CN110585091A - Preparation method of skin care product raw material containing desert rose leaf cell extract - Google Patents
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/10—General cosmetic use
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
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Abstract
The invention discloses a method for preparing a skin care product raw material containing desert rose leaf cell extract, which is characterized by comprising the following steps of: the skin care product raw material containing desert rose leaf cell extract comprises A phase, B phase and C phase; wherein the phase A comprises: betaine: 0.05 part; glycerol polyacrylate: 0.05 part; glycerol: 0.05 part; water: 0.05 part; acryloyl dimethyl ammonium taurate/behenyl polyether-25: 0.12 part; methacrylate crosslinked polymer: 0.12 part; polyacrylate crosslinked polymer-6: 0.15 part; sodium hyaluronate: 0.05 part; water: 90 parts of a mixture; the phase B comprises: desert rose leaf cell extract: 0.5-2 parts; the phase C comprises: 1.2 hexanediol: 0.5 part; 0.5 part of caprylyl hydroximic acid; 0.5 part of p-hydroxyacetophenone; 0.5 part of glyceryl caprylate, and the invention can be applied to formulations of essences, water aqua, cream, emulsion and the like in personal care products.
Description
Technical Field
The invention relates to the field of skin care products, in particular to a method for preparing a skin care product raw material containing desert rose leaf cell extract.
Background
At present, the skin care products on the market have various types and different efficacies, including whitening, moisturizing, freckle removing, aging resisting and the like. However, many products are added with a few chemical substances which are harmful to human bodies, and although the substances have skin care effects of short-term whitening, anti-aging and the like on human skin, if the substances are used for a long time, the skin is seriously damaged, and acne, color spots, lipid secretion disorder and the like appear; the imitation skin care products contain a plurality of plant extracts, however, in the personal care products, the skin care products taking the plant extracts as active substances are more than hundreds of skin care products, the effect brought by the method in the personal care product is more complete according to the development of the extraction method or the biotechnology in the field of plant extraction sources, furthermore, the varieties of plant cell extracts are still few, and the living pressure of people is increasingly tense and increased due to climate change, so that the skin barrier moisturizing function is low, in view of the fact that the conventional plant extracts have a limited ability to improve the skin barrier function, further researches show that the invention can effectively improve the skin barrier moisturizing function, improve the synthesis of glycosaminoglycan in the dermis and reduce the lipid peroxidation reaction translated from MDA, therefore, a method for preparing a skin care product raw material containing the desert rose leaf cell extract is provided.
Disclosure of Invention
The invention aims to solve the defects in the prior art and provides a method for preparing a skin care product raw material containing desert rose leaf cell extract.
In order to achieve the purpose, the invention adopts the following technical scheme: a method for preparing skin care product raw materials containing desert rose leaf cell extracts is characterized in that: the skin care product raw material containing desert rose leaf cell extract comprises A phase, B phase and C phase;
wherein the phase A comprises: betaine: 0.05 part; glycerol polyacrylate: 0.05 part; glycerol: 0.05 part; water: 0.05 part; acryloyl dimethyl ammonium taurate/behenyl polyether-25: 0.12 part; methacrylate crosslinked polymer: 0.12 part; polyacrylate crosslinked polymer-6: 0.15 part; sodium hyaluronate: 0.05 part; water: 90 parts of a mixture;
the phase B comprises: desert rose leaf cell extract: 0.5-2 parts;
the phase C comprises: 1.2 hexanediol: 0.5 part; 0.5 part of caprylyl hydroximic acid; 0.5 part of p-hydroxyacetophenone; 0.5 part of glycerol caprylate.
Preferably, the preparation method of the skin care product raw material containing the desert rose leaf cell extract comprises the following steps:
s1: preparing desert rose leaf cell extract: pulverizing fresh leaves of Rosa desertorum; feeding the raw material powder into a supercritical extraction kettle for supercritical CO2 extraction; feeding the extraction mixture into a supercritical separation kettle for separation; adding the separated product into distilled water for distillation, and condensing and recovering steam to obtain a desert rose leaf cell extract;
s2: screening raw materials: preparing basic ingredients according to the component ratio of the formula: betaine: 0.05 part, glycerol polyacrylate: 0.05 part, glycerin: 0.05 part, water: 0.05 part; acryloyl dimethyl ammonium taurate/behenyl polyether-25: 0.12 part; methacrylate crosslinked polymer: 0.12 part; polyacrylate crosslinked polymer-6: 0.15 part; sodium hyaluronate: 0.05 part; water: 90 parts of a mixture; 1.2 hexanediol: 0.5 part; 0.5 part of caprylyl hydroximic acid; 0.5 part of p-hydroxyacetophenone; 0.5 part of glycerol caprylate; desert rose leaf cell extract: 0.5-2 parts;
s3: stirring for the first time: mixing the betaine selected in the step S2: 0.05 part, glycerol polyacrylate: 0.05 part, glycerin: 0.05 part, water: 0.05 part; acryloyl dimethyl ammonium taurate/behenyl polyether-25: 0.12 part; methacrylate crosslinked polymer: 0.12 part; polyacrylate crosslinked polymer-6: 0.15 part; sodium hyaluronate: 0.05 part; water: fully mixing 90 parts of the mixture, heating the mixture to 80 ℃, then pouring the mixture into a homogenizer for homogenizing for 3min, and then cooling the mixture to 35 ℃ to obtain a phase A mixture;
s4: stirring for the second time: extracting the desert rose leaf cell extract selected in the step S2: 0.5-2 parts of the mixture is added into the phase A mixture obtained in the step S3 and fully and uniformly mixed to obtain an AB phase mixture;
s5: stirring for the third time: mixing the 1.2 hexanediol selected in the step S2: 0.5 part; 0.5 part of caprylyl hydroximic acid; 0.5 part of p-hydroxyacetophenone and 0.5 part of glyceryl caprylate are put into the AB phase mixture obtained in the step S4 and are fully and uniformly mixed, and then the finished product is obtained.
Preferably, in the step S1, the desert rose leaf is physically crushed to obtain raw material powder with the particle size not larger than 40 meshes, when supercritical CO2 is used for extraction, the CO2 flow rate is 20-25 kg/h, the extraction pressure is 20-25 MPa, the extraction temperature is 35 ℃, the extraction time is 1-3 hours, the separation pressure during supercritical separation is 8-12 MPa, the temperature is 40 ℃, the separation is carried out for 1 hour, and the product of supercritical separation is added into water for distillation according to the proportion of 1 (40-60) g/L.
Preferably, in the preparation method of the skin care product raw material containing the desert rose leaf cell extract, the temperature reduction in the step S3 is natural cooling.
Preferably, in the preparation method of the skin care product raw material containing the desert rose leaf cell extract, the model of the homogenizer in the step S3 is RX-200 l.
The invention provides a preparation method of a skin care product raw material containing desert rose leaf cell extract, which improves the skin barrier moisturizing function, improves the synthesis of glycosaminoglycan in the dermis layer, reduces lipid peroxidation reaction translated from MDA and lipid peroxidation reaction induced by UVB, and has visual observation of the desert rose leaf cell extract on the appearance of the product.
Drawings
FIG. 1 is a flow chart of the preparation of the present invention;
FIG. 2 is a table showing the comparison between the new synthesis of glycosaminoglycan found in coculture with human fibroblasts according to the present invention;
FIG. 3 is a table showing the decrease in lipid peroxidation resulting from the translation of MDA of the present invention.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is further described in detail with reference to the following embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.
Example one
A method for preparing skin care product raw material containing desert rose leaf cell extract comprises A phase, B phase and C phase;
wherein the phase A comprises: betaine: 0.05 part; glycerol polyacrylate: 0.05 part; glycerol: 0.05 part; water: 0.05 part; acryloyl dimethyl ammonium taurate/behenyl polyether-25: 0.12 part; methacrylate crosslinked polymer: 0.12 part; polyacrylate crosslinked polymer-6: 0.15 part; sodium hyaluronate: 0.05 part; water: 90 parts of a mixture;
the phase B comprises: desert rose leaf cell extract: 0.5-2 parts;
the phase C comprises: 1.2 hexanediol: 0.5 part; 0.5 part of caprylyl hydroximic acid; 0.5 part of p-hydroxyacetophenone; 0.5 part of glycerol caprylate.
The preparation method of the skin care product raw material containing the desert rose leaf cell extract comprises the following steps:
s1: preparing desert rose leaf cell extract: pulverizing fresh leaves of Rosa desertorum; feeding the raw material powder into a supercritical extraction kettle for supercritical CO2 extraction; feeding the extraction mixture into a supercritical separation kettle for separation; adding the separated product into distilled water for distillation, and condensing and recovering steam to obtain a desert rose leaf cell extract;
s2: screening raw materials: preparing basic ingredients according to the component ratio of the formula: betaine: 0.05 part, glycerol polyacrylate: 0.05 part, glycerin: 0.05 part, water: 0.05 part; acryloyl dimethyl ammonium taurate/behenyl polyether-25: 0.12 part; methacrylate crosslinked polymer: 0.12 part; polyacrylate crosslinked polymer-6: 0.15 part; sodium hyaluronate: 0.05 part; water: 90 parts of a mixture; 1.2 hexanediol: 0.5 part; 0.5 part of caprylyl hydroximic acid; 0.5 part of p-hydroxyacetophenone; 0.5 part of glycerol caprylate; desert rose leaf cell extract: 0.5-2 parts;
s3: stirring for the first time: mixing the betaine selected in the step S2: 0.05 part, glycerol polyacrylate: 0.05 part, glycerin: 0.05 part, water: 0.05 part; acryloyl dimethyl ammonium taurate/behenyl polyether-25: 0.12 part; methacrylate crosslinked polymer: 0.12 part; polyacrylate crosslinked polymer-6: 0.15 part; sodium hyaluronate: 0.05 part; water: fully mixing 90 parts of the mixture, heating the mixture to 80 ℃, then pouring the mixture into a homogenizer for homogenizing for 3min, and then cooling the mixture to 35 ℃ to obtain a phase A mixture;
s4: stirring for the second time: extracting the desert rose leaf cell extract selected in the step S2: 0.5 part of the mixture is added into the phase A mixture obtained in the step S3 and fully and uniformly mixed to obtain an AB phase mixture;
s5: stirring for the third time: mixing the 1.2 hexanediol selected in the step S2: 0.5 part; 0.5 part of caprylyl hydroximic acid; 0.5 part of p-hydroxyacetophenone and 0.5 part of glyceryl caprylate are put into the AB phase mixture obtained in the step S4 and are fully and uniformly mixed, and then the finished product is obtained.
Wherein, in the step S1, the leaves of the rosa deserticola are physically crushed to raw material powder with the grain diameter not more than 40 meshes, when supercritical CO2 is used for extraction, the flow rate of CO2 is 20-25 kg/h, the extraction pressure is 20-25 MPa, the extraction temperature is 35 ℃, the extraction time is 1-3 hours, the separation pressure during supercritical separation is 8-12 MPa, the temperature is 40 ℃, the separation time is 1 hour, and the product of the supercritical separation is added into water for distillation according to the proportion of the material-liquid ratio of 1 (40-60) g/L; the temperature reduction in the step S3 is natural cooling; the model of the homogenizer in the step S3 is RX-200 l.
Example two
A method for preparing skin care product raw material containing desert rose leaf cell extract comprises A phase, B phase and C phase;
wherein the phase A comprises: betaine: 0.05 part; glycerol polyacrylate: 0.05 part; glycerol: 0.05 part; water: 0.05 part; acryloyl dimethyl ammonium taurate/behenyl polyether-25: 0.12 part; methacrylate crosslinked polymer: 0.12 part; polyacrylate crosslinked polymer-6: 0.15 part; sodium hyaluronate: 0.05 part; water: 90 parts of a mixture;
the phase B comprises: desert rose leaf cell extract: 0.5-2 parts;
the phase C comprises: 1.2 hexanediol: 0.5 part; 0.5 part of caprylyl hydroximic acid; 0.5 part of p-hydroxyacetophenone; 0.5 part of glycerol caprylate.
The preparation method of the skin care product raw material containing the desert rose leaf cell extract comprises the following steps:
s1: preparing desert rose leaf cell extract: pulverizing fresh leaves of Rosa desertorum; feeding the raw material powder into a supercritical extraction kettle for supercritical CO2 extraction; feeding the extraction mixture into a supercritical separation kettle for separation; adding the separated product into distilled water for distillation, and condensing and recovering steam to obtain a desert rose leaf cell extract;
s2: screening raw materials: preparing basic ingredients according to the component ratio of the formula: betaine: 0.05 part, glycerol polyacrylate: 0.05 part, glycerin: 0.05 part, water: 0.05 part; acryloyl dimethyl ammonium taurate/behenyl polyether-25: 0.12 part; methacrylate crosslinked polymer: 0.12 part; polyacrylate crosslinked polymer-6: 0.15 part; sodium hyaluronate: 0.05 part; water: 90 parts of a mixture; 1.2 hexanediol: 0.5 part; 0.5 part of caprylyl hydroximic acid; 0.5 part of p-hydroxyacetophenone; 0.5 part of glycerol caprylate; desert rose leaf cell extract: 0.5-2 parts;
s3: stirring for the first time: mixing the betaine selected in the step S2: 0.05 part, glycerol polyacrylate: 0.05 part, glycerin: 0.05 part, water: 0.05 part; acryloyl dimethyl ammonium taurate/behenyl polyether-25: 0.12 part; methacrylate crosslinked polymer: 0.12 part; polyacrylate crosslinked polymer-6: 0.15 part; sodium hyaluronate: 0.05 part; water: fully mixing 90 parts of the mixture, heating the mixture to 80 ℃, then pouring the mixture into a homogenizer for homogenizing for 3min, and then cooling the mixture to 35 ℃ to obtain a phase A mixture;
s4: stirring for the second time: extracting the desert rose leaf cell extract selected in the step S2: adding 1 part of the mixture into the phase A mixture obtained in the step S3, and fully and uniformly mixing to obtain an AB phase mixture;
s5: stirring for the third time: mixing the 1.2 hexanediol selected in the step S2: 0.5 part; 0.5 part of caprylyl hydroximic acid; 0.5 part of p-hydroxyacetophenone and 0.5 part of glyceryl caprylate are put into the AB phase mixture obtained in the step S4 and are fully and uniformly mixed, and then the finished product is obtained.
Wherein, in the step S1, the leaves of the rosa deserticola are physically crushed to raw material powder with the grain diameter not more than 40 meshes, when supercritical CO2 is used for extraction, the flow rate of CO2 is 20-25 kg/h, the extraction pressure is 20-25 MPa, the extraction temperature is 35 ℃, the extraction time is 1-3 hours, the separation pressure during supercritical separation is 8-12 MPa, the temperature is 40 ℃, the separation time is 1 hour, and the product of the supercritical separation is added into water for distillation according to the proportion of the material-liquid ratio of 1 (40-60) g/L; the temperature reduction in the step S3 is natural cooling; the model of the homogenizer in the step S3 is RX-200 l.
EXAMPLE III
A method for preparing skin care product raw material containing desert rose leaf cell extract comprises A phase, B phase and C phase;
wherein the phase A comprises: betaine: 0.05 part; glycerol polyacrylate: 0.05 part; glycerol: 0.05 part; water: 0.05 part; acryloyl dimethyl ammonium taurate/behenyl polyether-25: 0.12 part; methacrylate crosslinked polymer: 0.12 part; polyacrylate crosslinked polymer-6: 0.15 part; sodium hyaluronate: 0.05 part; water: 90 parts of a mixture;
the phase B comprises: desert rose leaf cell extract: 0.5-2 parts;
the phase C comprises: 1.2 hexanediol: 0.5 part; 0.5 part of caprylyl hydroximic acid; 0.5 part of p-hydroxyacetophenone; 0.5 part of glycerol caprylate.
The preparation method of the skin care product raw material containing the desert rose leaf cell extract comprises the following steps:
s1: preparing desert rose leaf cell extract: pulverizing fresh leaves of Rosa desertorum; feeding the raw material powder into a supercritical extraction kettle for supercritical CO2 extraction; feeding the extraction mixture into a supercritical separation kettle for separation; adding the separated product into distilled water for distillation, and condensing and recovering steam to obtain a desert rose leaf cell extract;
s2: screening raw materials: preparing basic ingredients according to the component ratio of the formula: betaine: 0.05 part, glycerol polyacrylate: 0.05 part, glycerin: 0.05 part, water: 0.05 part; acryloyl dimethyl ammonium taurate/behenyl polyether-25: 0.12 part; methacrylate crosslinked polymer: 0.12 part; polyacrylate crosslinked polymer-6: 0.15 part; sodium hyaluronate: 0.05 part; water: 90 parts of a mixture; 1.2 hexanediol: 0.5 part; 0.5 part of caprylyl hydroximic acid; 0.5 part of p-hydroxyacetophenone; 0.5 part of glycerol caprylate; desert rose leaf cell extract: 0.5-2 parts;
s3: stirring for the first time: mixing the betaine selected in the step S2: 0.05 part, glycerol polyacrylate: 0.05 part, glycerin: 0.05 part, water: 0.05 part; acryloyl dimethyl ammonium taurate/behenyl polyether-25: 0.12 part; methacrylate crosslinked polymer: 0.12 part; polyacrylate crosslinked polymer-6: 0.15 part; sodium hyaluronate: 0.05 part; water: fully mixing 90 parts of the mixture, heating the mixture to 80 ℃, then pouring the mixture into a homogenizer for homogenizing for 3min, and then cooling the mixture to 35 ℃ to obtain a phase A mixture;
s4: stirring for the second time: extracting the desert rose leaf cell extract selected in the step S2: 2 parts of the mixture is added into the phase A mixture obtained in the step S3 and fully and uniformly mixed to obtain an AB phase mixture;
s5: stirring for the third time: mixing the 1.2 hexanediol selected in the step S2: 0.5 part; 0.5 part of caprylyl hydroximic acid; 0.5 part of p-hydroxyacetophenone and 0.5 part of glyceryl caprylate are put into the AB phase mixture obtained in the step S4 and are fully and uniformly mixed, and then the finished product is obtained.
Wherein, in the step S1, the leaves of the rosa deserticola are physically crushed to raw material powder with the grain diameter not more than 40 meshes, when supercritical CO2 is used for extraction, the flow rate of CO2 is 20-25 kg/h, the extraction pressure is 20-25 MPa, the extraction temperature is 35 ℃, the extraction time is 1-3 hours, the separation pressure during supercritical separation is 8-12 MPa, the temperature is 40 ℃, the separation time is 1 hour, and the product of the supercritical separation is added into water for distillation according to the proportion of the material-liquid ratio of 1 (40-60) g/L; the temperature reduction in the step S3 is natural cooling; the model of the homogenizer in the step S3 is RX-200 l.
The results of the extracellular tests, which were found by two tests and by visual tests added to the product, have demonstrated improved skin barrier moisturizing function and increased synthesis of glycosaminoglycans in the dermis with a decrease in lipid peroxidation translated from MDA and a decrease in lipid peroxidation induced by UVB.
Claims (5)
1. A method for preparing skin care product raw materials containing desert rose leaf cell extracts is characterized in that: the skin care product raw material containing desert rose leaf cell extract comprises A phase, B phase and C phase;
wherein the phase A comprises: betaine: 0.05 part; glycerol polyacrylate: 0.05 part; glycerol: 0.05 part; water: 0.05 part; acryloyl dimethyl ammonium taurate/behenyl polyether-25: 0.12 part; methacrylate crosslinked polymer: 0.12 part; polyacrylate crosslinked polymer-6: 0.15 part; sodium hyaluronate: 0.05 part; water: 90 parts of a mixture;
the phase B comprises: desert rose leaf cell extract: 0.5-2 parts;
the phase C comprises: 1.2 hexanediol: 0.5 part; 0.5 part of caprylyl hydroximic acid; 0.5 part of p-hydroxyacetophenone; 0.5 part of glycerol caprylate.
2. The method for preparing skin care product raw material containing desert rose leaf cell extract as claimed in claim 1, characterized in that: the preparation method of the skin care product raw material containing the desert rose leaf cell extract comprises the following steps:
s1: preparing desert rose leaf cell extract: pulverizing fresh leaves of Rosa desertorum; feeding the raw material powder into a supercritical extraction kettle for supercritical CO2 extraction; feeding the extraction mixture into a supercritical separation kettle for separation; adding the separated product into distilled water for distillation, and condensing and recovering steam to obtain a desert rose leaf cell extract;
s2: screening raw materials: preparing basic ingredients according to the component ratio of the formula: betaine: 0.05 part, glycerol polyacrylate: 0.05 part, glycerin: 0.05 part, water: 0.05 part; acryloyl dimethyl ammonium taurate/behenyl polyether-25: 0.12 part; methacrylate crosslinked polymer: 0.12 part; polyacrylate crosslinked polymer-6: 0.15 part; sodium hyaluronate: 0.05 part; water: 90 parts of a mixture; 1.2 hexanediol: 0.5 part; 0.5 part of caprylyl hydroximic acid; 0.5 part of p-hydroxyacetophenone; 0.5 part of glycerol caprylate; desert rose leaf cell extract: 0.5-2 parts;
s3: stirring for the first time: mixing the betaine selected in the step S2: 0.05 part, glycerol polyacrylate: 0.05 part, glycerin: 0.05 part, water: 0.05 part; acryloyl dimethyl ammonium taurate/behenyl polyether-25: 0.12 part; methacrylate crosslinked polymer: 0.12 part; polyacrylate crosslinked polymer-6: 0.15 part; sodium hyaluronate: 0.05 part; water: fully mixing 90 parts of the mixture, heating the mixture to 80 ℃, then pouring the mixture into a homogenizer for homogenizing for 3min, and then cooling the mixture to 35 ℃ to obtain a phase A mixture;
s4: stirring for the second time: extracting the desert rose leaf cell extract selected in the step S2: 0.5-2 parts of the mixture is added into the phase A mixture obtained in the step S3 and fully and uniformly mixed to obtain an AB phase mixture;
s5: stirring for the third time: mixing the 1.2 hexanediol selected in the step S2: 0.5 part; 0.5 part of caprylyl hydroximic acid; 0.5 part of p-hydroxyacetophenone and 0.5 part of glyceryl caprylate are put into the AB phase mixture obtained in the step S4 and are fully and uniformly mixed, and then the finished product is obtained.
3. The method for preparing skin care product raw material containing desert rose leaf cell extract as claimed in claim 2, characterized in that: in the step S1, the leaves of the rosa deserticola are physically crushed to be raw material powder with the grain diameter not larger than 40 meshes, when supercritical CO2 is used for extraction, the flow rate of CO2 is 20-25 kg/h, the extraction pressure is 20-25 MPa, the extraction temperature is 35 ℃, the extraction time is 1-3 hours, the separation pressure during supercritical separation is 8-12 MPa, the temperature is 40 ℃, the separation time is 1 hour, and the product of the supercritical separation is added into water for distillation according to the proportion that the material-to-liquid ratio is 1 (40-60) g/L.
4. The method for preparing skin care product raw material containing desert rose leaf cell extract as claimed in claim 2, characterized in that: the temperature reduction in step S3 is natural cooling.
5. The method for preparing skin care product raw material containing desert rose leaf cell extract as claimed in claim 2, characterized in that: the model of the homogenizer in the step S3 is RX-200 l.
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| CN113633605A (en) * | 2021-08-13 | 2021-11-12 | 广州赛莱拉生物基因工程有限公司 | Composition and application thereof in preparing anti-allergy cosmetics |
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