CN104894862A - Preparation method of real silk fabric having uvioresistant function - Google Patents
Preparation method of real silk fabric having uvioresistant function Download PDFInfo
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- CN104894862A CN104894862A CN201510268597.2A CN201510268597A CN104894862A CN 104894862 A CN104894862 A CN 104894862A CN 201510268597 A CN201510268597 A CN 201510268597A CN 104894862 A CN104894862 A CN 104894862A
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Abstract
The invention relates to the field of preparation of functional textile fabrics and aims at providing a preparation method of a real silk fabric having an uvioresistant function. The method comprises the following steps: uniformly mixing a sanguisorba officinalis extract, a mordant, anhydrous sodium sulphate and water to prepare a finishing liquid; putting the real silk fabric in the finishing liquid for treating for 50-80min under the conditions that the pH value is 4-6 and the temperature is 60-80 DEG C; and after the finishing is finished, washing the raw real silk fabric clean and drying so as to obtain the real silk fabric having the uvioresistant function. The invention provides the environment-friendly novel technology for preparing the real silk fabric having the uvioresistant function; the extract is fixedly attached to the raw real silk fabric so that the real silk fabric has the uvioresistant function. The method is simple, the treatment process can be carried out on a dyeing and finishing device and therefore the production efficiency is improved; the fabric can come into direct contact with the skin, is good in safety, is free of carcinogenic and teratogenic effects or anaphylactic reaction, is good in compatibility with ecological environments, is biodegradable, is a novel environment-friendly product and is wide in application range.
Description
Technical field
The present invention relates to functional textile fabric preparation field, particularly relate to a kind of preparation method with the real silk fabric of anti-ultraviolet function.
Background technology
In recent years, the use of a large amount of fluorochemical result in the destruction of ozone layer in atmosphere, the destruction serious threat of this road natural obstacle health of the mankind.Report display, In The Atmosphere Over China ozone layer decreased 14% between 20 years.The minimizing of ozone layer result in the ultraviolet quantity being irradiated to earth surface to be increased, and ultraviolet can cause dermatitis, even can cause cutaneum carcinoma.Reducing the ultraviolet quantity being irradiated to human body skin, is the important channel of reducing cutaneum carcinoma.Therefore, the development tool with anti-ultraviolet function textiles is of great significance.
Garden burnet, have another name called garden burnet, beautiful to prick, beautiful fermented soya beans, salted or other wise or acid reddish brown etc., be the plant of rose family burnet.Mainly be distributed in north temperate zone, Asia, be widely distributed in Europe and China, be grown on the area of height above sea level 30 meters to 3000 meters, be often born in shrubbery, patana, grassland, under grassy marshland and sparse woods, by artificial introducing and planting.China's main product in the Northeast, the Inner Mongol, Shanxi, Shaanxi, Henan, Gansu, Shandong, the ground such as Guizhou.Garden burnet bitter, acid, puckery, cold nature, returns liver, large intestine channel; There is the effect such as cooling blood and hemostasis, removing toxic substances sore; Clinical be used for the treatment of have blood in stool, mole blood, bloody flux, uterine bleeding, scald, the illness such as the swollen sore of pain.Existing data shows, commercially available Radix Sangusorbae extract contains multiple medicinal chemistry composition, comprises flavone compound.
Utilize Radix Sangusorbae extract as the research of anti UV finishing agent, there are no report.
Summary of the invention
The technical problem to be solved in the present invention is, overcomes deficiency of the prior art, provides a kind of preparation method with the real silk fabric of anti-ultraviolet function.
For technical solution problem, the technical solution adopted in the present invention is:
A kind of preparation method with the real silk fabric of uvioresistant function is provided, comprises the following steps:
(1) arrangement of real silk fabric
(1) arrangement of real silk fabric
Be 1: 30 ~ 60 by the bath raio of real silk fabric, Radix Sangusorbae extract, glauber salt and water mixed and is mixed with dressing liquid; In dressing liquid, the quality of Radix Sangusorbae extract is 0.5 ~ 2% of real silk fabric quality, and the consumption of glauber salt is 10 ~ 12g/L, and surplus is water;
Real silk fabric is put into dressing liquid process, during process, control ph is 4 ~ 6, and temperature is 60 ~ 80 DEG C, and the time is 40 ~ 60min; After process, real silk fabric cleaned, dry;
(2) the rear mordant dyeing process of real silk fabric
Mix with alum or ferrous sulfate and water and be mixed with rear mordant dyeing treatment fluid; The consumption of mordant is 1 ~ 3g/L, and surplus is water;
Real silk fabric after arrangement is put into rear mordant dyeing treatment fluid process; Controlling bath raio during process is 1: 30 ~ 60, and temperature is 60 ~ 80 DEG C, and the time is 25 ~ 40min; After process, real silk fabric cleaned, dry, obtain the real silk fabric with uvioresistant function.
Present invention also offers the preparation method that another kind has the real silk fabric of uvioresistant function, comprise the following steps:
(1) preparation of dressing liquid
Be 1: 30 ~ 60 by the bath raio of real silk fabric, Radix Sangusorbae extract and mordant, glauber salt, water mixed and is mixed with dressing liquid; In dressing liquid, the quality of Radix Sangusorbae extract is 0.5 ~ 2% of real silk fabric quality, and the consumption of glauber salt is 10 ~ 12g/L, and mordant is alum or ferrous sulfate, and the consumption of mordant is 1 ~ 3g/L, and surplus is water;
(2) arrangement of real silk fabric
Real silk fabric is put into dressing liquid process; During process, control ph is 4 ~ 6, and temperature is 60 ~ 80 DEG C, and the time is 50 ~ 80min; After arrangement, real silk fabric cleaned, dry, obtain the real silk fabric with uvioresistant function.
Above-mentioned Radix Sangusorbae extract is the extract of Chinese medicine Radix Sangusorbae, is commercially available prod.
Compared with prior art, the invention has the beneficial effects as follows:
(1) the present invention proposes a kind of green new technology preparing the anti-ultraviolet real silk fabric of energy, namely the method process real silk fabric that the extract of Chinese medicine garden burnet floods at high temperature is utilized, make extract and real silk fabric set, thus make real silk fabric have anti-ultraviolet function;
(2) present invention process is simple, can process, enhance productivity on equipment for dyeing and finishing;
(3) fabric using preparation method of the present invention to obtain can directly and skin contact, and security is good, do not have carcinogenic, teratogenesis or cause allergic reaction; Good with ecological environment compatibility, biodegradable, be a kind of novel green product, its market prospects are very wide, the field such as can be used for garment material, family is spun.
Accompanying drawing explanation
Fig. 1 is the absorption spectrogram of the present invention's garden burnet extract used between 200 ~ 400nm ultraviolet region.
Detailed description of the invention
Below in conjunction with specific embodiment, implementation procedure of the present invention is described in detail.
The definition of bath raio: the ratio of dye liquor volume (L) and pollutant quality (kg).As pollutant 50kg, bath raio 20:1, then dye liquor volume is 1000L.In industry, bath raio is generally write as 1:20.
Embodiment 1:
(1) 0.05g Radix Sangusorbae extract is joined in 300ml water, add 3g glauber salt, and to add glacial acetic acid adjust ph be 4; 10g real silk fabric is added in above solution, temperature be 60 DEG C, bath raio processes 50min under being the condition of 1:30; Then real silk fabric taken out and clean, dry;
(2) measure 300ml distilled water, add 0.3g ferrous sulfate; Add in the above solution obtained by the real silk fabric cleaned in step (1), dry, be 60 DEG C in temperature, bath raio is process 30min under the condition of 1:30; Then real silk fabric taken out and clean, dry, obtaining the real silk fabric with anti-ultraviolet function.After tested, the UPF value of this real silk fabric is: 50.29.
Embodiment 2:
(1) 0.12g Radix Sangusorbae extract is joined in 450ml water, add 4.95g glauber salt, and to add glacial acetic acid adjust ph be 5; 10g real silk fabric is added in above solution, temperature be 80 DEG C, bath raio processes 40min under being the condition of 1:45; Then real silk fabric taken out and clean, dry;
(2) measure 450ml distilled water, add 1.35g alum; Add in the above solution obtained by the real silk fabric cleaned in step (1), dry, be 80 DEG C in temperature, bath raio is process 25min under the condition of 1:45; Then real silk fabric taken out and clean, dry, obtaining the real silk fabric with anti-ultraviolet function.After tested, the UPF value of this real silk fabric is: 82.41.
Embodiment 3:
(1) joined in 600ml water by 0.2g Radix Sangusorbae extract, add and 7.2g glauber salt, adding glacial acetic acid adjust ph is 6; 10g real silk fabric is added in above solution, temperature be 70 DEG C, bath raio processes 60min under being the condition of 1:60; Then real silk fabric taken out and clean, dry;
(2) measure 600ml distilled water, add 1.2g ferrous sulfate; Add in the above mixed liquor obtained by the real silk fabric cleaned in step (1), dry, be 70 DEG C in temperature, bath raio is process 40min under the condition of 1:60; Then real silk fabric taken out and clean, dry, obtaining the real silk fabric with anti-ultraviolet function.After tested, the UPF value of this real silk fabric is: 115.92.
Embodiment 4:
(1) 0.075g Radix Sangusorbae extract is joined in 300ml water, add 3g glauber salt, add 0.3g alum; And to add glacial acetic acid adjust ph be 5;
(2) adding in above solution by 10g real silk fabric, is 60 DEG C in temperature, and bath raio is process 50min under the condition of 1:30; Then real silk fabric taken out and clean, dry, obtaining the real silk fabric with anti-ultraviolet function.After tested, the UPF value of this real silk fabric is: 66.18.
Embodiment 5:
(1) 0.2g Radix Sangusorbae extract is joined in 600ml water, add 6.6g glauber salt, add 1.2g alum; And to add glacial acetic acid adjust ph be 4;
(2) adding in above solution by 10g real silk fabric, is 80 DEG C in temperature, and bath raio is process 60min under the condition of 1:60; Then real silk fabric taken out and clean, dry, obtaining the real silk fabric with anti-ultraviolet function.After tested, the UPF value of this real silk fabric is: 50.03.
Embodiment 6:
(1) 0.17g Radix Sangusorbae extract is joined in 450ml water, add 5.4g glauber salt, add 1.35g ferrous sulfate; And to add glacial acetic acid adjust ph be 6;
(2) adding in above solution by 10g real silk fabric, is 70 DEG C in temperature, and bath raio is process 80min under the condition of 1:45; Then real silk fabric taken out and clean, dry, obtaining the real silk fabric with anti-ultraviolet function.After tested, the UPF value of this real silk fabric is: 78.04.
As seen from Figure 1, Radix Sangusorbae extract is dark brown, and its maximum absorption wavelength is at 272nm.
In addition, garden burnet extract is as the uvioresistant finishing agent of real silk fabric, and the real silk fabric after process has excellent anti-ultraviolet property.
Claims (2)
1. there is a preparation method for the real silk fabric of uvioresistant function, it is characterized in that, comprise the following steps:
(1) arrangement of real silk fabric
Be 1: 30 ~ 60 by the bath raio of real silk fabric, Radix Sangusorbae extract, glauber salt and water mixed and is mixed with dressing liquid; In dressing liquid, the quality of Radix Sangusorbae extract is 0.5 ~ 2% of real silk fabric quality, and the consumption of glauber salt is 10 ~ 12g/L, and surplus is water;
Real silk fabric is put into dressing liquid process, during process, control ph is 4 ~ 6, and temperature is 60 ~ 80 DEG C, and the time is 40 ~ 60min; After process, real silk fabric cleaned, dry;
(2) the rear mordant dyeing process of real silk fabric
Mix with alum or ferrous sulfate and water and be mixed with rear mordant dyeing treatment fluid; The consumption of mordant is 1 ~ 3g/L, and surplus is water;
Real silk fabric after arrangement is put into rear mordant dyeing treatment fluid process; Controlling bath raio during process is 1: 30 ~ 60, and temperature is 60 ~ 80 DEG C, and the time is 25 ~ 40min; After process, real silk fabric cleaned, dry, obtain the real silk fabric with uvioresistant function.
2. there is a preparation method for the real silk fabric of uvioresistant function, it is characterized in that, comprise the following steps:
(1) preparation of dressing liquid
Be 1: 30 ~ 60 by the bath raio of real silk fabric, Radix Sangusorbae extract and mordant, glauber salt, water mixed and is mixed with dressing liquid; In dressing liquid, the quality of Radix Sangusorbae extract is 0.5 ~ 2% of real silk fabric quality, and the consumption of glauber salt is 10 ~ 12g/L, and mordant is alum or ferrous sulfate, and the consumption of mordant is 1 ~ 3g/L, and surplus is water;
(2) arrangement of real silk fabric
Real silk fabric is put into dressing liquid process; During process, control ph is 4 ~ 6, and temperature is 60 ~ 80 DEG C, and the time is 50 ~ 80min; After arrangement, real silk fabric cleaned, dry, obtain the real silk fabric with uvioresistant function.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109385885A (en) * | 2018-09-03 | 2019-02-26 | 台华高新染整(嘉兴)有限公司 | The preparation method of nylon fabric with uvioresistant function |
| CN110184810A (en) * | 2019-03-22 | 2019-08-30 | 浙江理工大学 | Preparation method with anti-ultraviolet function fabric |
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- 2015-05-25 CN CN201510268597.2A patent/CN104894862B/en active Active
Patent Citations (5)
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| CN101046067A (en) * | 2007-04-12 | 2007-10-03 | 苏州大学 | Process of dyeing silk with dye yam extract |
| CN102454119A (en) * | 2010-10-18 | 2012-05-16 | 南通曙光染织有限公司 | Extraction of tea-leaf natural dye and dyeing method for silk broadcloth |
| CN102493219A (en) * | 2011-12-01 | 2012-06-13 | 江南大学 | Ecological preparation method of anti-ultraviolet wool and silk textiles based on orange peel |
| CN102587153A (en) * | 2011-12-31 | 2012-07-18 | 浙江工业职业技术学院 | Method for dyeing silk broadcloth by using plant dye solution extracted from lily |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109385885A (en) * | 2018-09-03 | 2019-02-26 | 台华高新染整(嘉兴)有限公司 | The preparation method of nylon fabric with uvioresistant function |
| CN110184810A (en) * | 2019-03-22 | 2019-08-30 | 浙江理工大学 | Preparation method with anti-ultraviolet function fabric |
| CN110184810B (en) * | 2019-03-22 | 2022-02-11 | 浙江理工大学 | Preparation method of fabric with anti-ultraviolet function |
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