following components in percentage by weight:
Figure BDA0002128187730000031
Figure BDA0002128187730000041
further preferably, the toothpaste or dentifrice further comprises other functional agents including one or more of sodium monofluorophosphate, vitamins and chlorophyll.
Further preferably, the toothpaste or dentifrice comprises the following components in percentage by weight:
Figure BDA0002128187730000042
the invention further provides an application method of the toothbrush tree powder, which comprises the following steps:
putting the humectant, the foaming agent, the stable thickening agent, the flavoring agent, the freshener, the sweetening agent and the preservative into a container, and uniformly stirring and mixing to obtain a mixture I;
if the abrasive comprises the toothbrush tree powder and silicon dioxide, and calcium carbonate and/or calcium hydrogen phosphate dihydrate;
adding silicon dioxide into the mixture I, and stirring and mixing uniformly to obtain a mixture II;
adding the toothbrush tree powder, calcium carbonate and/or calcium hydrogen phosphate dihydrate into the mixture II, stirring and mixing uniformly, and taking out to obtain the toothpaste or tooth powder.
The preparation process of the application method of the toothbrush tree powder is simple, and the application method is suitable for popularization and application of the toothbrush tree powder.
Detailed Description
The implementations described in the exemplary embodiments below are not intended to represent all implementations consistent with the present disclosure. Rather, they are merely examples of methods consistent with certain aspects of the present disclosure, as detailed in the appended claims.
The terminology used in the present disclosure is for the purpose of describing particular embodiments only and is not intended to be limiting of the disclosure. As used in this disclosure and the appended claims, the singular forms "a," "an," and "the" are intended to include the plural forms as well, unless the context clearly indicates otherwise. It should also be understood that the term "and/or" as used herein refers to and encompasses any and all possible combinations of one or more of the associated listed items.
The components of the formulations in the following examples are, unless otherwise specified, conventional commercial products.
The preparation method of the toothbrush tree powder comprises the following steps:
step 101, removing impurities and leaves from fresh toothbrush branches without diseases and insect pests, preliminarily cleaning, disinfecting, cleaning with purified water, draining and drying.
Specifically, the preliminary cleaning includes: putting the toothbrush branches into a cleaning pool for primary cleaning and secondary cleaning.
The disinfecting, comprising: and (3) putting the preliminarily cleaned toothbrush branches into a disinfection tank, adding disinfectant, and performing soaking disinfection and sterilization treatment.
The draining and drying process comprises the following steps: draining the cleaned toothbrush branches, and drying in a drying box or a tunnel dryer.
102, crushing the dried toothbrush branches to form fine powder with the fineness of 120 meshes and 500 meshes.
Specifically, the dried toothbrush branches are firstly put into a universal pulverizer to be pulverized into particles with the size of 2-10mm, and then the particles are put into an ultrafine pulverizer to form fine powder with the fineness of 120-mesh and 500-mesh.
The size of the fine powder is 20-120 μm.
And 103, carrying out magnetic separation on the fine powder by a magnetic separator, detecting by a metal detector, and obtaining the toothbrush tree powder after the detection is qualified.
The prepared toothbrush tree powder can be further packaged to obtain a qualified finished product.
The preparation method of the invention prepares the toothbrush tree powder with special functions and effects into pure plant fine powder, can completely or partially replace an abrasive in modern toothpaste, can better meet the pursuit of modern people advocating nature and enjoying the traditional functions of natural plants, can be applied to oral care products, and achieves the effects of tooth care, tooth prevention and whitening.
The invention also provides an application of the toothbrush tree powder prepared by the preparation method of the toothbrush tree powder in oral care products.
The application of the following examples is the use of the tooth brush powder in toothpaste or tooth powder.
Example one
The toothpaste or dentifrice of this embodiment includes an abrasive agent, a humectant, a foaming agent, a buffering agent, a stabilizing thickener, a flavoring agent, a cooling agent, a sweetener, and a preservative.
The abrasive agent comprises the toothbrush tree powder and one or more of calcium carbonate, calcium hydrogen phosphate dihydrate salt and silicon dioxide.
The humectant comprises glycerin and/or sorbitol.
The foaming agent comprises sodium dodecyl sulfate and/or sodium lauroyl sarcosinate.
The buffer comprises monocalcium phosphate and/or tetrasodium pyrophosphate.
The stabilizing thickener comprises sodium carboxymethylcellulose and/or xanthan gum.
The flavoring agent comprises edible essence.
The cooling agent comprises menthol.
The sweetener comprises saccharin and/or xylitol.
The preservative comprises sodium benzoate.
There are 3 examples of the toothpaste or dentifrice of this example.
The toothpaste or dentifrice of examples 1 to 3 comprises the following components in weight percent:
Figure BDA0002128187730000071
Figure BDA0002128187730000081
the toothpaste or the tooth powder has stable quality and comfortable mouthfeel, has the whitening and tooth-protecting effects after being used for a long time, and has the quality guarantee period of one year.
Example two
The toothpaste or dentifrice of this embodiment includes an abrasive agent, a humectant, a foaming agent, a stabilizing thickener, a flavoring agent, a cooling agent, a sweetener, a preservative, and other functional agents.
The abrasive includes the toothbrush tree powder and includes one or more of calcium carbonate, dibasic calcium phosphate dihydrate and silica.
The humectant includes glycerin and/or sorbitol.
The foaming agent comprises sodium dodecyl sulfate and/or sodium lauroyl sarcosinate.
The stabilizing thickener comprises sodium carboxymethylcellulose and/or xanthan gum.
The flavoring agent comprises edible essence.
The cooling agent comprises menthol.
The sweetener comprises saccharin and/or xylitol.
The preservative comprises sodium benzoate.
The other functional agents include one or more of sodium monofluorophosphate, vitamins and chlorophyll.
There are 3 examples of the toothpaste or dentifrice of this example.
The toothpaste or dentifrice of examples 4 to 6 comprises the following components in weight percent:
Figure BDA0002128187730000082
Figure BDA0002128187730000091
the toothpaste or the tooth powder prepared by adding the toothbrush tree powder into the abrasive has the effects of strengthening and protecting teeth, preventing caries and whitening, the oral cavity is fresh and comfortable after use, foreign odor can be obviously eliminated, and the quality guarantee period can reach one year.
The invention further provides an application method of the toothbrush tree powder, which can be used for preparing toothpaste or tooth powder in the first embodiment and the second embodiment and comprises the following steps:
s1, putting the humectant, the foaming agent, the stable thickening agent, the flavoring agent, the freshener, the sweetener and the preservative into a container, and uniformly stirring and mixing to obtain a mixture I.
For the toothpaste or tooth powder of example one, the buffer may be added to the mix at this step.
For the toothpaste or dentifrice of example two, the other functional agents may be added to mix during this step.
Preferably, the mixture can be stirred and mixed for about 10 min.
S2, if the abrasive comprises the toothbrush tree powder and silicon dioxide, and calcium carbonate and/or calcium hydrogen phosphate dihydrate salt;
adding silicon dioxide into the mixture I, and stirring and uniformly mixing to obtain a mixture II.
Preferably, the mixture can be stirred for about 10 min.
S3, adding the toothbrush tree powder, calcium carbonate and/or calcium hydrogen phosphate dihydrate into the mixture II, stirring and mixing uniformly, and taking out to obtain the toothpaste or tooth powder.
Preferably, the mixture can be stirred for about 40 min.
The preparation method of the toothbrush tree powder also comprises the step of packaging the toothbrush tree powder to obtain a qualified finished product.
The application method of the toothbrush tree powder has simple preparation process and is suitable for popularization and application of the toothbrush tree powder.
The above-mentioned embodiments only express several embodiments of the present invention, and the description thereof is more specific and detailed, but not construed as limiting the scope of the invention. It should be noted that, for a person skilled in the art, several variations and modifications can be made without departing from the inventive concept, which falls within the scope of the present invention.

Claims (5)

1. The application of the toothbrush tree powder is characterized by comprising the following components:
the application of the toothbrush tree powder is the application in toothpaste or tooth powder;
the toothpaste or dentifrice comprises an abrasive agent, a humectant, a foaming agent, a stable thickening agent, a flavoring agent, a freshener, a sweetening agent and a preservative;
the abrasive comprises the toothbrush tree powder and one or more of calcium carbonate, calcium hydrophosphate dihydrate and silicon dioxide;
the humectant comprises glycerin and/or sorbitol;
the foaming agent comprises sodium dodecyl sulfate and/or sodium lauroyl sarcosinate;
the stabilizing thickener comprises sodium carboxymethylcellulose and/or xanthan gum;
the flavoring agent comprises edible essence;
the cooling agent comprises menthol;
the sweetener comprises saccharin and/or xylitol;
the preservative comprises sodium benzoate;
the toothpaste or the tooth powder also comprises other functional agents, and the other functional agents comprise one or more of sodium monofluorophosphate, vitamins and chlorophyll;
the preparation method of the toothbrush tree powder comprises the following steps:
removing impurities and leaves from fresh toothbrush branches without diseases and insect pests, preliminarily cleaning, disinfecting, cleaning with purified water, draining and drying;
crushing the dried toothbrush branches to form fine powder with the fineness of 120 meshes;
magnetically separating the fine powder by a magnetic separator, detecting by a metal detector, and preparing the toothbrush tree powder after the detection is qualified;
the preliminary cleaning comprises: putting the toothbrush branches into a cleaning pool for primary cleaning and secondary cleaning;
the disinfecting, comprising: putting the preliminarily cleaned toothbrush branches into a disinfection tank, adding disinfectant, and performing soaking disinfection and sterilization treatment;
the draining and drying process comprises the following steps: draining the cleaned toothbrush branches, and drying in a drying box or a tunnel dryer.
2. The application of the toothbrush tree powder as claimed in claim 1, wherein the crushing of the dried toothbrush tree branches to form fine powder with fineness of 120-500 meshes comprises: firstly, putting the dried toothbrush branches into a universal pulverizer to pulverize into particles with the size of 2-10mm, and then putting the particles into an ultrafine pulverizer to form 120-mesh 500-mesh fine powder.
3. The use of the toothbrash tree powder of claim 1, wherein the toothpaste or toothbrash further comprises a buffering agent comprising monocalcium phosphate and/or tetrasodium pyrophosphate.
4. The use of the toothbrash tree powder according to claim 3, characterized in that the toothpaste or toothpowder comprises the following components in percentage by weight:
3 to 20 percent of toothbrush tree powder, 20 to 40 percent of calcium hydrophosphate or calcium carbonate, 5 to 15 percent of silicon dioxide, 20 to 30 percent of sorbitol, 10 to 20 percent of glycerin, 2 to 5 percent of sodium dodecyl sulfate, 0.5 to 3 percent of sodium lauroyl sarcosinate, 0.1 to 0.5 percent of calcium dihydrogen phosphate, 0.2 to 1.0 percent of tetrasodium pyrophosphate, 1 to 2 percent of sodium carboxymethyl cellulose, 0.2 to 1.0 percent of xanthan gum, 1 to 3 percent of edible essence, 0.2 to 1.0 percent of menthol, 0.2 to 0.5 percent of saccharin and 0.1 to 0.2 percent of sodium benzoate.
5. The use of the toothbrash tree powder according to claim 1, wherein the toothpaste or toothpowder comprises the following components in percentage by weight:
10-40% of toothbrush tree powder, 30-60% of calcium carbonate, 2-10% of silicon dioxide, 2-5% of glycerol, 2-6% of sodium lauroyl sarcosinate, 0.5-2% of sodium carboxymethyl cellulose, 1-3% of edible essence, 0.2-1.0% of menthol, 1-5% of xylitol, 0.1% of saccharin, 0.1% of sodium benzoate, 0.1% of sodium monofluorophosphate, 1% of vitamin D and 0.02% of chlorophyll.
CN201910629192.5A 2019-07-12 2019-07-12 Preparation method, application and application method of toothbrush tree powder Active CN110279625B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910629192.5A CN110279625B (en) 2019-07-12 2019-07-12 Preparation method, application and application method of toothbrush tree powder

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201910629192.5A CN110279625B (en) 2019-07-12 2019-07-12 Preparation method, application and application method of toothbrush tree powder

Publications (2)

Publication Number Publication Date
CN110279625A CN110279625A (en) 2019-09-27
CN110279625B true CN110279625B (en) 2022-09-13

Family

ID=68022198

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201910629192.5A Active CN110279625B (en) 2019-07-12 2019-07-12 Preparation method, application and application method of toothbrush tree powder

Country Status (1)

Country Link
CN (1) CN110279625B (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI817111B (en) * 2021-04-28 2023-10-01 歐萊德國際股份有限公司 Compositions for oral cleaning

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101229112A (en) * 2008-01-31 2008-07-30 许盛英 Attapulgite herbaceous tooth powder
CN206227650U (en) * 2016-10-25 2017-06-09 北京市农林科学院 A kind of intelligent cleaning product line of ternip

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101229112A (en) * 2008-01-31 2008-07-30 许盛英 Attapulgite herbaceous tooth powder
CN206227650U (en) * 2016-10-25 2017-06-09 北京市农林科学院 A kind of intelligent cleaning product line of ternip

Also Published As

Publication number Publication date
CN110279625A (en) 2019-09-27

Similar Documents

Publication Publication Date Title
US20210275437A1 (en) Oral Care Composition Comprising Cuttlefish Bone Powder and Uses Thereof
KR101854418B1 (en) Toothpaste composition comprising jade ingredient
TW201622693A (en) Oral care composition containing silica and zinc citrate
US9114097B1 (en) Composition of natural toothpaste
EA022986B1 (en) Oral care composition
CN110279625B (en) Preparation method, application and application method of toothbrush tree powder
CN111000772A (en) New use of exocarpium Citri Grandis extract
KR101102476B1 (en) Functional Toothpaste Composition for Removal of Oral Odor
JP2007197393A (en) Dentifrice
JP5907075B2 (en) Dentifrice composition
JP2020040944A (en) Composition for oral cavity containing nipa extract as active ingredient
KR20110129046A (en) Functional toothpaste component
CN100398091C (en) An anti-cavity toothpaste with natural substances for children and method for making same
EP2883532A1 (en) Diamond dust polishing agent for dental veneers and teeth
CN113318020A (en) Multifunctional tooth powder
CN107802507B (en) Application of thorn-reducing composition in preparation of oral care product and oral care product
CN105853316A (en) Toothpaste and preparation method thereof
KR101627825B1 (en) Composition for toothpaste using cuttlefish bone and preparation method thereof
KR100704585B1 (en) Toothpaste composition
JP2013155169A (en) Dentifrice composition
CN110801417A (en) Toothpaste for children
KR102527525B1 (en) Oral hygienic composition enhanced teeth scaling for pet dogs
US20210283042A1 (en) Oral care compositions and method of making same
JP6874688B2 (en) Toothpaste composition and oral biofilm remover
JP6772906B2 (en) Toothpaste composition

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant