CN110051745A - A kind of mellowness steams the concocting method of dried orange peel - Google Patents
A kind of mellowness steams the concocting method of dried orange peel Download PDFInfo
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- CN110051745A CN110051745A CN201910474309.7A CN201910474309A CN110051745A CN 110051745 A CN110051745 A CN 110051745A CN 201910474309 A CN201910474309 A CN 201910474309A CN 110051745 A CN110051745 A CN 110051745A
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- orange peel
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- mellowness
- dried orange
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/75—Rutaceae (Rue family)
- A61K36/752—Citrus, e.g. lime, orange or lemon
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/17—Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting
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Abstract
The invention belongs to Chinese medicine preparation technical fields, and in particular to a kind of mellowness steams the concocting method of dried orange peel.The present invention first cleans fresh orange peel, is cut into piece, impregnates 15-25 min in protection liquid, takes out；Then by orange peel being transferred in Chinese medicine steaming machine after immersion, vapor steams 15-25 min, is freeze-dried 1-2h after natural cooling, then through high temperature steaming-freeze-drying process 2-3 times；Finally resulting orange peel is put into steam stove, 20-25 min is steamed using alcohol-water steam, is freeze-dried and steams dried orange peel up to mellowness.It is high through dried orange peel active component content prepared by the present invention and mellowness is dense, it is best in quality.
Description
Technical field
The invention belongs to Chinese medicine preparation technical fields, and in particular to a kind of mellowness steams the concocting method of dried orange peel.
Background technique
Dried orange peel is from rutaceae orange and its dry mature skin of variety.Dried orange peel also known as orange peel, warm-natured,
It is bitter, pungent, enter spleen, lung channel has regulating qi-flowing for strengthening spleen, and eliminating dampness and eliminating phlegm function is used for chest gastral cavity turgor, and deficiency of food is vomited and diarrhoea, cough ant phlegm
Equal diseases.Main active in dried orange peel is flavonoids and volatile oil, is shown in epidemic disease investigation report in recent years, yellow
Ketone compounds can blood pressure lowering, reducing blood lipid prevention and improves cardiovascular and cerebrovascular disease, and volatile oil active constituent can remove body
Interior free radical, the effects of playing anti-oxidant and anti-aging.
Dried orange peel is used as traditional medicinal material, with a long history, and processing procedure document report is more, according to practical application
Difference, concocting method are also different.Traditional concocting method has more than 20 kinds of salt system, frying, vinegar system, bran etc.. 2010
The concocting method recorded in year version " Chinese Pharmacopoeia " are as follows: remove impurity, shower water moisturizes, and chopping is dried in the shade.It is in all parts of the country at present
Area's dried orange peel concocting method is taken clean after wash profit, chopping is raw to be used.But the dried orange peel processed in this way is pungent, eating mouth feel is bad,
Processing appropriate can increase its effect, mitigate dry property.Such as a kind of (the processing side of Chinese medicine dried orange peel 102085262 A of patent CN
Method) the bored profit of one kind and the method steamed are provided to improve the pungent dry of dried orange peel.But method is significantly reduced in dried orange peel and is volatilized
The content of oils active constituent, thus the effect of will affect dried orange peel；A kind of 103989781 A of patent CN (fragrant old of efficient speed
Skin concocting method) it is bored using wine, it steams pungent dry to remove with the method for long-term preservation, improves the mellowness of dried orange peel.This method is same
It eliminates a large amount of volatile active constituents in dried orange peel and the resting period is long, product quality is difficult to control.Therefore, exploitation is able to maintain
Dried orange peel active constituent improves the concocting method of dried orange peel mouthfeel simultaneously, has great importance to dried orange peel market value is improved.
Summary of the invention
In order to keep dried orange peel active constituent while improve dried orange peel mouthfeel, the present invention provides a kind of processing side of mellowness steaming dried orange peel
Method impregnates dried orange peel using the protection liquid of safety edible, avoids wandering away for dried orange peel volatile component；Using steaming and freeze
Dry mode improves the inversion quantity of aurantiamarin；The mellowness and mouthfeel for improving dried orange peel are finally steamed using ethyl alcohol.
In order to achieve the above-mentioned object of the invention, the invention provides the following technical scheme:
A kind of mellowness steams the concocting method of dried orange peel, which is characterized in that comprises the steps of:
(1) after cleaning fresh orange peel, it is cut into piece, 15-25 min is impregnated in protection liquid, takes out;
(2) orange peel after immersion is transferred in Chinese medicine steaming machine, vapor steams 15-25 min, and natural cooling is freeze-dried 1-
2 h, then through high temperature steaming-freeze-drying process 2-3 times；
(3) step (2) resulting orange peel is put into steam stove, after steaming 20-25 min using alcohol-water steam, freeze-drying is
It obtains mellowness and steams dried orange peel.
Preferably, size is not more than the cm of 2 cm × 2 after fresh orange peel shearing as described in step (1).
Preferably, protection liquid as described in step (1) is made of water, glycerol, sodium chloride, wherein glycerol, sodium chloride it is dense
Degree is respectively 2-4 g/mL and 0.1-0.15 g/mL.
Preferably, temperature is 35-45 DEG C when immersion as described in step (1).
Preferably, vacuum degree described in step (2) is 1-10Pa, and temperature is -55 to -70 DEG C.
Preferably, the concentration of ethyl alcohol is 20-35% when alcohol-water steam described in step (3) steams.
Compared with prior art, the concocting method that a kind of mellowness described in this patent steams dried orange peel has the advantages that
Using the protection liquid of safety edible dried orange peel is impregnated, dried orange peel volatile component when processing is avoided to wander away；Using steaming
The inversion quantity for improving aurantiamarin with the mode of freeze-drying also further avoids wandering away for volatile component；It is steamed using ethyl alcohol
Improve the mellowness and mouthfeel of dried orange peel.Through dried orange peel prepared by the present invention, active component content is high and mellowness is dense, best in quality.
Specific embodiment
Below with reference to embodiment, the present invention is described in further detail, but embodiment is not to the technology of the present invention
The restriction of scheme, it is all based on present invention teach that made variation or equivalent replacement, is within the scope of protection of the invention.
Embodiment 1
A kind of mellowness steams the concocting method of dried orange peel, which is characterized in that comprises the steps of:
(1) fresh orange peel is cleaned, is cut into no more than the cm piece of 2 cm × 2, in the glycerol and 0.12 g/mL chlorine for containing 3 g/mL
Change in sodium protection liquid and impregnate 20 min, takes out;
(2) orange peel after immersion is transferred in Chinese medicine steaming machine, vapor steams 18 min, and -65 DEG C of freezings are dry after natural cooling
Dry 1.5 h, then through high temperature steaming-freeze-drying process 2 times；
(3) step (2) resulting orange peel is put into steam stove, after steaming 25 min using 30% alcohol-water steam, freeze-drying is
It obtains mellowness and steams dried orange peel.
Embodiment 2
A kind of mellowness steams the concocting method of dried orange peel, which is characterized in that comprises the steps of:
(1) it after cleaning fresh orange peel, is cut into no more than the cm piece of 2 cm × 2, in the glycerol and 0.10 g/mL for containing 2.5 g/mL
25 min are impregnated in sodium chloride protection liquid, are taken out;
(2) orange peel after immersion is transferred in Chinese medicine steaming machine, vapor steams 20 min, and -55 DEG C of freezings are dry after natural cooling
Dry 1.5 h, then through high temperature steaming-freeze-drying process 3 times；
(3) step (2) resulting orange peel is put into steam stove, after steaming 25min using 25% alcohol-water steam, is freeze-dried to obtain the final product
Mellowness steams dried orange peel.
Embodiment 3
A kind of mellowness steams the concocting method of dried orange peel, which is characterized in that comprises the steps of:
(1) it after cleaning fresh orange peel, is cut into no more than the cm piece of 2 cm × 2, in the glycerol and 0.13 g/mL for containing 3 g/mL
20 min are impregnated in sodium chloride protection liquid, are taken out;
(2) orange peel after immersion is transferred in Chinese medicine steaming machine, vapor steams 22 min, and -60 DEG C of freezings are dry after natural cooling
Dry 1.5 h, then through high temperature steaming-freeze-drying process 3 times；
(3) step (2) resulting orange peel is put into steam stove, after steaming 20 min using 35% alcohol-water steam, freeze-drying is
It obtains mellowness and steams dried orange peel.
Comparative example 1 (102085262 A method of patent CN)
(1) it after cleaning fresh orange peel, is cut into no more than 2cm × 2cm piece；
(2) orange peel piece is moved in Chinese medicine steaming machine, 2 times of Quality of Pericarpium of water, the bored profit 2h of room temperature, under the conditions of 90 DEG C is added
75min is steamed, takes out, dries, chopping is to get dried orange peel.
103989781 A of comparative example 2(CN)
(1) fresh orange peel is cleaned, is dried, is cut into no more than 2cm × 2cm piece；
(2) white wine is sprayed into orange peel two sides with sprayer, orange peel piece is moved in Chinese medicine steaming machine, be added 2 times of Quality of Pericarpium
Water, 40 DEG C of bored profit 1h, steams 5min under the conditions of 100 DEG C, takes out, dries, be sealed 1 year to get dried orange peel.
Comparative example 3(Chinese Pharmacopoeia concocting method)
(1) it after cleaning fresh orange peel, is cut into no more than 2cm × 2cm piece；
(2) water moves back the wetting of orange peel piece into Chinese medicine steaming machine, and the bored profit 2h of room temperature takes out, dries, chopping is to get dried orange peel.
The unused protection liquid of comparative example 4(impregnates)
(1) it after cleaning fresh orange peel, is cut into no more than 2cm × 2cm piece；
(2) orange peel is transferred in Chinese medicine steaming machine, vapor steams 22 min, -60 DEG C of 1.5 h of freeze-drying after natural cooling
Afterwards；Again through high temperature steaming-freeze-drying process 3 times；
(3) step (2) resulting orange peel is put into steam stove, after steaming 20 min using 35% alcohol-water steam, freeze-drying is
It obtains mellowness and steams dried orange peel.
Dried orange peel obtained by embodiment 1-3 and comparative example 1-4 carries out constituent analysis
Content of hesperidin measurement: referring to the method for 2015 editions Chinese Pharmacopoeias, dried orange peel test solution is prepared, using Chinese Pharmacopoeia height
Effect liquid phase chromatogram method (general rule 0512) measurement, and calculate the content of aurantiamarin.
Volatile active: dried orange peel is crushed, and sieves to obtain tangerine peel powder.Accurately weigh 50 g tangerine peel powders in a round bottom flask,
100 mL petroleum ethers are added, twice, combined extract is cooling, and filtering, filtrate decompression is concentrated into paste for heating and refluxing extraction,
Medicinal extract and dehydrated alcohol are mixed with the ratio of 1 ︰ 10 of volume ratio, stirs evenly, 4 h is freezed at -20 DEG C；It is filtered with filter paper,
Filtrate decompression concentration, obtains dried orange peel volatile extract；Extract is analyzed using gas chromatography-mass spectrum.Chromatostrip
Part: HP-INNOWAX capillary chromatographic column (0.25 μm of the μ m of 30 m × 250), carrier gas He, flow velocity are 1.0 mL/
min；Using temperature programming mode, 50 DEG C of initial temperature, 5 min is kept, are raised to 160 DEG C with 2 DEG C/min of speed,
5 min are kept, then are raised to 250 DEG C with 12 DEG C/min, keep 5 min.250 DEG C of injector temperature, split ratio 40
: 1.Mass Spectrometry Conditions: full scan type collection signal, ionization source EI, 70 eV of ionizing energy are used；Interface temperature 280
DEG C, 200 DEG C of ion source temperature, 150 DEG C of level four bars temperature, scanning quality range 35 amu~500 amu.
The type and total content of Determination of hesperidin in pericarpium citri reticulatae obtained by 1. embodiment 1-6 of table and volatile component.
From table 1 it follows that the content of aurantiamarin is significantly improved in dried orange peel after steaming, and using protection
After liquid protection, the type and content of volatile active are all significantly improved in dried orange peel.Concocting method of the invention, system
The dried orange peel active component content obtained is high.
For the ordinary skill in the art, specific embodiment is only exemplarily described the present invention,
Obviously the present invention specific implementation is not subject to the restrictions described above, as long as use the inventive concept and technical scheme of the present invention into
The improvement of capable various unsubstantialities, or not improved the conception and technical scheme of the invention are directly applied to other occasions
, it is within the scope of the present invention.
Claims (6)
1. the concocting method that a kind of mellowness steams dried orange peel, which is characterized in that comprise the steps of:
(1) after cleaning fresh orange peel, it is cut into piece, 15-25 min is impregnated in protection liquid, takes out；
(2) orange peel after immersion is transferred in Chinese medicine steaming machine, vapor steams 15-25 min, and natural cooling is freeze-dried 1-
2 h, then through high temperature steaming-freeze-drying process 2-3 times；
(3) step (2) resulting orange peel is put into steam stove, after steaming 20-25 min using alcohol-water steam, freeze-drying is
It obtains mellowness and steams dried orange peel.
2. the concocting method that a kind of mellowness according to claim 1 steams dried orange peel, it is characterised in that as described in step (1) fresh
Size is not more than the cm of 2 cm × 2 after orange peel shearing.
3. the concocting method that a kind of mellowness according to claim 1 steams dried orange peel, it is characterised in that guarantor as described in step (1)
Shield liquid be made of water, glycerol, sodium chloride, wherein glycerol, sodium chloride concentration be respectively 2-4 g/mL and 0.1-0.15 g/mL.
4. the concocting method that a kind of mellowness according to claim 1 steams dried orange peel, it is characterised in that leaching as described in step (1)
Temperature is 35-45 DEG C when bubble.
5. the concocting method that a kind of mellowness according to claim 1 steams dried orange peel, it is characterised in that true described in step (2)
Reciprocal of duty cycle is 1-10 Pa, and temperature is -55 to -70 DEG C.
6. the concocting method that a kind of mellowness according to claim 1 steams dried orange peel, it is characterised in that second described in step (3)
The concentration of ethyl alcohol is 20-35% when alcohol-vapor steams.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910474309.7A CN110051745A (en) | 2019-06-03 | 2019-06-03 | A kind of mellowness steams the concocting method of dried orange peel |
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| CN201910474309.7A CN110051745A (en) | 2019-06-03 | 2019-06-03 | A kind of mellowness steams the concocting method of dried orange peel |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113057991A (en) * | 2021-04-09 | 2021-07-02 | 建昌帮药业有限公司 | Steamed dried orange peel and preparation method thereof |
| CN113262254A (en) * | 2021-06-21 | 2021-08-17 | 河北旭宇金坤药业有限公司 | Processing method of pummelo peel and pummelo peel processed product |
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| CN103989781A (en) * | 2014-06-17 | 2014-08-20 | 陈智辉 | High-efficiency rapid aromatic tangerine peel preparation method |
| CN108553500A (en) * | 2018-05-31 | 2018-09-21 | 遵义源创生产力促进中心有限公司 | A kind of concocting method of honeysuckle |
| CN109432208A (en) * | 2018-12-25 | 2019-03-08 | 陇西广药采芝林药业有限公司 | A kind of concocting method for steaming dried orange peel |
| CN109646572A (en) * | 2019-01-23 | 2019-04-19 | 南通美日养中医药科技有限公司 | A kind of concocting method of sealwort decoction piece |
-
2019
- 2019-06-03 CN CN201910474309.7A patent/CN110051745A/en active Pending
Patent Citations (4)
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|---|---|---|---|---|
| CN103989781A (en) * | 2014-06-17 | 2014-08-20 | 陈智辉 | High-efficiency rapid aromatic tangerine peel preparation method |
| CN108553500A (en) * | 2018-05-31 | 2018-09-21 | 遵义源创生产力促进中心有限公司 | A kind of concocting method of honeysuckle |
| CN109432208A (en) * | 2018-12-25 | 2019-03-08 | 陇西广药采芝林药业有限公司 | A kind of concocting method for steaming dried orange peel |
| CN109646572A (en) * | 2019-01-23 | 2019-04-19 | 南通美日养中医药科技有限公司 | A kind of concocting method of sealwort decoction piece |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113057991A (en) * | 2021-04-09 | 2021-07-02 | 建昌帮药业有限公司 | Steamed dried orange peel and preparation method thereof |
| CN113057991B (en) * | 2021-04-09 | 2022-05-20 | 建昌帮药业有限公司 | Steamed dried orange peel and preparation method thereof |
| CN113262254A (en) * | 2021-06-21 | 2021-08-17 | 河北旭宇金坤药业有限公司 | Processing method of pummelo peel and pummelo peel processed product |
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