CN110101632A - A kind of plant source repairs facial mask liquid and preparation method thereof - Google Patents

A kind of plant source repairs facial mask liquid and preparation method thereof Download PDF

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Publication number
CN110101632A
CN110101632A CN201910386022.9A CN201910386022A CN110101632A CN 110101632 A CN110101632 A CN 110101632A CN 201910386022 A CN201910386022 A CN 201910386022A CN 110101632 A CN110101632 A CN 110101632A
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parts
facial mask
extract
mask liquid
plant source
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何敬忠
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Guangzhou Yanshan Cosmetics Co Ltd
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Guangzhou Yanshan Cosmetics Co Ltd
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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    • A61K8/345—Alcohols containing more than one hydroxy group
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
    • A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
    • A61K8/496—Triazoles or their condensed derivatives, e.g. benzotriazoles
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
    • A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9706—Algae
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9789—Magnoliopsida [dicotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9794—Liliopsida [monocotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/08—Anti-ageing preparations
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95

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  • Oil, Petroleum & Natural Gas (AREA)
  • Cosmetics (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention proposes a kind of plant sources to repair facial mask liquid, is prepared by weight by following raw material: 5-12 parts of Euglena, extract 2-5 parts of Chinese medicine reparation, 0.5-1 parts of cedar oil, 0.1-0.3 parts of allantoin, 0.01-0.05 parts of castor oil, 1-3 parts of tea polyphenols, 0.1-0.3 parts of benzotriazole, 0.5-1.5 parts of EDETATE SODIUM, 2-4 parts of butanediol, 3-5 parts of glycerol, 1-3 parts of polyethylene wax and 150-200 parts of water.Preparation method of the present invention is simple; Chinese medicine is obtained by extraction using supercritical extraction technique and repairs extract bioactivity with higher; have the effect of for the reparations such as skin antiallergic, anti-inflammatory, anti-oxidant fabulous; added ingredient natural no stimulation; help that skin barrier is protected not to be destroyed; preservative free addition and long shelf-life, have extraordinary development prospect.

Description

A kind of plant source repairs facial mask liquid and preparation method thereof
Technical field
The present invention relates to cosmetic technical fields, and in particular to a kind of plant source Face-protecting mask liquid and preparation method thereof.
Background technique
Cosmetics long history, just about change in classical TCM masterpiece the Classic of Mountains and Rivers Shennong's Herbal Compendium of Material Medica The record of cosmetic.Facial mask is as common State of cosmetics, and easy to carry, small to skin side-effects and easy-to-use, curative effect is aobvious It writes, market prospects are become better and better, increasing in cosmetic field portion.Wherein, effect facial mask has damage capacitive skin Significant curative effect, and have maintenance type, maintenance type, grow the types such as shield type, whitening type, desalination spot type, anti-aging smooth out wrinkles type, Facial mask has comparable research and development temperature in cosmetics research field.
Although there are still very big defects, in violation of rules and regulations currently, the management of China's cosmetics and technology are continuous perfect The phenomenon that addition, is very serious, causes many beauty accidents for many years, very big injury is caused to consumer, has caused state The great attention of family and consumer.The logical maintenance product of surface current all has preservative and chemical odor type, day currently on the market The substance of right plant extraction is pollution-free, no hormone, noresidue, and has the characteristics such as vdiverse in function, widely applicable, safe, because And by attention increasingly.Exploitation has good safety, stability, the no added anti-corrosion that effect is obvious, cost performance is good and perfume (or spice) The cosmetics of the natural plant Face-protecting mask of type have extraordinary development prospect.
Summary of the invention
In order to solve the above technical problems, the present invention provides a kind of plant source Face-protecting mask liquid and preparation method thereof, Purpose is, provides a kind of plant source Face-protecting mask liquid, and Chinese medicine reparation is obtained by extraction by using supercritical extraction technique and extracts Object extracts its nutriment by supercritical extraction technique, is a kind of low-temperature extraction technology, avoids the broken words nutrition of high temperature Ingredient is to reduce its activity, to improve yield, obtains the higher nutritional ingredient of activity；Solvent can be recycled simultaneously, Reduce cost.
The present invention provides a kind of plant source reparation facial mask liquid, is prepared from the following materials: Euglena, Chinese medicine reparation are extracted Object, cedar oil, allantoin, castor oil, tea polyphenols, benzotriazole, EDETATE SODIUM, butanediol, glycerol, polyethylene wax and water.
As further improvement of the invention, it is prepared by weight by following raw material: 5-12 parts of Euglena, Chinese medicine reparation 2-5 parts of extract, 0.5-1 parts of cedar oil, 0.1-0.3 parts of allantoin, 0.01-0.05 parts of castor oil, 1-3 parts of tea polyphenols, benzo 0.1-0.3 parts of triazole, 0.5-1.5 parts of EDETATE SODIUM, 2-4 parts of butanediol, 3-5 parts of glycerol, 1-3 parts of polyethylene wax and water 150- 200 parts.
As further improvement of the invention, it is prepared by weight by following raw material: 7-10 parts of Euglena, Chinese medicine reparation 3-5 parts of extract, 0.6-0.8 parts of cedar oil, 0.1-0.2 parts of allantoin, 0.02-0.04 parts of castor oil, 1-2 parts of tea polyphenols, benzene And 0.1-0.2 parts of triazole, 0.7-1.2 parts of EDETATE SODIUM, 3-4 parts of butanediol, 3-4 parts of glycerol, 1-2 parts of polyethylene wax and water 170- 180 parts.
As further improvement of the invention, be prepared by weight by following raw material: 8 parts of Euglena, Chinese medicine reparation are mentioned Take 4 parts of object, 0.7 part of cedar oil, 0.15 part of allantoin, 0.03 part of castor oil, 1.5 parts of tea polyphenols, 0.12 part of benzotriazole, EDTA 0.9 part of disodium, 3.5 parts of butanediol, 3.7 parts of glycerol, 1.2 parts of polyethylene wax and 175 parts of water.
As further improvement of the invention, the Chinese medicine is repaired extract and is prepared by weight by following raw material: 5-10 parts of centella, 5-10 parts of the rhizome of nutgrass flatsedge, 10-15 parts of perfume thatch, 2-5 parts of wild cabbage, 1-3 parts of henbane seed, 5-10 parts of corn poppy, hole 10-15 parts and oenothera biennis 5-15 parts of sparrow grass.
As further improvement of the invention, the Chinese medicine is repaired extract and is prepared by following methods:
S1. the processing of raw material: weighing each raw material in proportion, cleans, and drying is crushed to 100 mesh hereinafter, spare；
S2. supercritical fluid extraction: supercritical fluid extraction tank is added in powder obtained in step S1, solvent is added CO2, preheat, after mixing evenly, carry out decompression and temperature adjustment operation, the solvent dissolved with extract is brought down below CO2Critical pressure Hereinafter, due to CO2Solubility extremely declines, through separator extract and CO2And extraction each component is separated, into extraction Tank obtains required Chinese medicine and repairs extract, while CO2It is recycled with circulating pump.
As further improvement of the invention, drying temperature described in step S1 is 40 DEG C, drying time 5-7h.
As further improvement of the invention, pressure is brought down below 7MPa, the tune in reduced pressure operation described in step S2 Temperature is adjusted to 30 DEG C or so in temperature operation.
The present invention further protects a kind of method for preparing above-mentioned plant source and repairing facial mask liquid, prepares in accordance with the following methods:
S1. the processing of Euglena: crushing after Euglena is dried and obtain Euglena powder, after the deionized water of 5 times of weight is added, boiling water 5-15min is extracted, is filtered, reject filter residue, dehydrated alcohol is added in filtrate, is precipitated, is filtered, solid is continued to employ；
S2. plant source repairs the preparation of facial mask liquid: by cedar oil, allantoin, castor oil, tea polyphenols, polyethylene wax and step The mixing of solid made from rapid S1, is added water, is heated to 60 DEG C and stirs evenly, be cooled to room temperature be added Chinese medicine repair extract, EDETATE SODIUM, butanediol and glycerol, stir evenly, packaging, and plant source is made and repairs facial mask liquid.
As further improvement of the invention, the speed of agitator is 500-700r/min.
The allantoin added the invention has the following beneficial effects: the present invention is natural maintenance ingredient, can promote cell Activated growth, mitigation and softening skin；Cedar oil has fabulous disinfection, anti-corrosion and has calm effect to skin, to skin It is non-stimulated；Castor oil is a kind of naturally occurring emulsifying agent, non-stimulated to skin for the emulsification of facial mask liquid；Tea polyphenols be it is a kind of efficiently, Natural inhibitor, reduced form nutritional ingredient in effective protection facial mask liquid；Euglena is rich in polysaccharose substance, has natural moisture preserving, resists The good skin holding effect such as quick, anti-inflammatory；
The Chinese medicine that the present invention adds repairs the traditional Chinese medicine ingredients used in extract and is rich in reparation skin-nourishing substance abundant, Basal layer cell vigor is activated, improves skin problem from the root, promotes the absorption of subsequent skin care products, it is multiple also to possess whitening etc. Effect, and it is safe and efficient, rich in effective plant components such as plant flavone, plant polyphenols, more carry out 3 balanced actions again to skin tape: Nutrient balance, pH value balance and metabolic balance, construct the health of skin；
The present invention is obtained by extraction Chinese medicine using supercritical extraction technique and repairs extract, by supercritical extraction technique to it Nutriment is extracted, and is a kind of low-temperature extraction technology, avoids the broken words nutritional ingredient of high temperature to reduce its activity, to mention High yield obtains the higher nutritional ingredient of activity；Solvent can be recycled simultaneously, reduce cost；
Preparation method of the present invention is simple, and it is with higher that Chinese medicine reparation extract is obtained by extraction using supercritical extraction technique Bioactivity has the effect of the reparations such as skin antiallergic, anti-inflammatory, anti-oxidant fabulous, added ingredient natural no stimulation, Help that skin barrier is protected not to be destroyed, preservative free addition and long shelf-life have extraordinary development prospect.
Specific embodiment
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the invention is clearly and completely described, Obviously, the embodiment described is the embodiment of part of representative of the invention, rather than whole embodiments, this field are general Other all embodiments obtained belong to protection of the invention to logical technical staff without making creative work Range.
Embodiment 1
Raw material forms (parts by weight): 5 parts of Euglena, Chinese medicine repair 2 parts of extract, 0.5 part of cedar oil, 0.1 part of allantoin, castor 0.01 part of sesame oil, 1 part of tea polyphenols, 0.1 part of benzotriazole, 0.5 part of EDETATE SODIUM, 2 parts of butanediol, 3 parts of glycerol, polyethylene wax 1 Part and 150 parts of water.
Chinese medicine is repaired extract and is prepared by weight by following raw material: 5 parts of centella, 5 parts of the rhizome of nutgrass flatsedge, perfume thatch 10 Part, 2 parts of wild cabbage, 1 part of henbane seed, 5 parts of corn poppy, 10 parts of maidenhair and 5 parts of oenothera biennis.
Chinese medicine is repaired extract and is prepared by following methods:
S1. the processing of raw material: weighing each raw material in proportion, cleans, drying, and drying temperature is 40 DEG C, drying time 5h, 100 mesh are crushed to hereinafter, spare；
S2. supercritical fluid extraction: supercritical fluid extraction tank is added in powder obtained in step S1, solvent is added CO2, preheat, after mixing evenly, be depressured, pressure is brought down below 7MPa, temperature adjustment, and temperature is adjusted to 30 DEG C or so, dissolved with extraction The solvent of object is taken to be brought down below CO2Critical pressure hereinafter, due to CO2Solubility extremely declines, through separator extract and CO2And extraction each component is separated, and into extractor, is obtained required Chinese medicine and is repaired extract, while CO2With circulating pump into Row is recycled.
A method of it preparing above-mentioned plant source and repairs facial mask liquid, prepare in accordance with the following methods:
S1. the processing of Euglena: crushing after Euglena is dried and obtain Euglena powder, after the deionized water of 5 times of weight is added, boiling water 5min is extracted, is filtered, reject filter residue, dehydrated alcohol is added in filtrate, is precipitated, is filtered, solid is continued to employ；
S2. plant source repairs the preparation of facial mask liquid: by cedar oil, allantoin, castor oil, tea polyphenols, polyethylene wax and step Solid mixing, is added water, is heated to 60 DEG C and stirs evenly, revolving speed 500r/min is cooled to room temperature in addition made from rapid S1 Medicine is repaired extract, EDETATE SODIUM, butanediol and glycerol, former speed and is stirred evenly, and packs, and plant source is made and repairs facial mask liquid.
Embodiment 2
Raw material forms (parts by weight): 12 parts of Euglena, Chinese medicine repair 5 parts of extract, 1 part of cedar oil, 0.3 part of allantoin, castor 0.05 part of sesame oil, 3 parts of tea polyphenols, 0.3 part of benzotriazole, 1.5 parts of EDETATE SODIUM, 4 parts of butanediol, 5 parts of glycerol, polyethylene wax 3 Part and 200 parts of water.
Chinese medicine is repaired extract and is prepared by weight by following raw material: 10 parts of centella, 10 parts of the rhizome of nutgrass flatsedge, perfume thatch 15 parts, 5 parts of wild cabbage, 3 parts of henbane seed, 10 parts of corn poppy, 15 parts of maidenhair and 15 parts of oenothera biennis.
Chinese medicine is repaired extract and is prepared by following methods:
S1. the processing of raw material: weighing each raw material in proportion, cleans, drying, and drying temperature is 40 DEG C, drying time 7h, 100 mesh are crushed to hereinafter, spare；
S2. supercritical fluid extraction: supercritical fluid extraction tank is added in powder obtained in step S1, solvent is added CO2, preheat, after mixing evenly, be depressured, pressure is brought down below 7MPa, temperature adjustment, and temperature is adjusted to 30 DEG C or so, dissolved with extraction The solvent of object is taken to be brought down below CO2Critical pressure hereinafter, due to CO2Solubility extremely declines, through separator extract and CO2And extraction each component is separated, and into extractor, is obtained required Chinese medicine and is repaired extract, while CO2With circulating pump into Row is recycled.
A method of it preparing above-mentioned plant source and repairs facial mask liquid, prepare in accordance with the following methods:
S1. the processing of Euglena: crushing after Euglena is dried and obtain Euglena powder, after the deionized water of 5 times of weight is added, boiling water 15min is extracted, is filtered, reject filter residue, dehydrated alcohol is added in filtrate, is precipitated, is filtered, solid is continued to employ；
S2. plant source repairs the preparation of facial mask liquid: by cedar oil, allantoin, castor oil, tea polyphenols, polyethylene wax and step Solid mixing, is added water, is heated to 60 DEG C and stirs evenly, revolving speed 700r/min is cooled to room temperature in addition made from rapid S1 Medicine is repaired extract, EDETATE SODIUM, butanediol and glycerol, former speed and is stirred evenly, and packs, and plant source is made and repairs facial mask liquid.
Embodiment 3
Raw material forms (parts by weight): 7 parts of Euglena, Chinese medicine repair 3 parts of extract, 0.6 part of cedar oil, 0.1 part of allantoin, castor 0.02 part of sesame oil, 1 part of tea polyphenols, 0.1 part of benzotriazole, 0.7 part of EDETATE SODIUM, 3 parts of butanediol, 3 parts of glycerol, polyethylene wax 1 Part and 170 parts of water.
Chinese medicine is repaired extract and is prepared by weight by following raw material: 6 parts of centella, 6 parts of the rhizome of nutgrass flatsedge, perfume thatch 11 Part, 3 parts of wild cabbage, 2 parts of henbane seed, 6 parts of corn poppy, 11 parts of maidenhair and 7 parts of oenothera biennis.
Chinese medicine is repaired extract and is prepared by following methods:
S1. the processing of raw material: weighing each raw material in proportion, cleans, drying, and drying temperature is 40 DEG C, drying time 6h, 100 mesh are crushed to hereinafter, spare；
S2. supercritical fluid extraction: supercritical fluid extraction tank is added in powder obtained in step S1, solvent is added CO2, preheat, after mixing evenly, be depressured, pressure is brought down below 7MPa, temperature adjustment, and temperature is adjusted to 30 DEG C or so, dissolved with extraction The solvent of object is taken to be brought down below CO2Critical pressure hereinafter, due to CO2Solubility extremely declines, through separator extract and CO2And extraction each component is separated, and into extractor, is obtained required Chinese medicine and is repaired extract, while CO2With circulating pump into Row is recycled.
A method of it preparing above-mentioned plant source and repairs facial mask liquid, prepare in accordance with the following methods:
S1. the processing of Euglena: crushing after Euglena is dried and obtain Euglena powder, after the deionized water of 5 times of weight is added, boiling water 7min is extracted, is filtered, reject filter residue, dehydrated alcohol is added in filtrate, is precipitated, is filtered, solid is continued to employ；
S2. plant source repairs the preparation of facial mask liquid: by cedar oil, allantoin, castor oil, tea polyphenols, polyethylene wax and step Solid mixing, is added water, is heated to 60 DEG C and stirs evenly, revolving speed 550r/min is cooled to room temperature in addition made from rapid S1 Medicine is repaired extract, EDETATE SODIUM, butanediol and glycerol, former speed and is stirred evenly, and packs, and plant source is made and repairs facial mask liquid.
Embodiment 4
Raw material form (parts by weight): 10 parts of Euglena, Chinese medicine repair 5 parts of extract, 0.8 part of cedar oil, 0.2 part of allantoin, 0.04 part of castor oil, 2 parts of tea polyphenols, 0.2 part of benzotriazole, 1.2 parts of EDETATE SODIUM, 4 parts of butanediol, 4 parts of glycerol, polyethylene wax 2 parts and 180 parts of water.
Chinese medicine is repaired extract and is prepared by weight by following raw material: 9 parts of centella, 9 parts of the rhizome of nutgrass flatsedge, perfume thatch 14 Part, 4 parts of wild cabbage, 2 parts of henbane seed, 9 parts of corn poppy, 14 parts of maidenhair and 12 parts of oenothera biennis.
Chinese medicine is repaired extract and is prepared by following methods:
S1. the processing of raw material: weighing each raw material in proportion, cleans, drying, and drying temperature is 40 DEG C, drying time 6h, 100 mesh are crushed to hereinafter, spare；
S2. supercritical fluid extraction: supercritical fluid extraction tank is added in powder obtained in step S1, solvent is added CO2, preheat, after mixing evenly, be depressured, pressure is brought down below 7MPa, temperature adjustment, and temperature is adjusted to 30 DEG C or so, dissolved with extraction The solvent of object is taken to be brought down below CO2Critical pressure hereinafter, due to CO2Solubility extremely declines, through separator extract and CO2And extraction each component is separated, and into extractor, is obtained required Chinese medicine and is repaired extract, while CO2With circulating pump into Row is recycled.
A method of it preparing above-mentioned plant source and repairs facial mask liquid, prepare in accordance with the following methods:
S1. the processing of Euglena: crushing after Euglena is dried and obtain Euglena powder, after the deionized water of 5 times of weight is added, boiling water 12min is extracted, is filtered, reject filter residue, dehydrated alcohol is added in filtrate, is precipitated, is filtered, solid is continued to employ；
S2. plant source repairs the preparation of facial mask liquid: by cedar oil, allantoin, castor oil, tea polyphenols, polyethylene wax and step Solid mixing, is added water, is heated to 60 DEG C and stirs evenly, revolving speed 650r/min is cooled to room temperature in addition made from rapid S1 Medicine is repaired extract, EDETATE SODIUM, butanediol and glycerol, former speed and is stirred evenly, and packs, and plant source is made and repairs facial mask liquid.
Embodiment 5
Raw material form (parts by weight): 8 parts of Euglena, Chinese medicine repair 4 parts of extract, 0.7 part of cedar oil, 0.15 part of allantoin, 0.03 part of castor oil, 1.5 parts of tea polyphenols, 0.12 part of benzotriazole, 0.9 part of EDETATE SODIUM, 3.5 parts of butanediol, 3.7 parts of glycerol, 1.2 parts and 175 parts of water of polyethylene wax.
Chinese medicine is repaired extract and is prepared by weight by following raw material: 7 parts of centella, 7 parts of the rhizome of nutgrass flatsedge, perfume thatch 12 Part, 3 parts of wild cabbage, 2 parts of henbane seed, 7 parts of corn poppy, 12 parts of maidenhair and 10 parts of oenothera biennis.
Chinese medicine is repaired extract and is prepared by following methods:
S1. the processing of raw material: weighing each raw material in proportion, cleans, drying, and drying temperature is 40 DEG C, drying time 6h, 100 mesh are crushed to hereinafter, spare；
S2. supercritical fluid extraction: supercritical fluid extraction tank is added in powder obtained in step S1, solvent is added CO2, preheat, after mixing evenly, be depressured, pressure is brought down below 7MPa, temperature adjustment, and temperature is adjusted to 30 DEG C or so, dissolved with extraction The solvent of object is taken to be brought down below CO2Critical pressure hereinafter, due to CO2Solubility extremely declines, through separator extract and CO2And extraction each component is separated, and into extractor, is obtained required Chinese medicine and is repaired extract, while CO2With circulating pump into Row is recycled.
A method of it preparing above-mentioned plant source and repairs facial mask liquid, prepare in accordance with the following methods:
S1. the processing of Euglena: crushing after Euglena is dried and obtain Euglena powder, after the deionized water of 5 times of weight is added, boiling water 10min is extracted, is filtered, reject filter residue, dehydrated alcohol is added in filtrate, is precipitated, is filtered, solid is continued to employ；
S2. plant source repairs the preparation of facial mask liquid: by cedar oil, allantoin, castor oil, tea polyphenols, polyethylene wax and step Solid mixing, is added water, is heated to 60 DEG C and stirs evenly, revolving speed 600r/min is cooled to room temperature in addition made from rapid S1 Medicine is repaired extract, EDETATE SODIUM, butanediol and glycerol, former speed and is stirred evenly, and packs, and plant source is made and repairs facial mask liquid.
1 human skin patch of test example
1. tested material: plant source prepared by embodiment 5 repairs facial mask liquid
2. negative control: deionized water
3. subject: totally 30 people, male 0 people, 30 people of female the age 21-48 years old, meet subject and volunteer inclusion criteria.
4. patch method: selecting qualified spot tester, with enclosed patch test method, about by tested material and negative control 0.020mL-0.025mL (semifluid) is dripped in spot tester, and external application special adhesive tape is pasted on subject back, removes after 24 hours Tested material, observation dermoreaction in 0.5,24,48 hour after removing respectively, by skin in " cosmetics health specification " (version in 2007) Reaction grade scale records its result.Test result is shown in Table 1:
1 human skin patch test result of table
Human skin patch test result is shown: 0 there is skin adverse reaction in 30 people；Illustrate plant source of the invention Reparation facial mask liquid uses safe.
Test case 2
Choose 200 female volunteers between 45-55 years old；This product (plant source being prepared with embodiment 5 on probation Repair facial mask liquid).Volunteer uses this product, test effect in left hand skin of arm, and right hand skin of arm does not use any product To compare (skin at the arm of volunteer lacks flexibility and the aging phenomena such as smooth delicacy).
Application method are as follows:
The plant source that embodiment 5 is prepared repairs facial mask liquid and commercial like product is diluted with water purification, ratio 1:40, First stoste is shaken up before dilution, is then charged into spray bottle.Spray bottle pump head is pressed lightly on apart from skin 30CM or so, sprays skin, It is 3-7 times daily.Effect is as shown in table 2.
2 product measure of merit tables of data of table
The judgment criteria of " effective " in table 2 are as follows: whether the skin of the skin of this product on probation this product more not on probation is obvious More flexible and more smooth delicacy.
From Table 2, it can be seen that plant source reparation facial mask liquid effective percentage has reached 94% after continuous use this product 30 days, It is substantially better than commercial product.Illustrate that the product that the present invention is prepared has good delay skin aging, restores skin elasticity And smooth delicacy.
Using the obtained plant source of embodiment 1-4 repair facial mask liquid carry out according to the above method human skin patch and Effect test obtains the test result similar with above-mentioned test result.
Compared with prior art, the allantoin that the present invention adds is natural maintenance ingredient, cell activation can be promoted to grow, It mitigates and softening skin；Cedar oil has fabulous disinfection, anti-corrosion and has calm effect to skin, non-stimulated to skin；Castor Sesame oil is a kind of naturally occurring emulsifying agent, non-stimulated to skin for the emulsification of facial mask liquid；Tea polyphenols are a kind of efficient, natural antioxygens Agent, reduced form nutritional ingredient in effective protection facial mask liquid；Euglena is rich in polysaccharose substance, has natural moisture preserving, antiallergic, anti-inflammatory etc. Good skin holding effect；
The Chinese medicine that the present invention adds repairs the traditional Chinese medicine ingredients used in extract and is rich in reparation skin-nourishing substance abundant, Basal layer cell vigor is activated, improves skin problem from the root, promotes the absorption of subsequent skin care products, it is multiple also to possess whitening etc. Effect, and it is safe and efficient, rich in effective plant components such as plant flavone, plant polyphenols, more carry out 3 balanced actions again to skin tape: Nutrient balance, pH value balance and metabolic balance, construct the health of skin；
The present invention is obtained by extraction Chinese medicine using supercritical extraction technique and repairs extract, by supercritical extraction technique to it Nutriment is extracted, and is a kind of low-temperature extraction technology, avoids the broken words nutritional ingredient of high temperature to reduce its activity, to mention High yield obtains the higher nutritional ingredient of activity；Solvent can be recycled simultaneously, reduce cost；
Preparation method of the present invention is simple, and it is with higher that Chinese medicine reparation extract is obtained by extraction using supercritical extraction technique Bioactivity has the effect of the reparations such as skin antiallergic, anti-inflammatory, anti-oxidant fabulous, added ingredient natural no stimulation, Help that skin barrier is protected not to be destroyed, preservative free addition and long shelf-life have extraordinary development prospect.
Those skilled in the art is not under conditions of departing from the spirit and scope of the present invention that claims determine, also Various modifications can be carried out to the above content.Therefore the scope of the present invention is not limited in above explanation, but by The range of claims determines.

Claims (10)

1. a kind of plant source repairs facial mask liquid, which is characterized in that be prepared from the following materials: Euglena, Chinese medicine repair extract, Cedar oil, allantoin, castor oil, tea polyphenols, benzotriazole, EDETATE SODIUM, butanediol, glycerol, polyethylene wax and water.
2. a kind of plant source repairs facial mask liquid according to claim 1, which is characterized in that prepared by weight by following raw material Form: 5-12 parts of Euglena, Chinese medicine repair extract 2-5 parts, 0.5-1 parts of cedar oil, 0.1-0.3 parts of allantoin, castor oil 0.01- 0.05 part, 1-3 parts of tea polyphenols, 0.1-0.3 parts of benzotriazole, 0.5-1.5 parts of EDETATE SODIUM, 2-4 parts of butanediol, 3-5 parts of glycerol, 1-3 parts and water 150-200 parts of polyethylene wax.
3. a kind of plant source repairs facial mask liquid according to claim 2, which is characterized in that prepared by weight by following raw material Form: 7-10 parts of Euglena, Chinese medicine repair extract 3-5 parts, 0.6-0.8 parts of cedar oil, 0.1-0.2 parts of allantoin, castor oil 0.02-0.04 parts, 1-2 parts of tea polyphenols, 0.1-0.2 parts of benzotriazole, 0.7-1.2 parts of EDETATE SODIUM, 3-4 parts of butanediol, glycerol 3-4 parts, 1-2 parts of polyethylene wax and 170-180 parts of water.
4. a kind of plant source repairs facial mask liquid according to claim 3, which is characterized in that prepared by weight by following raw material Form: 8 parts of Euglena, Chinese medicine repair 4 parts of extract, 0.7 part of cedar oil, 0.15 part of allantoin, 0.03 part of castor oil, tea polyphenols 1.5 parts, 0.12 part of benzotriazole, 0.9 part of EDETATE SODIUM, 3.5 parts of butanediol, 3.7 parts of glycerol, 1.2 parts of polyethylene wax and water 175 Part.
5. a kind of plant source repairs facial mask liquid according to claim 1, which is characterized in that the Chinese medicine repair extract by with Lower raw material is prepared by weight: 5-10 parts of centella, 5-10 parts of the rhizome of nutgrass flatsedge, 10-15 parts of perfume thatch, 2-5 parts of wild cabbage, beauty 1-3 parts sub-, 5-10 parts of corn poppy, 10-15 parts of maidenhair and 5-15 parts of oenothera biennis.
6. a kind of plant source repairs facial mask liquid according to claim 5, which is characterized in that the Chinese medicine repair extract by with Lower section method is prepared:
S1. the processing of raw material: weighing each raw material in proportion, cleans, and drying is crushed to 100 mesh hereinafter, spare；
S2. supercritical fluid extraction: supercritical fluid extraction tank is added in powder obtained in step S1, solvent C O is added2, in advance Heat carries out decompression and temperature adjustment operation, the solvent dissolved with extract is brought down below CO after mixing evenly2Critical pressure hereinafter, Due to CO2Solubility extremely declines, through separator extract and CO2And extraction each component is separated, and into extractor, is obtained Extract, while CO are repaired to required Chinese medicine2It is recycled with circulating pump.
7. a kind of plant source repairs facial mask liquid according to claim 6, which is characterized in that drying temperature described in step S1 is 40 DEG C, drying time 5-7h.
8. a kind of plant source repairs facial mask liquid according to claim 6, which is characterized in that in reduced pressure operation described in step S2 Pressure is brought down below 7MPa, and temperature is adjusted to 30 DEG C or so in the temperature adjustment operation.
9. a kind of method for preparing the plant source as described in any one of claim 1-8 claim and repairing facial mask liquid, feature exist In preparing in accordance with the following methods:
S1. the processing of Euglena: crushing after Euglena is dried and obtain Euglena powder, after the deionized water of 5 times of weight is added, extracting in boiling water 5-15min is filtered, reject filter residue, and dehydrated alcohol is added in filtrate, is precipitated, and is filtered, and solid is continued to employ；
S2. plant source repairs the preparation of facial mask liquid: by cedar oil, allantoin, castor oil, tea polyphenols, polyethylene wax and step S1 Solid mixing obtained, is added water, is heated to 60 DEG C and stirs evenly, and is cooled to room temperature and Chinese medicine reparation extract, EDTA bis- is added Sodium, butanediol and glycerol, stir evenly, packaging, and plant source is made and repairs facial mask liquid.
10. preparation method according to claim 9, which is characterized in that the speed of agitator is 500-700r/min.
CN201910386022.9A 2019-05-09 2019-05-09 A kind of plant source repairs facial mask liquid and preparation method thereof Pending CN110101632A (en)

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Publication number Priority date Publication date Assignee Title
CN115634179A (en) * 2022-11-01 2023-01-24 欧迪玛(湖北)生物科技有限公司 Rosa roxburghii dreg extract repairing mask and preparation method thereof

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CN108653160A (en) * 2018-05-31 2018-10-16 苏州蔻美新材料有限公司 A kind of preparation method of herb extracts anti-wrinkle cosmetic
CN108815037A (en) * 2018-08-02 2018-11-16 广州航美化妆品有限公司 A kind of whitening shines face skin care compositions and its application in cosmetics
CN109223634A (en) * 2018-09-27 2019-01-18 广州航美化妆品有限公司 Clear and rich moisturizing whitening mask
CN109363976A (en) * 2018-11-21 2019-02-22 广州艾蓓生物科技有限公司 It is a kind of to lift compact facial mask and preparation method thereof

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WO2006075311A1 (en) * 2005-01-14 2006-07-20 Sederma Cosmetic or dermopharmaceutical composition comprising an euglena extract
CN108653160A (en) * 2018-05-31 2018-10-16 苏州蔻美新材料有限公司 A kind of preparation method of herb extracts anti-wrinkle cosmetic
CN108815037A (en) * 2018-08-02 2018-11-16 广州航美化妆品有限公司 A kind of whitening shines face skin care compositions and its application in cosmetics
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115634179A (en) * 2022-11-01 2023-01-24 欧迪玛(湖北)生物科技有限公司 Rosa roxburghii dreg extract repairing mask and preparation method thereof

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