CN110079246A - A kind of water seep through and preparation method thereof for Sticky Note - Google Patents

A kind of water seep through and preparation method thereof for Sticky Note Download PDF

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Publication number
CN110079246A
CN110079246A CN201910334436.7A CN201910334436A CN110079246A CN 110079246 A CN110079246 A CN 110079246A CN 201910334436 A CN201910334436 A CN 201910334436A CN 110079246 A CN110079246 A CN 110079246A
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CN
China
Prior art keywords
water
sticky note
mixture
agent
minutes
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201910334436.7A
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Chinese (zh)
Inventor
林森碧
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Zhongshan Sen Sen Coating Material Co Ltd
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Zhongshan Sen Sen Coating Material Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Priority to CN201910334436.7A priority Critical patent/CN110079246A/en
Publication of CN110079246A publication Critical patent/CN110079246A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J11/00Features of adhesives not provided for in group C09J9/00, e.g. additives
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J129/00Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal, or ketal radical; Adhesives based on hydrolysed polymers of esters of unsaturated alcohols with saturated carboxylic acids; Adhesives based on derivatives of such polymers
    • C09J129/02Homopolymers or copolymers of unsaturated alcohols
    • C09J129/04Polyvinyl alcohol; Partially hydrolysed homopolymers or copolymers of esters of unsaturated alcohols with saturated carboxylic acids

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Laminated Bodies (AREA)

Abstract

The water seep through and preparation method thereof that the invention discloses a kind of for Sticky Note, it is characterised in that it includes following weight ratio: PVA45~50%, brightening agent 0.005~0.009, lotion 0.4~0.6%, curing agent 0.01~0.02%, wetting agent 0.001%, defoaming agent 0.001%, water 45~55%.Mixing requirement by certain technique, manufacture craft is simple, easy to make, and colloidality realizes that water is saturating, and manufactured glue bottom has preferable adhesion strength and cohesive force higher, keeps the creep resistance of Sticky Note excellent under long-term stress effect;It is coated in release paper and is fitted in transparent PVC or the face PP or PET, the conjugation of super Sticky Note can be achieved, the quality for substantially increasing product improves product practicability and usability, and the super water seep through fitting for being highly suitable for spray printed or single Sticky Note thoroughly uses.

Description

A kind of water seep through and preparation method thereof for Sticky Note
Technical field
The present invention relates to Sticky Note technical field, water seep through of specifically a kind of Sticky Note and preparation method thereof.
Background technique
Sticky Note is applied to:
One, the application of air brushing outdoor advertising:
Urban Transportation, subway light rail, public transit vehicle, taxi, city rapid transit, company (mechanism) vehicle, individual character are private Family's vehicle;Urban architecture glass curtain wall, retail shop's show window, convenience store doorway, the phone Room.
Two, the application of the indoor description of picture is sprayed:
Office's poster, room decorating, meeting room glass door, exhibition scene wall newspaper, the POP advertisement of sales field inside, cold drink The glass door of machine.Especially being used for advertising poster is the application side that air brushing is current very universal ad production and indoor decoration Formula can give people that good effect is presented, therefore many enterprises can select this mode to prepare advertising, individual decoration etc., because It can be used to publicize corporate image or product, while also have good decorative effect.
On decoration and advertisement, have and much need super Sticky Note, due to transparency requirement is high, not only film will be into The transparent requirement of row, in-between glue-line are also required to the saturating requirement of super water, some have reached adherency force request, again less than more beautiful The transparent cooperation decoration seen, some have reached requirement, but with film be bonded and the requirement of upper periodical is not achieved, in long-term stress It is poor to act on lower creep resistant, due to the demand of adhesion strength and cohesive force, more when in use, since product fitting is of poor quality, It cannot effectively use.
Summary of the invention
The purpose of the present invention is to provide a kind of water seep throughs and its manufacture craft for Sticky Note, to solve above-mentioned background The problem of being proposed in technology.
To achieve the above object, the invention provides the following technical scheme:
A kind of water seep through for Sticky Note, which is characterized in that including following weight ratio:
PVA45~50%, brightening agent 0.005~0.009, lotion 0.4~0.6%, curing agent 0.01~0.02%, wetting Agent 0.001%, defoaming agent 0.001%, water 45~55%.
The weight ratio include the following: PVA50%, brightening agent 0.006%, lotion 0.43%, curing agent 0.0143%, Wetting agent 0.001%, defoaming agent 0.001%, water 49.5477%.
A kind of preparation method based on the above-mentioned water seep through for Sticky Note, which comprises the following steps:
1) material is matched by a certain percentage;
2) lotion and curing agent add water and stir 5 minutes, form mixture A;
3) wetting agent and defoaming agent is added to be stirred for again 20 minutes mixture A, speed of agitator is 800 turns, forms mixture B;
4) brightening agent is mixed with water, is stirred 5 minutes using blender, 50 turns of speed of agitator are stirred 30 minutes, are mixed Close drug A;
5) intermixture A made of is added PVA and is stirred machine stirring, and 50 turns of speed of agitator are stirred 30 minutes, is mixed Object C;
6) mixture C made of uses blender to continue speed of agitator as 50 again, and is heated up to 84 DEG C, and soaking time is 90 minutes;Then 45 DEG C are cooled to, temperature-fall period speed of agitator is 30;
7) when being cooled to 45 DEG C, be put into step it is poly- 3) made of mixture B stir to form mixture D
8) mixture D uses the filter plant of 600 mesh to filter twice again, stands 6~8 hours, obtains the water that Sticky Note uses Seep through.
Compared with prior art, the beneficial effects of the present invention are:
Simple using manufacture craft of the invention, easy to make, colloidality realizes that water is saturating, and manufactured glue bottom has preferable viscous Attached power and cohesive force are higher, keep the creep resistance of Sticky Note excellent under long-term stress effect;It is coated in release paper And be fitted in transparent PVC or the face PP or PET, it can be achieved that super Sticky Note conjugation, substantially increase the quality of product, mention High product practicability and usability, the super water seep through fitting for being highly suitable for spray printed or single Sticky Note thoroughly use.
In order to explain the structural features and functions of the invention more clearly, come to carry out the present invention combined with specific embodiments below It is described in detail.
Specific embodiment
Technical solution of the present invention is described in more detail With reference to embodiment.
Embodiment 1
A kind of water seep through for Sticky Note, which is characterized in that curing degree is up to 38%, including following weight ratio:
PVA50%, brightening agent 0.006%, lotion 0.43%, curing agent 0.0143%, wetting agent 0.001%, defoaming agent 0.001%, water 49.5477%.
A kind of preparation method based on the above-mentioned water seep through for Sticky Note, which comprises the following steps:
1) material is matched by a certain percentage;
2) lotion lotion 0.43% and curing agent add water 15% to stir 5 minutes, form mixture A;
3) wetting agent and defoaming agent is added to be stirred for again 20 minutes mixture A, speed of agitator is 800 turns, forms mixture B;
4) brightening agent is mixed with water 34.5477%, is stirred 5 minutes using blender, 50 turns of speed of agitator are stirred 30 points Clock obtains mixing drug A;
5) intermixture A made of is added PVA and is stirred machine stirring, and 50 turns of speed of agitator are stirred 30 minutes, is mixed Object C;
6) mixture C made of uses blender to continue speed of agitator as 50 again, and is heated up to 84 DEG C, and soaking time is 90 minutes;Then 45 DEG C are cooled to, temperature-fall period speed of agitator is 30;
7) when being cooled to 45 DEG C, be put into step it is poly- 3) made of mixture B stir to form mixture D
8) mixture D uses the filter plant of 600 mesh to filter twice again, stands 6~8 hours, obtains the water that Sticky Note uses Seep through.
In step 3), formed mixture B, Ji Buju 6) formed mixture C, it can be achieved that super water transparent adhesive tape main body is uniformly mixed It closes, is very suitable to the Sticky Note cooperation sticking effect in later period, reaches the saturating decorative effect of super water, manufactured glue bottom has preferable Adhesion strength and cohesive force are higher.
Simple using manufacture craft of the invention, easy to make, colloidality realizes that water is saturating, and manufactured glue bottom has preferable viscous Attached power and cohesive force are higher, keep the creep resistance of Sticky Note excellent under long-term stress effect;It is coated in release paper And be fitted in transparent PVC or the face PP or PET, it can be achieved that super Sticky Note conjugation, substantially increase the quality of product, mention High product practicability and usability, the super water seep through fitting for being highly suitable for spray printed or single Sticky Note thoroughly use.
Embodiment 2
A kind of water seep through for Sticky Note, which is characterized in that curing degree is up to 39%, including following material:
PVA11.1g, brightening agent 0.138g, lotion 0.961g, curing agent 0.323g, wetting agent 0.0144g, defoaming agent 0.0073g, water 10g.
A kind of preparation method based on the above-mentioned water seep through for Sticky Note, which comprises the following steps:
1) prepare material: PVA11.1g, brightening agent 0.138g, lotion 0.961g, curing agent 0.323g, wetting agent 0.0144g, defoaming agent 0.0073g, water 10g
2) lotion 0.961g, curing agent 0.323g add water 3g to stir 5 minutes, form mixture A;
3) wetting agent 0.0144g, defoaming agent 0.0073g is added to be stirred for again 20 minutes mixture A, speed of agitator 800 Turn, forms mixture B;
4) brightening agent 0.138g is mixed with water 7g, is stirred 5 minutes using blender, 50 turns of speed of agitator are stirred 30 points Clock obtains mixing drug A;
5) intermixture A made of is added PVA11.1g and is stirred machine stirring, and 50 turns of speed of agitator are stirred 30 minutes, obtains Mixture C;
6) mixture C made of uses blender to continue speed of agitator as 50 again, and is heated up to 84 DEG C, and soaking time is 90 minutes;Then 45 DEG C are cooled to, temperature-fall period speed of agitator is 30;
7) when being cooled to 45 DEG C, be put into step it is poly- 3) made of mixture B stir to form mixture D
8) mixture D uses the filter plant of 600 mesh to filter twice again, stands 6~8 hours, obtains curing degree up to 39% The water seep through that Sticky Note uses.
In step 3), formed mixture B, Ji Buju 6) formed mixture C, it can be achieved that super water transparent adhesive tape main body is uniformly mixed It closes, is very suitable to the Sticky Note cooperation sticking effect in later period, reaches the saturating decorative effect of super water, manufactured glue bottom has preferable Adhesion strength and cohesive force are higher.
Simple using manufacture craft of the invention, easy to make, colloidality realizes that water is saturating, and manufactured glue bottom has preferable viscous Attached power and cohesive force are higher, keep the creep resistance of Sticky Note excellent under long-term stress effect;It is coated in release paper And be fitted in transparent PVC or the face PP or PET, it can be achieved that super Sticky Note conjugation, substantially increase the quality of product, mention High product practicability and usability, the pressure-sensitive glue laminating of grey for being highly suitable for spray printed or single Sticky Note thoroughly use.
Embodiment 3
A kind of water seep through for Sticky Note, which is characterized in that curing degree is up to 35%, including following weight ratio:
PVA50%, brightening agent 0.005%, lotion 0.6%, curing agent 0.02%, wetting agent 0.001%, defoaming agent 0.001%, water 49.373%.
A kind of preparation method based on the above-mentioned water seep through for Sticky Note, which comprises the following steps:
1) material is matched by a certain percentage;
2) lotion 0.6% and curing agent 0.02% plus water 14.5% stir 5 minutes, form mixture A;
3) wetting agent and defoaming agent is added to be stirred for again 20 minutes mixture A, speed of agitator is 800 turns, forms mixture B;
4) brightening agent 0.005% is mixed with water 34.873%, is stirred 5 minutes using blender, 50 turns of speed of agitator are stirred It mixes 30 minutes, obtains mixing drug A;
5) intermixture A made of is added PVA50% and is stirred machine stirring, and 50 turns of speed of agitator are stirred 30 minutes, obtains Mixture C;
6) mixture C made of uses blender to continue speed of agitator as 50 again, and is heated up to 84 DEG C, and soaking time is 90 minutes;Then 45 DEG C are cooled to, temperature-fall period speed of agitator is 30;
7) when being cooled to 45 DEG C, be put into step it is poly- 3) made of mixture B stir to form mixture D
8) mixture D uses the filter plant of 600 mesh to filter twice again, stands 6~8 hours, obtains the water that Sticky Note uses Seep through.
In step 3), formed mixture B, Ji Buju 6) formed mixture C, it can be achieved that super water transparent adhesive tape main body is uniformly mixed It closes, is very suitable to the Sticky Note cooperation sticking effect in later period, reaches the saturating decorative effect of super water, manufactured glue bottom has preferable Adhesion strength and cohesive force are higher.
Simple using manufacture craft of the invention, easy to make, colloidality realizes that water is saturating, and manufactured glue bottom has preferable viscous Attached power and cohesive force are higher, keep the creep resistance of Sticky Note excellent under long-term stress effect;It is coated in release paper And be fitted in transparent PVC or the face PP or PET, it can be achieved that super Sticky Note conjugation, substantially increase the quality of product, mention High product practicability and usability, the pressure-sensitive glue laminating of grey for being highly suitable for spray printed or single Sticky Note thoroughly use.
Better embodiment of the invention is explained in detail above, but the present invention is not limited to above-mentioned embodiment party Formula within the knowledge of one of ordinary skill in the art can also be without departing from the purpose of the present invention It makes a variety of changes.

Claims (3)

1. a kind of water seep through for Sticky Note, which is characterized in that including following weight ratio:
PVA45~50%, brightening agent 0.005~0.009, lotion 0.4~0.6%, curing agent 0.01~0.02%, wetting agent 0.001%, defoaming agent 0.001%, water 45~55%.
2. a kind of water seep through for Sticky Note according to claim 1, which is characterized in that including following weight ratio: PVA50%, brightening agent 0.006%, lotion 0.43%, curing agent 0.0143%, wetting agent 0.001%, defoaming agent 0.001%, Water 49.5477%.
3. a kind of preparation method based on any water seep through for Sticky Note of claim 1~2, which is characterized in that The following steps are included:
1) material is matched by a certain percentage;
2) lotion and curing agent add water and stir 5 minutes, form mixture A;
3) wetting agent and defoaming agent is added to be stirred for again 20 minutes mixture A, speed of agitator is 800 turns, forms mixture B;
4) brightening agent is mixed with water, is stirred 5 minutes using blender, 50 turns of speed of agitator are stirred 30 minutes, and mixing drug is obtained A;
5) intermixture A made of is added PVA and is stirred machine stirring, and 50 turns of speed of agitator are stirred 30 minutes, obtains mixture C;
6) mixture C made of uses blender to continue speed of agitator as 50 again, and is heated up to 84 DEG C, and soaking time is 90 points Clock;Then 45 DEG C are cooled to, temperature-fall period speed of agitator is 30;
7) when being cooled to 45 DEG C, be put into step it is poly- 3) made of mixture B stir to form mixture D
8) mixture D uses the filter plant of 600 mesh to filter twice again, stands 6~8 hours, obtains the water seep through that Sticky Note uses.
CN201910334436.7A 2019-04-24 2019-04-24 A kind of water seep through and preparation method thereof for Sticky Note Pending CN110079246A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910334436.7A CN110079246A (en) 2019-04-24 2019-04-24 A kind of water seep through and preparation method thereof for Sticky Note

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201910334436.7A CN110079246A (en) 2019-04-24 2019-04-24 A kind of water seep through and preparation method thereof for Sticky Note

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Publication Number Publication Date
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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103694930A (en) * 2013-12-20 2014-04-02 陕西科技大学 Method for preparing waterproof polyvinyl alcohol trademark adhesive
CN105349069A (en) * 2015-12-04 2016-02-24 常德市雄鹰科技有限责任公司 Water-based back glue for transfer paper and preparation method of water-based back glue
CN106753064A (en) * 2016-12-21 2017-05-31 李晓慧 Modified water-tolerant polyvinyl alcohol trade mark adhesive and preparation method thereof
CN106833439A (en) * 2017-03-14 2017-06-13 武汉市华林粘合剂有限公司 A kind of environmentally friendly paper tube adhesive and preparation method thereof
CN107488419A (en) * 2017-09-08 2017-12-19 武汉市华林粘合剂有限公司 One kind pastes wallpaper wall paper adhesive and preparation method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103694930A (en) * 2013-12-20 2014-04-02 陕西科技大学 Method for preparing waterproof polyvinyl alcohol trademark adhesive
CN105349069A (en) * 2015-12-04 2016-02-24 常德市雄鹰科技有限责任公司 Water-based back glue for transfer paper and preparation method of water-based back glue
CN106753064A (en) * 2016-12-21 2017-05-31 李晓慧 Modified water-tolerant polyvinyl alcohol trade mark adhesive and preparation method thereof
CN106833439A (en) * 2017-03-14 2017-06-13 武汉市华林粘合剂有限公司 A kind of environmentally friendly paper tube adhesive and preparation method thereof
CN107488419A (en) * 2017-09-08 2017-12-19 武汉市华林粘合剂有限公司 One kind pastes wallpaper wall paper adhesive and preparation method thereof

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
周丽等: "耐水聚乙烯醇商标胶的制备与性能研究 ", 《中国胶粘剂》 *
石松林等: "改性聚乙烯醇商标胶的研制 ", 《粘接》 *

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Application publication date: 20190802

RJ01 Rejection of invention patent application after publication