CN110013463A - Whitening and softening skin freeze-drying facial mask containing desert rose essence and preparation method thereof - Google Patents
Whitening and softening skin freeze-drying facial mask containing desert rose essence and preparation method thereof Download PDFInfo
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- CN110013463A CN110013463A CN201910356558.6A CN201910356558A CN110013463A CN 110013463 A CN110013463 A CN 110013463A CN 201910356558 A CN201910356558 A CN 201910356558A CN 110013463 A CN110013463 A CN 110013463A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/66—Enzymes
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/99—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/84—Products or compounds obtained by lyophilisation, freeze-drying
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Abstract
The invention discloses a kind of, and facial mask and preparation method thereof is lyophilized in the whitening and softening skin containing desert rose essence, facial mask contains freeze-dried powder, the freeze-dried powder includes following components: 0.1~15 part of desert japanese rose leaf cell extract, 0.1~5 part of ethoxy urea, 0.5~5 part of -8/5/3/ glycerol of PEG/PPG/ polytetramethylene glycol, 0.1~5 part of glycerol, 0.1~8 part of Sodium Hyaluronate, 0.5~5 part of natural thickener, 0.1~5 part of papain, 0.1~3 part of calcium pantothenate, 0.1~3 part of urea, 0.1~5 part of pungent glycol, 0.1~5 part of amino acid, 0.1~5 part of moisturizing factor, 0.1~5 part of Sensiva SC50, 5~60 parts of water.After freeze-drying facial mask of the invention, skin present health it is pale, moist with it is compact, be used for a long time, delaying sanility, repair damaged cell, enhancing skin resistance.
Description
Technical field
The present invention relates to technical field of skin care, and in particular to the whitening and softening skin freeze-dried powder containing desert rose essence freezes
Dried noodle film and preparation method thereof.
Background technique
Facial mask is lyophilized, also known as freeze-dried powder facial mask, freeze-drying solid-state stoste facial mask is carried out moisture using vacuum freeze drying
Distillation forms the facial mask of solid-state dry film form.It can be used for maintaining facial skin, play replenishing water and preserving moisture, whitening and anti-aging, put down
Weigh grease etc. and other effects.
Desert rose (adenium obesum) also known as Tian Bao flower, category Apocynaceae, perennial shrub shape succulent plant,
Originate in East Africa to Arabia Peninsula south.The pyrophilous drying of desert rose and sunny environment, it is heat-resistant, it is drought-resistant, it can be
It is produced in rugged environment, moisture can be obtained from the arid desert environment, and can firmly lock moisture, reduce moisture
Loss, have it is very strong keep moisture ability.
With the growth in man-year age, the metabolism of body becomes slowly, and human skin can depositing black element.Melanin by
Melanocyte generates, and internal melanin gradually increases, will be deposited in the basal cell of skin.Internal tyrosine is in junket ammonia
3,4- dihydroxy propyl benzene propylhomoserin (i.e. DOPA) is generated under sour enzymatic, DOPA, which further aoxidizes, generates DOPA quinone.DOPA quinone is through more
Dimerization reaction and oxidation reaction generate dopachrome, and dopachrome is converted into 5,6- dihydroxy under dopachrome color structure enzyme effect
Indole-carboxylic acid (DHICA), 5,6- dihydroxy indole carboxylic acid (DHICA) decarboxylations are at 5,6- dihydroxy indole, then again in tyrosine
5,6- istain is oxidized under enzymatic, 5,6- istains finally form melanin in conjunction with other intermediate products.Melanin
Grain can reach epidermal cell to epithelial cells transfer by melanocyte dendritic processes after generating, so that skin be caused to become
It is black.
Current most skin-whitening or nti-freckle product are mainly in the rate-limiting enzyme (tyrosinase) of melanin production
It works, inhibits tyrosinase activity or block tyrosine to generate the oxidative pathway of melanin, to reduce melanin production
Achieve the effect that skin whitening.Effect raw material added by the whitening and skin-protecting product of commercial type mainly includes that cell is raw at present
The long factor, animal placenta extract, kojic acid, tartaric acid, quinhydrones etc., these ingredients with whitening effect can also cause skin
Certain injury, and product is made to be easy to produce discoloration, phenomenon spoiled, unstable, storage life is short.Such as cell growth factor
Son, the active shelf-life of animal placenta extract are shorter, are not easy long-term preservation, are easy to cause discoloration, spoiled；The additive amount of kojic acid
It is easy to cause contact dermatitis when reaching a certain level；The whitening effect of pure chemicals is preferable, but side effect is larger, is easy wound
Skin；Pure natural plant extract side effect is smaller, but active constituent difficulty is also easy by other objects with being absorbed by body skin
Matter is covered, and whitening effect tends not to give full play of again, causes effect not satisfactory.Skin-lightening cosmetic can also exist certain
Security risk because typically using concentration it is higher, pH is lower, and whitening effect can be more obvious, but irritation also can be bigger,
Possible permanent damage even is caused to skin when serious, this mode is simultaneously undesirable.
Now in order to lighten the stain, wrinkle and colour of skin whitening, cosmetics, concealing product can only be leaned on to come skin whitening, but this
Skin is only covered, surface is good-looking but does not effect a permanent cure.Accordingly, it is now desired to a kind of preferable mask product of essence whitening effect, energy
The effects of enough playing whitening, tender skin, moisturizing, anti-aging repairs skin, and be used for a long time and do not damage to maintain the elasticity of skin
Skin.
Summary of the invention
In view of the problems of the existing technology, one of the objects of the present invention is to provide a kind of containing desert rose essence
Whitening and softening skin freeze-dried powder.
Another object of the present invention is to provide a kind of, and facial mask is lyophilized in the whitening and softening skin containing desert rose essence.
Another object of the present invention is to provide a kind of preparation side of whitening and softening skin freeze-dried powder containing desert rose essence
Method.
Further, another object of the present invention is to provide a kind of whitening and softening skin freeze-drying face containing desert rose essence
The preparation method of film.
Further, another object of the present invention is to provide a kind of whitening and softening skin freeze-drying face containing desert rose essence
The application method of film.
The invention adopts the following technical scheme:
Whitening and softening skin freeze-dried powder containing desert rose essence, according to parts by weight, the freeze-dried powder includes following raw material:
Optionally, the whitening and softening skin freeze-dried powder containing desert rose essence, according to parts by weight, including following original
Material:
Further, the desert japanese rose leaf cell extract passes through supercritical CO2Extraction process is made, desert japanese rose leaf
Cell extract accounts for 0.1~10 part, for example, 0.1,0.2,0.3,0.4,0.5,0.6,0.7,0.8,0.9,1,2,3,4,5,6,7,
8,9,10 parts.
Specifically, desert rose leaf is cleaned out, such as washed, be then ground into 50~100 using grinding device
The clast of mesh (such as 50~60 mesh, 60~70 mesh, 70~80 mesh, 80~90 mesh, 90~100 mesh).
Further, the supercritical CO2The condition of extraction process are as follows: with CO2For supercritical fluid, extracting pressure is
200~500bar (for example, 200bar, 300bar, 400bar, 500bar), time are 1~3h (for example, 1h, 2h, 3h), temperature
For 40 DEG C~50 DEG C (for example, 40 DEG C, 41 DEG C, 42 DEG C, 43 DEG C, 44 DEG C, 45 DEG C, 46 DEG C, 47 DEG C, 48 DEG C, 49 DEG C, 50 DEG C), CO2
Flow velocity is 10~20g/min (for example, 10,11,12,13,14,15,16,17,18,19,20g/min).
Term " supercritical CO used herein2Extraction " (Supercritical Fluids Extraction, SFE),
Refer to and utilizes the fluid (CO under supercriticality2) it is used as extractant, constituent part is extracted from solid or liquid charging stock
Isolation technics.Supercritical fluid not only solvability with higher, mass transfer rate also with higher, preferable mobility
It can and quickly reach the ability of balance.Moreover, because temperature and pressure can cause to dissolve in the minor change of Near The Critical Point
The significant changes of ability, this makes supercritical fluid have good controllability and selectivity.
Further, supercritical extract overcome tradition extract or extracting process time-consuming, process is cumbersome, the rate of recovery is low,
The problems such as seriously polluted, is especially a cancellation harm of the organic solvent to human body and environment.Fluid CO used in it2With nothing
Malicious, tasteless, non-ignitable, noresidue, it is cheap, easily purification the features such as.
Particularly, the freeze-dried powder of the application or freeze-drying facial mask are free of preservative, such as without chemical preservative: benzoic acid and
Its esters, sorbic acid and its esters, dehydroactic acid and its esters, parabens etc., specifically, without such as methyl hydroxybenzoate,
Nipasol, Phenoxyethanol, benzyl alcohol, benzyl carbinol, Bis(hydroxymethyl)imidazolidinyl urea, potassium sorbate, sodium benzoate, chlorobenzene are sweet
Ether, dehydroactic acid sodium etc..
Further, the dosage of the natural thickener be 0.5~5 part, such as 0.5,0.6,0.7,0.8,0.9,1,2,
3,4,5 parts.
In various embodiments, the natural thickener include pectin, locust bean gum, Arabic gum, alginic acid, gellan gum,
At least one of tragacanth, tara gum, tamarind gum, xanthan gum.For example, the natural thickener is xanthan gum；Optionally,
The natural thickener is the locust bean gum, Arabic gum, tragacanth that mass ratio is 1:1~3:1~3.
Further, the papain (commercially available, Spain) be 0.1~5 part, such as 0.1,0.2,0.3,
0.4,0.5,0.6,0.7,0.8,0.9,1,2,3,4,5 part.Papain can promote self metabolism of skin, help to update
Skin cutin simultaneously softens it, and appears newborn skin, moisturizes the skin and improves the whole colour of skin.
Further, the amino acid includes at least one of dried meat amino, the third amino, silk amino.Preferably, the ammonia
Base acid is made of dried meat amino, the third amino and silk amino.Specifically, the amino acid is 1:0.5~2:0.5~2 by mass ratio
Dried meat amino, the third amino and silk amino composition.Alternatively, the amino acid is 0.1~1.5 part of dried meat amino, 0.1~1.5 part third
Amino and 0.1~1.5 part of silk amino.
Further, the amino acid be 0.1~5 part, such as 0.1,0.2,0.3,0.4,0.5,0.6,0.7,0.8,
0.9,1,2,3,4,5 part.
Further, the moisturizing factor includes at least one of magnesium lactate, potassium lactate, magnesium chloride, sodium citrate.It is excellent
Selection of land, the moisturizing factor are made of magnesium lactate, potassium lactate, magnesium chloride, sodium citrate.Specifically, the moisturizing factor is by matter
Amount is than being 1:0.5~2:0.5~2:0.5~2 magnesium lactate, potassium lactate, magnesium chloride, sodium citrate composition.Alternatively, described
Moisturizing factor is 0.1~1 part of magnesium lactate, 0.1~1 part of potassium lactate, 0.1~1 part of magnesium chloride and 0.1~1 part of sodium citrate.
Further, the moisturizing factor be 0.1~5 part, such as 0.1,0.2,0.3,0.4,0.5,0.6,0.7,0.8,
0.9,1,2,3,4,5 part.
Further, water can be distilled water, deionized water, ultrapure water etc., preferably deionized water.The dosage of water be 5~
60 parts, such as 5,6,7,8,9,10,11,12,13,14,15,16,17,18,19,20,30,40,50 or 60 parts.
In various embodiments, facial mask is lyophilized in whitening and softening skin containing desert rose essence, including the freeze-dried powder and
Facial mask cloth.The material of the facial mask cloth is cotton, terylene, blended, silk or fruit fiber.
Preferably, the facial mask cloth is day cortina cloth, cellulose of the raw material of tencel in trees, the pure day of a hundred percent
Right material, in addition loopful, which protects no added production process, forms absolutely pure tencel fiber.Tencel facial mask is after use about
12 weeks can be degradable, water and carbon dioxide are formed, do not can cause environmental pollution.Tencel fiber is than general cotton fiber
It is softer, more smooth, there is fabulous biocompatibility with human skin.Apply sense soft comfortable do not stimulate skin, apply on the face from
Right transparent, close docile.Tencel facial mask possesses good moisture absorbing, and water imbibition is more superior than common non-woven fabric, can adsorb
The Essence that 8 times of facial mask cloth own wt makes skin keep the wet of longer time and nourish.In addition, the stretching of day cortina cloth
Degree preferably, is suitble to the tight of any shape of face.Natural activity composition and nutriment are attached to day by unique lyophilized technique
Cortina cloth, can be persistently fresh-keeping, meets water, that is, release vigor.
Further, the freeze-dried powder is free of preservative, hormone or antibacterial agent.
In various embodiments, the preparation method of the whitening and softening skin freeze-dried powder containing desert rose essence, including following step
It is rapid:
(1) mix: by desert japanese rose leaf cell extract, ethoxy urea, -8/5/3/ glycerol of PEG/PPG/ polytetramethylene glycol,
Glycerol, Sodium Hyaluronate, natural thickener, papain, calcium pantothenate, urea, pungent glycol, amino acid, moisturizing factor, ethyl
Hexyl glycerol, water (pressing each composition proportion) mixing, stir evenly, obtain mixture；
(2) precooling: by mixture at -20 DEG C to -30 DEG C 1~3h of precooling；
(3) it vacuum freeze drying: is then freeze-dried, vacuum at -180 DEG C to -196 DEG C (the optional liquid nitrogen of refrigerated source)
Degree be 5~50Pa (for example, 5,6,7,8,9,10,11,12,13,14,15,16,17,18,19,20,21,22,23,24,25,
26,27,28,30,32,35,38,42,45,48 or 50Pa), sublimation drying≤10min (for example,≤5min ,≤3min,
Or 1~2min or 0.5~1min or 10~30s).
Above-mentioned vacuum refrigeration be flash freezing, in gnotobasis, by vacuum drying, active constituent is dehydrated completely to
Solid-state can be used nitrogen and be sealed preservation, so that optional do not need to add any preservative, antistaling agent, can more sufficiently,
More muchly retain essence activity.Active constituent therein can efficiently remove free radical, prevent free radical aging, damage skin
Skin cell.
Term " free radical " used herein refers to the original with unpaired electron that homolysis occurs for covalent bond and is formed
Son or group, it is including but not limited to following: ultra-oxygen anion free radical (O2 -), hydrogen peroxide (H2O2), hydroxyl radical free radical (
OH), single oxygen (1O2), carbon center's (CH-R) lipid free radical or L free radical, etc..The intracorporal free radical of people be activity very
Strong atom or group can aoxidize other materials in human body.
In various embodiments, the preparation method of the whitening and softening skin freeze-drying facial mask containing desert rose essence, including it is following
Step:
(1) mix: by desert japanese rose leaf cell extract, ethoxy urea, -8/5/3/ glycerol of PEG/PPG/ polytetramethylene glycol,
Glycerol, Sodium Hyaluronate, natural thickener, papain, calcium pantothenate, urea, pungent glycol, amino acid, moisturizing factor, ethyl
Hexyl glycerol, water (pressing each composition proportion) mixing, stir evenly, obtain mixture；
(2) mixture is coated on to or is soaked facial mask cloth；
(3) precooling: by the facial mask cloth with mixture at -20 DEG C to -30 DEG C 1~3h of precooling；
(4) it vacuum freeze drying: is freeze-dried at -180 DEG C to -196 DEG C (the optional liquid nitrogen of refrigerated source), vacuum degree is
5~50Pa (for example, 5,6,7,8,9,10,11,12,13,14,15,16,17,18,19,20,21,22,23,24,25,26,27,
28,30,32,35,38,42,45,48,50Pa), sublimation drying≤10min (for example,≤5min ,≤3min or 1~
2min or 0.5~1min or 10~30s)；
(5) it is vacuum-packed.
Further, the application method of the whitening and softening skin freeze-drying facial mask containing desert rose essence: after face cleaning, a piece of elder generation is taken
With water-soaked (such as facial mask cloth being put into the water (being contained with facial mask tray) of 10~40ml, such as 25ml), facial mask cloth is abundant
Absorb water, the essence being impregnated in the facial mask cloth of moisture activated, then will (after immersion) facial mask cloth be pasted on again face (or
It is first pasted on face, with water-soaked), it applies 10~30 minutes (preferably 15-20 minutes) and removes, without cleaning after removing, directly
It connects to pat and promotes to fully absorb, can continue to using other skin care item.
Traditional facial mask, every, all containing the water of 15-30ml, and compounds with various other ingredients, and under liquid environment, lead to
Often needing to add preservative just can guarantee that its long-time is never degenerated, while the activity of some of ingredients can have a greatly reduced quality, very
Extremely sensitivity response can be brought to skin.The application uses freeze drying technology, carries out cooling in advance and is frozen into solid, then in vacuum
Under the conditions of (while ultralow temperature, short time) make solid water directly distil to come out, and active constituent is retained in facial mask cloth when freezing
In, in this case, keep or lockked the original activity of active constituent.After frozen dried, for thermally labile, easy
Oxidation, degradable ingredient can still keep very high activity.
The storage method of the product of the application: it is saved under dry cool environment.It is suitble to crowd: any skin quality.
By the freeze-dried powder being prepared or freeze-drying facial mask inspection, product is qualified, then discharges, and sampling observation is qualified, storage.
As it is used herein, "and/or" includes any and one or more associations list all combined terms of item.
Term used herein is only used for description specific embodiment, without being intended to the limitation present invention.As it is used herein, singular
Form " one ", "one", "an" and "the" are also intended to include plural form, unless the context clearly indicates otherwise.Further
Understanding, " comprising " when using in the present specification, specifies stated feature, integer, step, operation, element and/or composition,
But one or more of the other feature is not precluded the presence or addition of, integer, step operates, element, composition and/or their combination.
Unless otherwise defined, all terms (including technical and scientific term) used herein have skill belonging to the present invention
The identical meaning that those of ordinary skill is commonly understood by art field.It further understands, term, it is fixed such as in common dictionary
Justice, explains consistent with their meanings in the environment of related fields, and not idealizes or meaning too formal, unless
Here it is clearly defined.
Exemplary invention described herein can suitably lack any one or more of element limitation, here without special
It is open.Therefore, "comprising", " comprising ", the term of " containing " etc. should be by wide in range and without limitation understand.In addition, being made herein
Term expression is used as describing, there is no limit, and do not include using these any equivalent characterizations term expression be
Unintentionally, their a part of characteristic is only described, but according to right, various modifications are possible within the scope of the invention.
Therefore, although the present invention has passed through preferred embodiment and optional feature is specifically disclosed, sheet of the modification disclosed herein to embody
The variation of invention may be recorded by those skilled in the art, and such modifications and variations can be considered of the invention
Within the scope of.
Compared with the prior art, beneficial effects of the present invention:
(1) freeze-drying facial mask of the invention is after frozen dried, for thermally labile, oxidizable, degradable ingredient
Very high activity can still be kept；
(2) freeze-drying facial mask of the invention is mildly non-stimulated, and zero burden makes skin be returned to the optimum state of natural equilibrium；
(3) freeze-drying facial mask of the invention is dried frozen aquatic products, does not add chemical preservative, obtains natural materials essence efficiency most
The generation of free radical is effectively resisted in big performance, and natural moisture preserving composition therein can make skin restore water profit, return clear
Thoroughly, beautiful；
(4) freeze-drying facial mask of the invention contains desert japanese rose leaf cell extract, and skin can be helped to go deep into lasting moisturizing, swashs
The natural moisturizing potential of skin is sent out, resists the formation of environment influence and aging, and the active constituent contained by it can be protected effectively
It protects cell membrane and increases the water storage function of skin, invade skin from free radical, reduce tanned and skin ageing phenomenon hair
It is raw；
(5) freeze-drying facial mask of the invention can supplement hyaluronic acid needed for skin, keep skin penetrating full full, deeply hold
Kubo is wet, moist, glossy, and skin is made to reply nature.
Specific embodiment
In order to preferably explain the present invention, it is described further now in conjunction with following specific embodiments, but the present invention is unlimited
In specific embodiment.
Embodiment 1
A kind of whitening and softening skin freeze-dried powder containing desert rose essence, according to parts by weight, including following raw material:
The amino acid is 0.1 part of dried meat amino, 0.1 part of third amino and 0.1 part of silk amino.The moisturizing factor is 0.1 part
Magnesium lactate, 0.1 part of potassium lactate, 0.1 part of magnesium chloride and 0.1 part of sodium citrate.
The preparation method of whitening and softening skin freeze-drying facial mask containing desert rose essence, comprising the following steps:
(1) mix: by desert japanese rose leaf cell extract, ethoxy urea, -8/5/3/ glycerol of PEG/PPG/ polytetramethylene glycol,
Glycerol, Sodium Hyaluronate, natural thickener, papain, calcium pantothenate, urea, pungent glycol, amino acid, moisturizing factor, ethyl
Hexyl glycerol, water mixing, stir evenly, obtain mixture；
(2) mixture is soaked into facial mask cloth；
(3) precooling: by the facial mask cloth with mixture at -25 DEG C precooling 2h；
(4) vacuum freeze drying: being freeze-dried, vacuum degree 30Pa -196 DEG C (refrigerated source selects liquid nitrogen), freezing
Drying time 3min；
(5) facial mask must be lyophilized after packing.
Embodiment 2
A kind of whitening and softening skin freeze-dried powder containing desert rose essence, according to parts by weight, including following raw material:
The amino acid is 1 part of dried meat amino, 1 part of third amino and 1 part of silk amino.The moisturizing factor is 1 part of magnesium lactate, 1
Part potassium lactate, 1 part of magnesium chloride and 1 part of sodium citrate.
The preparation method is the same as that of Example 1 for the extracting process and facial mask of desert japanese rose leaf cell extract.
Embodiment 3
A kind of whitening and softening skin freeze-dried powder containing desert rose essence, according to parts by weight, including following raw material:
The amino acid is 1 part of dried meat amino, 1 part of third amino and 1 part of silk amino.The moisturizing factor be 0.1 part of magnesium lactate,
0.1 part of potassium lactate, 0.1 part of magnesium chloride and 0.1 part of sodium citrate.
The preparation method is the same as that of Example 1 for the extracting process and facial mask of desert japanese rose leaf cell extract.
Comparative example 1
Japanese rose leaf cell extract in desert is free of in comparative example 1, remaining place is same as Example 2.
Comparative example 2
Papain and moisturizing factor are free of in comparative example 2, remaining place is same as Example 2.
Comparative example 3
The ingredient of comparative example 3 is with embodiment 2, but facial mask uses following preparation method:
(1) mix: by desert japanese rose leaf cell extract, ethoxy urea, -8/5/3/ glycerol of PEG/PPG/ polytetramethylene glycol,
Glycerol, Sodium Hyaluronate, natural thickener, papain, calcium pantothenate, urea, pungent glycol, amino acid, moisturizing factor, ethyl
Hexyl glycerol, water mixing, stir evenly, obtain mixture；
(2) mixture is soaked into facial mask cloth；
(3) (i.e. wet type facial mask does not use wink freezing dry) is vacuum-packed in an aseptic environment.
Product effect assessment: human body application test
1, test method: 210 people of volunteer (women, one full year of life at age 18-30), health status: subjects skin's health, nothing
Skin disease allergies meet subject and volunteer inclusion criteria.7 groups are randomly divided by the principle of parallel control, every group of 30 people distinguish
Use the facial mask and commercially available freeze-drying facial mask of embodiment 1-3, comparative example 1-3.1 facial mask is respectively taken after test volunteer's morning and evening face cleaning
Finished product spreads on face, and using the case where moisture of skin variation and melanin change after 30 days, test 3 times, are averaged every time.
2, detecting instrument:
Skinanalysis apparatus (South Korea EHANG, EH-990U), the moisture for detecting skin changes and melanin situation of change.
3, experimental result standard:
Effective: for moisture value between 40-50%, melanin value is lower than 20；
Effective: moisture value is between 20-30%, melanin value 20-30；
Invalid: moisture value is lower than 20%, and melanin value is 30 or more.
Table 1: volunteer's skin-whitening and moisturizing test result (people).
From table 1 it follows that 1-3 of the embodiment of the present invention has significant whitening effect, with comparative example 1-3 and commercially available jelly
Dried noodle film is compared, the cold lyophilized technique tool of desert japanese rose leaf cell extract, papain, moisturizing factor and wink in the present invention
There is synergistic function, the activity of each component can be retained to the greatest extent using moment lyophilized technique of the invention, and be
The shelf-life of effective active significantly extends and (is 5 years or more), and the validity period of the mask product of comparative example 3 only has 2 years.This
Outside, after preparing according to a certain ratio between them, whitening active can be given full play of, skin care, whitening, moisture-keeping function are aobvious
It writes.In addition it is also tested for using suspending again after 30 days using the situation after 30 days, the skin care of embodiment 1-3, whitening function are still
Obviously, it has used the whitening of the volunteer of comparative example 1-3 and commercially available freeze-drying facial mask to improve degree and apparent rebound has occurred, said
Bright facial mask of the invention has more lasting whitening, skin effect.
Above is only a specific embodiment of the present invention, it is not intended to limit the scope of the invention, all utilizations
The equivalent transformation that the present invention makees, is applied directly or indirectly in other relevant technical fields, similarly includes of the invention
Among scope of patent protection.
Claims (11)
1. the whitening and softening skin freeze-dried powder containing desert rose essence, which is characterized in that according to parts by weight, the freeze-dried powder includes
Following raw material:
2. the whitening and softening skin freeze-dried powder according to claim 1 containing desert rose essence, which is characterized in that the desert
Japanese rose leaf cell extract passes through supercritical CO2Extraction process is made.
3. the whitening and softening skin freeze-dried powder according to claim 2 containing desert rose essence, which is characterized in that described super to face
Boundary CO2The condition of extraction process are as follows: with CO2For supercritical fluid, extracting pressure is 200~500bar, and the time is 1~3h, temperature
It is 40 DEG C~50 DEG C, CO2Flow velocity is 10~20g/min.
4. the whitening and softening skin freeze-dried powder according to claim 1 containing desert rose essence, which is characterized in that described natural
Thickener include pectin, locust bean gum, Arabic gum, alginic acid, gellan gum, tragacanth, tara gum, tamarind gum, in xanthan gum
At least one.
5. the whitening and softening skin freeze-dried powder according to claim 1 containing desert rose essence, which is characterized in that the amino
Acid includes at least one of dried meat amino, the third amino, silk amino.
6. the whitening and softening skin freeze-dried powder according to claim 1 containing desert rose essence, which is characterized in that the moisturizing
The factor includes at least one of magnesium lactate, potassium lactate, magnesium chloride, sodium citrate.
7. the whitening and softening skin freeze-dried powder according to claim 1 to 6 containing desert rose essence, feature exist
In the freeze-dried powder is free of preservative, hormone, antibacterial agent.
8. the preparation method of the whitening and softening skin freeze-dried powder of any of claims 1-7 containing desert rose essence,
It is characterized in that, comprising the following steps:
(1) mix: by desert japanese rose leaf cell extract, ethoxy urea, -8/5/3/ glycerol of PEG/PPG/ polytetramethylene glycol, glycerol,
Sodium Hyaluronate, natural thickener, papain, calcium pantothenate, urea, pungent glycol, amino acid, moisturizing factor, ethylhexyl
Glycerol, water mixing, stir evenly；
(2) precooling: 1~3h of precooling at -20 DEG C to -30 DEG C；
(3) vacuum freeze drying: being freeze-dried at -180 DEG C to -196 DEG C, and vacuum degree is 5~50Pa, sublimation drying
≤10min。
9. facial mask is lyophilized in the whitening and softening skin containing desert rose essence, which is characterized in that including any one of claim 1-7 institute
The freeze-dried powder and facial mask cloth stated.
10. the preparation method of the whitening and softening skin freeze-drying facial mask as claimed in claim 9 containing desert rose essence, feature exist
In, comprising the following steps:
(A) mix: by desert japanese rose leaf cell extract, ethoxy urea, -8/5/3/ glycerol of PEG/PPG/ polytetramethylene glycol, glycerol,
Sodium Hyaluronate, natural thickener, papain, calcium pantothenate, urea, pungent glycol, amino acid, moisturizing factor, ethylhexyl
Glycerol, water mixing, stir evenly, obtain mixture；
(B) mixture is coated on to or is soaked facial mask cloth；
(C) precooling: by the facial mask cloth with mixture at -20 DEG C to -30 DEG C 1~3h of precooling；
(D) vacuum freeze drying: being freeze-dried at -180 DEG C to -196 DEG C, and vacuum degree is 5~50Pa, sublimation drying
≤10min。
11. the application method of the whitening and softening skin freeze-drying facial mask as claimed in claim 9 containing desert rose essence, feature exist
In, comprising the following steps:
(a) facial mask is put into the water of 10~40ml and is soaked；
(b) facial mask after soaking is spread on into face 10~30 minutes.
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| CN110585091A (en) * | 2019-10-25 | 2019-12-20 | 广州市拉凯尔干细胞研究所 | Preparation method of skin care product raw material containing desert rose leaf cell extract |
| CN110893169A (en) * | 2019-12-23 | 2020-03-20 | 广州微肽生物科技有限公司 | Whitening and moisturizing mask and preparation method thereof |
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| WO2021045504A1 (en) * | 2019-09-03 | 2021-03-11 | 주식회사 엘지생활건강 | Cosmetic material composition comprising solid phase polymer having improved solubility |
| CN113827503A (en) * | 2021-11-09 | 2021-12-24 | 浙江臻艾控股(集团)有限公司 | Hyaluronic acid-containing mask essence and preparation method thereof |
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| CN110302130A (en) * | 2019-07-19 | 2019-10-08 | 广州艾蓓生物科技有限公司 | A kind of multiple-effect freeze-drying facial mask and preparation method thereof |
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| CN110893169A (en) * | 2019-12-23 | 2020-03-20 | 广州微肽生物科技有限公司 | Whitening and moisturizing mask and preparation method thereof |
| CN111568819A (en) * | 2020-05-28 | 2020-08-25 | 广州隆翔化妆品有限公司 | Facial mask essence and freeze-dried crystal facial mask containing facial mask essence |
| CN113827503A (en) * | 2021-11-09 | 2021-12-24 | 浙江臻艾控股(集团)有限公司 | Hyaluronic acid-containing mask essence and preparation method thereof |
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