CN110200841A - A kind of cicada fungus tremella face mask liquid and preparation method thereof - Google Patents
A kind of cicada fungus tremella face mask liquid and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a kind of cicada fungus tremella face mask liquid and preparation method thereof, the cicada fungus tremella face mask liquid includes the component of following mass percentage: 0.3%-0.4% cicada fungus polysaccharide, 1%-3% tremella polysaccharides extract, 0.1-0.2% carboxymethyl chitosan, 0.2%-0.3% fructus lycii berry extract, 0.3-0.5% carbomer, 0.5-0.8% xanthan gum, 1-1.5% Semen Coicis extract, 0.02%-0.04% vitamin E, 0.3%-0.5% pearl powder and 0.3-0.5% hyaluronic acid, surplus are water;The cicada fungus tremella face mask liquid and preparation method thereof comprises the steps of raw material preparation, mixing, heating for dissolving, homogeneous, cooling, degassing, sterilizing.The present invention is compounded by using pure natural ingredient, no hormone, without fluorescer etc..It can effectively solve the problems, such as that face, the facial mask liquids such as fuel-displaced, dry decortication, coarse, the obscure unglazed and hyperkeratosis of pore have natural no stimulation, integrate the feature of moisturizing moisturizing, heavy, glossy shining color, the compact soft and moist multi-efficiency of desalination color.
Description
Technical field
The present invention relates to a kind of facial mask liquid and preparation method thereof, in particular to a kind of cicada fungus tremella face mask liquid and its preparation side
Method.
Background technique
Cicada fungus (Ophiocordyceps sobolifera) is also known as cicada bacterium cicada pupa grass, is Clavicipitaceae fungi Paecilomyces cicadae
Complex after parasitic bamboo cicada nymph, the cordyceps sinensis similar with cordyceps sinensis are rare Chinese medicine.
Tremella (Tremella fueiformis Berk), also known as tremella, tremella are a kind of common macro fungis,
Because of its edible value and medical value with higher, it is often assigned the laudatory title of " hat of strain ".Tremella polysaccharides are that tremella is real
One of body acid heteroglycan can form colloid with certain gelation, because of its unique bioactivity and antioxygen in water
The pharmacological characteristics such as change are widely used in food and medicine industry.In addition, studies have shown that tremella polysaccharides can significantly increase human body
Immune function delays senescence, inhibited to tumour.Tremella polysaccharides are that the water-soluble natural biology that extracts from tremella is big
Molecule, average molecular weight are more than ten thousand, have good water holding capacity, and tremella polysaccharides can combine moisture and can manage it in skin surface
At layer protecting film, has effects that good moisturizing water lock.Tremella polysaccharides can improve the immunocompetence of cell and self repair simultaneously
Reactivation power promotes cytokine growth, restores skin health gloss, and protection cell is not easily susceptible to oxidative damage, has to skin
Skin-care effect is nourished well.
Polysaccharides has the light injury effect for protecting Human keratinocytes to induce from UVB.Therefore polysaccharides can
To be potentially served as in anti-oxidant skin care item.Skin aging is mainly caused by free-radical oxidation, and polysaccharides is a variety of in vitro
Oxidation resistance is shown in antioxidant system, can also be improved skin SOD activity, be reduced MDA content, increases skin hydroxyl dried meat
Histidine content has the function of anti-aging.
Summary of the invention
Goal of the invention: the present invention provides a kind of cicada fungus tremella face mask liquid and preparation method thereof, and facial mask liquid is green safe, is applicable in
In a variety of skin skin quality, has the characteristics that synergy whitening, toxic side effect be small, obvious effect, be edible mushroom deep processed product in day
The application for changing aspect provides a new route.
Technical solution: a kind of cicada fungus tremella face mask liquid of the present invention, the component comprising following mass percentage:
0.3%-0.4% cicada fungus polysaccharide, 1%-3% tremella polysaccharides extract, 0.1-0.2% carboxymethyl chitosan, 0.2%-0.3% Chinese holly
Fructus lycii extract, 0.3-0.5% carbomer, 0.5-0.8% xanthan gum, 1-1.5% Semen Coicis extract, 0.02%-0.04%
Vitamin E, 0.3%-0.5% pearl powder and 0.3-0.5% hyaluronic acid, surplus are water;
The cicada fungus polysaccharide is prepared by the following method: weighing quantitative cicada fungus powder, addition cicada fungus powder mass ratio is 1:8-10
Times deionized water under conditions of controlling 2000-3000rmp, is centrifuged 15-20min, takes supernatant, the 90- of 3-5 times of volume is added
95% ethyl alcohol, 4-6 DEG C of standing 10-12h, centrifugation abandon supernatant, obtain cicada fungus polysaccharide precipitation, take and are deposited in baking oven dry 24-
36h is to get cicada fungus polysaccharide;
The tremella polysaccharides extract the preparation method comprises the following steps: tremella picking after, remove culture medium, clean drain after, in 40-
1-2h is dried under the conditions of 45 DEG C, oven temperature is then turned up to 55-60 DEG C, drying to constant weight, and the tremella after drying crushes
Afterwards, it is sieved, water is added into the tremella powder after sieving, the mass ratio for controlling tremella powder and water is 1:10-15, is warming up to 40-45
DEG C, 1.5-2h is cooked, is stirred continuously in boiling process, mixing speed 80-100r/min after the completion of cooking, is cooled to room temperature, double
Layer nylon cloth filtering, filtrate is tremella polysaccharides extract;
The Semen Coicis extract the preparation method comprises the following steps: semen coicis crushed 80-100 mesh, weigh quantitative semen coicis
Powder, addition mass concentration are 90-95% ethanol solution circumfluence distillation, and solid-liquid ratio 1:8-10g/mL controls extraction time
1.5-2h, Extracting temperature are 60-65 DEG C, after filtrate is concentrated, are drying to obtain Semen Coicis extract;
The fructus lycii berry extract the preparation method comprises the following steps: weigh quantitative fructus lycii, 80- is added by solid-liquid ratio 1:8-10g/mL
In 90% ethyl alcohol, it is heated to reflux 1-1.5h in 75-80 DEG C, filters, washing, is heated to reflux 1- in 80-85 DEG C of hot water
1.5h is filtered, and after extracting solution is concentrated with Rotary Evaporators, with the ethyl alcohol alcohol precipitation of 80-90%, is stood 36-48h, is taken and be deposited in
Dry 36-48h is in baking oven to get fructus lycii berry extract.
Preferably, the facial mask liquid includes the component of following mass percentage: 0.35% cicada fungus polysaccharide, 2% tremella are more
Sugar extract, 0.15% carboxymethyl chitosan, 0.25% fructus lycii berry extract, 0.4% carbomer, 0.6% xanthan gum, 1.3%
Semen Coicis extract, 0.03% vitamin E, 0.4% pearl powder and 0.4% hyaluronic acid, surplus are water.
The preparation method of above-mentioned cicada fungus tremella face mask liquid comprising the steps of:
(1) preparation of cicada fungus polysaccharide: weighing quantitative cicada fungus powder, and addition cicada fungus powder mass ratio is 1:8-10 times of deionized water,
Under conditions of controlling 2000-3000rmp, it is centrifuged 15-20min, takes supernatant, the 90-95% ethyl alcohol of 3-5 times of volume, 4-6 is added
DEG C 10-12h is stood, centrifugation abandons supernatant, obtains cicada fungus polysaccharide precipitation, takes that be deposited in baking oven dry 24-36h more to get cicada fungus
Sugar;
(2) preparation of tremella polysaccharides extract: after tremella picking, culture medium is removed, is cleaned after draining, in 40-45 DEG C of item
1-2h is dried under part, oven temperature is then turned up to 55-60 DEG C, drying to constant weight, by the tremella after drying, after crushing, sieving,
Water is added into the tremella powder after sieving, the mass ratio for controlling tremella powder and water is 1:10-15, is warming up to 40-45 DEG C, cooks
1.5-2h is stirred continuously in boiling process, and mixing speed 80-100r/min after the completion of cooking, is cooled to room temperature, double-layer nylon
Cloth filtering, filtrate is tremella polysaccharides extract;
(3) preparation of Semen Coicis extract: crushed 80-100 mesh for semen coicis, weigh quantitative coix seed powder, be added
Mass concentration is 90-95% ethanol solution circumfluence distillation, and solid-liquid ratio 1:8-10g/mL controls extraction time 1.5-2h, mentions
Taking temperature is 60-65 DEG C, after filtrate is concentrated, is drying to obtain Semen Coicis extract;
(4) preparation of fructus lycii berry extract: weighing quantitative fructus lycii, and the second of 80-90% is added by solid-liquid ratio 1:8-10g/mL
In alcohol, it is heated to reflux 1-1.5h in 75-80 DEG C, filters, washing, 1-1.5h is heated to reflux in 80-85 DEG C of hot water, filter,
After extracting solution is concentrated with Rotary Evaporators, with the ethyl alcohol alcohol precipitation of 80-90%, 36-48h is stood, takes and is deposited in drying in baking oven
36-48h is to get fructus lycii berry extract;
(5) after proportionally weighing required cicada fungus polysaccharide, tremella polysaccharides extract and the mixing of fructus lycii berry extract respectively,
50-60 DEG C of deionized water is added, 20min-30nin dissolution is mixed;
(6) proportionally by load weighted carboxymethyl chitosan, xanthan gum, carbomer, pearl powder carry out it is dry-mixed after, be added
8-10 times of deionized water is mixed 10-15min under the conditions of being kept for 55-60 DEG C and is swollen, then obtained with step (6)
Solution mixing, obtains mixed liquor;
(7) Semen Coicis extract, vitamin E and hyaluronic acid are slowly added in mixed liquor, are stirred again, controlled
Mixing speed processed is 50-60r/min, stirs 20-30min, carries out homogenization, and control homogenization pressure is 24-30MPa;
(8) it uses to vacuumize and be de-gassed, vacuum degree control is 90.3-93.3KPa in vacuum tank, handles 45-
60min obtains cicada fungus tremella face mask liquid.
Preferably, in step (9), resulting cicada fungus tremella face mask liquid cooling is but packed afterwards, is then carried out at irradiation
Reason, irradiation sterilization CO60Radiation sterilizing is carried out, irradiation dose control is 800-1000kGy, sterilization time 24-36h.
Preferably, in step (2), the slot size of the sieving is 150 mesh.
Preferably, in step (2), the specification of the nylon cloth is 100 mesh.
Unless otherwise indicated, " % " of the present invention is mass percentage concentration.
The utility model has the advantages that the ingredients such as tremella polysaccharides, cicada fungus polysaccharide are added on the basis of common facial mask formula of liquid in (1) present invention,
In addition to having the features such as whitening and moistening skin, anti-aging, permanent moisturizing, product simultaneously passes through the processing modes such as irradiation sterilization, enhances facial mask
The safety and reliability that liquid uses;(2) the cicada fungus tremella face mask processing method that the present invention is illustrated has easily operated, face
The homogeneous exquisiteness of film liquid, natural no stimulation, easy the features such as absorbing, and can promote the metabolism of skin, there is anti-aging, protect
The effect of wet water lock, nourishing skin care.
Specific embodiment
One, raw material sources
Carbomer is Acritamer 940, and the average molecular weight of hyaluronic acid is 10~150,000 KDa, and carboxymethyl chitosan is put down
Average molecular weight is 1~50,000 KDa.
Two, sample preparation
2.1 raw material preparation
The preparation of cicada fungus polysaccharide: weighing quantitative cicada fungus powder, and addition cicada fungus powder mass ratio is 1:8 times of deionized water, control
Under conditions of 2000rmp, it is centrifuged 15min, takes supernatant, 95% ethyl alcohol of 5 times of volumes is added, 4 DEG C of standing 10h are centrifuged, in abandoning
Clear liquid obtains cicada fungus polysaccharide precipitation, takes and is deposited in baking oven dry 36h, obtains cicada fungus polysaccharide.
The preparation of tremella polysaccharides extract: after tremella picking, culture medium is removed, cleans after draining, is dried under the conditions of 45 DEG C
Oven temperature is then turned up to 55 DEG C in dry 2h, and drying to constant weight, by the tremella after drying, after crushing, crosses 150 meshes, controls grain
Diameter is less than 0.1mm, and water is added into the tremella powder after sieving, and the mass ratio for controlling tremella powder and water is 1:10, is warming up to 40 DEG C,
2h is cooked, is stirred continuously in boiling process, mixing speed 100r/min after the completion of cooking, is cooled to room temperature, the double-deck 100 mesh Buddhist nuns
Imperial cloth filtering, filtrate are tremella polysaccharides extract;
The preparation of Semen Coicis extract: semen coicis crushing is sieved with 100 mesh sieve, and is weighed quantitative coix seed powder after sieving, is added
Mass concentration is 95% ethanol solution circumfluence distillation, and solid-liquid ratio 1:10g/mL controls extraction time 1.5h, and Extracting temperature is
65 DEG C, after filtrate is concentrated, dry Semen Coicis extract.
The preparation of fructus lycii berry extract: weighing quantitative fructus lycii, is added in 90% ethyl alcohol by solid-liquid ratio 1:8g/mL, in 80
It DEG C is heated to reflux 1.5h, filters, washing, 1h is heated to reflux in 85 DEG C of hot water, filter, extracting solution Rotary Evaporators are dense
After contracting, with 90% ethyl alcohol alcohol precipitation, 48h is stood, takes and is deposited in baking oven dry 48h, obtain fructus lycii berry extract.
Embodiment 1:
Step (1): 0.3% required cicada fungus polysaccharide, 2% tremella polysaccharides extract and 0.2% are proportionally weighed respectively
After the mixing of fructus lycii berry extract, 55 DEG C of deionized waters are added, 25nin dissolution is mixed;
Step (2): by load weighted 0.2% carboxymethyl chitosan, 0.8% xanthan gum, 0.3% Acritamer 940,0.3%
After progress is dry-mixed, 10 times of deionized waters are added in pearl powder etc., and 10min is mixed under the conditions of being kept for 60 DEG C and is swollen, to molten
Without obvious particle in liquid, the solution mixing that step (1) obtains then is added, obtains mixed liquor.
Step (3): 1% Semen Coicis extract, 0.02% vitamin E and 0.3% hyaluronic acid are slowly added to above step
In resulting mixed solution, secondary agitation is carried out, control mixing speed is 60r/min, stirs 20min, carries out homogeneous after the completion
Processing, control homogenization pressure are 25MPa, homogeneous 15min.
Step (4): the solution after homogeneous obtained in step (3) is de-gassed, vacuum degree control in vacuum tank
For 92kPa, 50min is handled.
Step (5): by the facial mask liquid after deaerating obtained in step (4), after suitably packing, using CO60It is irradiated
Sterilization, irradiation dose control is 800kGy, sterilization time 36h, up to cicada fungus tremella face mask liquid after the completion of processing.
0.3%-0.4% cicada fungus polysaccharide, 1%-3% tremella polysaccharides extract, 0.1-0.2% carboxymethyl chitosan, 0.2-
0.3% fructus lycii berry extract, 0.3-0.5% carbomer, 0.5-0.8% xanthan gum, 1-1.5% Semen Coicis extract, 0.02-
0.04% vitamin E, 0.30.5% pearl powder and 0.3-0.5% hyaluronic acid, surplus are water;
Embodiment 2:
Step (1): proportionally weigh respectively 0.4% required cicada fungus polysaccharide, 2.5% tremella polysaccharides extract and
After the mixing of 0.3% fructus lycii berry extract, 55 DEG C of deionized waters are added, 25nin dissolution is mixed.
Step (2): by load weighted 0.1% carboxymethyl chitosan, 0.5% xanthan gum, 0.5% Acritamer 940,0.5%
After progress is dry-mixed, 8 times of deionized waters are added in pearl powder etc., and 10min is mixed under the conditions of being kept for 55 DEG C and is swollen, to molten
Without obvious particle in liquid, the solution mixing that step (1) obtains then is added, obtains mixed liquor.
Step (3): 1.5% Semen Coicis extract, 0.04% vitamin E and 0.5% hyaluronic acid are slowly added to the above step
In rapid resulting mixed solution, secondary agitation is carried out, control mixing speed is 55r/min, stirs 30min, is carried out after the completion equal
Matter processing, control homogenization pressure are 25MPa, homogeneous 20min.
Step (4): the solution after homogeneous obtained in step (3) is de-gassed, vacuum degree control in vacuum tank
For 93kPa, 60min is handled.
Step (5): by the facial mask liquid after deaerating obtained in step (4), after suitably packing, using CO60It is irradiated
Sterilization, irradiation dose control are 1000kGy, and sterilization time is for 24 hours, up to cicada fungus tremella face mask liquid after the completion of processing.
Embodiment 3:
Step (1): proportionally weigh respectively 0.35% required cicada fungus polysaccharide, 2% tremella polysaccharides extract and
After the mixing of 0.25% fructus lycii berry extract, 60 DEG C of deionized waters are added, 30nin dissolution is mixed.
Step (2): by load weighted 0.15% carboxymethyl chitosan, 0.6% xanthan gum, 0.4% Acritamer 940,0.4%
After progress is dry-mixed, 8 times of deionized waters are added in pearl powder etc., and 10min is mixed under the conditions of being kept for 55 DEG C and is swollen, to molten
Without obvious particle in liquid, the solution mixing that step (1) obtains then is added, obtains mixed liquor.
Step (3): 1.3% Semen Coicis extract, 0.03% vitamin E and 0.4% hyaluronic acid are slowly added to the above step
In rapid resulting mixed solution, secondary agitation is carried out, control mixing speed is 55r/min, stirs 30min, is carried out after the completion equal
Matter processing, control homogenization pressure are 25MPa, homogeneous 20min.
Step (4): the solution after homogeneous obtained in step (3) is de-gassed, vacuum degree control in vacuum tank
For 93kPa, 60min is handled.
Step (5): by the facial mask liquid after deaerating obtained in step (4), after suitably packing, using CO60It is irradiated
Sterilization, irradiation dose control are 1000kGy, and sterilization time is for 24 hours, up to cicada fungus tremella face mask liquid after the completion of processing.
Claims (6)
1. a kind of cicada fungus tremella face mask liquid, which is characterized in that the component comprising following mass percentage: 0.3%-0.4% cicada
Flower polysaccharide, 1%-3% tremella polysaccharides extract, 0.1-0.2% carboxymethyl chitosan, 0.2%-0.3% fructus lycii berry extract,
0.3-0.5% carbomer, 0.5-0.8% xanthan gum, 1-1.5% Semen Coicis extract, 0.02%-0.04% vitamin E,
0.3%-0.5% pearl powder and 0.3-0.5% hyaluronic acid, surplus are water;
The cicada fungus polysaccharide is prepared by the following method: weighing quantitative cicada fungus powder, cicada fungus powder mass ratio is added and goes for 1:8-10 times
Ionized water under conditions of controlling 2000-3000rmp, is centrifuged 15-20min, takes supernatant, the 90-95% of 3-5 times of volume is added
Ethyl alcohol, 4-6 DEG C of standing 10-12h, centrifugation abandon supernatant, obtain cicada fungus polysaccharide precipitation, take and are deposited in baking oven dry 24-36h, i.e.,
Obtain cicada fungus polysaccharide;
The tremella polysaccharides extract the preparation method comprises the following steps: tremella picking after, remove culture medium, clean drain after, in 40-45 DEG C
Under the conditions of dry 1-2h, then be turned up oven temperature to 55-60 DEG C, drying to constant weight, by the tremella after drying, after crushing, mistake
Water is added into the tremella powder after sieving for sieve, and the mass ratio for controlling tremella powder and water is 1:10-15, is warming up to 40-45 DEG C, boils
1.5-2h processed is stirred continuously in boiling process, and mixing speed 80-100r/min after the completion of cooking, is cooled to room temperature, the double-deck Buddhist nun
Imperial cloth filtering, filtrate is tremella polysaccharides extract;
The Semen Coicis extract the preparation method comprises the following steps: semen coicis crushed 80-100 mesh, weigh quantitative coix seed powder, add
Entering mass concentration is 90-95% ethanol solution circumfluence distillation, and solid-liquid ratio 1:8-10g/mL controls extraction time 1.5-2h,
Extracting temperature is 60-65 DEG C, after filtrate is concentrated, is drying to obtain Semen Coicis extract;
The fructus lycii berry extract the preparation method comprises the following steps: weigh quantitative fructus lycii, be added 80-90%'s by solid-liquid ratio 1:8-10g/mL
In ethyl alcohol, it is heated to reflux 1-1.5h in 75-80 DEG C, filters, washing, 1-1.5h is heated to reflux in 80-85 DEG C of hot water, take out
Filter after extracting solution is concentrated with Rotary Evaporators, with the ethyl alcohol alcohol precipitation of 80-90%, stands 36-48h, takes to be deposited in baking oven and do
Dry 36-48h is to get fructus lycii berry extract.
2. cicada fungus tremella face mask liquid according to claim 1, which is characterized in that the group comprising following mass percentage
Point: 0.35% cicada fungus polysaccharide, 2% tremella polysaccharides extract, 0.15% carboxymethyl chitosan, 0.25% fructus lycii berry extract,
0.4% carbomer, 0.6% xanthan gum, 1.3% Semen Coicis extract, 0.03% vitamin E, 0.4% pearl powder and 0.4%
Hyaluronic acid, surplus are water.
3. the preparation method of cicada fungus tremella face mask liquid according to claim 1 or 2, which is characterized in that comprise the steps of:
(1) preparation of cicada fungus polysaccharide: weighing quantitative cicada fungus powder, and addition cicada fungus powder mass ratio is 1:8-10 times of deionized water, control
Under conditions of 2000-3000rmp, it is centrifuged 15-20min, takes supernatant, the 90-95% ethyl alcohol of 3-5 times of volume is added, 4-6 DEG C quiet
10-12h is set, is centrifuged, supernatant is abandoned, obtains cicada fungus polysaccharide precipitation, takes and is deposited in baking oven dry 24-36h to get cicada fungus polysaccharide;
(2) preparation of tremella polysaccharides extract: after tremella picking, culture medium is removed, is cleaned after draining, under the conditions of 40-45 DEG C
1-2h is dried, oven temperature is then turned up to 55-60 DEG C, drying to constant weight, by the tremella after drying, after crushing, sieving, to mistake
Water is added in tremella powder after sieve, the mass ratio for controlling tremella powder and water is 1:10-15, is warming up to 40-45 DEG C, cooks 1.5-
2h is stirred continuously in boiling process, and mixing speed 80-100r/min after the completion of cooking, is cooled to room temperature, double-layer nylon cloth mistake
Filter, filtrate is tremella polysaccharides extract;
(3) preparation of Semen Coicis extract: crushed 80-100 mesh for semen coicis, weigh quantitative coix seed powder, and quality is added
Concentration is 90-95% ethanol solution circumfluence distillation, and solid-liquid ratio 1:8-10g/mL controls extraction time 1.5-2h, extracts temperature
Degree is 60-65 DEG C, after filtrate is concentrated, is drying to obtain Semen Coicis extract;
(4) preparation of fructus lycii berry extract: weighing quantitative fructus lycii, is added in the ethyl alcohol of 80-90% by solid-liquid ratio 1:8-10g/mL,
It is heated to reflux 1-1.5h in 75-80 DEG C, filters, washing, 1-1.5h is heated to reflux in 80-85 DEG C of hot water, filter, will extract
After liquid is concentrated with Rotary Evaporators, with the ethyl alcohol alcohol precipitation of 80-90%, 36-48h is stood, takes and is deposited in baking oven dry 36-48h,
Up to fructus lycii berry extract;
(5) it after proportionally weighing required cicada fungus polysaccharide, tremella polysaccharides extract and the mixing of fructus lycii berry extract respectively, is added
20min-30nin dissolution is mixed in 50-60 DEG C of deionized water;
(6) proportionally by load weighted carboxymethyl chitosan, xanthan gum, carbomer, pearl powder carry out it is dry-mixed after, be added 8-10
Times deionized water is mixed 10-15min under the conditions of being kept for 55-60 DEG C and is swollen, the solution then obtained with step (6)
Mixing, obtains mixed liquor;
(7) Semen Coicis extract, vitamin E and hyaluronic acid are slowly added in mixed liquor, are stirred again, control is stirred
Mixing speed is 50-60r/min, stirs 20-30min, carries out homogenization, and control homogenization pressure is 24-30MPa;
(8) it using to vacuumize and be de-gassed, vacuum degree control is 90.3-93.3KPa in vacuum tank, 45-60min is handled,
Obtain cicada fungus tremella face mask liquid.
4. the preparation method of cicada fungus tremella face mask liquid according to claim 3, which is characterized in that in step (9), by gained
Cicada fungus tremella face mask liquid cooling but packed afterwards, then carry out radiation treatment, irradiation sterilization CO60Carry out radiation sterilizing, spoke
It is 800-1000kGy, sterilization time 24-36h according to dosage control.
5. the preparation method of cicada fungus tremella face mask liquid according to claim 3, which is characterized in that in step (2), the mistake
The slot size of sieve is 150 mesh.
6. the preparation method of cicada fungus tremella face mask liquid according to claim 3, which is characterized in that in step (2), the Buddhist nun
The specification of imperial cloth is 100 mesh.
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Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105078876A (en) * | 2015-09-17 | 2015-11-25 | 成都朴锐生物科技有限公司 | cordyceps sobolifera skin care composition and preparation method thereof |
CN105726439A (en) * | 2016-02-05 | 2016-07-06 | 浙江理工大学 | Cordyceps cicadae whitening and moisturizing cosmeceutical and preparing method thereof |
CN106606452A (en) * | 2017-01-10 | 2017-05-03 | 广州源理生物科技有限公司 | Essence capable of adjusting moisture-oil balance and whitening skin |
CN106727155A (en) * | 2017-01-13 | 2017-05-31 | 广州美中生物科技有限公司 | A kind of facial mask of natural skin care composition and preparation method thereof |
CN107019657A (en) * | 2016-12-14 | 2017-08-08 | 上海辉文生物技术股份有限公司 | A kind of skin whitening, moisturizing composition and preparation method thereof and application method |
CN109172404A (en) * | 2018-10-18 | 2019-01-11 | 周君梅 | A kind of anti-wrinkle essence and preparation method thereof |
CN109288738A (en) * | 2018-11-29 | 2019-02-01 | 福建天眼视界健康科技有限公司 | Eye protection composition, eye mask and preparation method thereof |
-
2019
- 2019-05-23 CN CN201910432703.4A patent/CN110200841A/en active Pending
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105078876A (en) * | 2015-09-17 | 2015-11-25 | 成都朴锐生物科技有限公司 | cordyceps sobolifera skin care composition and preparation method thereof |
CN105726439A (en) * | 2016-02-05 | 2016-07-06 | 浙江理工大学 | Cordyceps cicadae whitening and moisturizing cosmeceutical and preparing method thereof |
CN107019657A (en) * | 2016-12-14 | 2017-08-08 | 上海辉文生物技术股份有限公司 | A kind of skin whitening, moisturizing composition and preparation method thereof and application method |
CN106606452A (en) * | 2017-01-10 | 2017-05-03 | 广州源理生物科技有限公司 | Essence capable of adjusting moisture-oil balance and whitening skin |
CN106727155A (en) * | 2017-01-13 | 2017-05-31 | 广州美中生物科技有限公司 | A kind of facial mask of natural skin care composition and preparation method thereof |
CN109172404A (en) * | 2018-10-18 | 2019-01-11 | 周君梅 | A kind of anti-wrinkle essence and preparation method thereof |
CN109288738A (en) * | 2018-11-29 | 2019-02-01 | 福建天眼视界健康科技有限公司 | Eye protection composition, eye mask and preparation method thereof |
Non-Patent Citations (3)
Title |
---|
刘艺等: ""枸杞多糖面膜的制备与性能评价"", 《日用化学工业》 * |
翁梁: ""野生蝉花与人工蝉花多糖的提取及抑菌试验"", 《农业科技与装备》 * |
陈明岭等: "《皮肤病常用中药药理及临床 第2版》", 31 October 2017, 中国科学技术出版社 * |
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