CN110184810A - Preparation method with anti-ultraviolet function fabric - Google Patents
Preparation method with anti-ultraviolet function fabric Download PDFInfo
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- CN110184810A CN110184810A CN201910220814.9A CN201910220814A CN110184810A CN 110184810 A CN110184810 A CN 110184810A CN 201910220814 A CN201910220814 A CN 201910220814A CN 110184810 A CN110184810 A CN 110184810A
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- Prior art keywords
- fabric
- preparation
- mordant
- ultraviolet function
- polyamide fibre
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/10—Animal fibres
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/34—Polyamides
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/25—Resistance to light or sun, i.e. protection of the textile itself as well as UV shielding materials or treatment compositions therefor; Anti-yellowing treatments
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
The invention discloses the preparation methods with anti-ultraviolet function fabric, preparation can be realized by two different modes, method processing silk, polyamide fibre and the modified cotton fabric impregnated using the extracting solution high temperature of Chinese medicine sweetberry jointfir, keep extracting solution and fabric fixed, to make silk, polyamide fibre and cotton fabric that there is anti-ultraviolet function.The fabric obtained using preparation method of the present invention is comfortable and easy to wear, does not have carcinogenic, teratogenesis problem or causes allergic reaction；It is good with ecological environment compatibility, it is biodegradable.The product is easy, and the resource of nature is taken full advantage of, and market prospects are very wide.
Description
Technical field
The invention belongs to the research and development field of anti-ultraviolet function fabric, and in particular to anti-ultraviolet function fabric
Preparation method.
Background technique
In recent years, the use of a large amount of fluorochemicals results in the destruction of ozone layer in atmosphere, has seriously threatened the mankind
Health.Report display, In The Atmosphere Over China ozone layer reduced 14% between 20 years.The reduction of ozone layer, which results in, is irradiated to the earth
The quantity of the ultraviolet light on surface increases, and ultraviolet light can cause skin disease, or even cause cutaneum carcinoma.Ultraviolet light is controlled to human body
Direct irradiation is one of the important channel for reducing cutaneum carcinoma.Therefore, the development with anti-ultraviolet function textile has important
Meaning.
Sweetberry jointfir is Gnetopsida (Ni rattan guiding principle) Gnetaceae Gnetum gymnosperm, and whole world only one category (is bought
Numb Calamus), more than totally 30 kinds.Usually said medicinal sweetberry jointfir, refers to Gnetum parvifolium.It is Gnetum parvifolium also known as the wooden peanut, big
Mesh rattan etc. is used as medicine with drying rattan, have relieving asthma, the pharmacological actions such as antiallergy, anti-snake venom, also have effect to cardiovascular system.The people
Between for treating the diseases such as rheumatic arthralgia, lumbar muscle strain, weapons wound, snake bite, bronchitis and ulcer bleeding.Sweetberry jointfir mentions
Taking liquid to contain, there are many medicinal chemistry ingredients, including flavone compound.
Using Caulis Gneti extractive liquid as the research of anti UV finishing agent, has no and have been reported that.
Summary of the invention
The purpose of the present invention is to provide the preparation methods with anti-ultraviolet function fabric, utilize mentioning for Chinese medicine sweetberry jointfir
Method processing silk, polyamide fibre and the modified cotton fabric for taking liquid high temperature to impregnate, keep extracting solution and fabric fixed, to make silk, brocade
Synthetic fibre and cotton fabric have anti-ultraviolet function.
In order to solve the above-mentioned technical problem, it adopts the following technical scheme that
A kind of preparation method with anti-ultraviolet function fabric, it is characterised in that include the following steps:
(1) it is 1:(40-60 by bath raio), Caulis Gneti extractive liquid and mordant, water mixing are configured to finishing fluid, sweetberry jointfir
The quality of extracting solution is the 20%-40% of finishing fluid gross mass, and the dosage of mordant is 1-3g/L, and surplus is water；
(2) cotton fabric after silk, polyamide fibre and modification is respectively put into finishing fluid and is arranged, when arrangement controls
PH value is 3.5-5.5, and temperature is 80-100 DEG C, time 50-70min；Fabric is cleaned after arrangement, is dried, obtains having anti-
The fabric of ultraviolet function.
After it is preferred that, before Cotton Fabric, modification, modified technique need to be first carried out are as follows: modifying agent 20g/L, sodium hydroxide
10g/L, bath raio 1:50 handle 30min under the conditions of 60 DEG C.
After it is preferred that, the modifying agent is cation modifier.
After it is preferred that, the cation modifier is LD-8201, LD-8202 or other cation modifiers.
After it is preferred that, the mordant is alum, ferrous sulfate or mixed chlorinated rare earth.
Another kind has the preparation method of anti-ultraviolet function fabric, it is characterised in that includes the following steps:
(1) prepared by finishing fluid:
It is 1:(40-60 by bath raio) Caulis Gneti extractive liquid and water mixing are configured to finishing fluid, the matter of Caulis Gneti extractive liquid
Amount is the 20%-40% of finishing fluid gross mass, and surplus is water, and adjusting finishing fluid pH value is 3.5-5.5；
(2) textile finishing:
Cotton fabric after silk, polyamide fibre and modification is respectively put into finishing fluid and is arranged, temperature 80-100
DEG C, the time is to clean fabric after 50-70min is handled, dry；
(3) mordant dyeing is handled after fabric:
It is configured to rear mordant dyeing treatment fluid with mordant and water mixing, wherein mordant dosage is 1-3g/L, and surplus is water；It is whole
Fabric after reason obtains the fabric with uvioresistant function after the mordant dyeing of mordant dyeing treatment fluid after.
After it is preferred that, the mordant is alum, ferrous sulfate or mixed chlorinated rare earth.
After it is preferred that, mordant dyeing treatment process in the step (3) are as follows: the fabric after arrangement is respectively put into rear mordant dyeing treatment fluid
In handled, control bath raio is 1:(40-60 when processing), temperature is 50-70 DEG C, time 20-40min；It will be knitted after processing
Object is cleaned, is dried, and the fabric with uvioresistant function is obtained.
As a result of the above technical solution, the following beneficial effects are obtained:
The present invention is the preparation method with anti-ultraviolet function fabric, is impregnated using the extracting solution high temperature of Chinese medicine sweetberry jointfir
Method processing silk, polyamide fibre and modified cotton fabric, keep extracting solution and fabric fixed, to make silk, polyamide fibre and cotton fabric tool
There is anti-ultraviolet function.
Present invention process is simple, can handle on equipment for dyeing and finishing, improves production efficiency；
The fabric obtained using preparation method of the present invention is comfortable and easy to wear, does not have carcinogenic, teratogenesis problem or causes allergy
Reaction；It is good with ecological environment compatibility, it is biodegradable.The product is easy, and the resource of nature, market are taken full advantage of
Prospect is very wide.
Specific embodiment
Below with reference to specific embodiment, realization process of the invention is described in detail.
The ratio between the definition dye liquor volume (L) of bath raio and pollutant quality (kg).Such as pollutant 10kg, dye liquor volume is
100L, then bath raio 10:1.Bath raio can be written generally as 1:10 in industry.
Not arranging real silk fabric UPF value is 6.58, and 6 fabric UPF value of polyamide fibre is 3.40,56 fabric UPF value of polyamide fibre is 3.66.
Non- finishing of cotton textiles original cloth UPF value is 5.18, and modified cotton fabric UPF value is 5.97.
Sweetberry jointfir used in the present invention is extracted by certain method and is obtained: the sweetberry jointfir after drying is cut into small pieces,
It is added in sodium hydrate aqueous solution, 60min-120min is extracted at 80 DEG C -100 DEG C and obtains extracting solution；Extracting solution is filtered, very
Sky is concentrated.
Embodiment 1:
(1) 80mL Caulis Gneti extractive liquid is added in 320mL water, it is 3.5 that glacial acetic acid, which is added, and adjusts pH value, is then added
1.2g ferrous sulfate.
(2) cotton fabric after 10g silk, polyamide fibre or modification is added separately in three parts of identical above solution,
70min is handled under conditions of bath raio is 1:40, temperature is 80 DEG C.Then fabric taken out and is cleaned, dried, obtain having anti-
The fabric of ultraviolet light function.Cotton fabric UPF value is 148.35 after tested, and real silk fabric UPF value is 98.51,6 fabric UPF of polyamide fibre
Value is 135.10, and 56 fabric UPF value of polyamide fibre is 136.12.After 20 times are soaped, cotton fabric UPF value is 110.72, real silk fabric UPF
Value is 59.66, and 6 fabric UPF value of polyamide fibre is 106.63, and 56 fabric UPF value of polyamide fibre is 107.33.
Embodiment 2:
(1) 240mL Caulis Gneti extractive liquid is added in 360mL water, be added glacial acetic acid adjust pH value be 5.5, then plus
Enter 0.6g alum.
(2) cotton fabric after 10g silk, polyamide fibre or modification is added separately to three parts of identical above solution
In, 50min is handled under conditions of bath raio 1:60, temperature are 100 DEG C.Then fabric taken out and is cleaned, dried, had
The fabric of anti-ultraviolet function.After tested, cotton fabric UPF value is 151.28, and real silk fabric UPF value is 61.31,6 fabric of polyamide fibre
UPF value is 241.20, and 56 fabric UPF value of polyamide fibre is 243.12.After 20 times are soaped, cotton fabric UPF value is 141.88, real silk fabric
UPF value is 48.51, and 6 fabric UPF value of polyamide fibre is 215.73, and 56 fabric UPF value of polyamide fibre is 217.13.
Embodiment 3:
(1) 150mL Caulis Gneti extractive liquid is added in 350mL water, be added glacial acetic acid adjust pH value be 4.5, then plus
Enter 1g mixed chlorinated rare earth.
(2) cotton fabric after 10g silk, polyamide fibre or modification is added separately to three parts of identical above solution
In, bath raio 1:50, it is at a temperature of 90 °C under the conditions of handle 60min.Then fabric taken out and is cleaned, dried, had
The fabric of anti-ultraviolet function.Cotton fabric UPF value is 87.28 after tested, and real silk fabric UPF value is 56.04,6 fabric UPF of polyamide fibre
Value is 83.37, and 56 fabric UPF value of polyamide fibre is 85.17.After 20 times are soaped, cotton fabric UPF value is 62.16, and silk fabrics UPF value is
43.65,6 fabric UPF value of polyamide fibre is 75.59, and 56 fabric UPF value of polyamide fibre is 76.69.
Embodiment 4:
(1) 150mL Caulis Gneti extractive liquid is added in 350mL water, and it is 4.5 that glacial acetic acid, which is added, to adjust pH value；By 10g
Cotton fabric after silk, polyamide fibre or modification is added separately in three parts of identical above solution, in bath raio 1:50, temperature
60min is handled under conditions of 90 DEG C；Then fabric taken out and is cleaned, dried；
(2) 500mL distilled water is measured, 1.5g mixed chlorinated rare earth is added；The fabric cleaned, dried in step (1) is added
Enter into the above solution, handles 30min under conditions of temperature is 60 DEG C, bath raio 1:50；Then fabric taken out and is cleaned, dried in the air
It is dry, obtain the fabric with anti-ultraviolet function.Cotton fabric UPF value is 49.80 after tested, and real silk fabric UPF value is 45.64,
6 fabric UPF value of polyamide fibre is 158.63, and 56 fabric UPF value of polyamide fibre is 159.83.After 20 times are soaped, cotton fabric UPF value is 46.72,
Real silk fabric UPF value is 50.14, and 6 fabric UPF value of polyamide fibre is 111.30, and 56 fabric UPF value of polyamide fibre is 113.13.
Embodiment 5:
(1) 240mL Caulis Gneti extractive liquid is added in 360mL water, and it is 3.5 that glacial acetic acid, which is added, to adjust pH value；By 10g
Cotton fabric after silk, polyamide fibre or modification is added separately in three parts of identical above solution, in bath raio 1:60, temperature
50min is handled under the conditions of being 100 DEG C；Then fabric taken out and is cleaned, dried；
(2) 600mL distilled water is measured, 1.2g alum is added；The fabric cleaned, dried in step (1) is added to above
In solution, 20min is handled under the conditions of temperature is 70 DEG C, bath raio 1:60；Then fabric taken out and is cleaned, dried, had
There is the fabric of anti-ultraviolet function.After tested, cotton fabric UPF value is 90.12, and real silk fabric UPF value is 36.18,6 fabric of polyamide fibre
UPF value is 155.26, and 56 fabric UPF value of polyamide fibre is 156.66.After 20 times are soaped, cotton fabric UPF value is 89.46, real silk fabric
UPF value is 35.08, and 6 fabric UPF value of polyamide fibre is 126.31, and 56 fabric UPF value of polyamide fibre is 127.39.
Embodiment 6:
(1) 80mL Caulis Gneti extractive liquid is added in 320mL water, and it is 5.5 that glacial acetic acid, which is added, to adjust pH value；By 10g
Cotton fabric after silk, polyamide fibre or modification is added separately in three parts of identical above solution, is 80 DEG C, is bathed in temperature
Than handling 70min under the conditions of 1:40；Then fabric taken out and is cleaned, dried；
(2) 400mL distilled water is measured, 0.4g ferrous sulfate is added；The fabric cleaned, dried in step (1) is added to
In the above solution, 40min is handled under the conditions of temperature is 50 DEG C, bath raio 1:40；Then fabric taken out and is cleaned, dried, obtained
To the fabric with anti-ultraviolet function.Cotton fabric UPF value is 121.13 after tested, and silk fabrics UPF value is 46.18, and polyamide fibre 6 is knitted
Object UPF value is 158.58, and 56 fabric UPF value of polyamide fibre is 159.78.After 20 times are soaped, cotton fabric UPF value is 111.01, silk fabrics
UPF value is 43.11, and 6 fabric UPF value of polyamide fibre is 148.96, and 56 fabric UPF value of polyamide fibre is 149.98.
Therefore, uvioresistant finishing agent of the Caulis Gneti extractive liquid as silk, cotton and nylon fabric, treated silk,
Cotton and nylon fabric have excellent anti-ultraviolet property.
The above is only specific embodiments of the present invention, but technical characteristic of the invention is not limited thereto.It is any with this hair
Based on bright, to solve essentially identical technical problem, essentially identical technical effect is realized, made ground simple change, etc.
With replacement or modification etc., all it is covered by among protection scope of the present invention.
Claims (8)
1. a kind of preparation method with anti-ultraviolet function fabric, it is characterised in that include the following steps:
(1) it is 1:(40-60 by bath raio), Caulis Gneti extractive liquid and mordant, water mixing are configured to finishing fluid, sweetberry jointfir is extracted
The quality of liquid is the 20%-40% of finishing fluid gross mass, and the dosage of mordant is 1-3g/L, and surplus is water；
(2) cotton fabric after silk, polyamide fibre and modification is respectively put into finishing fluid and is arranged, when arrangement controls pH value
For 3.5-5.5, temperature is 80-100 DEG C, time 50-70min；Fabric is cleaned after arrangement, is dried, is obtained with uvioresistant
The fabric of function.
2. a kind of preparation method with anti-ultraviolet function fabric according to claim 1, it is characterised in that: cotton fabric
Before arrangement, modification, modified technique need to be first carried out are as follows: modifying agent 20g/L, sodium hydroxide 10g/L, bath raio 1:50,60 DEG C of items
30min is handled under part.
3. a kind of preparation method with anti-ultraviolet function fabric according to claim 2, it is characterised in that: described to change
Property agent be cation modifier.
4. a kind of preparation method with anti-ultraviolet function fabric according to claim 3, it is characterised in that: the sun
Ion modification agent is LD-8201 or LD-8202.
5. a kind of preparation method with anti-ultraviolet function fabric according to claim 1, it is characterised in that: the matchmaker
Stain is alum, ferrous sulfate or mixed chlorinated rare earth.
6. the preparation method that another kind has anti-ultraviolet function fabric, it is characterised in that include the following steps:
(1) prepared by finishing fluid:
It is 1:(40-60 by bath raio) Caulis Gneti extractive liquid and water mixing are configured to finishing fluid, the quality of Caulis Gneti extractive liquid is
The 20%-40% of finishing fluid gross mass, surplus are water, and adjusting finishing fluid pH value is 3.5-5.5；
(2) textile finishing:
Cotton fabric after silk, polyamide fibre and modification is respectively put into finishing fluid and is arranged, temperature is 80-100 DEG C, when
Between fabric cleaned, to dry after 50-70min processing；
(3) mordant dyeing is handled after fabric:
It is configured to rear mordant dyeing treatment fluid with mordant and water mixing, wherein mordant dosage is 1-3g/L, and surplus is water；After arrangement
Fabric obtain the fabric with uvioresistant function after the mordant dyeing of mordant dyeing treatment fluid after.
7. another preparation method with anti-ultraviolet function fabric according to claim 6, it is characterised in that: described
Mordant is alum, ferrous sulfate or mixed chlorinated rare earth.
8. another preparation method with anti-ultraviolet function fabric according to claim 6, it is characterised in that: described
Mordant dyeing treatment process in step (3) are as follows: the fabric after arrangement is respectively put into rear mordant dyeing treatment fluid and is handled, time control is handled
Bath raio processed is 1:(40-60), temperature is 50-70 DEG C, time 20-40min；Fabric is cleaned after processing, is dried, is had
The fabric of uvioresistant function.
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| CN201910220814.9A CN110184810B (en) | 2019-03-22 | 2019-03-22 | Preparation method of fabric with anti-ultraviolet function |
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