CN110038663B - Ceramic material teaching experiment table - Google Patents
Ceramic material teaching experiment table Download PDFInfo
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- CN110038663B CN110038663B CN201910447109.2A CN201910447109A CN110038663B CN 110038663 B CN110038663 B CN 110038663B CN 201910447109 A CN201910447109 A CN 201910447109A CN 110038663 B CN110038663 B CN 110038663B
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- 229910010293 ceramic material Inorganic materials 0.000 title claims abstract description 28
- 238000002474 experimental method Methods 0.000 title claims abstract description 25
- 238000005245 sintering Methods 0.000 claims abstract description 47
- 238000005303 weighing Methods 0.000 claims abstract description 32
- 239000007790 solid phase Substances 0.000 claims abstract description 20
- 238000000975 co-precipitation Methods 0.000 claims abstract description 19
- 238000003825 pressing Methods 0.000 claims description 49
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 40
- 238000007789 sealing Methods 0.000 claims description 35
- 239000003814 drug Substances 0.000 claims description 33
- 230000007246 mechanism Effects 0.000 claims description 32
- 238000005192 partition Methods 0.000 claims description 20
- 239000011521 glass Substances 0.000 claims description 18
- 238000005520 cutting process Methods 0.000 claims description 17
- 238000010438 heat treatment Methods 0.000 claims description 17
- 238000011084 recovery Methods 0.000 claims description 16
- 238000002156 mixing Methods 0.000 claims description 8
- 239000004570 mortar (masonry) Substances 0.000 claims description 8
- 230000009286 beneficial effect Effects 0.000 abstract description 3
- 229940079593 drug Drugs 0.000 description 15
- 238000010586 diagram Methods 0.000 description 9
- 238000000034 method Methods 0.000 description 7
- 239000002244 precipitate Substances 0.000 description 6
- 239000002245 particle Substances 0.000 description 5
- 239000000843 powder Substances 0.000 description 4
- 238000002360 preparation method Methods 0.000 description 4
- 239000000919 ceramic Substances 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 238000001035 drying Methods 0.000 description 2
- 239000011259 mixed solution Substances 0.000 description 2
- 238000003980 solgel method Methods 0.000 description 2
- 238000010532 solid phase synthesis reaction Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 230000001360 synchronised effect Effects 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01L—CHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
- B01L9/00—Supporting devices; Holding devices
- B01L9/02—Laboratory benches or tables; Fittings therefor
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- Health & Medical Sciences (AREA)
- Clinical Laboratory Science (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Cultivation Receptacles Or Flower-Pots, Or Pots For Seedlings (AREA)
- Sampling And Sample Adjustment (AREA)
- Ceramic Products (AREA)
Abstract
The invention relates to a ceramic material teaching experiment table, which comprises a weighing system, a sol-gel system, a coprecipitation system, a solid phase system and a sintering system; the sol-gel system, the coprecipitation system and the solid phase system are sequentially and equidistantly arranged on one side of the weighing system, and the sintering system and the solid phase system are arranged side by side; the experiment table provided by the invention has the experimental conditions for preparing the ceramic materials in various modes simultaneously, can synchronously carry out teaching, develop contrast teaching and effectively improve the teaching quality. The experiment table disclosed by the invention has the advantages of small occupied area, capability of saving the occupied space for teaching, multiple functions, suitability for operation experiments of multiple persons and capability of saving teaching tool resources. The experiment table provided by the invention has the conditions of preparing ceramic materials in multiple combinations, is beneficial to developing teaching competition, and can realize teaching projects such as single teaching or multiple competition.
Description
Technical Field
The invention relates to an experiment table, in particular to a ceramic material teaching experiment table.
Background
The teaching experiment table is a teaching table specially manufactured by teachers for experimental demonstration and for facilitating students to perform experimental operation. In the ceramic material preparation teaching of university, because the preparation is no longer more, current laboratory bench function is comparatively simple, and teaching experiment is difficult to complete in a teaching laboratory bench entirely, can't effectively carry out teaching demonstration. The existing experiment table also does not have the conditions for preparing ceramic materials by multiple methods at the same time, cannot realize synchronous teaching, cannot compare teaching, cannot develop teaching competition, has poor teaching quality and has poor practice effect for students. Moreover, the existing experiment table has large occupied space, few functions and high teaching tool resource cost, and cannot meet the condition of multi-user operation.
Therefore, the design and development of a ceramic material teaching experiment table is an urgent problem to be solved.
Disclosure of Invention
In order to solve the problems in the background technology, the invention provides a ceramic material teaching experiment table.
The technical proposal is as follows:
the ceramic material teaching experiment table comprises a weighing system, a sol-gel system, a coprecipitation system, a solid phase system and a sintering system; the sol-gel system, the coprecipitation system and the solid phase system are sequentially and equidistantly arranged on one side of the weighing system, and the sintering system and the solid phase system are arranged side by side;
the weighing system comprises a weighing box body, a first sealing door, a weighing platform, a sliding chute, a first operation platform, a rotary upright post, a medicine cabinet, a first table, a sliding rod, a first fixed sliding rod, a hinged sliding rod, a second fixed sliding rod, a pulley and a medicine box; the rotary upright post is arranged on the first table, the top of the rotary upright post is sequentially provided with a medicine cabinet and a first operation table, the top of the first operation table is provided with three sliding grooves, two fixed sliding rods and a sliding rod, the box body is arranged on the sliding grooves in a sliding manner, one side of the box body is provided with a first sealing door, the weighing platform is arranged in the box body, the sliding rods and the fixed sliding rods are respectively provided with a pulley in a sliding manner, a plurality of medicine boxes are arranged on the pulleys, and the tail ends of the fixed sliding rods are sequentially connected with a hinged sliding rod and a fixed sliding rod II;
the sol-gel system comprises a table II, a cabinet I, a water tank, a working table II, a glass rod box I, a container I, a cabinet II, a working table III, a heating table, a glass rod box II, a baking oven I, a baffle I, a sealing door II, a target pressing mechanism I, a cabinet III, a writing board I, a working table IV, a vernier caliper I, a control panel I and a vibration machine I; the first glass rod box is arranged on the first side of the table, the second glass rod box is arranged on the second top of the table, the heating table and the second glass rod box are arranged on the third working table, the first partition board is arranged in the middle of the first baking box, the second sealing door is arranged on one side of the baking box, the first writing board is arranged on one side of the third cabinet, the fourth working table is arranged on the top of the third cabinet, the first vernier caliper and the first vibration machine are respectively arranged on the fourth working table, and the first control panel is connected to the first side of the vibration machine;
the coprecipitation system comprises a table III, a cabinet IV, a water tank, a working table V, a water tap, a stirrer, a water pipe, a recovery box, a sliding rail, a sliding frame, a flow hopper, a mixing container II, a cabinet V, a working table V, a centrifugal machine, wing plates, caulking grooves, a supporting frame, a filter box, a recovery groove, a baking oven II, a partition plate II, a sealing door III, a target pressing mechanism II, a cabinet V, a writing board II, a working table V, a vernier caliper II, a control panel II and a vibration machine II; the three-stage type automatic feeding machine comprises a table, a cabinet body I, a cabinet body II, a baking oven II, a target pressing mechanism II and a cabinet body II, wherein the table is arranged on the table I; the centrifugal machine is arranged on the working table six, one side of the working table six is connected with a wing plate, a round opening is formed in the wing plate, a plurality of caulking grooves are formed in the edge of the opening, a filter box is arranged right below the opening, the filter box is arranged on the support frame, and a recovery groove is formed right below the filter box; a second partition plate is arranged in the second oven, a third sealing door is arranged on one side of the second oven, a second writing board is arranged on the sixth side surface of the cabinet body, a seventh operation table is arranged at the sixth top of the cabinet body, a second vernier caliper and a second vibration machine are arranged on the seventh operation table, and a second control panel is connected to one side of the second vibration machine;
the solid-phase system comprises a table top IV, a cabinet body IV, an operation table IV, a mortar, a pestle box, a target pressing mechanism III, a cabinet body IV, a writing board III, an operation table IV, a vernier caliper III, a control panel III and a vibration machine III; the four-stage machine is characterized in that the four-stage machine is arranged on one side of the first stage machine, a cabinet body seven, a target pressing mechanism three and a cabinet body eight are sequentially arranged on the four-stage machine, an operation table eight is arranged at the top of the cabinet body seven, a mortar and a pestle box are arranged on the operation table eight, a writing board three is arranged on one side surface of the cabinet body eight, an operation table nine is arranged at the top of the cabinet body eight, a vernier caliper three and a vibration machine three are arranged on the operation table nine, and one side of the vibration machine three is connected with a control panel three;
the sintering system comprises a table five, a sintering box body, a sliding sealing door, a power supply box, a heating rod and a temperature thermocouple; the sintering device is characterized in that a table five is arranged side by side with a table four, three sintering boxes are arranged on the table five, a sliding sealing door is arranged on one side of each sintering box, a temperature thermocouple is arranged on the other side of each sintering box, a power supply box is arranged at the top of each sintering box, and a plurality of heating rods are uniformly arranged on two side walls in each sintering box.
Further optimizing, the first target pressing mechanism comprises a first lifting base, a first die, a first cutting, a first bracket and a first rotary pressing head; the first lifting base is arranged on the second table, the first die is arranged on the first lifting base, the first cutting insert is arranged in the first die, the first bracket is arranged above the first lifting base, the first rotary pressing head is spirally inserted on the first bracket, and one end of the first rotary pressing head is located right above the first die.
Further optimizing, the second target pressing mechanism comprises a second lifting base, a second die, a second cutting, a second bracket and a second rotary pressing head; the second lifting base is arranged on the third table, the second die is arranged on the second lifting base, the second cutting is arranged in the second die, the second support is arranged above the second lifting base, the second rotary pressing head is spirally inserted on the second support, and one end of the second rotary pressing head is located right above the second die.
Further optimizing, the third target pressing mechanism comprises a third lifting base, a third die, a third cutting, a third bracket and a third rotary pressing head; the lifting base III is arranged on the table top IV, the mould III is arranged on the lifting base III, the cutting III is arranged in the mould III, the support III is arranged above the lifting base III, the rotary pressure head three-screw is inserted on the support III, and one end of the rotary pressure head three-screw is positioned right above the mould III.
Further optimized, the first lifting base, the second lifting base and the third lifting base are provided with a panel and an instrument.
Further preferably, a water tap is arranged on the water tank.
Further preferably, a control valve is arranged on the flow hopper.
Further preferably, the centrifuge is provided with a jack.
Further preferably, the first cabinet body, the fifth cabinet body and the seventh cabinet body are respectively internally provided with a laminated plate.
Further preferably, the first partition board and the second partition board are provided with strip holes.
Further optimizing, be provided with observation window and handle on sealing door two, the sealing door three.
Further preferably, the filter box is provided with filter holes.
Further optimizing, the first cabinet body, the second cabinet body, the fourth cabinet body, the fifth cabinet body and the seventh cabinet body are provided with openings on one side.
Compared with the prior art, the technical scheme has the following beneficial effects:
(1) The experiment table provided by the invention has the experimental conditions for preparing the ceramic materials in various modes simultaneously, can synchronously carry out teaching, develop contrast teaching and effectively improve the teaching quality.
(2) The experiment table disclosed by the invention has the advantages of small occupied area, capability of saving the occupied space for teaching, multiple functions, suitability for operation experiments of multiple persons and capability of saving teaching tool resources.
(3) The experiment table provided by the invention has the conditions of preparing ceramic materials in multiple combinations, is beneficial to developing teaching competition, and can realize teaching projects such as single teaching or multiple competition.
Drawings
FIG. 1 is a schematic diagram of the overall structure of the present invention;
FIG. 2 is a schematic diagram of the weighing system of the present invention;
FIG. 3 is a schematic view of a portion of a weighing system according to the present invention;
FIG. 4 is a schematic diagram of a portion of a weighing system according to the present invention;
FIG. 5 is a schematic view of the structure of the sol-gel system of the present invention;
FIG. 6 is a schematic view of the structure of a first cabinet of the present invention;
FIG. 7 is a schematic diagram of a second embodiment of the cabinet of the present invention;
FIG. 8 is a schematic view of the structure of a first oven according to the present invention;
FIG. 9 is a schematic diagram of a first embodiment of a target pressing mechanism according to the present invention;
FIG. 10 is a schematic view of the structure of a third cabinet of the present invention;
FIG. 11 is a schematic diagram of the co-precipitation system of the present invention;
FIG. 12 is a schematic view of a fourth embodiment of the cabinet of the present invention;
FIG. 13 is a schematic view of a fifth embodiment of the cabinet of the present invention;
FIG. 14 is a schematic view of the structure of the support frame of the present invention;
FIG. 15 is a schematic view of the structure of the cartridge of the present invention;
FIG. 16 is a schematic diagram of the structure of a solid phase system of the present invention;
FIG. 17 is a schematic diagram of a seventh embodiment of the cabinet of the present invention;
FIG. 18 is a schematic diagram of a sintering system according to the present invention;
FIG. 19 is a schematic view showing the structure of the sintering box of the present invention;
wherein: weighing box 1, sealing door 1, weighing platform 102, chute 103, table 2, rotating column 201, medicine cabinet 202, table 3, slide rod 4, fixed slide rod 401, hinged slide rod 402, fixed slide rod 403, pulley 404, medicine box 405, table 5, cabinet 6, water tank 601, table 602, glass rod box 603, container 604, cabinet 7, table 701, heating platform 702, glass rod box 703, oven 8, partition 801, sealing door 802, lifting base 9, mold 901, cutting 902, bracket 903, rotating ram 904, cabinet 10, writing board 1001, table 1002, vernier caliper 1003, control panel 1004, vibrator 1005, table 11, cabinet 12, water tank 1201, table 1202, faucet 1203, stirrer 1204, water pipe 1205, recovery box 1206, slide rail 13, carriage 1301, cabinet 1301, slide rail flow hopper 1302, mixing vessel 1303, vessel two 1304, cabinet five 14, work bench six 1401, centrifuge 1402, wing 1403, caulking groove 1404, support frame 1405, filter cartridge 1406, recovery groove 1407, oven two 15, partition two 1501, sealing door three 1502, lifting base two 16, mold two 1601, slip two 1602, support two 1603, rotary ram two 1604, cabinet six 17, tablet two 1701, work bench seven 1702, vernier caliper two 1703, control panel two 1704, shaker two 1705, table four 18, cabinet seven 19, work bench eight 1901, mortar 1902, pestle box 1903, lifting base three 20, mold three 2001, slip three 2002, support three 2003, rotary ram three 2004, cabinet eight 21, writing board three 2101, work bench nine, vernier caliper three 2103, control panel three 2104, shaker three 2105, table five 22, sintering box 23, sliding sealing door 2301, power box 2302, heating rod 2303 A temperature thermocouple 2304.
Detailed Description
The following description of the embodiments of the present invention will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present invention, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
Referring to fig. 1 to 19, the ceramic material teaching experiment table of the present embodiment includes a weighing system, a sol-gel system, a coprecipitation system, a solid phase system, and a sintering system; the sol-gel system, the coprecipitation system and the solid phase system are sequentially and equidistantly arranged on one side of the weighing system, and the sintering system and the solid phase system are arranged side by side;
the weighing system comprises a weighing box body 1, a first sealing door 101, a weighing platform 102, a sliding chute 103, a first operating platform 2, a rotary upright column 201, a medicine cabinet 202, a first table platform 3, a sliding rod 4, a first fixed sliding rod 401, a hinged sliding rod 402, a second fixed sliding rod 403, a pulley 404 and a medicine box 405; the rotary upright column 201 is arranged on the first table 3, the top of the rotary upright column 201 is sequentially provided with a medicine cabinet 202 and a first operation table 2, the top of the first operation table 2 is provided with three sliding grooves 103, two first fixed sliding rods 401 and a sliding rod 4, the box body 1 is arranged on the sliding grooves 103 in a sliding manner, one side of the box body 1 is provided with a first sealing door 101, the weighing platform 102 is arranged in the box body 1, the sliding rods 4 and the first fixed sliding rods 401 are respectively provided with a pulley 404 in a sliding manner, the pulleys 404 are provided with a plurality of medicine boxes 405, and the tail ends of the first fixed sliding rods 401 are sequentially connected with a hinged sliding rod 402 and a second fixed sliding rod 403;
the sol-gel system comprises a second table 5, a first cabinet 6, a water tank 601, a second working table 602, a first glass rod box 603, a first container 604, a second cabinet 7, a third working table 701, a heating table 702, a second glass rod box 703, a first oven 8, a first partition plate 801, a second sealing door 802, a first target pressing mechanism, a third cabinet 10, a first writing board 1001, a fourth working table 1002, a first vernier caliper 1003, a first control panel 1004 and a first vibration machine 1005; the first cabinet body 6, the second cabinet body 7, the first oven 8, the first target pressing mechanism 10 and the third cabinet body 10 are sequentially arranged on the second table 5, the inner bottom of the first cabinet body 6 is provided with a water tank 601, the top of the first cabinet body 6 is provided with a second operation table 602, the second operation table 602 is provided with a first glass rod box 603 and a plurality of first containers 604, the top of the second cabinet body 7 is provided with a third operation table 701, the third operation table 701 is provided with a heating table 702 and a second glass rod box 703, the middle part in the first oven 8 is provided with a first partition plate 801, one side of the first oven 8 is provided with a second sealing door 802, one side of the third cabinet body 10 is provided with a first writing board 1001, the top of the third cabinet body 10 is provided with a fourth operation table 1002, the fourth operation table 1002 is respectively provided with a vernier caliper 1003 and a first vibration machine 1005, and one side of the vibration machine 1005 is connected with a control panel 1004;
the coprecipitation system comprises a table III 11, a cabinet IV 12, a water tank 1201, a working table V1202, a water tap 1203, a stirrer 1204, a water pipe 1205, a recovery box 1206, a sliding rail 13, a sliding frame 1301, a flow funnel 1302, a mixing container 1303, a container II 1304, a cabinet V14, a working table VI 1401, a centrifugal machine 1402, a wing plate 1403, a caulking groove 1404, a supporting frame 1405, a filter box 1406, a recovery groove 1407, a baking oven II 15, a baffle II 1501, a sealing door III 1502, a target pressing mechanism II, a cabinet VI 17, a writing board II 1701, a working table seven 1702, a vernier caliper II 1703, a control panel II 1704 and a vibration machine II 1705; the three-stage device comprises a three-stage device, a three-stage device and a four-stage device, wherein the three-stage device 11 is arranged on one side of a first stage device 3, the three-stage device 11 is sequentially provided with a fourth cabinet body 12, a fifth cabinet body 14, a second oven 15, a target pressing mechanism II and a sixth cabinet body 17, one side in the fourth cabinet body 12 is provided with a water tank 1201, the other side in the fourth cabinet body 12 is divided into a plurality of areas by a plurality of partition plates, the top of the fourth cabinet body 12 is provided with a fifth operation platform 1202, one side on the fifth operation platform 1202 is provided with a water tank, two sides of the water tank are respectively provided with a water tap 1203 and a stirrer 1204, the water tap 1203 is communicated with the water tank 1201 through an internally arranged pipeline, one side outside the fourth cabinet body 12 is provided with a recovery box 1206, the top of the recovery box 1206 is communicated with the water tank through a water pipe 1205, the fifth operation platform 1202 is also provided with a slide rail 13 and a plurality of containers 1304, the slide frame 1301 is slidingly arranged on the slide rail 13, a plurality of flow hoppers 1302 are arranged on the slide frame 1301, and a mixing container 1303 is arranged on the fifth operation platform 1202 below the flow hoppers 1302; a workbench six 1401 is arranged at the top of the cabinet body five 14, a centrifuge 1402 is arranged on the workbench six 1401, one side of the workbench six 1401 is connected with a wing plate 1403, a round opening is formed in the wing plate 1403, a plurality of caulking grooves 1404 are formed in the edge of the opening, a filter box 1406 is arranged right below the opening, the filter box 1406 is arranged on the support frame 1405, and a recovery groove 1407 is formed right below the filter box 1406; a second partition plate 1501 is arranged in the second oven 15, a third sealing door 1502 is arranged on one side of the second oven 15, a second writing board 1701 is arranged on one side of the sixth cabinet 17, a seventh operating platform 1702 is arranged on the top of the sixth cabinet 17, a second vernier caliper 1703 and a second oscillator 1705 are arranged on the seventh operating platform 1702, and a second control panel 1704 is connected to one side of the second oscillator 1705;
the solid-phase system comprises a table top four 18, a cabinet body seven 19, an operation table eight 1901, a mortar 1902, a pestle box 1903, a target pressing mechanism three, a cabinet body eight 21, a writing board three 2101, an operation table nine 2102, a vernier caliper three 2103, a control panel three 2104 and a vibration machine three 2105; the four-table 18 is arranged on one side of the first table 3, the four-table 18 is sequentially provided with a seven-cabinet 19, a three-target pressing mechanism and a eight-cabinet 21, the top of the seven-cabinet 19 is provided with an eight-cabinet 1901, the eight-cabinet 1901 is provided with a mortar 1902 and a three-rod box 1903, one side surface of the eight-cabinet 21 is provided with a three-writing board 2101, the top of the eight-cabinet 21 is provided with a nine-cabinet 2102, the nine-cabinet 2102 is provided with a three-vernier caliper 2103 and a three-vibration machine 2105, and one side of the three-vibration machine 2105 is connected with a three-control panel 2104;
the sintering system comprises a fifth table 22, a sintering box 23, a sliding sealing door 2301, a power box 2302, a heating rod 2303 and a temperature thermocouple 2304; the five-table 22 and the four-table 18 are arranged side by side, three sintering boxes 23 are arranged on the five-table 22, a sliding sealing door 2301 is arranged on one side of each sintering box 23, a temperature thermocouple 2304 is arranged on the other side of each sintering box 23, a power supply box 2302 is arranged at the top of each sintering box 23, and a plurality of heating rods 2303 are uniformly arranged on two side walls in each sintering box 23.
The first target pressing mechanism comprises a first lifting base 9, a first die 901, a first cutting 902, a first bracket 903 and a first rotary pressing head 904; the first lifting base 9 is arranged on the second table 5, the first mould 901 is arranged on the first lifting base 9, the first cutting 902 is arranged in the first mould 901, the first bracket 903 is arranged above the first lifting base 9, the first rotary pressing head 904 is spirally inserted on the first bracket 903, and one end of the first rotary pressing head 904 is positioned right above the first mould 901.
The second target pressing mechanism comprises a second lifting base 16, a second die 1601, a second cutting 1602, a second bracket 1603 and a second rotary pressure head 1604; the second lifting base 16 is arranged on the third table 11, the second mold 1601 is arranged on the second lifting base 16, the second insert 1602 is arranged in the second mold 1601, the second bracket 1603 is arranged above the second lifting base 16, the second rotating press head 1604 is spirally inserted on the second bracket 1603, and one end of the second rotating press head 1604 is positioned right above the second mold 1601.
The third target pressing mechanism comprises a third lifting base 20, a third die 2001, a third cutting 2002, a third bracket 2003 and a third rotary pressing head 2004; the lifting base III 20 is arranged on the table top IV 18, the die III 2001 is arranged on the lifting base III 20, the cutting III 2002 is arranged in the die III 2001, the support III 2003 is arranged above the lifting base III 20, the rotary pressure head III 2004 is spirally inserted on the support III 2003, and one end of the rotary pressure head III 2004 is positioned right above the die III 2001.
The first lifting base 9, the second lifting base 16 and the third lifting base 20 are provided with panels and meters. The water tank 601 is provided with a faucet. The flow hopper 1302 is provided with a control valve. The centrifuge 1402 is provided with a receptacle. And laminated plates are arranged in the first cabinet body 6, the fifth cabinet body 14 and the seventh cabinet body 19. And strip holes are formed in the first partition plate 801 and the second partition plate 1501. The second sealing door 802 and the third sealing door 1502 are provided with a viewing window and a handle. The filter cartridge 1406 is provided with filter holes. Openings are formed in one side of the first cabinet body 6, the second cabinet body 7, the fourth cabinet body 12, the fifth cabinet body 14 and the seventh cabinet body 19.
The invention works as follows: the teaching staff and students can finish the weighing operation of medicines in the weighing system, finish the operation of preparing ceramic materials by using a sol-gel method in the sol-gel system, finish the operation of preparing ceramic materials by using a coprecipitation method in the coprecipitation system, finish the operation of preparing ceramic materials by using a solid phase method in the solid phase system, and finish sintering ceramic targets obtained by the three systems in the sintering system. The teaching staff can demonstrate the demonstration operation of preparing ceramic materials by using the test table, students can use the test table to simultaneously perform competition of preparing ceramic materials by using three different methods, and the sol-gel system, the coprecipitation system and the solid phase system can support students to simultaneously prepare ceramic materials by using three methods.
During weighing, medicines are taken out of the medicine cabinet 202 according to the requirement, the medicine cabinet 202 can be driven by the rotary upright column 201 to rotate so as to conveniently take the medicines, the medicines are placed on the weighing platform 102, the first sealing door 101 is closed to weigh the medicines, the medicines are taken out and placed in the medicine box 405 after the weighing is completed, the medicine box 405 is placed in the pulley 404, the medicines are sent into the coprecipitation system through the sliding rod 4, and the medicines are respectively sent into the sol-gel system and the solid phase system through the first fixed sliding rod 401, the hinged sliding rod 402 and the second fixed sliding rod 403. When three methods are simultaneously carried out to prepare the ceramic material, the three weighing boxes 1 are correspondingly used by operators of three systems of the three preparation methods.
The preparation method comprises the steps of finishing the operation of preparing ceramic materials by a sol-gel method in a sol-gel system, firstly dissolving the weighed medicines on a second operation table 602 by utilizing a first glass rod box 603, a first container 604 and a water tank 601 to obtain sol, moving the sol to a third operation table 701, finishing the gel operation by utilizing a first heating table 702 and a second glass rod box 703, moving the gel to a first baking oven 8, closing a second sealing door 802, drying the gel to powder, moving the obtained powder to a first mold 901, pressing the powder to form a target by utilizing a first rotary press head 904 and a first lifting base 9, taking out the target by utilizing a first lifting insert 902, then measuring the diameter of the target by utilizing a first vernier caliper 1003 on a fourth operation table 1002 and recording on a first writing board 1001, placing the target on a first oscillating machine 1005, controlling and starting the oscillating machine 1005, observing the flatness of the target and recording on the first writing board 1001, then moving the target to a sintering system in a sintering box 23, returning the fourth operation table 1002 to measure the diameter and flatness of the target after the sintering is finished, and obtaining the rough quality judgment of the target, and the ceramic quality judgment of the target is achieved.
The operation of preparing ceramic materials by a coprecipitation method is completed in a coprecipitation system, firstly, the weighed medicines are placed in a second container 1304, water is added into the medicines through a water tap 1203 and a stirrer 1204, the medicines after dissolution are respectively placed in a flow hopper 1302, the solutions quantitatively flowing out of the three flow hoppers 1302 are received through a mixing container 1303, solid precipitates are generated after the reaction of the obtained mixed solutions, the mixed solutions are placed in a centrifuge 1402 for solid-liquid separation, then poured onto coarse gauze fixed by a caulking groove 1404 for filtering large-particle precipitates, small-particle precipitates and liquid penetrate through the gauze and fall into a filter box 1406, the small-particle precipitates are collected by the filter box 1406 and the liquid flows into a recovery groove 1407 through the filter box 1406, the obtained small-particle precipitates are then placed into a second oven 15 for drying into powder, the obtained small-particle precipitates are placed into a second die 1601 for pressing a target mechanism, the obtained target is pressed by a second rotary pressure head 1604 for weighing, then the diameter of the target is measured on a seventh operating table 1703, the flatness of the target is measured by a second vernier caliper 1703, the target is measured by a second control panel, the flatness is then the target is measured, the target is subjected to rough flatness is measured, the target is measured, the quality and the sintering quality is measured again, and the sintering quality is calculated, and the sintering quality is then the target is judged.
The operation of preparing ceramic materials by a solid-phase method is completed in a solid-phase system, all weighed medicines are placed into a mortar 1902 and are ground by a pestle in a pestle box 1903, the ground medicines are placed into a die III 2001 of a target pressing mechanism III, the ground medicines are pressed into targets by a lifting base III 20 and a rotary pressure head III 2004, the targets are taken out by tilting a cutting III 2002, the diameters of the targets are measured by a vernier caliper III 2103 in a work table nine 2102, the flatness of the targets is measured by a control panel III 2104 and a shaker III 2105, the targets are placed into a sintering box 23 of a sintering system, a sliding sealing door 2301 is closed to complete sintering, the diameters and the flatness of the targets are measured in the work table nine, the shrinkage rate of the targets is calculated, and the target quality can be roughly judged, and compared with the target quality prepared by a sol-gel system and a coprecipitation system.
The power box 2302 controls the heating rate of the heating rod 2303 to control the sintering temperature in the sintering box 23, and the temperature thermocouple 2304 monitors the sintering temperature in real time. The pressing conditions of the first target pressing mechanism, the second target pressing mechanism and the third target pressing mechanism can be used for pressing targets or judging the quality of ceramics, and demonstration and judgment during teaching or competition are available.
While the embodiments have been described above, other variations and modifications will occur to those skilled in the art once the basic inventive concepts are known, and it is therefore intended that the foregoing description and drawings illustrate only embodiments of the invention and not limit the scope of the invention, and it is therefore intended that the invention not be limited to the specific embodiments described, but that the invention may be practiced with their equivalent structures or with their equivalent processes or with their use directly or indirectly in other related fields.
Claims (4)
1. The ceramic material teaching experiment table is characterized by comprising a weighing system, a sol-gel system, a coprecipitation system, a solid phase system and a sintering system; the sol-gel system, the coprecipitation system and the solid phase system are sequentially and equidistantly arranged on one side of the weighing system, and the sintering system and the solid phase system are arranged side by side;
the weighing system comprises a weighing box body (1), a first sealing door (101), a weighing platform (102), a sliding chute (103), a first operating platform (2), a rotary upright post (201), a medicine cabinet (202), a first table (3), a sliding rod (4), a first fixed sliding rod (401), a hinged sliding rod (402), a second fixed sliding rod (403), a pulley (404) and a medicine box (405); the rotary upright post (201) is arranged on the first table (3), the medicine cabinet (202) and the first operation table (2) are sequentially arranged at the top of the rotary upright post (201), three sliding grooves (103), two first fixed sliding rods (401) and one sliding rod (4) are arranged at the top of the first operation table (2), the box body (1) is arranged on the sliding grooves (103) in a sliding mode, the first sealing door (101) is arranged on one side of the box body (1), the weighing platform (102) is arranged in the box body (1), the sliding rods (4) and the first fixed sliding rods (401) are respectively provided with a pulley (404), a plurality of medicine boxes (405) are arranged on the pulleys (404), and the tail ends of the first fixed sliding rods (401) are sequentially connected with the hinged sliding rods (402) and the second fixed sliding rods (403);
the sol-gel system comprises a table II (5), a cabinet I (6), a water tank (601), a working table II (602), a glass rod box I (603), a container I (604), a cabinet II (7), a working table III (701), a heating table (702), a glass rod box II (703), an oven I (8), a partition board I (801), a sealing door II (802), a target pressing mechanism I, a cabinet III (10), a writing board I (1001), a working table IV (1002), a vernier caliper I (1003), a control panel I (1004) and an oscillating machine I (1005); the novel glass cabinet is characterized in that the second table (5) is arranged on one side of the first table (3), the first cabinet (6), the second cabinet (7), the first oven (8), the first target pressing mechanism and the third cabinet (10) are sequentially arranged on the second table (5), a water tank (601) is arranged at the inner bottom of the first cabinet (6), a second operation table (602) is arranged at the top of the first cabinet (6), a first glass rod box (603) and a plurality of first containers (604) are arranged on the second operation table (602), a third operation table (701) is arranged at the top of the second cabinet (7), a heating table (702) and a second glass rod box (703) are arranged on the third operation table (701), a first partition plate (801) is arranged in the middle of the first oven (8), a sealing door (802) is arranged on one side of the first oven (8), a first writing board (1001) is arranged on one side of the third cabinet (10), a fourth operation table (1002) is arranged at the top of the third cabinet (10), a first callipers (1003) and a first vibration machine (1005) are respectively arranged on the fourth operation table (1002), and a first vibration machine (1005) is connected with a second vernier control panel (1005);
the coprecipitation system comprises a third table (11), a fourth cabinet (12), a water tank (1201), a fifth operation table (1202), a faucet (1203), a stirrer (1204), a water pipe (1205), a recovery box (1206), a sliding rail (13), a sliding frame (1301), a flow hopper (1302), a mixing container (1303), a second container (1304), a fifth cabinet (14), a sixth operation table (1401), a centrifuge (1402), a wing plate (1403), a caulking groove (1404), a support frame (1405), a filter box (1406), a recovery groove (1407), a second oven (15), a second partition plate (1501), a third sealing door (1502), a second target pressing mechanism, a sixth cabinet (17), a second writing board (1701), a seventh operation table (1702), a second vernier caliper (1703), a second control panel (1704) and a second vibration machine (1705); the novel multifunctional automatic mixing device comprises a first table (3), a second table (11), a third cabinet (12), a fifth cabinet (14), a second oven (15), a second target pressing mechanism and a sixth cabinet (17), wherein the third table (11) is arranged on one side of the first table (3), a water tank (1201) is arranged on one side of the fourth cabinet (12), the other side of the fourth cabinet (12) is divided into a plurality of areas by a plurality of partition plates, a fifth operation table (1202) is arranged on the top of the fourth cabinet (12), a water tank is arranged on one side of the fifth operation table (1202), water faucets (1203) and a stirrer (1204) are respectively arranged on two sides of the water tank, the water faucets (1203) are communicated with the water tank (1201) through built-in pipelines, a recovery tank (1206) is arranged on one side of the fourth cabinet (12), the top of the recovery tank (1206) is communicated with the water tank through a water pipe (1205), a sliding rail (13) and a plurality of containers (1304) are also arranged on the fifth operation table (1202), a plurality of flow funnels (1302) are arranged on the sliding frame (1301), and a mixing operation container (1303) is arranged below the fifth operation table (1302); a workbench six (1401) is arranged at the top of the cabinet body five (14), a centrifuge (1402) is arranged on the workbench six (1401), one side of the workbench six (1401) is connected with a wing plate (1403), a round opening is formed in the wing plate (1403), a plurality of caulking grooves (1404) are formed in the edge of the opening, a filter box (1406) is arranged right below the opening, the filter box (1406) is arranged on a supporting frame (1405), and a recovery groove (1407) is formed right below the filter box (1406); a second partition plate (1501) is arranged in the second baking oven (15), a third sealing door (1502) is arranged on one side of the second baking oven (15), a second writing board (1701) is arranged on one side of the sixth cabinet (17), a seventh operating platform (1702) is arranged at the top of the sixth cabinet (17), a second vernier caliper (1703) and a second oscillating machine (1705) are arranged on the seventh operating platform (1702), and a second control panel (1704) is connected to one side of the second oscillating machine (1705);
the solid-phase system comprises a table top IV (18), a cabinet top seventh (19), a working table eight (1901), a mortar (1902), a pestle box (1903), a target pressing mechanism III, a cabinet top eighth (21), a writing board III (2101), a working table nine (2102), a vernier caliper III (2103), a control panel III (2104) and a vibration machine III (2105); the novel multifunctional desk comprises a desk body I (3), a desk II (18), a desk III (19), a pressing target mechanism III and a desk II (21) are sequentially arranged on the desk II (18), an operation desk II (1901) is arranged at the top of the desk II (19), a mortar (1902) and a pestle box (1903) are arranged on the operation desk II (1901), a writing board III (2101) is arranged on one side surface of the desk II (21), an operation desk III (2102) is arranged at the top of the desk II (21), a vernier caliper III (2103) and a vibration machine III (2105) are arranged on the operation desk III (2102), and a control panel III (2104) is connected to one side of the vibration machine III (2105);
the sintering system comprises a table five (22), a sintering box body (23), a sliding sealing door (2301), a power box (2302), a heating rod (2303) and a temperature thermocouple (2304); the five-table (22) and the four-table (18) are arranged side by side, three sintering boxes (23) are arranged on the five-table (22), a sliding sealing door (2301) is arranged on one side of each sintering box (23), a temperature thermocouple (2304) is arranged on the other side of each sintering box (23), a power box (2302) is arranged at the top of each sintering box (23), and a plurality of heating rods (2303) are uniformly arranged on two inner side walls of each sintering box (23);
the first target pressing mechanism comprises a first lifting base (9), a first die (901), a first cutting (902), a first bracket (903) and a first rotary pressing head (904); the lifting base I (9) is arranged on the table II (5), the die I (901) is arranged on the lifting base I (9), the insert I (902) is arranged in the die I (901), the bracket I (903) is arranged above the lifting base I (9), the rotary press head I (904) is spirally inserted on the bracket I (903), and one end of the rotary press head I (904) is positioned right above the die I (901);
the second target pressing mechanism comprises a second lifting base (16), a second die (1601), a second cutting (1602), a second bracket (1603) and a second rotary pressing head (1604); the lifting base II (16) is arranged on the table III (11), the die II (1601) is arranged on the lifting base II (16), an inserting strip II (1602) is arranged in the die II (1601), a bracket II (1603) is arranged above the lifting base II (16), a rotary pressure head II (1604) is spirally inserted on the bracket II (1603), and one end of the rotary pressure head II (1604) is positioned right above the die II (1601);
the third target pressing mechanism comprises a third lifting base (20), a third die (2001), a third cutting (2002), a third bracket (2003) and a third rotary pressing head (2004); the lifting base III (20) is arranged on the table top IV (18), the die III (2001) is arranged on the lifting base III (20), the cutting III (2002) is arranged in the die III (2001), the bracket III (2003) is arranged above the lifting base III (20), the rotary pressure head III (2004) is spirally inserted on the bracket III (2003), and one end of the rotary pressure head III (2004) is positioned right above the die III (2001);
the lifting base I (9), the lifting base II (16) and the lifting base III (20) are provided with a panel and an instrument;
a water tap is arranged on the water tank (601);
the flow hopper (1302) is provided with a control valve.
2. The ceramic material teaching experiment table as claimed in claim 1, wherein a jack is provided on the centrifuge (1402).
3. The teaching experiment table for ceramic materials according to claim 1, wherein laminated plates are arranged in the first cabinet body (6), the fifth cabinet body (14) and the seventh cabinet body (19).
4. The teaching experiment table for ceramic materials according to claim 1, wherein strip holes are formed in the first partition plate (801) and the second partition plate (1501).
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910164744.XA CN109759166A (en) | 2019-03-05 | 2019-03-05 | Ceramic material teaching experiment tables |
| CN201910164744X | 2019-03-05 |
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| CN201920772917.1U Active CN210206933U (en) | 2019-03-05 | 2019-05-27 | Teaching experiment table for ceramic material |
| CN201910447109.2A Active CN110038663B (en) | 2019-03-05 | 2019-05-27 | Ceramic material teaching experiment table |
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| CN201920772917.1U Active CN210206933U (en) | 2019-03-05 | 2019-05-27 | Teaching experiment table for ceramic material |
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| DE2510850A1 (en) * | 1975-03-12 | 1976-11-04 | Schaffizel Kg Schulmoebel | Experimenting bench with ceramic or plastics top - allowing easy inspection of and access to fittings |
| JP2001097768A (en) * | 1999-09-29 | 2001-04-10 | Daiichi Kigensokagaku Kogyo Co Ltd | Yag-based ceramic raw material and its production |
| CN106882963A (en) * | 2017-03-31 | 2017-06-23 | 天津大学 | A kind of method that CaCu 3 Ti 4 O is prepared based on sol-gal process |
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| CN108623311A (en) * | 2018-07-05 | 2018-10-09 | 何莉 | A kind of function ceramics process units |
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| CN109227924A (en) * | 2018-09-13 | 2019-01-18 | 蒙城县弘文信息科技有限公司 | A kind of ceramic material synthesis device |
| CN210206933U (en) * | 2019-03-05 | 2020-03-31 | 卢明鑫 | Teaching experiment table for ceramic material |
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2019
- 2019-03-05 CN CN201910164744.XA patent/CN109759166A/en not_active Withdrawn
- 2019-05-27 CN CN201920772917.1U patent/CN210206933U/en active Active
- 2019-05-27 CN CN201910447109.2A patent/CN110038663B/en active Active
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| DE2510850A1 (en) * | 1975-03-12 | 1976-11-04 | Schaffizel Kg Schulmoebel | Experimenting bench with ceramic or plastics top - allowing easy inspection of and access to fittings |
| JP2001097768A (en) * | 1999-09-29 | 2001-04-10 | Daiichi Kigensokagaku Kogyo Co Ltd | Yag-based ceramic raw material and its production |
| CN106882963A (en) * | 2017-03-31 | 2017-06-23 | 天津大学 | A kind of method that CaCu 3 Ti 4 O is prepared based on sol-gal process |
| CN108465497A (en) * | 2018-03-26 | 2018-08-31 | 井昌平 | A kind of composite type Physical Chemistry Experiment platform |
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| CN210206933U (en) * | 2019-03-05 | 2020-03-31 | 卢明鑫 | Teaching experiment table for ceramic material |
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|---|---|
| CN110038663A (en) | 2019-07-23 |
| CN210206933U (en) | 2020-03-31 |
| CN109759166A (en) | 2019-05-17 |
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