CN110100984A - Health care blueberry concentrate and its production technology - Google Patents
Health care blueberry concentrate and its production technology Download PDFInfo
- Publication number
- CN110100984A CN110100984A CN201910439400.5A CN201910439400A CN110100984A CN 110100984 A CN110100984 A CN 110100984A CN 201910439400 A CN201910439400 A CN 201910439400A CN 110100984 A CN110100984 A CN 110100984A
- Authority
- CN
- China
- Prior art keywords
- blueberry
- concentrate
- health care
- temperature
- obtains
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 235000003095 Vaccinium corymbosum Nutrition 0.000 title claims abstract description 75
- 235000017537 Vaccinium myrtillus Nutrition 0.000 title claims abstract description 75
- 235000021014 blueberries Nutrition 0.000 title claims abstract description 75
- 240000000851 Vaccinium corymbosum Species 0.000 title claims abstract description 69
- 239000012141 concentrate Substances 0.000 title claims abstract description 58
- 230000036541 health Effects 0.000 title claims abstract description 39
- 238000005516 engineering process Methods 0.000 title claims abstract description 26
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 25
- 241000382353 Pupa Species 0.000 claims abstract description 52
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 32
- 239000003963 antioxidant agent Substances 0.000 claims abstract description 25
- 230000003078 antioxidant effect Effects 0.000 claims abstract description 24
- 235000006708 antioxidants Nutrition 0.000 claims abstract description 24
- 239000002002 slurry Substances 0.000 claims abstract description 21
- 239000000706 filtrate Substances 0.000 claims abstract description 19
- 238000000034 method Methods 0.000 claims abstract description 18
- 235000017807 phytochemicals Nutrition 0.000 claims abstract description 14
- 229930000223 plant secondary metabolite Natural products 0.000 claims abstract description 14
- 230000001954 sterilising effect Effects 0.000 claims abstract description 13
- 238000004659 sterilization and disinfection Methods 0.000 claims abstract description 7
- 239000007788 liquid Substances 0.000 claims description 46
- 241000255789 Bombyx mori Species 0.000 claims description 33
- 239000000843 powder Substances 0.000 claims description 28
- 238000000227 grinding Methods 0.000 claims description 21
- 239000004365 Protease Substances 0.000 claims description 18
- 238000005360 mashing Methods 0.000 claims description 15
- 235000012054 meals Nutrition 0.000 claims description 14
- 102000004190 Enzymes Human genes 0.000 claims description 13
- 108090000790 Enzymes Proteins 0.000 claims description 13
- 229940088598 enzyme Drugs 0.000 claims description 13
- 238000003756 stirring Methods 0.000 claims description 13
- 238000000108 ultra-filtration Methods 0.000 claims description 13
- 239000012528 membrane Substances 0.000 claims description 12
- 238000006243 chemical reaction Methods 0.000 claims description 11
- 108090000526 Papain Proteins 0.000 claims description 9
- 108091005804 Peptidases Proteins 0.000 claims description 9
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 claims description 9
- 239000003513 alkali Substances 0.000 claims description 9
- 239000000084 colloidal system Substances 0.000 claims description 9
- 229940055729 papain Drugs 0.000 claims description 9
- 235000019834 papain Nutrition 0.000 claims description 9
- 235000019419 proteases Nutrition 0.000 claims description 9
- 240000002234 Allium sativum Species 0.000 claims description 8
- 230000009849 deactivation Effects 0.000 claims description 8
- 230000007071 enzymatic hydrolysis Effects 0.000 claims description 8
- 238000006047 enzymatic hydrolysis reaction Methods 0.000 claims description 8
- 235000004611 garlic Nutrition 0.000 claims description 8
- 239000007787 solid Substances 0.000 claims description 8
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 7
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 claims description 7
- 239000004744 fabric Substances 0.000 claims description 7
- 238000001914 filtration Methods 0.000 claims description 7
- 239000008103 glucose Substances 0.000 claims description 7
- 238000004321 preservation Methods 0.000 claims description 7
- 238000009210 therapy by ultrasound Methods 0.000 claims description 7
- 238000010792 warming Methods 0.000 claims description 7
- XJMPAUZQVRGFRE-SCHFUKFYSA-N Gardenoside Natural products O=C(OC)C=1[C@H]2[C@H]([C@H](O[C@H]3[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O3)OC=1)[C@@](O)(CO)C=C2 XJMPAUZQVRGFRE-SCHFUKFYSA-N 0.000 claims description 6
- 235000014360 Punica granatum Nutrition 0.000 claims description 6
- 239000000835 fiber Substances 0.000 claims description 6
- XJMPAUZQVRGFRE-AYDWLWLASA-N methyl (1s,4as,7s,7as)-7-hydroxy-7-(hydroxymethyl)-1-[(2s,3r,4s,5s,6r)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxy-4a,7a-dihydro-1h-cyclopenta[c]pyran-4-carboxylate Chemical compound O([C@@H]1OC=C([C@@H]2[C@H]1[C@](C=C2)(O)CO)C(=O)OC)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O XJMPAUZQVRGFRE-AYDWLWLASA-N 0.000 claims description 6
- 150000008442 polyphenolic compounds Chemical class 0.000 claims description 6
- 235000013824 polyphenols Nutrition 0.000 claims description 6
- 241000196324 Embryophyta Species 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- 229910052760 oxygen Inorganic materials 0.000 claims description 2
- 239000001301 oxygen Substances 0.000 claims description 2
- 230000001376 precipitating effect Effects 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 claims description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 1
- 244000294611 Punica granatum Species 0.000 claims 1
- 229910052708 sodium Inorganic materials 0.000 claims 1
- 239000011734 sodium Substances 0.000 claims 1
- 235000016709 nutrition Nutrition 0.000 abstract description 6
- 235000013399 edible fruits Nutrition 0.000 abstract description 5
- 230000035764 nutrition Effects 0.000 abstract description 5
- 235000019614 sour taste Nutrition 0.000 abstract description 4
- 230000001093 anti-cancer Effects 0.000 abstract description 3
- 235000009508 confectionery Nutrition 0.000 abstract description 3
- 235000015097 nutrients Nutrition 0.000 abstract description 3
- 230000001151 other effect Effects 0.000 abstract description 3
- 230000008569 process Effects 0.000 abstract description 3
- 238000012545 processing Methods 0.000 abstract description 3
- 239000000047 product Substances 0.000 abstract description 3
- 235000019605 sweet taste sensations Nutrition 0.000 abstract description 3
- 230000003712 anti-aging effect Effects 0.000 abstract description 2
- 125000003118 aryl group Chemical group 0.000 abstract description 2
- 230000003796 beauty Effects 0.000 abstract description 2
- 230000015556 catabolic process Effects 0.000 abstract description 2
- 238000006731 degradation reaction Methods 0.000 abstract description 2
- 230000035622 drinking Effects 0.000 abstract description 2
- 239000000796 flavoring agent Substances 0.000 abstract description 2
- 235000019634 flavors Nutrition 0.000 abstract description 2
- 230000036039 immunity Effects 0.000 abstract description 2
- 230000007774 longterm Effects 0.000 abstract description 2
- 235000019640 taste Nutrition 0.000 abstract description 2
- 239000000243 solution Substances 0.000 description 14
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 12
- 238000009777 vacuum freeze-drying Methods 0.000 description 7
- 244000077233 Vaccinium uliginosum Species 0.000 description 6
- 235000010208 anthocyanin Nutrition 0.000 description 6
- 229930002877 anthocyanin Natural products 0.000 description 6
- 239000004410 anthocyanin Substances 0.000 description 6
- 150000004636 anthocyanins Chemical class 0.000 description 6
- 239000007864 aqueous solution Substances 0.000 description 6
- 238000001816 cooling Methods 0.000 description 6
- 238000001035 drying Methods 0.000 description 6
- 230000000694 effects Effects 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- 238000002156 mixing Methods 0.000 description 6
- 239000001397 quillaja saponaria molina bark Substances 0.000 description 6
- 229930182490 saponin Natural products 0.000 description 6
- 150000007949 saponins Chemical class 0.000 description 6
- 235000011121 sodium hydroxide Nutrition 0.000 description 6
- 241000219991 Lythraceae Species 0.000 description 5
- HHEAADYXPMHMCT-UHFFFAOYSA-N dpph Chemical compound [O-][N+](=O)C1=CC([N+](=O)[O-])=CC([N+]([O-])=O)=C1[N]N(C=1C=CC=CC=1)C1=CC=CC=C1 HHEAADYXPMHMCT-UHFFFAOYSA-N 0.000 description 5
- 238000007710 freezing Methods 0.000 description 5
- 230000008014 freezing Effects 0.000 description 5
- 230000006870 function Effects 0.000 description 5
- 238000000859 sublimation Methods 0.000 description 5
- 230000008022 sublimation Effects 0.000 description 5
- 238000005119 centrifugation Methods 0.000 description 4
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 4
- 239000003814 drug Substances 0.000 description 4
- -1 makeups.Currently Substances 0.000 description 4
- 102000004169 proteins and genes Human genes 0.000 description 4
- 108090000623 proteins and genes Proteins 0.000 description 4
- 238000000527 sonication Methods 0.000 description 4
- 238000002835 absorbance Methods 0.000 description 3
- 230000032683 aging Effects 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- 238000007689 inspection Methods 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- 238000005057 refrigeration Methods 0.000 description 3
- 239000013049 sediment Substances 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 2
- 206010028980 Neoplasm Diseases 0.000 description 2
- 229930014669 anthocyanidin Natural products 0.000 description 2
- 150000001453 anthocyanidins Chemical class 0.000 description 2
- 235000008758 anthocyanidins Nutrition 0.000 description 2
- 239000008280 blood Substances 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 239000011575 calcium Substances 0.000 description 2
- 229910052791 calcium Inorganic materials 0.000 description 2
- 201000011510 cancer Diseases 0.000 description 2
- 235000012000 cholesterol Nutrition 0.000 description 2
- 235000021022 fresh fruits Nutrition 0.000 description 2
- BJRNKVDFDLYUGJ-RMPHRYRLSA-N hydroquinone O-beta-D-glucopyranoside Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1OC1=CC=C(O)C=C1 BJRNKVDFDLYUGJ-RMPHRYRLSA-N 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- NOESYZHRGYRDHS-UHFFFAOYSA-N insulin Chemical compound N1C(=O)C(NC(=O)C(CCC(N)=O)NC(=O)C(CCC(O)=O)NC(=O)C(C(C)C)NC(=O)C(NC(=O)CN)C(C)CC)CSSCC(C(NC(CO)C(=O)NC(CC(C)C)C(=O)NC(CC=2C=CC(O)=CC=2)C(=O)NC(CCC(N)=O)C(=O)NC(CC(C)C)C(=O)NC(CCC(O)=O)C(=O)NC(CC(N)=O)C(=O)NC(CC=2C=CC(O)=CC=2)C(=O)NC(CSSCC(NC(=O)C(C(C)C)NC(=O)C(CC(C)C)NC(=O)C(CC=2C=CC(O)=CC=2)NC(=O)C(CC(C)C)NC(=O)C(C)NC(=O)C(CCC(O)=O)NC(=O)C(C(C)C)NC(=O)C(CC(C)C)NC(=O)C(CC=2NC=NC=2)NC(=O)C(CO)NC(=O)CNC2=O)C(=O)NCC(=O)NC(CCC(O)=O)C(=O)NC(CCCNC(N)=N)C(=O)NCC(=O)NC(CC=3C=CC=CC=3)C(=O)NC(CC=3C=CC=CC=3)C(=O)NC(CC=3C=CC(O)=CC=3)C(=O)NC(C(C)O)C(=O)N3C(CCC3)C(=O)NC(CCCCN)C(=O)NC(C)C(O)=O)C(=O)NC(CC(N)=O)C(O)=O)=O)NC(=O)C(C(C)CC)NC(=O)C(CO)NC(=O)C(C(C)O)NC(=O)C1CSSCC2NC(=O)C(CC(C)C)NC(=O)C(NC(=O)C(CCC(N)=O)NC(=O)C(CC(N)=O)NC(=O)C(NC(=O)C(N)CC=1C=CC=CC=1)C(C)C)CC1=CN=CN1 NOESYZHRGYRDHS-UHFFFAOYSA-N 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 239000000049 pigment Substances 0.000 description 2
- 238000005728 strengthening Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 230000035922 thirst Effects 0.000 description 2
- 235000013343 vitamin Nutrition 0.000 description 2
- 239000011782 vitamin Substances 0.000 description 2
- 229940088594 vitamin Drugs 0.000 description 2
- 229930003231 vitamin Natural products 0.000 description 2
- 150000003722 vitamin derivatives Chemical class 0.000 description 2
- 239000011701 zinc Substances 0.000 description 2
- 229910052725 zinc Inorganic materials 0.000 description 2
- FPIPGXGPPPQFEQ-UHFFFAOYSA-N 13-cis retinol Natural products OCC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-UHFFFAOYSA-N 0.000 description 1
- 241000255783 Bombycidae Species 0.000 description 1
- 206010006895 Cachexia Diseases 0.000 description 1
- 241000244203 Caenorhabditis elegans Species 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 206010008909 Chronic Hepatitis Diseases 0.000 description 1
- 206010010904 Convulsion Diseases 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 208000035150 Hypercholesterolemia Diseases 0.000 description 1
- 208000031226 Hyperlipidaemia Diseases 0.000 description 1
- 206010020772 Hypertension Diseases 0.000 description 1
- 206010061218 Inflammation Diseases 0.000 description 1
- 102000004877 Insulin Human genes 0.000 description 1
- 108090001061 Insulin Proteins 0.000 description 1
- 102000004895 Lipoproteins Human genes 0.000 description 1
- 108090001030 Lipoproteins Proteins 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 206010037660 Pyrexia Diseases 0.000 description 1
- 208000034189 Sclerosis Diseases 0.000 description 1
- 208000007536 Thrombosis Diseases 0.000 description 1
- FPIPGXGPPPQFEQ-BOOMUCAASA-N Vitamin A Natural products OC/C=C(/C)\C=C\C=C(\C)/C=C/C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-BOOMUCAASA-N 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 238000009098 adjuvant therapy Methods 0.000 description 1
- FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical compound OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 229960000271 arbutin Drugs 0.000 description 1
- 210000001367 artery Anatomy 0.000 description 1
- 235000010323 ascorbic acid Nutrition 0.000 description 1
- 229960005070 ascorbic acid Drugs 0.000 description 1
- 239000011668 ascorbic acid Substances 0.000 description 1
- 208000003464 asthenopia Diseases 0.000 description 1
- 238000010009 beating Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 210000004204 blood vessel Anatomy 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 235000014633 carbohydrates Nutrition 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 230000036461 convulsion Effects 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 210000003792 cranial nerve Anatomy 0.000 description 1
- 238000005138 cryopreservation Methods 0.000 description 1
- 229960000935 dehydrated alcohol Drugs 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 206010012601 diabetes mellitus Diseases 0.000 description 1
- 235000013325 dietary fiber Nutrition 0.000 description 1
- 230000001079 digestive effect Effects 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 208000026500 emaciation Diseases 0.000 description 1
- 230000004438 eyesight Effects 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 229910052732 germanium Inorganic materials 0.000 description 1
- GNPVGFCGXDBREM-UHFFFAOYSA-N germanium atom Chemical compound [Ge] GNPVGFCGXDBREM-UHFFFAOYSA-N 0.000 description 1
- 229930182470 glycoside Natural products 0.000 description 1
- 150000002338 glycosides Chemical class 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 235000013402 health food Nutrition 0.000 description 1
- 208000006454 hepatitis Diseases 0.000 description 1
- 230000036737 immune function Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 229940125396 insulin Drugs 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 235000014058 juice drink Nutrition 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 230000003908 liver function Effects 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 239000002366 mineral element Substances 0.000 description 1
- 230000001537 neural effect Effects 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- BJRNKVDFDLYUGJ-UHFFFAOYSA-N p-hydroxyphenyl beta-D-alloside Natural products OC1C(O)C(O)C(CO)OC1OC1=CC=C(O)C=C1 BJRNKVDFDLYUGJ-UHFFFAOYSA-N 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 230000000144 pharmacologic effect Effects 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000006187 pill Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 108090000765 processed proteins & peptides Proteins 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 210000001525 retina Anatomy 0.000 description 1
- 230000002000 scavenging effect Effects 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 210000000952 spleen Anatomy 0.000 description 1
- 238000013112 stability test Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- ANRHNWWPFJCPAZ-UHFFFAOYSA-M thionine Chemical compound [Cl-].C1=CC(N)=CC2=[S+]C3=CC(N)=CC=C3N=C21 ANRHNWWPFJCPAZ-UHFFFAOYSA-M 0.000 description 1
- 230000002936 tranquilizing effect Effects 0.000 description 1
- 235000019155 vitamin A Nutrition 0.000 description 1
- 239000011719 vitamin A Substances 0.000 description 1
- 229940045997 vitamin a Drugs 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/385—Concentrates of non-alcoholic beverages
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/42—Preservation of non-alcoholic beverages
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/17—Amino acids, peptides or proteins
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
- Mycology (AREA)
- Medicines Containing Plant Substances (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
Abstract
The invention discloses a kind of health care blueberry concentrate and its production technology, the production technology is the following steps are included: blueberry is washed with water, drained by (1)；(2) it takes the blueberry after draining, water, anti-oxidant pupa albumen, anioxidant phytochemicals to be added in beater and be beaten, obtains slurries；(3) slurries are filtered using plate filter, obtains filtrate；(4) filter vacuum is concentrated, obtains concentrate；(5) ultra high temperature short time sterilization.Health care blueberry concentrate of the present invention, it is in good taste, the smell of fruits is very sweet, flavor is aromatic, sweet and sour taste, in process by control processing factors and anti-oxidant treatment two in terms of come reduce blueberry nutrient element degradation loss, remain nutrition and the functional component of blueberry, promote product quality, long-term drinking, have improve the immunity of the human body, beauty, anti-aging, anti-cancer and other effects.
Description
Technical field
The present invention relates to food processing technology fields, and in particular to a kind of health care blueberry concentrate and its production technology.
Background technique
In Blueberry other than conventional sugar, acid and VC, it is rich in VE, VA, VB, SOD, arbutin, protein, cyanine
The mineral elements such as glycosides, dietary fibre and K, Fe, Zn, Ca abundant.According to the Blueberry to 14 kinds introduced from the U.S.
Analysis measurement, anthocyanin pigments content is up to 163mg in every hectogram blueberry fresh fruit, and 400~700 milligrams of protein, fat 500~
600 milligrams, 12.3~15.3 milligrams of carbohydrate, it is micro- that vitamin A is up to 81~100 international units, vitamin E2 .7~9.5
Gram, SOD5.39 international unit, vitamin content is high.Microelement is also very high, 220~920 microgram of calcium in every gram of fresh fruit, phosphorus 98
~274 micrograms, 114~249 microgram of magnesium, 2.1~4.3 microgram of zinc, 7.6~30.0 microgram of iron, 0.8~1.2 microgram of germanium, copper 2.0
~3.2 micrograms.Not only have good nutrition health-care functions, also have prevent cranial nerve aging, heart tonifying, anticancer softening blood vessel,
The functions such as enhance the immune of the body.
Wild blueberry anthocyanin content is 330~380mg/100g, and cultivar Anthocyanin from Blueberry content is 70~280mg/
100g.Anthocyanidin has the characteristics that nutrition and doctor safe and nontoxic, while that have certain as a kind of natural edible pigment
Medicine value, therefore play an important role in fields such as food, medicine, makeups.Currently, anthocyanin content has been in fruit
The important indicator for judging fruit quality is measured through becoming.Blueberry is referred to as natural as fruit queen, anthocyanin,
It is extremely precious functional natural colorants.Currently, Anthocyanin from Blueberry is gradually applied in medicine, healthcare function is main
It include: to activate retina enzyme, erythrolabe is promoted to synthesize, relieving eye strain, raising eyesight, improvement yctalopia, reduction cholesterol,
Inhibit lipoprotein oxidation, increases the permeability effect of capillary, delay neural aging, improve memory, eliminate internal inflammation, in advance
Preventing thrombosis and artery sclerosis, scavenging capacity oxygen radical adjust diabetes blood glucose's value, reduce the functions such as injection of insulin.
But nutrient component damages are larger in the process of prior art blueberry concentrate, need further to be studied.
Summary of the invention
The invention mainly solves the technical problem of providing a kind of health care blueberry concentrate and its production technology, ingredient days
So, sweet and sour taste, it is full of nutrition.
To achieve the above object, the technical solution adopted by the present invention is that:
A kind of production technology of health care blueberry concentrate, comprising the following steps:
(1) blueberry washed with water, drained；
(2) it takes the blueberry after draining, water, anti-oxidant pupa albumen, anioxidant phytochemicals to be added in beater and be beaten, obtains
Slurries；
(3) slurries are filtered using plate filter, obtains filtrate；
(4) filter vacuum is concentrated, obtains concentrate；
(5) ultra high temperature short time sterilization.
A kind of production technology of health care blueberry concentrate, comprising the following steps:
(1) blueberry washed with water, drained；
(2) take the blueberry 5-15 parts by weight after draining, water 85-95 parts by weight, anti-oxidant pupa albumen 0.3-1 parts by weight,
Anioxidant phytochemicals 0.05-0.35 parts by weight be added beater in temperature be 1-5 DEG C mashing 2-6 minutes, obtain slurries；
(3) slurries are filtered using plate filter, obtains filtrate；
(4) by filtrate temperature is 40-60 DEG C, absolute pressure is that 0.1-0.2MPa is concentrated in vacuo to soluble solid and contains
50-65Brix is measured, concentrate is obtained；
(5) by concentrate carry out ultra high temperature short time sterilization to get.
The revolving speed of the mashing is 300-800 revs/min.
The filter sizes of the plate filter are 0.5-1.5 μm, filter pressure 0.1-0.3MPa.
The temperature of the ultra high temperature short time sterilization is 120-130 DEG C, time 2-6s.
The anioxidant phytochemicals is garlic total saponin and/or gardenoside antioxidant.Further, the plant antioxygen
Agent is garlic total saponin, gardenoside antioxidant is 1:(0.4-0.6 in mass ratio) mixture.
Silkworm chrysalis is the drying pupa of Bombycidae insect silkworm Bymbyx mori (Linnaeus).By being taken in the silk cocoon after filature
Out, dry or low temperature under dry.Chinese medicine thinks that silkworm chrysalis is sweet natured, has wind-dispelling, invigorating the spleen, only quenches one's thirst, tranquillizing the mind by relieving convulsion, strengthening the essence
It is supporing yang and other effects.Prescriptions Worth Thousand Gold for Emergencies says its " strengthening the essence gas, strong man Yang Dao, control and let out essence ".Compendium of Material Medica is recorded: " for end
Infantile emaciation is controlled in drink-service, and long flesh is brought down a fever, and removes roundworm；Juice drink is decocted, is only quenched one's thirst ".Pharmacological research shows silkworm chrysalis to body sugar, rouge
Fat metabolism can play certain corrective action.Larva of a silkworm with batrytis pupal fat plays the role of reducing blood lipid；Pill is made with silkworm chrysalis oil purification product, uses
In treatment hypercholesterolemia, there is significant curative effect to reducing cholesterol and improving liver function.Proper amount of edible silkworm chrysalis, to hypertension,
Hyperlipidemia, chronic hepatitis and malnutritive patient have preferable adjuvant treatment efficacy.In addition, containing a kind of broad immune in silkworm chrysalis
Substance has special efficacy to cancer.It is reported that the states such as Japan have produced alpha-interferon from silkworm chrysalis, it is clinically used for resisting
Cancer treatment.Pupa albumen is the protein and peptide extracted from silkworm chrysalis with bioengineering and zymolysis technique.Containing abundant
Protein and a variety of amino acid, purity is 98% or so, and for activity rate 97.7% or more, dissolubility and digestive utilization ratio are high,
The without side-effects, no dependence of safety, can effectively improve leucocyte level in human body, to improve immune function of human body, delay people
Body function aging, especially suitable operating pressure is big, have a delicate constitution, resistance is poor, recovery, middle old man and pregnant and lying-in women etc. are sub- strong after being ill
Kang Renqun is edible.
The anti-oxidant pupa albumen is prepared by the following method: by silkworm chrysalis temperature be 50-70 DEG C, absolute pressure 100-
200Pa dries 20-50h, crushed 10-50 mesh, obtains dried silkworm chrysalis meal；By dried silkworm chrysalis meal and 75-85wt% ethanol water with matter
Then amount is than using 300-900 mesh filter-cloth filtering, obtaining degreased pupa powder to be ultrasonically treated 30-90min after 1:(3-8) mixing；It will
Degreased pupa powder is 1:(15-35 with mass ratio with water) it is uniformly mixed and is placed on fine grinding 2-8min in colloid mill and obtains fine grinding liquid,
Fine grinding liquid 0.1-0.5mol/L sodium hydrate aqueous solution is adjusted into pH to 7.2-8, adds degreased pupa powder weight 1-2%'s
Alkali protease, the papain of degreased pupa powder weight 1-2% are uniformly mixed, in 45-60 DEG C of temperature, revolving speed 100-300
Rev/min stirring enzymatic hydrolysis 1-5h obtain enzymolysis liquid；Enzymolysis liquid is warming up to 90-100 DEG C of heat preservation 8-18min enzyme deactivation to live, enzyme is added
Solve the pomegranate peel polyphenol of the glucose of liquid weight 4-7%, enzymolysis liquid weight 2-5% turn in 75-95 DEG C of temperature, revolving speed 100-300/
Minute stirring 2-5h obtains reaction solution；Reaction solution is centrifuged off precipitating, the hollow fibre for being then 2000-8000Da with membrane aperture
Tie up film ultrafiltration, by ultrafiltrate be freeze-dried to get.
The ultrasonic power of the ultrasonic treatment is 250-450W, supersonic frequency 25-45kHz.
The revolving speed of the centrifuge separation is 5000-9000 revs/min, time 20-40min.
The temperature of the ultrafiltration is 15-25 DEG C, pressure 0.1-0.2MPa.
The present invention also provides a kind of health care blueberry concentrates, by the production technology preparation of above-mentioned health care blueberry concentrate
At.
The beneficial effects of the present invention are:
Health care blueberry concentrate of the present invention, it is in good taste, the smell of fruits is very sweet, flavor is aromatic, sweet and sour taste, lead in process
Cross in terms of control processing factors and anti-oxidant treatment two and reduce the degradation loss of blueberry nutrient element, remain the nutrition of blueberry with
Functional component, promotes product quality, long-term drinking, have improve the immunity of the human body, beauty, anti-aging, anti-cancer and other effects.
Specific embodiment
Technical solution of the present invention is further described combined with specific embodiments below.
Be described below using raw material: beater is beating for the model KL-150 that Ke Li Machinery Co., Ltd. in Zhucheng provides
Pulp grinder.Plate filter is the stainless steel sheet frame mistake for the model SHF-150 that Guangzhou Feng Yuan chemical machinery Co., Ltd provides
Filter, filter sizes are 0.8 μm, filter pressure 0.15MPa.Pomegranate peel polyphenol is according to application No. is 201210530634.9
In Chinese patent prepared by method shown in embodiment 2.Colloid mill is the type that hundred open country Li Shilong light equipment Co., Ltd of Zhejiang provides
Number be JML-50 colloid mill, revolving speed 2800r/min.Alkali protease is what Han Hong Science and Technology Co., Ltd. in Shanghai provided
Enzyme activity is the alkali protease of 100000U/g.Papain is the enzyme activity that Wei Xing Biotechnology Co., Ltd in Hunan provides
The papain of 100,000 U/g of power.Silkworm chrysalis is the fresh quick-frozen silkworm chrysalis that Gaozhou City Guangzhou-Hongkong food product refrigeration Co., Ltd provides.Garlic
Total saposins are prepared according to method shown in embodiment 1 in the Chinese patent application No. is 200910104250.9.Gardenoside is anti-oxidant
Agent is prepared according to method shown in embodiment 1 in the Chinese patent application No. is 201611013179.X.Blueberry is Sichuan cotton clothes agriculture
The kind that husband's agricultural science and technology Co., Ltd provides is the blueberry of cotton clothes farmer.
Embodiment 1
The production technology of health care blueberry concentrate, comprising the following steps:
(1) blueberry is washed with water completely, temperature is 28 DEG C, relative humidity is to place 3h under 60% environment to drain；
(2) taking the blueberry 10kg after draining, pure water 90kg to be added in beater in temperature is 2 DEG C of mashing 4 minutes, is obtained
Slurries；
(3) slurries are filtered using plate filter, obtains filtrate；
(4) by filtrate temperature is 50 DEG C, absolute pressure is that 0.15MPa is concentrated in vacuo to soluble solid content
60Brix obtains concentrate；
(5) it is 121 DEG C of insulated sterilizing 4s in temperature by concentrate, is then that 12 DEG C/s is quickly cooled to 30 with cooling rate
DEG C to get health care blueberry concentrate.
The revolving speed of the mashing is 600 revs/min.
The filter sizes of the plate filter are 0.8 μm, filter pressure 0.15MPa.
Embodiment 2
The production technology of health care blueberry concentrate, comprising the following steps:
(1) blueberry is washed with water completely, temperature is 28 DEG C, relative humidity is to place 3h under 60% environment to drain；
(2) the blueberry 10kg after draining, pure water 90kg, anti-oxidant pupa albumen 0.5kg, anioxidant phytochemicals are taken
It is 2 DEG C of mashing 4 minutes that 0.15kg, which is added in beater in temperature, obtains slurries；
(3) slurries are filtered using plate filter, obtains filtrate；
(4) by filtrate temperature is 50 DEG C, absolute pressure is that 0.15MPa is concentrated in vacuo to soluble solid content
60Brix obtains concentrate；
(5) it is 121 DEG C of insulated sterilizing 4s in temperature by concentrate, is then that 12 DEG C/s is quickly cooled to 30 with cooling rate
DEG C to get health care blueberry concentrate.
The revolving speed of the mashing is 600 revs/min.
The filter sizes of the plate filter are 0.8 μm, filter pressure 0.15MPa.
The anioxidant phytochemicals is garlic total saponin.
The anti-oxidant pupa albumen is prepared by the following method: by silkworm chrysalis temperature is 60 DEG C, absolute pressure is that 130Pa is done
Dry 30h crushed 20 meshes, obtain dried silkworm chrysalis meal；Surpass after dried silkworm chrysalis meal is mixed with 80wt% ethanol water with mass ratio for 1:5
Sonication 60min obtains degreased pupa powder then with 600 mesh filter-cloth filterings；It with mass ratio is 1:20 by degreased pupa powder and water
It is uniformly mixed and is placed on fine grinding 4min in colloid mill and obtains fine grinding liquid, fine grinding liquid 0.2mol/L sodium hydrate aqueous solution is adjusted
PH to 7.5 adds the alkali protease of degreased pupa powder weight 2%, the papain mixing of degreased pupa powder weight 1%
Uniformly, enzymolysis liquid is obtained in 180 revs/min of 55 DEG C of temperature, revolving speed stirring enzymatic hydrolysis 3h；Enzymolysis liquid is warming up to 95 DEG C of heat preservations
10min enzyme deactivation is living, and the pomegranate peel polyphenol of glucose, enzymolysis liquid weight 3% that enzymolysis liquid weight 6% is added is in temperature 90 DEG C, turn
180 revs/min of stirring 3h of speed obtain reaction solution；Reaction solution is removed bottoms with revolving speed for 8000 revs/min of centrifugation 30min to sink
It forms sediment, ultrafiltrate is carried out vacuum freeze drying, the vacuum refrigeration by the hollow-fibre membrane ultrafiltration for being then 5000Da with membrane aperture
Dry condition is control material thickness 6mm, sets pre-freezing temperature as -25 DEG C, keeps 2 after sample temperature drops to set temperature
Hour, sublimation temperature is set as 10 DEG C, and resolution temperature is 35 DEG C, absolute pressure 15pa, and drying time is 12 hours to get anti-
Aoxidize pupa albumen.
The ultrasonic power of the ultrasonic treatment is 300W, supersonic frequency 40kHz.
The temperature of the ultrafiltration is 20 DEG C, pressure 0.1MPa.
Embodiment 3
The production technology of health care blueberry concentrate, comprising the following steps:
(1) blueberry is washed with water completely, temperature is 28 DEG C, relative humidity is to place 3h under 60% environment to drain；
(2) the blueberry 10kg after draining, pure water 90kg, pupa albumen 0.5kg, anioxidant phytochemicals 0.15kg is taken to be added
It is 2 DEG C in temperature in beater to be beaten 4 minutes, obtains slurries；
(3) slurries are filtered using plate filter, obtains filtrate；
(4) by filtrate temperature is 50 DEG C, absolute pressure is that 0.15MPa is concentrated in vacuo to soluble solid content
60Brix obtains concentrate；
(5) it is 121 DEG C of insulated sterilizing 4s in temperature by concentrate, is then that 12 DEG C/s is quickly cooled to 30 with cooling rate
DEG C to get health care blueberry concentrate.
The revolving speed of the mashing is 600 revs/min.
The filter sizes of the plate filter are 0.8 μm, filter pressure 0.15MPa.
The anioxidant phytochemicals is garlic total saponin.
The pupa albumen is prepared by the following method: by silkworm chrysalis temperature is 60 DEG C, absolute pressure is the dry 30h of 130Pa,
It crushed 20 meshes, obtain dried silkworm chrysalis meal；It is ultrasonically treated after dried silkworm chrysalis meal is mixed with 80wt% ethanol water with mass ratio for 1:5
60min obtains degreased pupa powder then with 600 mesh filter-cloth filterings；Degreased pupa powder is mixed with mass ratio for 1:20 with water
It is even to be placed on fine grinding 4min in colloid mill and obtain fine grinding liquid, by fine grinding liquid 0.2mol/L sodium hydrate aqueous solution adjust pH to
7.5, the papain mixing of the alkali protease, degreased pupa powder weight 1% that add degreased pupa powder weight 2% is equal
It is even, enzymolysis liquid is obtained in 180 revs/min of 55 DEG C of temperature, revolving speed stirring enzymatic hydrolysis 3h；Enzymolysis liquid is warming up to 95 DEG C of heat preservation 10min
Enzyme deactivation is living, enzyme deactivation enzymolysis liquid living is carried out vacuum freeze drying, the condition of the vacuum freeze drying is control material thickness
6mm, sets pre-freezing temperature as -25 DEG C, kept after sample temperature drops to set temperature 2 it is small when, set sublimation temperature as 10 DEG C,
Resolution temperature is 35 DEG C, absolute pressure 15pa, and drying time is 12 hours to get pupa albumen.
The ultrasonic power of the ultrasonic treatment is 300W, supersonic frequency 40kHz.
The temperature of the ultrafiltration is 20 DEG C, pressure 0.1MPa.
Embodiment 4
The production technology of health care blueberry concentrate, comprising the following steps:
(1) blueberry is washed with water completely, temperature is 28 DEG C, relative humidity is to place 3h under 60% environment to drain；
(2) the blueberry 10kg after draining, pure water 90kg, anti-oxidant pupa albumen 0.5kg, anioxidant phytochemicals are taken
It is 2 DEG C of mashing 4 minutes that 0.15kg, which is added in beater in temperature, obtains slurries；
(3) slurries are filtered using plate filter, obtains filtrate；
(4) by filtrate temperature is 50 DEG C, absolute pressure is that 0.15MPa is concentrated in vacuo to soluble solid content
60Brix obtains concentrate；
(5) it is 121 DEG C of insulated sterilizing 4s in temperature by concentrate, is then that 12 DEG C/s is quickly cooled to 30 with cooling rate
DEG C to get health care blueberry concentrate.
The revolving speed of the mashing is 600 revs/min.
The filter sizes of the plate filter are 0.8 μm, filter pressure 0.15MPa.
The anioxidant phytochemicals is garlic total saponin.
The anti-oxidant pupa albumen is prepared by the following method: by silkworm chrysalis temperature is 60 DEG C, absolute pressure is that 130Pa is done
Dry 30h crushed 20 meshes, obtain dried silkworm chrysalis meal；Surpass after dried silkworm chrysalis meal is mixed with 80wt% ethanol water with mass ratio for 1:5
Sonication 60min obtains degreased pupa powder then with 600 mesh filter-cloth filterings；It with mass ratio is 1:20 by degreased pupa powder and water
It is uniformly mixed and is placed on fine grinding 4min in colloid mill and obtains fine grinding liquid, fine grinding liquid 0.2mol/L sodium hydrate aqueous solution is adjusted
PH to 7.5 adds the alkali protease of degreased pupa powder weight 2%, the papain mixing of degreased pupa powder weight 1%
Uniformly, enzymolysis liquid is obtained in 180 revs/min of 55 DEG C of temperature, revolving speed stirring enzymatic hydrolysis 3h；Enzymolysis liquid is warming up to 95 DEG C of heat preservations
10min enzyme deactivation is living, and the glucose that enzymolysis liquid weight 6% is added is reacted in 180 revs/min of 90 DEG C of temperature, revolving speed stirring 3h
Liquid；Reaction solution is removed into bottom precipitations with revolving speed for 8000 revs/min of centrifugation 30min, is then in 5000Da with membrane aperture
Ultrafiltrate is carried out vacuum freeze drying by empty fiber membrane ultrafiltration, and the condition of the vacuum freeze drying is control material thickness
6mm, sets pre-freezing temperature as -25 DEG C, kept after sample temperature drops to set temperature 2 it is small when, set sublimation temperature as 10 DEG C,
Resolution temperature is 35 DEG C, absolute pressure 15pa, and drying time is 12 hours to get anti-oxidant pupa albumen.
The ultrasonic power of the ultrasonic treatment is 300W, supersonic frequency 40kHz.
The temperature of the ultrafiltration is 20 DEG C, pressure 0.1MPa.
Embodiment 5
The production technology of health care blueberry concentrate, comprising the following steps:
(1) blueberry is washed with water completely, temperature is 28 DEG C, relative humidity is to place 3h under 60% environment to drain；
(2) the blueberry 10kg after draining, pure water 90kg, anti-oxidant pupa albumen 0.5kg, anioxidant phytochemicals are taken
It is 2 DEG C of mashing 4 minutes that 0.15kg, which is added in beater in temperature, obtains slurries；
(3) slurries are filtered using plate filter, obtains filtrate；
(4) by filtrate temperature is 50 DEG C, absolute pressure is that 0.15MPa is concentrated in vacuo to soluble solid content
60Brix obtains concentrate；
(5) it is 121 DEG C of insulated sterilizing 4s in temperature by concentrate, is then that 12 DEG C/s is quickly cooled to 30 with cooling rate
DEG C to get health care blueberry concentrate.
The revolving speed of the mashing is 600 revs/min.
The filter sizes of the plate filter are 0.8 μm, filter pressure 0.15MPa.
The anioxidant phytochemicals is gardenoside antioxidant.
The anti-oxidant pupa albumen is prepared by the following method: by silkworm chrysalis temperature is 60 DEG C, absolute pressure is that 130Pa is done
Dry 30h crushed 20 meshes, obtain dried silkworm chrysalis meal；Surpass after dried silkworm chrysalis meal is mixed with 80wt% ethanol water with mass ratio for 1:5
Sonication 60min obtains degreased pupa powder then with 600 mesh filter-cloth filterings；It with mass ratio is 1:20 by degreased pupa powder and water
It is uniformly mixed and is placed on fine grinding 4min in colloid mill and obtains fine grinding liquid, fine grinding liquid 0.2mol/L sodium hydrate aqueous solution is adjusted
PH to 7.5 adds the alkali protease of degreased pupa powder weight 2%, the papain mixing of degreased pupa powder weight 1%
Uniformly, enzymolysis liquid is obtained in 180 revs/min of 55 DEG C of temperature, revolving speed stirring enzymatic hydrolysis 3h；Enzymolysis liquid is warming up to 95 DEG C of heat preservations
10min enzyme deactivation is living, and the pomegranate peel polyphenol of glucose, enzymolysis liquid weight 3% that enzymolysis liquid weight 6% is added is in temperature 90 DEG C, turn
180 revs/min of stirring 3h of speed obtain reaction solution；Reaction solution is removed bottoms with revolving speed for 8000 revs/min of centrifugation 30min to sink
It forms sediment, ultrafiltrate is carried out vacuum freeze drying, the vacuum refrigeration by the hollow-fibre membrane ultrafiltration for being then 5000Da with membrane aperture
Dry condition is control material thickness 6mm, sets pre-freezing temperature as -25 DEG C, keeps 2 after sample temperature drops to set temperature
Hour, sublimation temperature is set as 10 DEG C, and resolution temperature is 35 DEG C, absolute pressure 15pa, and drying time is 12 hours to get anti-
Aoxidize pupa albumen.
The ultrasonic power of the ultrasonic treatment is 300W, supersonic frequency 40kHz.
The temperature of the ultrafiltration is 20 DEG C, pressure 0.1MPa.
Embodiment 6
The production technology of health care blueberry concentrate, comprising the following steps:
(1) blueberry is washed with water completely, temperature is 28 DEG C, relative humidity is to place 3h under 60% environment to drain；
(2) take the blueberry 10kg after draining, pure water 90kg, anti-oxidant pupa albumen 0.5kg, garlic total saponin 0.1kg,
It is 2 DEG C of mashing 4 minutes that gardenoside antioxidant 0.05kg, which is added in beater in temperature, obtains slurries；
(3) slurries are filtered using plate filter, obtains filtrate；
(4) by filtrate temperature is 50 DEG C, absolute pressure is that 0.15MPa is concentrated in vacuo to soluble solid content
60Brix obtains concentrate；
(5) it is 121 DEG C of insulated sterilizing 4s in temperature by concentrate, is then that 12 DEG C/s is quickly cooled to 30 with cooling rate
DEG C to get health care blueberry concentrate.
The revolving speed of the mashing is 600 revs/min.
The filter sizes of the plate filter are 0.8 μm, filter pressure 0.15MPa.
The anti-oxidant pupa albumen is prepared by the following method: by silkworm chrysalis temperature is 60 DEG C, absolute pressure is that 130Pa is done
Dry 30h crushed 20 meshes, obtain dried silkworm chrysalis meal；Surpass after dried silkworm chrysalis meal is mixed with 80wt% ethanol water with mass ratio for 1:5
Sonication 60min obtains degreased pupa powder then with 600 mesh filter-cloth filterings；It with mass ratio is 1:20 by degreased pupa powder and water
It is uniformly mixed and is placed on fine grinding 4min in colloid mill and obtains fine grinding liquid, fine grinding liquid 0.2mol/L sodium hydrate aqueous solution is adjusted
PH to 7.5 adds the alkali protease of degreased pupa powder weight 2%, the papain mixing of degreased pupa powder weight 1%
Uniformly, enzymolysis liquid is obtained in 180 revs/min of 55 DEG C of temperature, revolving speed stirring enzymatic hydrolysis 3h；Enzymolysis liquid is warming up to 95 DEG C of heat preservations
10min enzyme deactivation is living, and the pomegranate peel polyphenol of glucose, enzymolysis liquid weight 3% that enzymolysis liquid weight 6% is added is in temperature 90 DEG C, turn
180 revs/min of stirring 3h of speed obtain reaction solution；Reaction solution is removed bottoms with revolving speed for 8000 revs/min of centrifugation 30min to sink
It forms sediment, ultrafiltrate is carried out vacuum freeze drying, the vacuum refrigeration by the hollow-fibre membrane ultrafiltration for being then 5000Da with membrane aperture
Dry condition is control material thickness 6mm, sets pre-freezing temperature as -25 DEG C, keeps 2 after sample temperature drops to set temperature
Hour, sublimation temperature is set as 10 DEG C, and resolution temperature is 35 DEG C, absolute pressure 15pa, and drying time is 12 hours to get anti-
Aoxidize pupa albumen.
The ultrasonic power of the ultrasonic treatment is 300W, supersonic frequency 40kHz.
The temperature of the ultrafiltration is 20 DEG C, pressure 0.1MPa.
Test case 1
The health care blueberry concentrate performance of embodiment is tested.Concrete outcome is shown in Table 1.
The clearance rate of DPPH free radical measures: using DPPH method.DPPH is accurately weighed, is configured to 0.2mmol/L DPPH's
Solution is protected from light cryo-conservation in brown bottle.Health care blueberry concentrate is diluted to 10mg/mL with deionized water, obtains sample liquid.
It takes 2mL, 10mg/mL sample liquid uniformly mixed in 2mL, 0.2mmol/L DPPH solution in test tube, is added, is protected from light standing at room temperature
After 30min, absorbance value at 517nm is measured with ultraviolet specrophotometer UV-2000 (You Nike (Shanghai) limited instrument company),
It is calculated as Ai, while measuring 2mL, 10mg/mL sample liquid and adding 2mL dehydrated alcohol, is protected from light after standing 30min at room temperature, with ultraviolet point
Light photometer UV-2000 (You Nike (Shanghai) limited instrument company) measurement absorbance value at 517nm, is calculated as Aj, and
2mL, 0.2mmol/L DPPH solution add 2mL distilled water to stand, and with ultraviolet specrophotometer UV-2000, (You Nike (Shanghai) has
Limit instrument company) measurement absorbance value at 517nm, it is calculated as Ac.The clearance rate of DPPH free radical is calculated as follows in sample: clear
Except rate=[1- (Ai-Aj)/Ac] × 100%.
Storage stability test: health care blueberry concentrate is placed in the climatic chamber that temperature is 5 DEG C, humidity is 75%
Sealing is placed 10 days, and each nutritional ingredient when measuring in health care blueberry concentrate 10 days was relative to the health care blueberry concentrate 0 day
When residual content.The anthocyanidin method of inspection: health food functional component and sanitary index inspection specification (version in 2003) second
Partial test method (12) restores the type ascorbic acid method of inspection: carrying out with reference to GB/T5009.159-2003.
Table 1: test result table
Claims (10)
1. a kind of production technology of health care blueberry concentrate, which comprises the following steps:
(1) blueberry washed with water, drained；
(2) it takes the blueberry after draining, water, anti-oxidant pupa albumen, anioxidant phytochemicals to be added in beater and be beaten, is starched
Liquid；
(3) slurries are filtered using plate filter, obtains filtrate；
(4) filter vacuum is concentrated, obtains concentrate；
(5) ultra high temperature short time sterilization.
2. a kind of production technology of health care blueberry concentrate, which comprises the following steps:
(1) blueberry washed with water, drained；
(2) the blueberry 5-15 parts by weight after draining, water 85-95 parts by weight, anti-oxidant pupa albumen 0.3-1 parts by weight, plant are taken
Antioxidant 0.05-0.35 parts by weight be added beater in temperature be 1-5 DEG C mashing 2-6 minutes, obtain slurries；
(3) slurries are filtered using plate filter, obtains filtrate；
(4) by filtrate temperature is 40-60 DEG C, absolute pressure is that 0.1-0.2MPa is concentrated in vacuo to soluble solid content
50-65Brix obtains concentrate；
(5) by concentrate carry out ultra high temperature short time sterilization to get.
3. the production technology of health care blueberry concentrate as claimed in claim 2, which is characterized in that the revolving speed of the mashing is 300-
800 revs/min.
4. the production technology of health care blueberry concentrate as claimed in claim 2, which is characterized in that the filter membrane of the plate filter
Aperture is 0.5-1.5 μm, filter pressure 0.1-0.3MPa.
5. the production technology of health care blueberry concentrate as claimed in claim 2, which is characterized in that the ultra high temperature short time sterilization
Temperature is 120-130 DEG C, time 2-6s.
6. the production technology of health care blueberry concentrate as claimed in claim 2, which is characterized in that the anioxidant phytochemicals is big
Garlic total saposins and/or gardenoside antioxidant.
7. the production technology of health care blueberry concentrate as claimed in claim 2, which is characterized in that the anti-oxidant pupa albumen by
Following methods preparation: by silkworm chrysalis temperature is 50-70 DEG C, absolute pressure is the dry 20-50h of 100-200Pa, it crushed 10-50
Mesh obtains dried silkworm chrysalis meal；With 75-85wt% ethanol water be 1:(3-8 with mass ratio by dried silkworm chrysalis meal) mix after be ultrasonically treated
Then 30-90min uses 300-900 mesh filter-cloth filtering, obtains degreased pupa powder；By degreased pupa powder and water with mass ratio for 1:
(15-35) is uniformly mixed and is placed on fine grinding 2-8min in colloid mill and obtains fine grinding liquid, by fine grinding liquid 0.1-0.5mol/L hydrogen-oxygen
Change sodium water solution and adjust pH to 7.2-8, adds alkali protease, the degreased pupa powder weight of degreased pupa powder weight 1-2%
The papain of 1-2% is uniformly mixed, and obtains enzyme in 100-300 revs/min of 45-60 DEG C of temperature, revolving speed stirring enzymatic hydrolysis 1-5h
Solve liquid；Enzymolysis liquid is warming up to 90-100 DEG C of heat preservation 8-18min enzyme deactivation to live, glucose, the enzymatic hydrolysis of enzymolysis liquid weight 4-7% is added
The pomegranate peel polyphenol of liquid weight 2-5% obtains reaction solution in 100-300 revs/min of 75-95 DEG C of temperature, revolving speed stirring 2-5h；It will
Reaction solution is centrifuged off precipitating, the hollow-fibre membrane ultrafiltration for being then 2000-8000Da with membrane aperture, ultrafiltrate is freezed dry
It is dry to get.
8. the production technology of health care blueberry concentrate as claimed in claim 7, which is characterized in that the ultrasonic function of the ultrasonic treatment
Rate is 250-450W, supersonic frequency 25-45kHz.
9. the production technology of health care blueberry concentrate as claimed in claim 7, which is characterized in that the temperature of the ultrafiltration is 15-
25 DEG C, pressure 0.1-0.2MPa.
10. a kind of health care blueberry concentrate, which is characterized in that using the concentration of health care blueberry described in any one of claim 1-9
The production technology of liquid is prepared.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910439400.5A CN110100984A (en) | 2019-05-24 | 2019-05-24 | Health care blueberry concentrate and its production technology |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910439400.5A CN110100984A (en) | 2019-05-24 | 2019-05-24 | Health care blueberry concentrate and its production technology |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN110100984A true CN110100984A (en) | 2019-08-09 |
Family
ID=67492119
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910439400.5A Pending CN110100984A (en) | 2019-05-24 | 2019-05-24 | Health care blueberry concentrate and its production technology |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110100984A (en) |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101596268A (en) * | 2009-07-03 | 2009-12-09 | 中国人民解放军第三军医大学 | Garlic total saponin is in preparation antioxidant stress injury medicine and Application in Food |
| CN107996915A (en) * | 2017-12-20 | 2018-05-08 | 彭裕民 | Blueberry pulp and its processing method |
| CN108066351A (en) * | 2016-11-18 | 2018-05-25 | 刘益 | A kind of preparation method of gardenoside antioxidant |
| CN108112837A (en) * | 2018-01-31 | 2018-06-05 | 黑河市坤鹏生物科技有限公司 | Anti-oxidant blueberry concentrate and preparation method thereof |
| CN108456707A (en) * | 2018-05-16 | 2018-08-28 | 西南大学 | A kind of preparation method of pupa albumen anti-oxidation peptide and the application of pupa albumen anti-oxidation peptide |
| CN108740626A (en) * | 2018-06-22 | 2018-11-06 | 郑州艾维恩佐生物科技有限公司 | Silkworm chrysalis fruit-vegetable juice beverage |
-
2019
- 2019-05-24 CN CN201910439400.5A patent/CN110100984A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101596268A (en) * | 2009-07-03 | 2009-12-09 | 中国人民解放军第三军医大学 | Garlic total saponin is in preparation antioxidant stress injury medicine and Application in Food |
| CN108066351A (en) * | 2016-11-18 | 2018-05-25 | 刘益 | A kind of preparation method of gardenoside antioxidant |
| CN107996915A (en) * | 2017-12-20 | 2018-05-08 | 彭裕民 | Blueberry pulp and its processing method |
| CN108112837A (en) * | 2018-01-31 | 2018-06-05 | 黑河市坤鹏生物科技有限公司 | Anti-oxidant blueberry concentrate and preparation method thereof |
| CN108456707A (en) * | 2018-05-16 | 2018-08-28 | 西南大学 | A kind of preparation method of pupa albumen anti-oxidation peptide and the application of pupa albumen anti-oxidation peptide |
| CN108740626A (en) * | 2018-06-22 | 2018-11-06 | 郑州艾维恩佐生物科技有限公司 | Silkworm chrysalis fruit-vegetable juice beverage |
Non-Patent Citations (9)
| Title |
|---|
| 左振宇等: "可控酶解蚕蛹蛋白制备抗氧化活性多肽的研究", 《化学与生物工程》 * |
| 左振宇等: "蚕蛹超声辅助常温脱脂工艺条件优化", 《生物技术通报》 * |
| 张晓峰等: "《中国虫草：历史•资源•科研》", 31 January 2008, 陕西科学技术出版社 * |
| 徐国钧等: "《常用中药材品种整理和质量研究 南方协作组 第三册》", 30 November 1999, 福建科学技术出版社 * |
| 李东光: "《精细化工产品配方与工艺.（二）》", 31 January 2001, 化学工业出版社 * |
| 李健等: "双酶水解蚕蛹蛋白工艺研究", 《食品研究与开发》 * |
| 段绍斌等: "《临床疾病营养学》", 28 February 2014, 科学技术文献出版社 * |
| 马自超等: "《天然食用色素化学》", 31 January 2016, 中国轻工业出版社 * |
| 鲁珍等: "蚕蛹蛋白酶法水解及美拉德反应改良其产物风味的研究", 《食品工业科技》 * |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN107549812B (en) | A skin caring and antiaging food prepared from acerola cherry extract, Haematococcus pluvialis and fish collagen peptide, and its preparation method | |
| CN111574618B (en) | Preparation method of whitening compound protein peptidase hydrolysate, whitening compound protein peptide beverage and preparation method thereof | |
| CN103989219B (en) | A kind of blueberry compound nutritional fruit dew and processing method thereof | |
| CN111670997A (en) | Preparation method of immune-enhancing compound protein peptidase hydrolyzed liquid, immune-enhancing compound protein peptide beverage and preparation method thereof | |
| CN107802543B (en) | Roxburgh rose element skin-refreshing biological fiber mask and preparation method thereof | |
| CN105146637A (en) | Functional Ziyu Chinese yam and fruit composite juice and preparation method thereof | |
| CN107232461A (en) | A kind of processing method of purple potato blueberry composite beverage | |
| CN109363008A (en) | A kind of the whitening plant beverage and its processing method of antioxidant and anti-aging | |
| CN113332354A (en) | Anti-saccharification anti-aging fermented composition and preparation method thereof | |
| CN101375715A (en) | Nutrient powder made from chickpea and grape and preparation method thereof | |
| CN100395325C (en) | Aloe grape dry red wine and its preparation method | |
| CN107149104A (en) | Mixed fruit ferment and its production technology | |
| CN107950826A (en) | A kind of SOD small molecule solid beverages with health-care efficacy and preparation method thereof | |
| CN102578452B (en) | Skin-nourishing nutritional food | |
| CN106635644A (en) | Red dragon fruit/pomegranate composite health-preserving fruit wine and preparation method thereof | |
| CN105936866B (en) | A kind of brew method of high calcium high polyphenolic content V. amurensis wine brewing skin slag vinegar | |
| CN110279054A (en) | A kind of collagen solid beverage and preparation method thereof improving " screen flesh " | |
| CN106497722B (en) | Walnut flower pomegranate fruit wine and preparation method thereof | |
| CN112430516B (en) | Fermented raspberry wine and preparation method thereof | |
| CN104585574A (en) | Propolis soft capsule product and preparation method thereof | |
| CN110100984A (en) | Health care blueberry concentrate and its production technology | |
| CN114128812A (en) | Ready-to-drink burdock bird's nest peptide liquid compound beverage easy to digest and preparation method thereof | |
| CN106967549A (en) | Grape health medicinal liquor and preparation method thereof | |
| CN107509838A (en) | A kind of preparation method of fermented black rice tea | |
| CN112471257A (en) | Yoghourt with functions of reducing blood sugar and blood fat |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20190809 |
|
| RJ01 | Rejection of invention patent application after publication |