CN104894862B - The preparation method of the real silk fabric with anti-ultraviolet function - Google Patents
The preparation method of the real silk fabric with anti-ultraviolet function Download PDFInfo
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- CN104894862B CN104894862B CN201510268597.2A CN201510268597A CN104894862B CN 104894862 B CN104894862 B CN 104894862B CN 201510268597 A CN201510268597 A CN 201510268597A CN 104894862 B CN104894862 B CN 104894862B
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- 239000004744 fabric Substances 0.000 title claims abstract description 86
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 239000000284 extract Substances 0.000 claims abstract description 25
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000007788 liquid Substances 0.000 claims abstract description 16
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims abstract description 15
- 239000010446 mirabilite Substances 0.000 claims abstract description 15
- 238000004043 dyeing Methods 0.000 claims abstract description 8
- 229940037003 alum Drugs 0.000 claims description 7
- 235000003891 ferrous sulphate Nutrition 0.000 claims description 7
- 239000011790 ferrous sulphate Substances 0.000 claims description 7
- BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical compound [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 claims description 7
- 229910000359 iron(II) sulfate Inorganic materials 0.000 claims description 7
- 239000012530 fluid Substances 0.000 claims description 4
- 238000000034 method Methods 0.000 abstract description 6
- 239000004753 textile Substances 0.000 abstract description 4
- 206010020751 Hypersensitivity Diseases 0.000 abstract description 2
- 208000031320 Teratogenesis Diseases 0.000 abstract description 2
- 208000030961 allergic reaction Diseases 0.000 abstract description 2
- 230000000711 cancerogenic effect Effects 0.000 abstract description 2
- 231100000315 carcinogenic Toxicity 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 12
- 229960000583 acetic acid Drugs 0.000 description 6
- 239000012362 glacial acetic acid Substances 0.000 description 6
- 235000008291 Poterium sanguisorba Nutrition 0.000 description 5
- 235000008282 Sanguisorba officinalis Nutrition 0.000 description 5
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 description 3
- 240000004064 Poterium sanguisorba Species 0.000 description 3
- 230000033228 biological regulation Effects 0.000 description 3
- 239000012153 distilled water Substances 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 244000173853 Sanguisorba officinalis Species 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000008280 blood Substances 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 230000006378 damage Effects 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 239000003344 environmental pollutant Substances 0.000 description 2
- 231100000719 pollutant Toxicity 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 244000025254 Cannabis sativa Species 0.000 description 1
- 201000009030 Carcinoma Diseases 0.000 description 1
- 201000004624 Dermatitis Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 244000068988 Glycine max Species 0.000 description 1
- 235000010469 Glycine max Nutrition 0.000 description 1
- 241000581682 Sanguisorba Species 0.000 description 1
- 208000000453 Skin Neoplasms Diseases 0.000 description 1
- 206010053615 Thermal burn Diseases 0.000 description 1
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 description 1
- 206010046788 Uterine haemorrhage Diseases 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 229930003944 flavone Natural products 0.000 description 1
- -1 flavone compound Chemical class 0.000 description 1
- 235000011949 flavones Nutrition 0.000 description 1
- 230000004907 flux Effects 0.000 description 1
- 208000035861 hematochezia Diseases 0.000 description 1
- 230000023597 hemostasis Effects 0.000 description 1
- 210000002429 large intestine Anatomy 0.000 description 1
- 239000012263 liquid product Substances 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 201000000849 skin cancer Diseases 0.000 description 1
- 239000003440 toxic substance Substances 0.000 description 1
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 description 1
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- Coloring (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The present invention relates to functional textile fabric preparation field, it is desirable to provide a kind of preparation method of the real silk fabric with anti-ultraviolet function.The method includes：Radix Sangusorbae extract and mordant, glauber salt, water are mixed and is configured to dressing liquid；Real silk fabric is put into dressing liquid and is processed；Control ph is 4~6 during treatment, and temperature is 60~80 DEG C, and the time is 50~80min；Real silk fabric is cleaned after arrangement, is dried, obtain the real silk fabric with uvioresistant function.The present invention proposes the green new technology for preparing the anti-ultraviolet real silk fabric of energy, makes extract and real silk fabric set, so that real silk fabric has anti-ultraviolet function；Present invention process is simple, can be processed on equipment for dyeing and finishing, improve production efficiency；Fabric can be contacted directly with skin, and security is good, carcinogenic, teratogenesis is not had or is caused allergic reaction；It is good with ecological environment compatibility, it is biodegradable, it is a kind of novel green product, wide market.
Description
Technical field
The present invention relates to functional textile fabric preparation field, more particularly to a kind of silk with anti-ultraviolet function
The preparation method of fabric.
Background technology
In recent years, the use of a large amount of fluorochemicals result in the destruction of ozone layer in atmosphere, this road natural obstacle
Destruction has seriously threatened the health of the mankind.Report display, In The Atmosphere Over China ozone layer reduced 14% between 20 years.Ozone layer subtracts
The quantity that result in the ultraviolet for being irradiated to earth surface less increases, and ultraviolet can cause dermatitis, or even can cause skin
Cancer.Reduction is irradiated to the ultraviolet quantity of human body skin, is the important channel for reducing cutaneum carcinoma.Therefore, with uvioresistant work(
The development tool of energy textile is of great significance.
Garden burnet, also known as garden burnet, it is beautiful prick, beautiful fermented soya beans, salted or other wise or acid it is reddish brown etc., be the plant of rose family burnet.It is mainly distributed on Asia
Continent north temperate zone, be widely distributed in Europe and China, be grown on the area of 30 meters to 3000 meters of height above sea level, be often born in shrubbery, hillside grass
Under ground, grassland, grassy marshland and sparse woods, by artificial introducing and planting.China's main product is in the Northeast, the Inner Mongol, Shanxi, Shaanxi, river
The ground such as south, Gansu, Shandong, Guizhou.Garden burnet bitter, acid, puckery, cold nature, Return liver, large intestine channel；There are cooling blood and hemostasis, removing toxic substances sore etc.
Effect；Be clinically used for treatment have blood in stool, mole blood, bloody flux, uterine bleeding, scald, the illness such as the swollen sore of pain.Existing data shows, city
The Radix Sangusorbae extract sold contains various medicinal chemistry compositions, including flavone compound.
By the use of Radix Sangusorbae extract as the research of anti UV finishing agent, have no and have been reported that.
The content of the invention
The technical problem to be solved in the present invention is to overcome deficiency of the prior art, there is provided one kind has uvioresistant work(
The preparation method of the real silk fabric of energy.
To solve technical problem, the technical solution adopted in the present invention is：
A kind of preparation method of the real silk fabric with uvioresistant function is provided, is comprised the following steps：
(1) arrangement of real silk fabric
(1) arrangement of real silk fabric
It is 1: 30~60 by the bath raio of real silk fabric, Radix Sangusorbae extract, glauber salt and water is mixed and is configured to dressing liquid；It is whole
In reason liquid, the quality of Radix Sangusorbae extract is the 0.5~2% of real silk fabric quality, and the consumption of glauber salt is 10~12g/L, surplus
It is water；
Real silk fabric is put into dressing liquid and is processed, control ph is 4~6 during treatment, temperature is 60~80 DEG C, when
Between be 40~60min；Real silk fabric is cleaned after treatment, is dried；
(2) the rear mordant dyeing treatment of real silk fabric
Mixed with water with alum or ferrous sulfate and be configured to rear mordant dyeing treatment fluid；The consumption of mordant is 1~3g/L, surplus
It is water；
Real silk fabric after arrangement is put into rear mordant dyeing treatment fluid and is processed；Controlled during treatment bath raio for 1: 30~
60, temperature is 60~80 DEG C, and the time is 25~40min；Real silk fabric is cleaned after treatment, is dried, obtained with uvioresistant work(
The real silk fabric of energy.
Present invention also offers the preparation method of real silk fabric of the another kind with uvioresistant function, comprise the following steps：
(1) preparation of dressing liquid
It is 1: 30~60 by the bath raio of real silk fabric, Radix Sangusorbae extract and mordant, glauber salt, water mixing is configured to whole
Reason liquid；The quality of Radix Sangusorbae extract is the 0.5~2% of real silk fabric quality in dressing liquid, and the consumption of glauber salt is 10~12g/
L, mordant is alum or ferrous sulfate, and the consumption of mordant is 1~3g/L, balance of water；
(2) arrangement of real silk fabric
Real silk fabric is put into dressing liquid and is processed；Control ph is 4~6 during treatment, and temperature is 60~80 DEG C, when
Between be 50~80min；Real silk fabric is cleaned after arrangement, is dried, obtain the real silk fabric with uvioresistant function.
Above-mentioned Radix Sangusorbae extract is the extract of Chinese medicine Radix Sangusorbae, is commercially available prod.
Compared with prior art, the beneficial effects of the invention are as follows：
(1) present invention proposes a kind of green new technology for preparing the anti-ultraviolet real silk fabric of energy, i.e., using Chinese medicine ground
The extract of elm processes real silk fabric in the method that high temperature impregnates, and makes extract and real silk fabric set, so that real silk fabric
With anti-ultraviolet function；
(2) present invention process is simple, can be processed on equipment for dyeing and finishing, improve production efficiency；
(3) fabric obtained using preparation method of the present invention can be contacted directly with skin, and security is good, do not have it is carcinogenic,
Teratogenesis causes allergic reaction；It is good with ecological environment compatibility, it is biodegradable, it is a kind of novel green product, its city
Field prospect is very wide, can be used for the fields such as garment material, home textile.
Brief description of the drawings
Fig. 1 is absorption spectrogram of the garden burnet extract solution used by the present invention between 200~400nm ultraviolet regions.
Specific embodiment
With reference to specific implementation example, implementation process of the invention is described in detail.
The definition of bath raio：The ratio between dye liquor volume (L) and pollutant quality (kg).Such as pollutant 50kg, bath raio 20:1, then contaminate
Liquid product is 1000L.Bath raio can be written generally as 1 in industry:20.
Embodiment 1：
(1) 0.05g Radix Sangusorbae extracts are added in 300ml water, add 3g glauber salt, and add glacial acetic acid to adjust pH value
It is 4；By 10g real silk fabrics add the above solution in, temperature be 60 DEG C, bath raio be 1:50min is processed under conditions of 30；So
Real silk fabric is taken out and cleaned afterwards, is dried；
(2) 300ml distilled water is measured, 0.3g ferrous sulfate is added；To be cleaned in step (1), the real silk fabric of drying adds
Enter in solution derived above, be 60 DEG C in temperature, bath raio is 1:30min is processed under conditions of 30；Then real silk fabric is taken
Go out and clean, dry, obtain the real silk fabric with anti-ultraviolet function.After tested, the UPF values of the real silk fabric are：
50.29。
Embodiment 2：
(1) 0.12g Radix Sangusorbae extracts are added in 450ml water, add 4.95g glauber salt, and add glacial acetic acid to adjust
PH value is 5；By 10g real silk fabrics add the above solution in, temperature be 80 DEG C, bath raio be 1:Processed under conditions of 45
40min；Then real silk fabric taken out and is cleaned, dried；
(2) 450ml distilled water is measured, 1.35g alum is added；Will in step (1) clean, drying real silk fabric add with
On in the solution that obtains, be 80 DEG C in temperature, bath raio is 1:25min is processed under conditions of 45；Then real silk fabric is taken out simultaneously
Clean, dry, obtain the real silk fabric with anti-ultraviolet function.After tested, the UPF values of the real silk fabric are：82.41.
Embodiment 3：
(1) 0.2g Radix Sangusorbae extracts are added in 600ml water, are added and 7.2g glauber salt, add glacial acetic acid regulation pH
Be worth is 6；By 10g real silk fabrics add the above solution in, temperature be 70 DEG C, bath raio be 1:60min is processed under conditions of 60；
Then real silk fabric taken out and is cleaned, dried；
(2) 600ml distilled water is measured, 1.2g ferrous sulfate is added；To be cleaned in step (1), the real silk fabric of drying adds
Enter in mixed liquor derived above, be 70 DEG C in temperature, bath raio is 1:40min is processed under conditions of 60；Then by real silk fabric
Take out and clean, dry, obtain the real silk fabric with anti-ultraviolet function.After tested, the UPF values of the real silk fabric are：
115.92。
Embodiment 4：
(1) 0.075g Radix Sangusorbae extracts are added in 300ml water, add 3g glauber salt, add 0.3g alum；And add
Glacial acetic acid regulation pH value is 5；
(2) 10g real silk fabrics are added in the solution of the above, is 60 DEG C in temperature, bath raio is 1:Processed under conditions of 30
50min；Then real silk fabric taken out and is cleaned, dried, obtain the real silk fabric with anti-ultraviolet function.After tested, should
The UPF values of real silk fabric are：66.18.
Embodiment 5：
(1) 0.2g Radix Sangusorbae extracts are added in 600ml water, add 6.6g glauber salt, add 1.2g alum；And add
Glacial acetic acid regulation pH value is 4；
(2) 10g real silk fabrics are added in the solution of the above, is 80 DEG C in temperature, bath raio is 1:Processed under conditions of 60
60min；Then real silk fabric taken out and is cleaned, dried, obtain the real silk fabric with anti-ultraviolet function.After tested, should
The UPF values of real silk fabric are：50.03.
Embodiment 6：
(1) 0.17g Radix Sangusorbae extracts are added in 450ml water, add 5.4g glauber salt, add 1.35g ferrous sulfate；
And it is 6 to add glacial acetic acid to adjust pH value；
(2) 10g real silk fabrics are added in the solution of the above, is 70 DEG C in temperature, bath raio is 1:Processed under conditions of 45
80min；Then real silk fabric taken out and is cleaned, dried, obtain the real silk fabric with anti-ultraviolet function.After tested, should
The UPF values of real silk fabric are：78.04.
As seen from Figure 1, Radix Sangusorbae extract is dark brown, and its maximum absorption wavelength is in 272nm.
Additionally, uvioresistant finishing agent of the garden burnet extract solution as real silk fabric, the real silk fabric after treatment has excellent
Anti-ultraviolet property.
Claims (2)
1. a kind of preparation method of the real silk fabric with uvioresistant function, it is characterised in that comprise the following steps：
(1) arrangement of real silk fabric
It is 1: 30~60 by the bath raio of real silk fabric, Radix Sangusorbae extract, glauber salt and water is mixed and is configured to dressing liquid；Dressing liquid
In, the quality of Radix Sangusorbae extract is the 0.5~2% of real silk fabric quality, and the consumption of glauber salt is 10~12g/L, balance of water；
Real silk fabric is put into dressing liquid and is processed, control ph is 4~6 during treatment, and temperature is 60~80 DEG C, and the time is
40~60min；Real silk fabric is cleaned after treatment, is dried；
(2) the rear mordant dyeing treatment of real silk fabric
Mixed with water with alum or ferrous sulfate and be configured to rear mordant dyeing treatment fluid；The consumption of mordant is 1~3g/L, balance of
Water；
Real silk fabric after arrangement is put into rear mordant dyeing treatment fluid and is processed；It is 1: 30~60 that bath raio is controlled during treatment, temperature
It is 60~80 DEG C to spend, and the time is 25~40min；Real silk fabric is cleaned after treatment, is dried, obtained with the true of uvioresistant function
Silk fabrics.
2. a kind of preparation method of the real silk fabric with uvioresistant function, it is characterised in that comprise the following steps：
(1) preparation of dressing liquid
It is 1: 30~60 by the bath raio of real silk fabric, Radix Sangusorbae extract and mordant, glauber salt, water is mixed and is configured to arrange
Liquid；The quality of Radix Sangusorbae extract is the 0.5~2% of real silk fabric quality in dressing liquid, and the consumption of glauber salt is 10~12g/L,
Mordant is alum or ferrous sulfate, and the consumption of mordant is 1~3g/L, balance of water；
(2) arrangement of real silk fabric
Real silk fabric is put into dressing liquid and is processed；Control ph is 4~6 during treatment, and temperature is 60~80 DEG C, and the time is
50~80min；Real silk fabric is cleaned after arrangement, is dried, obtain the real silk fabric with uvioresistant function.
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| CN201510268597.2A CN104894862B (en) | 2015-05-25 | 2015-05-25 | The preparation method of the real silk fabric with anti-ultraviolet function |
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| CN104894862B true CN104894862B (en) | 2017-05-31 |
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| CN109385885A (en) * | 2018-09-03 | 2019-02-26 | 台华高新染整(嘉兴)有限公司 | The preparation method of nylon fabric with uvioresistant function |
| CN110184810B (en) * | 2019-03-22 | 2022-02-11 | 浙江理工大学 | Preparation method of fabric with anti-ultraviolet function |
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| CN100540799C (en) * | 2007-04-12 | 2009-09-16 | 苏州大学 | The dye yam extract is to the colouring method of silk broadcloth |
| CN102454119A (en) * | 2010-10-18 | 2012-05-16 | 南通曙光染织有限公司 | Extraction of tea-leaf natural dye and dyeing method for silk broadcloth |
| CN102493219A (en) * | 2011-12-01 | 2012-06-13 | 江南大学 | Ecological preparation method of anti-ultraviolet wool and silk textiles based on orange peel |
| CN102587153A (en) * | 2011-12-31 | 2012-07-18 | 浙江工业职业技术学院 | Method for dyeing silk broadcloth by using plant dye solution extracted from lily |
| CN102634994A (en) * | 2012-03-29 | 2012-08-15 | 江南大学 | Ecological preparation method for anti-ultraviolet wool and silk textile based on granatum |
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