CN110101623A - A kind of bathing salt and preparation method thereof with antibacterial effect of releiving - Google Patents
A kind of bathing salt and preparation method thereof with antibacterial effect of releiving Download PDFInfo
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Abstract
The invention discloses a kind of bathing salts with antibacterial effect of releiving, it is related to bathing salt and its preparation technical field, its key points of the technical solution are that, by including the following raw material by weight, 60-80 parts of salt, 5-20 parts of silica 1,5-10 parts of alkaline agent, 1-5 parts of saltcake, 1-5 parts of glycerol, 5-10 parts of tartaric acid sodium, 2-6 parts of natural plant extraction liquid, 1-2 parts of cactus seed oil, 1-3 parts of phytosphingosine, grinding, is modulated and is obtained at mixing, and with safety, fungistatic effect is good and has both the advantage of anti-inflammatory effect of releiving.The present invention further correspondingly discloses a kind of preparation method of above-mentioned bathing salt with antibacterial effect of releiving.
Description
Technical field
The present invention relates to bathing salt and its preparation technical fields, more specifically, it relates to which a kind of have antibacterial function of releiving
Bathing salt of effect and preparation method thereof.
Background technique
Bath salt or bathing salt mostly by herbal medicine, natural land salt, natural sea salt, minerals and plants essential oil etc. at being grouped as,
The various trace elements such as iron, calcium, selenium, magnesium rich in needed by human body, bath salt, which is used for a long time, can eliminate the melanin on skin, allow
Skin is gradually recovered thin white, soft, elastic, has positive effect to facial dark sore, acne, color spot is dispelled also.And with life
Horizontal and the level of consumption the raising, people are also higher and higher to the attention degree of skin health care, to the functional requirements day of bath salt
It contains.
If application publication number is that the British patent of GB189815807A discloses a kind of bath salt in the prior art, with purification
Salt, borax, sodium bicarbonate, glycerol, cottonseed oil and plants essential oil etc. are raw material, in addition to cleaning effect is good, also have antibacterial, low mistake
Quick advantage.But the borax toxicity as main material is higher, countries in the world are forbidden as food additives more, if human body
The retention toxicosis of multi viscera can be caused by taking in excessive boron.Using borax as the bath salt raw material directly contacted with skin,
Genotoxic potential is worth noting.
Application publication number is JP2003095920A Japanese patent discloses a kind of showering agent, except containing normal in formula
Advise bath salt component: the inorganic salts such as sodium sulphate, sodium bicarbonate, sodium chloride, the water-insoluble particle such as titanium dioxide, calcium carbonate, coloring
Agent, the fragrance such as wood extract oil, the oils with moistening effect, outside the thickeners such as pectin and foaming agent；Also it is added with polyene alcohols
Antimycotic antibiotic.This kind of showering agent has and can kill most of body surface superficial type Candida, remove fungi and cause
The drawbacks of, restore the advantages of physiological function and natural curability of skin, but this kind of showering agent is due to introducing as medicinal
Antibiotic limit its frequency of usage must, it is understood that there may be antibiotic sensitization but also not all crowd be applicable in.
Authorization Notice No. is that the Chinese patent of CN1287762C discloses a kind of Bathing milk salt, by by weight:
93-94 parts of sodium chloride, milk 4-5 parts natural 0.04-0.06 parts of 0.04-0.06 parts of nano silver, pearl powder with silver oxide surface
Composition.It has the nano silver of silver oxide surface as bacteriostatic agent by adding, to obtain fungistatic effect.But contain into
This high nano silver and pearl powder with silver oxide surface increases Bathing milk salt preparation cost, is unfavorable for promoting and applying.
Thus, how to research and develop a kind of relative inexpensiveness, safety and the good functional bath salt of fungistatic effect is to need in the industry
It solves the problems, such as.
Summary of the invention
In view of the deficiencies of the prior art, the present invention intends to provide a kind of shower with antibacterial effect of releiving
Salt, with safety, fungistatic effect is good and has both the advantage of anti-inflammatory effect of releiving.
To achieve the above object, the present invention provides the following technical scheme that
A kind of bathing salt with antibacterial effect of releiving, by including the following raw material by weight,
60-80 parts of salt
5-20 parts of silica 1
5-10 parts of alkaline agent
1-5 parts of saltcake
1-5 parts of glycerol
5-10 parts of tartaric acid sodium
2-6 parts of natural plant extraction liquid
1-2 parts of cactus seed oil
1-3 parts of phytosphingosine,
Grinding, is modulated and is obtained at mixing.
In addition to conventionally used for configuring the salt of bath salt, alkaline agent, saltcake, silica, in the bath salt formula of the application also mixed with
Glycerol is as hygroscopic agent and water-retaining agent, so that the bath salt of the application can be used as massage bath salt, is able to maintain water using rear skin and moistens.Fruit
Sour sodium molecule amount is small, hygroscopicity is good, is easy to can promote skin blood circulation by percutaneous absorption and aging cutin is fallen off, may make
Skin emolliency and high resilience.
Natural plant extraction liquid has many-sided effect, first, the natural fragrance substance that can use natural plants plays
The fragrance effect of recuperating, makes user be in a cheerful frame of mind；Secondly, the natural plant pigment that contains in natural plant extraction liquid, can assign
Bath salt is with color；Third, natural inhibitor, bacteriostatic agent etc. in natural plants, so that bath salt has anti-oxidant, bactericidal etc.
The problems such as acting on, scytitis, acne, allergy can be effectively relieved.Cactus seed oil is rolled by cactus fruit and seed through removal of impurities
Low-temperature extraction forms after the pretreatment such as embryo, in natural faint yellow or pistac, has splendid anti-oxidant and crease-resistant function.
Cactus seed oil contains its abnormal vitamin E (about 1000 mgs/kg) abundant, and (about 10 grams/public of sterol
Jin) and a large amount of essential fatty acids, it can effectively prevent the infringement of free radical, deep layer, which is nourished, assigns skin living, delaying skin aging；It is right
It eliminates black eye and wrinkle, scar healing, treatment acne papule is promoted to have obvious effect.On the other hand, cactus seed oil
Moisturizing layer also is formed in skin surface, has the function of slowing down skin moisture loss.
Cuticula in skin has effects that defence prevents bacterial invasion and avoids the important of moisture loss, and cuticula
Phytosphingosine accounts for 60% or so in main component.The phytosphingosine of above-mentioned volume can help skin to restore elastic force, simultaneously also
Have the function of inflammation-diminishing function, antibacterial functions and promotes ceramide synthesis delay skin aging.
Further, the salt is purification sea salt, Jewish's salt, Himalaya rock salt, black salt, pottery salt, Persian indigo plant salt, salt efflorescence
One of or a variety of mixtures.
Sea salt is in granular form, and is rich in minerals, and purification sea salt pollution impurity is few.Jewish's salt (Kosher Salt) shape
Irregularly, crystal is coarse is suitable for production exfoliating bath salt.Himalaya rock salt (Himalayan Salt) has beautiful powder
Color or rose are rich in minerals.Black salt (Black Salt) includes two kinds: originate from India's production is Kala Namak, contains
A small amount of sulphur has anti-mite bactericidal effect；What Hawaii produced is Black lava salt, is volcano rock salt, containing a small amount of living
Property charcoal there is absorption to eliminate the unusual smell effect.Pottery salt (Grey Salt) is also known as Celtic Sea salt, and content of mineral substances is very rich, can help
It helps and maintains body electrolyte balance.Persian indigo plant salt (Persian Blue) is a kind of sea salt of bit bluish.Salt efflorescence (Fleur de
Sel it) is crystallized and is made by salt lake surface layer, fine platy quality, content of mineral substances height.Aforementioned various salt are edible salts, are used as bath
The main component of salt is safe and healthy, has no toxic side effect.
Further, the tartaric acid sodium is sodium gluconate, natrium malicum, sodium lactate, sodium glycolate, one in citric acid sodium
Kind or a variety of mixtures.
By using above-mentioned technical proposal, above-mentioned various tartaric acid sodium promote the cuticula accumulated on the skin to fall off, make
Obtain the effect that skin Lightening moistens, promotes blood circulation.
Further, the tartaric acid sodium by sodium glycolate and sodium lactate 1:(0.5-0.8 in mass ratio) ratio mix
And it obtains.
By using above-mentioned technical proposal, the effect that sodium glycolate promotes keratoderma to fall off is good, and sodium lactate promotes thin
The effect that born of the same parents update is good, and the two is used in combination the excellent for improving skin texture according to aforementioned proportion.
Further, the alkaline agent is sodium bicarbonate.
By using above-mentioned technical proposal, sodium bicarbonate is weak base, can help to remove skin keratin, worm mite and sebum.
Further, the natural plant extraction liquid by parts by weights meter the following raw material,
1-3 parts of the root of Dahurain angelica
1-3 parts of ligusticum sinense oliver
1-7 parts of peppermint
1-5 parts of lotus leaf
1-4 parts of tealeaves
It extracts and obtains.
The root of Dahurain angelica contains Isomperatorin (isoimperatorin), Imperatorin (imperatorin), bergapten
(bergapten), phellopterin (phellopterin), oxypeucedanin (oxypeucedanin) etc., containing aromatic odor,
Get rid of illness the functions such as dehumidifying, apocenosis myogenic, promoting blood circulation and stopping pain, anti-inflammatory.
Ligusticum sinense oliver contains volatile oil, main ingredient be 3- Ding Yuetai, the cnidium monnieri moon too lactones, distant ligusticum sinense oliver root containing volatile oil 1.5%.
Ligusticum sinense oliver neutral oil has calm, analgesia, antipyretic and anti-inflammatory effect, moreover it is possible to obviously slow down keto consumpting speed, to common pathogenic skin
Tinea bacterium has antibacterial action.
Peppermint contains menthol, menthones, and topical application can control headache, neuralgia, itch etc., is applied to skin, there is cool feeling.
Meanwhile with strong special aroma, have effects that promote restoring consciouness.
Lotus leaf taste faint scent is turned into containing substances such as organic acids, the vitamin Cs such as alkaloids, the tartaric acid such as nuciferine with antioxygen
With, conducive to skin toxin expelling, rush down antipyretic, with all worries set aside calm the nerves and other effects clearly.
Tealeaves is containing substances such as tea polyphenols, Tea Pigment, theanine, tea polysaccharide, γ-aminobutyric acid, pyrroloquinoline quinone.Wherein
Theine (phenol) has anti-oxidant, anti-inflammatory, antibacterial and other effects；Tea Pigment mainly includes chlorophyll, beta carotene etc., has and prolongs
The effects of slow skin aging and beauty；Theanine can improve skin cell activity, promote skin metabolism；Υ-amino fourth
Acid, with expansion blood vessel, promote blood circulation effect；Pyrroloquinoline quinone has the function of anti-oxidant and protection nerve.
It can not only assign bathing salt strong fragrance according to natural plant extraction liquid made from said ratio raw material, also assign
Given bathing salt it is antibacterial, it is anti-inflammatory, promote skin metabolism the effects of.
Further, the natural plant extraction liquid is prepared via following technique,
Raw material weighing: weighing the raw material comprising the root of Dahurain angelica, ligusticum sinense oliver, peppermint, lotus leaf and tealeaves according to the proportion, and Zhan Zongyuan is added in chopping
The calcium carbonate powder of material quality 1-1.5wt% is ground, and crushing raw material is obtained；
Vacuum distillation: being added the ethanol water for accounting for the 50Vol% for crushing 0.8-1.0 times of material quality toward crushing in raw material, in
50-80 DEG C, vacuum degree be 12-15KPa condition, be evaporated under reduced pressure 15-30min；The steam of generation is carried out in vacuum distillation process
It is condensed back；
It is primary to filter: reaction substrate being filtered while hot, obtains extraction liquid mixture；
Secondary suction filtration: the active powdered carbon of 1-5wt% is added into extraction liquid mixture, is filtered after ultrasonic disperse is uniform, gained
Filtrate is natural plant extraction liquid.
By using above-mentioned technical proposal, aromatic substance, the antibacterial material etc. in raw material can be utmostly extracted, is obtained
Natural plant extraction liquid containing it is miscellaneous less, aromatic flavour, antibacterial bacteriostatic effect it is good.
Another object of the present invention is to provide a kind of preparation methods of bathing salt with antibacterial effect of releiving, using this
Method be made bath salt have safety, fungistatic effect is good and has both the advantage of anti-inflammatory effect of releiving.
To achieve the above object, the present invention provides the following technical scheme that
A kind of preparation method of the bathing salt with antibacterial effect of releiving, includes the following steps,
P1, it is weighed according to the ratio comprising salt, silica, alkaline agent, saltcake, glycerol, tartaric acid sodium, natural plant extraction liquid, cactus
The raw material of seed oil, phytosphingosine；
P2, silica, natural plant extraction liquid, tartaric acid sodium, cactus seed oil and phytosphingosine are uniformly mixed；
P3, alkaline agent, saltcake and glycerol are continuously added, be uniformly mixed；
P4, addition salt are uniformly mixed to get bathing salt.
Silica has oil absorption, and silica can be by natural plant extraction liquid, cactus seed oil in P2 step
It is adsorbed with phytosphingosine, on the one hand can be uniformly dispersed by the ingredient that silica adsorbs, on the other hand can slow down aromatic substance
The volatilization loss of matter etc..Alkaline agent, saltcake and glycerol are added in P3 step, can since mixing equipment is in opposing seal state
To reduce because mixed material absorbs moisture, and cause the oily matters such as cactus seed oil bad by silica assimilation effect
Phenomenon.P4 step is eventually adding salt and is uniformly mixed to get bath salt.Material is blended in high speed mixer and completes, and mixing revolving speed exists
3000-5000rpm。
Further, the natural plant extraction liquid by parts by weights meter the following raw material,
1-3 parts of the root of Dahurain angelica
1-3 parts of ligusticum sinense oliver
1-7 parts of peppermint
1-5 parts of lotus leaf
1-4 parts of tealeaves
It extracts and obtains.
Further, the natural plant extraction liquid is prepared via following technique,
Raw material weighing: weighing the raw material comprising the root of Dahurain angelica, ligusticum sinense oliver, peppermint, lotus leaf and tealeaves according to the proportion, and Zhan Zongyuan is added in chopping
The calcium carbonate powder of material quality 1-1.5wt% is ground, and crushing raw material is obtained；
Vacuum distillation: being added the ethanol water for accounting for the 50Vol% for crushing 0.8-1.0 times of material quality toward crushing in raw material, in
50-80 DEG C, vacuum degree be 12-15KPa condition, be evaporated under reduced pressure 15-30min；The steam of generation is carried out in vacuum distillation process
It is condensed back；
It is primary to filter: reaction substrate being filtered while hot, obtains extraction liquid mixture；
Secondary suction filtration: the active powdered carbon of 1-5wt% is added into extraction liquid mixture, is filtered after ultrasonic disperse is uniform, gained
Filtrate is natural plant extraction liquid.
In conclusion the invention has the following advantages:
In addition to conventionally used for the salt of configuration bath salt, alkaline agent, saltcake, silica, also mixed with glycerol in the bath salt formula of the application
As hygroscopic agent and water-retaining agent, so that the bath salt of the application can be used as massage bath salt, water is able to maintain using rear skin and is moistened.It adds suitable
Measure tartaric acid sodium, using tartaric acid sodium molecule amount is small, hygroscopicity is good, be easy to by percutaneous absorption the characteristics of, can play promote skin blood
Circulation and the aging cutin effect of falling off, so that skin emolliency and high resilience.It adds by the root of Dahurain angelica, rhizoma ligustici, peppermint, lotus leaf, tealeaves
The natural plant extraction liquid being obtained by extraction can effectively delay so that bath salt fragrant odour also has the effects that anti-oxidant, bactericidal
The problems such as solving scytitis, acne, allergy.The incorporation of cactus seed oil then assigns bath salt splendid anti-oxidant and crease-resistant function
Can, while cactus seed oil also has the stimulation slowed down tartaric acid sodium, alkaline agent, root of Dahurain angelica extract etc. to skin, reduction sensitization
Effect.Phytosphingosine can then help skin to restore elastic force, while also having inflammation-diminishing function, antibacterial functions and promoting nerve
The effect of amide synthesis delay skin aging.
Detailed description of the invention
Fig. 1 is the preparation technology flow chart of natural plant extraction liquid in embodiment；
Fig. 2 is the preparation technology flow chart of the bathing salt in embodiment with antibacterial effect of releiving.
Specific embodiment
Below in conjunction with attached drawing, invention is further described in detail.
Embodiment 1:
A kind of bathing salt with antibacterial effect of releiving, is prepared by the following raw material by weight:
60 parts of sea salt of purification
5 parts of silica 1
5 parts of sodium bicarbonate
1 part of saltcake
1 part of glycerol
5 parts of sodium glycolate
2 parts of natural plant extraction liquid
1 part of cactus seed oil
1 part of phytosphingosine.
Wherein, natural plant extraction liquid is prepared according to process flow shown in Fig. 1, is specifically comprised the following steps:
Raw material weighing: weighing 1 part of the root of Dahurain angelica, 3 parts of ligusticum sinense oliver, 1 part of peppermint, 5 parts of lotus leaf and 3 parts of tealeaves, chopping by weight, and addition accounts for
The calcium carbonate powder of total raw material quality 1wt% is ground, and crushing raw material is obtained；
Vacuum distillation: toward crush raw material in be added account for crushing 0.8 times of material quality 50Vol% ethanol water, in 50 DEG C,
Vacuum degree is evaporated under reduced pressure 30min under the conditions of being 12KPa；The steam of generation is condensed back in vacuum distillation process；
It is primary to filter: reaction substrate being filtered while hot, obtains extraction liquid mixture；
Secondary suction filtration: the active powdered carbon of 1wt% being added into extraction liquid mixture, is filtered after ultrasonic disperse is uniform, gained filter
Liquid is natural plant extraction liquid.
The step of preparation process of the bathing salt of the present embodiment is as shown in Fig. 2, specifically comprise the following steps:
P1, purification sea salt, silica, sodium bicarbonate, saltcake, glycerol, sodium glycolate, natural plants extraction are weighed according to said ratio
Take liquid, cactus seed oil and phytosphingosine；
P2, silica, natural plant extraction liquid, sodium glycolate, cactus seed oil and phytosphingosine are added to high speed
In mixing apparatus, it is uniformly mixed with the revolving speed of 3000rpm；
P3, sodium bicarbonate, saltcake and glycerol are continuously added, is uniformly mixed with the revolving speed of 3000rpm；
P4, addition purification sea salt are uniformly mixed with the revolving speed of 3000rpm to get bathing salt.
Embodiment 2:
A kind of bathing salt with antibacterial effect of releiving, is prepared by the following raw material by weight:
60 parts of sea salt of purification
10 parts of Himalaya rock salt
8 parts of silica 1
8 parts of sodium bicarbonate
3 parts of saltcake
3 parts of glycerol
8 parts of citric acid sodium
4 parts of natural plant extraction liquid
1.5 parts of cactus seed oil
2 parts of phytosphingosine.
Wherein, natural plant extraction liquid is prepared according to process flow shown in Fig. 1, is specifically comprised the following steps:
Raw material weighing: weighing 2 parts of the root of Dahurain angelica, 2 parts of ligusticum sinense oliver, 4 parts of peppermint, 2 parts of lotus leaf and 4 parts of tealeaves, chopping by weight, and addition accounts for
The calcium carbonate powder of total raw material quality 1.5wt% is ground, and crushing raw material is obtained；
Vacuum distillation: toward crush raw material in be added account for crush 1 times of material quality 50Vol% ethanol water, in 65 DEG C, very
Reciprocal of duty cycle is evaporated under reduced pressure 20min under the conditions of being 13.5KPa；The steam of generation is condensed back in vacuum distillation process；
It is primary to filter: reaction substrate being filtered while hot, obtains extraction liquid mixture；
Secondary suction filtration: the active powdered carbon of 5wt% being added into extraction liquid mixture, is filtered after ultrasonic disperse is uniform, gained filter
Liquid is natural plant extraction liquid.
The step of preparation process of the bathing salt of the present embodiment is as shown in Fig. 2, specifically comprise the following steps:
P1, purification sea salt, Himalaya rock salt, silica, sodium bicarbonate, saltcake, glycerol, citric acid are weighed according to said ratio
Sodium, natural plant extraction liquid, cactus seed oil and phytosphingosine；
P2, silica, natural plant extraction liquid, citric acid sodium, cactus seed oil and phytosphingosine are added to high speed
In mixing apparatus, it is uniformly mixed with the revolving speed of 4000rpm；
P3, sodium bicarbonate, saltcake and glycerol are continuously added, is uniformly mixed with the revolving speed of 4000rpm；
P4, addition purification sea salt, Himalaya rock salt are uniformly mixed with the revolving speed of 4000rpm to get bathing salt.
Embodiment 3:
A kind of bathing salt with antibacterial effect of releiving, is prepared by the following raw material by weight:
70 parts of Jewish's salt
10 parts of black salt
20 parts of silica
10 parts of sodium bicarbonate
5 parts of saltcake
5 parts of glycerol
10 parts of natrium malicum
6 parts of natural plant extraction liquid
2 parts of cactus seed oil
3 parts of phytosphingosine.
Wherein, natural plant extraction liquid is prepared according to process flow shown in Fig. 1, is specifically comprised the following steps:
Raw material weighing: weighing 3 parts of the root of Dahurain angelica, 1 part of ligusticum sinense oliver, 7 parts of peppermint, 1 part of lotus leaf and 1 part of tealeaves, chopping by weight, and addition accounts for
The calcium carbonate powder of total raw material quality 1wt% is ground, and crushing raw material is obtained；
Vacuum distillation: toward crush raw material in be added account for crushing 0.9 times of material quality 50Vol% ethanol water, in 80 DEG C,
Vacuum degree is evaporated under reduced pressure 15min under the conditions of being 15KPa；The steam of generation is condensed back in vacuum distillation process；
It is primary to filter: reaction substrate being filtered while hot, obtains extraction liquid mixture；
Secondary suction filtration: the active powdered carbon of 2.5wt% is added into extraction liquid mixture, is filtered after ultrasonic disperse is uniform, gained
Filtrate is natural plant extraction liquid.
The step of preparation process of the bathing salt of the present embodiment is as shown in Fig. 2, specifically comprise the following steps:
P1, Jewish's salt, black salt, silica, sodium bicarbonate, saltcake, glycerol, natrium malicum, natural plant are weighed according to said ratio
Object extract liquor, cactus seed oil and phytosphingosine；
P2, silica, natural plant extraction liquid, natrium malicum, cactus seed oil and phytosphingosine are added to high speed
In mixing apparatus, it is uniformly mixed with the revolving speed of 5000rpm；
P3, sodium bicarbonate, saltcake and glycerol are continuously added, is uniformly mixed with the revolving speed of 5000rpm；
P4, addition Jewish's salt, black salt are uniformly mixed with the revolving speed of 5000rpm to get bathing salt.
Embodiment 4:
A kind of bathing salt with antibacterial effect of releiving, is prepared by the following raw material by weight:
60 parts of sea salt of purification
5 parts of Persian salt
6 parts of silica 1
7 parts of sodium bicarbonate
2 parts of saltcake
2 parts of glycerol
4 parts of sodium glycolate
2 parts of sodium lactate
3 parts of natural plant extraction liquid
1 part of cactus seed oil
1.5 parts of phytosphingosine.
Wherein, natural plant extraction liquid is prepared according to process flow shown in Fig. 1, is specifically comprised the following steps:
Raw material weighing: weighing 1 part of the root of Dahurain angelica, 3 parts of ligusticum sinense oliver, 1 part of peppermint, 5 parts of lotus leaf and 3 parts of tealeaves, chopping by weight, and addition accounts for
The calcium carbonate powder of total raw material quality 1wt% is ground, and crushing raw material is obtained；
Vacuum distillation: toward crush raw material in be added account for crushing 0.8 times of material quality 50Vol% ethanol water, in 50 DEG C,
Vacuum degree is evaporated under reduced pressure 30min under the conditions of being 12KPa；The steam of generation is condensed back in vacuum distillation process；
It is primary to filter: reaction substrate being filtered while hot, obtains extraction liquid mixture；
Secondary suction filtration: the active powdered carbon of 1wt% being added into extraction liquid mixture, is filtered after ultrasonic disperse is uniform, gained filter
Liquid is natural plant extraction liquid.
The step of preparation process of the bathing salt of the present embodiment is as shown in Fig. 2, specifically comprise the following steps:
P1, purification sea salt, Persian salt, silica, sodium bicarbonate, saltcake, glycerol, sodium glycolate, cream are weighed according to said ratio
Sour sodium, natural plant extraction liquid, cactus seed oil and phytosphingosine；
P2, silica, natural plant extraction liquid, sodium glycolate, sodium lactate, cactus seed oil and phytosphingosine are added
Into high-speed mixing equipment, it is uniformly mixed with the revolving speed of 3500rpm；
P3, sodium bicarbonate, saltcake and glycerol are continuously added, is uniformly mixed with the revolving speed of 3500rpm；
P4, addition purification sea salt, Persian salt are uniformly mixed with the revolving speed of 3500rpm to get bathing salt.
Embodiment 5:
A kind of bathing salt with antibacterial effect of releiving, is prepared by the following raw material by weight:
60 parts of sea salt of purification
15 parts of salt of pottery
9 parts of silica 1
8 parts of sodium bicarbonate
4 parts of saltcake
4 parts of glycerol
5 parts of sodium glycolate
4 parts of sodium lactate
4 parts of natural plant extraction liquid
2 parts of cactus seed oil
2.5 parts of phytosphingosine.
Wherein, natural plant extraction liquid is prepared according to process flow shown in Fig. 1, is specifically comprised the following steps:
Raw material weighing: weighing 2 parts of the root of Dahurain angelica, 2 parts of ligusticum sinense oliver, 4 parts of peppermint, 2 parts of lotus leaf and 4 parts of tealeaves, chopping by weight, and addition accounts for
The calcium carbonate powder of total raw material quality 1.5wt% is ground, and crushing raw material is obtained；
Vacuum distillation: toward crush raw material in be added account for crush 1 times of material quality 50Vol% ethanol water, in 65 DEG C, very
Reciprocal of duty cycle is evaporated under reduced pressure 20min under the conditions of being 13.5KPa；The steam of generation is condensed back in vacuum distillation process；
It is primary to filter: reaction substrate being filtered while hot, obtains extraction liquid mixture；
Secondary suction filtration: the active powdered carbon of 5wt% being added into extraction liquid mixture, is filtered after ultrasonic disperse is uniform, gained filter
Liquid is natural plant extraction liquid.
The step of preparation process of the bathing salt of the present embodiment is as shown in Fig. 2, specifically comprise the following steps:
P1, according to said ratio weigh purification sea salt, pottery salt, silica, sodium bicarbonate, saltcake, glycerol, sodium glycolate acid sodium,
Sodium lactate, natural plant extraction liquid, cactus seed oil and phytosphingosine；
P2, silica, natural plant extraction liquid, sodium glycolate, sodium lactate, cactus seed oil and phytosphingosine are added
Into high-speed mixing equipment, it is uniformly mixed with the revolving speed of 4500rpm；
P3, sodium bicarbonate, saltcake and glycerol are continuously added, is uniformly mixed with the revolving speed of 4500rpm；
P4, addition purification sea salt, pottery salt are uniformly mixed with the revolving speed of 4500rpm to get bathing salt.
Embodiment 6:
A kind of bathing salt with antibacterial effect of releiving, is prepared by the following raw material by weight:
70 parts of sea salt of purification
8 parts of silica 1
7.5 parts of sodium bicarbonate
3 parts of saltcake
3 parts of glycerol
4.5 parts of sodium glycolate
3 parts of sodium lactate
4 parts of natural plant extraction liquid
1.5 parts of cactus seed oil
2 parts of phytosphingosine.
Wherein, natural plant extraction liquid is prepared according to process flow shown in Fig. 1, is specifically comprised the following steps:
Raw material weighing: weighing 3 parts of the root of Dahurain angelica, 1 part of ligusticum sinense oliver, 7 parts of peppermint, 1 part of lotus leaf and 1 part of tealeaves, chopping by weight, and addition accounts for
The calcium carbonate powder of total raw material quality 1wt% is ground, and crushing raw material is obtained；
Vacuum distillation: toward crush raw material in be added account for crushing 0.9 times of material quality 50Vol% ethanol water, in 80 DEG C,
Vacuum degree is evaporated under reduced pressure 15min under the conditions of being 15KPa；The steam of generation is condensed back in vacuum distillation process；
It is primary to filter: reaction substrate being filtered while hot, obtains extraction liquid mixture；
Secondary suction filtration: the active powdered carbon of 2.5wt% is added into extraction liquid mixture, is filtered after ultrasonic disperse is uniform, gained
Filtrate is natural plant extraction liquid.
The step of preparation process of the bathing salt of the present embodiment is as shown in Fig. 2, specifically comprise the following steps:
P1, purification sea salt, silica, sodium bicarbonate, saltcake, glycerol, sodium glycolate, sodium lactate, day are weighed according to said ratio
Right plant extraction liquid, cactus seed oil and phytosphingosine；
P2, silica, natural plant extraction liquid, sodium glycolate, sodium lactate, cactus seed oil and phytosphingosine are added
Into high-speed mixing equipment, it is uniformly mixed with the revolving speed of 3800rpm；
P3, sodium bicarbonate, saltcake and glycerol are continuously added, is uniformly mixed with the revolving speed of 3800rpm；
P4, addition purification sea salt are uniformly mixed with the revolving speed of 3800rpm to get bathing salt.
Reference examples 1:
A kind of bathing salt, the difference with embodiment 3 are only that: natural plant extraction liquid is not contained in formula.
Reference examples 2:
A kind of bathing salt, the difference with embodiment 3 are only that: cactus seed oil is not contained in formula.
Reference examples 3:
A kind of bathing salt, the difference with embodiment 3 are only that: phytosphingosine is not contained in formula.
Performance test
A, degerming is tested
9 groups of experimenters are randomly selected, every group of 5 people are entire to test 45 people.
Each group personnel are tested as unit of group, after acquiring finger sample to experimenter, are first drenched hand, respectively
It is fallen with the bathing salt of 1.5g embodiment 1-6 and embodiment 1-3 in the palm of the hand, is washed by rubbing with the hands by the hand washing of " disinfection technology standard " double
Hand and wrist retain 30s, to its natural drying, are leaving and taking finger culture sample after about 2min.The method of sampling and detection method are equal
According to Ministry of Public Health's " disinfection technology standard " (Ministry of Health of the People's Republic of China, disinfection technology standard [M], Beijing: Ministry of Public Health's health Rule and supervision department, 2002:200 ~ 201) in finger Disinfection Effect the method for sampling and detection method carry out.
The average value of each group experimenter finger culture degerming rate is recorded, as shown in table 1:
1. degerming experimental result table of table
From upper table experimental data: for bathing salt of the invention to the removal rate of bacterium up to 92.5% or more, bactericidal effect is excellent.
Meanwhile natural plant extraction liquid, cactus seed oil and plant sheath known to comparative example 3 and the experimental data of reference examples 1-3
There is synergic remove, bactericidal effect is best when three adds simultaneously between ammonia alcohol.
B, bacteriostatic experiment
Using Escherichia coli, staphylococcus aureus and Candida albicans as experimental strain.Existed with continuous 3 34h of each experimental strain
Last time secondary culture in tryptone soya broth culture medium uses bacterium as bacteriostatic experiment.It is outstanding that bacterium is adjusted by transmissometer
Liquid concentration is to 1.0 ~ 9.0 × 105cfu/mL.It uniformly weighs and is used with the test of the bathing salt configuration of embodiment 1-6, reference examples 1-3
Liquid is added to various concentration and is melted in agar medium, plate is made, and is cultivated 48h through 37 DEG C of inversions, is discarded by living contaminants
Plate.0.1ml bacterial suspension inoculation is pipetted to test panel, planar surface is spread evenly across with L-type glass bar, is inverted in 37 DEG C
48h is cultivated, the bacterium condition of production of each experimental bacteria on plate is observed.Every kind is tested respectively, and does respective markers, real
It tests repeatedly.Experimental result record is as shown in table 2:
2. bacteriostatic experiment result table of table
Note: "+" representative has bacterium growth, and "-" represents asepsis growth.
By upper table experimental data it is found that bathing salt of the invention is to Escherichia coli, staphylococcus aureus and Candida albicans
Bacterium all has preferable fungistatic effect.Comparative example 3 and the experimental data of reference examples 1-3 are it is found that in of the invention simultaneously
There is collaboration bacteriostasis, suppression when three adds simultaneously between natural plant extraction liquid, cactus seed oil and phytosphingosine
Bacterium effect is optimal.
Above-mentioned specific embodiment is only explanation of the invention, is not limitation of the present invention, art technology
Personnel can according to need the modification that not creative contribution is made to the present embodiment after reading this specification, but as long as
All by the protection of Patent Law in scope of the presently claimed invention.
Claims (10)
1. a kind of bathing salt with antibacterial effect of releiving, it is characterised in that: by including the following raw material by weight,
60-80 parts of salt
5-20 parts of silica 1
5-10 parts of alkaline agent
1-5 parts of saltcake
1-5 parts of glycerol
5-10 parts of tartaric acid sodium
2-6 parts of natural plant extraction liquid
1-2 parts of cactus seed oil
1-3 parts of phytosphingosine,
Grinding, is modulated and is obtained at mixing.
2. a kind of bathing salt with antibacterial effect of releiving according to claim 1, it is characterised in that: the salt is purification
One of sea salt, Jewish's salt, Himalaya rock salt, black salt, pottery salt, Persian indigo plant salt, salt efflorescence or a variety of mixtures.
3. a kind of bathing salt with antibacterial effect of releiving according to claim 1, it is characterised in that: the tartaric acid sodium is
One of sodium gluconate, natrium malicum, sodium lactate, sodium glycolate, citric acid sodium or a variety of mixtures.
4. a kind of bathing salt with antibacterial effect of releiving according to claim 3, it is characterised in that: the tartaric acid sodium by
Sodium glycolate and sodium lactate 1:(0.5-0.8 in mass ratio) ratio be obtained by mixing.
5. a kind of bathing salt with antibacterial effect of releiving according to claim 1, it is characterised in that: the alkaline agent is small
Soda.
6. a kind of bathing salt with antibacterial effect of releiving according to claim 1-5, it is characterised in that: described
Natural plant extraction liquid by parts by weights meter the following raw material,
1-3 parts of the root of Dahurain angelica
1-3 parts of ligusticum sinense oliver
1-7 parts of peppermint
1-5 parts of lotus leaf
1-4 parts of tealeaves
It extracts and obtains.
7. a kind of bathing salt with antibacterial effect of releiving according to claim 6, it is characterised in that: the natural plants
Extract liquor is prepared via following technique,
Raw material weighing: weighing the raw material comprising the root of Dahurain angelica, ligusticum sinense oliver, peppermint, lotus leaf and tealeaves according to the proportion, and Zhan Zongyuan is added in chopping
The calcium carbonate powder of material quality 1-1.5wt% is ground, and crushing raw material is obtained；
Vacuum distillation: being added the ethanol water for accounting for the 50Vol% for crushing 0.8-1.0 times of material quality toward crushing in raw material, in
50-80 DEG C, vacuum degree be 12-15KPa condition, be evaporated under reduced pressure 15-30min；The steam of generation is carried out in vacuum distillation process
It is condensed back；
It is primary to filter: reaction substrate being filtered while hot, obtains extraction liquid mixture；
Secondary suction filtration: the active powdered carbon of 1-5wt% is added into extraction liquid mixture, is filtered after ultrasonic disperse is uniform, gained
Filtrate is natural plant extraction liquid.
8. a kind of a kind of preparation method of the bathing salt with antibacterial effect of releiving as described in claim 1, it is characterised in that:
Include the following steps,
P1, it is weighed according to the ratio comprising salt, silica, alkaline agent, saltcake, glycerol, tartaric acid sodium, natural plant extraction liquid, cactus
The raw material of seed oil, phytosphingosine；
P2, silica, natural plant extraction liquid, tartaric acid sodium, cactus seed oil and phytosphingosine are uniformly mixed；
P3, alkaline agent, saltcake and glycerol are continuously added, be uniformly mixed；
P4, addition salt are uniformly mixed to get bathing salt.
9. a kind of preparation method of bathing salt with antibacterial effect of releiving according to claim 8, it is characterised in that: institute
Natural plant extraction liquid is stated by the following raw material of parts by weights meter,
1-3 parts of the root of Dahurain angelica
1-3 parts of ligusticum sinense oliver
1-7 parts of peppermint
1-5 parts of lotus leaf
1-4 parts of tealeaves
It extracts and obtains.
10. a kind of preparation method of bathing salt with antibacterial effect of releiving according to claim 8, it is characterised in that:
The natural plant extraction liquid is prepared via following technique,
Raw material weighing: weighing the raw material comprising the root of Dahurain angelica, ligusticum sinense oliver, peppermint, lotus leaf and tealeaves according to the proportion, and Zhan Zongyuan is added in chopping
The calcium carbonate powder of material quality 1-1.5wt% is ground, and crushing raw material is obtained；
Vacuum distillation: being added the ethanol water for accounting for the 50Vol% for crushing 0.8-1.0 times of material quality toward crushing in raw material, in
50-80 DEG C, vacuum degree be 12-15KPa condition, be evaporated under reduced pressure 15-30min；The steam of generation is carried out in vacuum distillation process
It is condensed back；
It is primary to filter: reaction substrate being filtered while hot, obtains extraction liquid mixture；
Secondary suction filtration: the active powdered carbon of 1-5wt% is added into extraction liquid mixture, is filtered after ultrasonic disperse is uniform, gained
Filtrate is natural plant extraction liquid.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112791032A (en) * | 2020-12-31 | 2021-05-14 | 康钰(福建)生物科技有限公司 | Explosive salt and preparation method thereof |
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2019
- 2019-06-10 CN CN201910498231.2A patent/CN110101623A/en active Pending
Non-Patent Citations (1)
| Title |
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| 胡本祥，等: "《生药学》", 30 September 2013, 西安交通大学出版社 * |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112791032A (en) * | 2020-12-31 | 2021-05-14 | 康钰(福建)生物科技有限公司 | Explosive salt and preparation method thereof |
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