CN109989298A - A kind of flowers and fruits odor type cigarette paper and preparation method thereof - Google Patents
A kind of flowers and fruits odor type cigarette paper and preparation method thereof Download PDFInfo
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- CN109989298A CN109989298A CN201910388127.8A CN201910388127A CN109989298A CN 109989298 A CN109989298 A CN 109989298A CN 201910388127 A CN201910388127 A CN 201910388127A CN 109989298 A CN109989298 A CN 109989298A
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- Prior art keywords
- flowers
- fruits
- cigarette paper
- odor type
- paper
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Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
- A24D1/02—Cigars; Cigarettes with special covers
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21F—PAPER-MAKING MACHINES; METHODS OF PRODUCING PAPER THEREON
- D21F11/00—Processes for making continuous lengths of paper, or of cardboard, or of wet web for fibre board production, on paper-making machines
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/02—Material of vegetable origin
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/03—Non-macromolecular organic compounds
- D21H17/05—Non-macromolecular organic compounds containing elements other than carbon and hydrogen only
- D21H17/06—Alcohols; Phenols; Ethers; Aldehydes; Ketones; Acetals; Ketals
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/63—Inorganic compounds
- D21H17/67—Water-insoluble compounds, e.g. fillers, pigments
- D21H17/675—Oxides, hydroxides or carbonates
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/63—Inorganic compounds
- D21H17/67—Water-insoluble compounds, e.g. fillers, pigments
- D21H17/68—Water-insoluble compounds, e.g. fillers, pigments siliceous, e.g. clays
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H19/00—Coated paper; Coating material
- D21H19/10—Coatings without pigments
- D21H19/14—Coatings without pigments applied in a form other than the aqueous solution defined in group D21H19/12
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
- D21H21/16—Sizing or water-repelling agents
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H27/00—Special paper not otherwise provided for, e.g. made by multi-step processes
- D21H27/10—Packing paper
Abstract
The present invention provides a kind of flowers and fruits odor type cigarette paper and preparation method thereof, belong to cigarette paper technical field.Flowers and fruits odor type cigarette paper provided by the invention includes the component of following mass parts: 65~85 parts of fiber；15~40 parts of filler；0.5~8 part of combustion adjuvant；0.1~3 part of flowers and fruits flavor essence.Flowers and fruits odor type cigarette paper provided by the invention has flowers and fruits class fragrance, can assign cigarette unique suction sense organ, and can modify flue gas, covers the irritation in cigarette smoking, improves smoking property of cigarette quality and mouthfeel, and fragrance stability is high.Flowers and fruits flavor essence is added in sizing agent by preparation method provided by the invention, dispersion is formed with ethyl alcohol, combustion adjuvant and water, flowers and fruits flavor essence is added in cigarette paper by way of top sizing, do not change existing equipment, additional process is not added, can be effectively reduced the flavoring cost of cigarette paper.
Description
Technical field
The present invention relates to cigarette paper technical field, in particular to a kind of flowers and fruits odor type cigarette paper and preparation method thereof.
Background technique
Auxiliary material of the cigarette paper as cigarette manufactures although its quality only accounts for the 5% of whole branch cigarette quality in cigarette
It is one of essential raw material in the process, compared with other cigarette supplementaries, cigarette paper is unique directly participation in addition to pipe tobacco
The component of burning can generate xylon gas in combustion process, will affect and suck taste quality.In recent years, as people are to cigarette
Product differentiation, personalized pursuit, cigarette enterprise are attempted to add other fragrant source substances into cigarette paper, and cigarette paper is made to have perfume (or spice)
Gas can also reduce and cover the wooden breath that cigarette paper comes out while playing the role of adjusting and modifying flue gas,
And then improve smoking property of cigarette quality and mouthfeel.Therefore, how to improve cigarette paper and cigarette is had become to the influence of cigarette odor-absorbing
The hot spot of paper industry exploitation.
Influence of the cigarette paper to cigarette odor-absorbing is promoted, one of method therein is exactly that various essence are added in cigarette paper,
Assign sense of taste of the cigarette with comfortable tastes such as red wine, dried orange peel, roses in aspiration procedure.But cigarette paper essence adds at present
Add mode is largely, using soluble perfume and metallic salt combustion adjuvant mixed configuration, to be added to volume in paper-making sizing workshop section
In cigarette paper.But the fragrant source substance of many flowers and fruits odor types mostlys come from alcohol, oily matter, such as rose, dried orange peel, walnut, pine
Son etc. is not particularly suited at present using water as the resin application methods of carrier.
In order to solve the problems, such as addition alcohol, oily matter essence, a variety of solutions have been proposed in the industry.Such as patent Shen
Number a kind of cigarette paper and preparation method thereof containing Red wine extract, method please be disclosed for 201610050851.6 patent
To use 95% ethanol solution and Red wine extract mixed configuration, added using the secondary coating feed liquid mode of offline coating machine.But
It is to need to purchase new equipment, the artificial, place of additional manpower etc., while repetition processing can reduce product using offline coating machine
Yield rate and raising production cost.
Application No. is the patents of CN201510810210.1 to disclose a kind of aloe cigarette paper and preparation method thereof, selects
Method be directly to be mixed with beating aloe and cigarette paper wood pulp cellulose, then by mashing, refining, upper net forming, squeezing, do
It is dry and etc. that aloe cigarette paper is prepared.The invention uses the method that fragrant source substance is added into wood pulp cellulose, fragrant source substance
It needing to act on by multiple machine with wood pulp and can just obtain product, these processes can cause biggish destruction to fragrant source raw material,
Product stability is reduced, and causes the waste of fragrant source raw material, improves cost.
Such as a kind of rose scent cigarette paper of the number of applying for a patent 201811177353.3 and preparation method thereof, using microcapsules packet
Modified method is wrapped up in, alcohol-soluble essence is made to switch to be dissolved in water, to realize the addition of alcohol-soluble essence in cigarette paper.The invention makes
With the modified method of encapsulation, but alcohol-soluble microcapsules preparation section is complicated, modified embedding rate only have 40~50% it
Between, while yield rate is low, has significantly drawn high the production preparation cost of cigarette paper.
How under conditions of not changing existing equipment and addition additional process, reach the perfume (or spice) with flowers and fruits odor type
Smart fragrance is added in cigarette paper, and there is presently no suitable methods.And to there is fragrance in existing flavoring cigarette paper steady mostly
The disadvantage of qualitative difference, odor characteristic can fade away after saving for a long time, so that cigarette aspirates taste bad.Therefore, how to protect
Demonstrate,prove the fragrance stability and a problem to be solved of flavoring cigarette paper.
Summary of the invention
In view of this, it is an object of that present invention to provide a kind of flowers and fruits odor type cigarette paper and preparation method thereof.The present invention provides
Flowers and fruits odor type cigarette paper flowers and fruits category feature it is aromatic strongly fragrant, fragrance stability is high；Preparation method provided by the invention does not change existing
Production equipment does not add additional process, and cigarette unique flowers and fruits odor type can be assigned while reducing cigarette paper flavoring cost
Mouthfeel.
In order to achieve the above-mentioned object of the invention, the present invention the following technical schemes are provided:
The present invention provides a kind of flowers and fruits odor type cigarette paper, the component including following mass parts:
Preferably, the fiber includes wood pulp cellulose and/or ramie pulp fiber.
Preferably, the filler includes one or more of calcium carbonate, talcum powder and diatomite；The partial size of the filler
It is 2~20 μm.
Preferably, the combustion adjuvant includes one of citrate, malate, tartrate and lactate or several
Kind.
Preferably, the flowers and fruits type essence includes sweet orange oil, dried orange peel essential oil, purple perilla leaf essential oil, lemon, olive essence
One or more of oil, vanilla essential oil, spearmint essential oil and walnut essential oil.
The present invention provides the preparation methods of above-mentioned flowers and fruits odor type cigarette paper, comprising the following steps:
(1) size degradation and mashing are successively carried out after mixing fiber with water, obtain fibre stuff；
(2) it manufactures paper with pulp after mixing the fibre stuff with filler, obtains mixed slurry；
(3) mixed slurry successively formed, be dehydrated, being embossed and first is dry, obtaining the first dry paper web；
(4) the described first dry paper web is successively subjected to top sizing and the second drying, obtains flowers and fruits odor type cigarette paper；
The top sizing sizing agent includes the component of following mass percentage:
Preferably, the beating degree of fibre stuff is 60~100 ° in the step (1).
Preferably, the described first dry initial temperature is 60~70 DEG C, and final temperature is 100~110 DEG C；Described second
Dry initial temperature is 40~50 DEG C, and final temperature is 70~80 DEG C.
Preferably, the sizing agent preparation method the following steps are included:
Flowers and fruits flavor essence is dissolved in ethyl alcohol, water is then sequentially added and combustion adjuvant is mixed, obtain sizing agent.
Preferably, the mode of top sizing is two-sided spray, one side coating, intaglio plate coating, comma roller in the step (4)
Coating or the coating of crack squash type.
The present invention provides a kind of flowers and fruits odor type cigarette paper, the component including following mass parts: 65~85 parts of fiber；Filler
15~40 parts；0.5~8 part of combustion adjuvant；0.1~3 part of flowers and fruits flavor essence.Flowers and fruits odor type cigarette paper provided by the invention has flower
Fruit fragrance can assign cigarette unique suction sense organ, and can modify flue gas, cover the irritation in cigarette smoking, improve volume
Cigarette sucking quality and mouthfeel, and fragrance stability is high.Embodiment the result shows that, flowers and fruits odor type cigarette paper flowers and fruits provided by the invention
Category feature is aromatic strongly fragrant, and flowers and fruits category feature odor characteristic is still obvious after 365 days.
The present invention provides a kind of preparation method of flowers and fruits odor type cigarette paper, flowers and fruits flavor essence is added to and applies by the present invention
In jelly, dispersion is formed with ethyl alcohol, combustion adjuvant and water, flowers and fruits flavor essence is added to volume by way of top sizing
It in cigarette paper, avoids spice material and is directly mixed with fiber, cause stability to decline by the mechanism of size degradation
Problem；The problem of avoiding secondary coating spice material leads to decrease in yield, and cost increases；And without microcapsules packet
Modification is buried, operation is simpler, and cost is lower.Meanwhile preparation method provided by the invention overcomes traditional perfuming process flavoring
The low problem of retention, gained cigarette paper flowers and fruits category feature is aromatic strongly fragrant, and fragrance stability is high.Preparation method provided by the invention is not
Change existing equipment, do not add additional process, can be effectively reduced the flavoring cost of cigarette paper, and do not pollute production line,
It is easy to operate.
Specific embodiment
The present invention provides a kind of flowers and fruits odor type cigarette paper, the component including following mass parts:
Unless otherwise specified, it is wanted without special in the source for the specific raw material that the present invention uses the flowers and fruits odor type cigarette paper
It asks, using commercial goods well-known to those skilled in the art.
In terms of mass fraction, flowers and fruits odor type cigarette paper provided by the invention includes 65~85 parts of fiber, preferably 70~
85 parts, more preferably 85 parts.In the present invention, the fiber preferably includes wood pulp cellulose and/or ramie pulp fiber；When the fiber
When simultaneously including wood pulp cellulose and ramie pulp fiber, in the fiber mass content of ramie pulp fiber preferably≤30%, more preferably
15~25%.
On the basis of the mass fraction of the fiber, flowers and fruits odor type cigarette paper provided by the invention includes 15~40 parts and fills out
Material, preferably 20~35 parts, more preferably 25~30 parts.In the present invention, the filler preferably include calcium carbonate, talcum powder and
One or more of diatomite；When the filler includes two or three of calcium carbonate, talcum powder and diatomite, the present invention
There is no special restriction for the additive amount of various components, using any proportion.In the present invention, the partial size of the filler
Preferably 2~20 μm, more preferably 5~15 μm.It, can be with by the present invention in that use calcium carbonate, talcum powder, diatomite as filler
Page is filled, fiber consumption is reduced, cigarette paper whiteness, opacity and paper is improved and is glued absorbability, while adjusting cigarette paper
Combustibility and air permeability performance.
On the basis of the mass fraction of the fiber, flowers and fruits odor type cigarette paper provided by the invention, which includes 0.5~8 part, to be helped
Fire agent, preferably 1~5 part, more preferably 2~3 parts.In the present invention, the combustion adjuvant preferably includes citrate, malic acid
One or more of salt, tartrate and lactate；The citrate preferably includes potassium citrate and/or sodium citrate,
The malate preferably includes potassium malate and/or natrium malicum, and the tartrate preferably includes potassium tartrate and/or wine
Stone acid sodium, the lactate preferably include potassium lactate and/or sodium lactate.In the present invention, when the combustion adjuvant is said components
In two kinds or more when, the present invention does not have the additive amount of each component special restriction, using any proportion.This hair
It is bright by using mentioned component as combustion adjuvant, the burning speed of cigarette paper can be controlled while guaranteeing cigarette paper full combustion
Degree improves cigarette grey and cigarette burning carbonization line color.
On the basis of the mass fraction of the fiber, flowers and fruits odor type cigarette paper provided by the invention includes 0.1~3 part of flower
Fruity type essence, preferably 0.3~2 part, more preferably 0.5~1 part.In the present invention, the flowers and fruits flavor essence preferably wraps
Include sweet orange oil, dried orange peel essential oil, purple perilla leaf essential oil, lemon, olive essential oil, vanilla essential oil, spearmint essential oil and walnut essence
One or more of oil；When the flowers and fruits flavor essence is two kinds or more in said components, the present invention is for each group
The additive amount divided does not have special restriction, using any proportion.In the present invention, it is only to assign cigarette for flowers and fruits flavor essence
Special suction sense organ can play the role of modification flue gas, cover the irritation in cigarette smoking, improve comfort.The present invention will
Flowers and fruits class essential oil is added in cigarette paper, and Consumers' Acceptance is high, is easy to marketing.
The present invention also provides the preparation methods of above-mentioned flowers and fruits odor type cigarette paper, comprising the following steps:
(1) size degradation and mashing are successively carried out after mixing fiber with water, obtain fibre stuff；
(2) it manufactures paper with pulp after mixing the fibre stuff with filler, obtains mixed slurry；
(3) mixed slurry successively formed, be dehydrated, being embossed and first is dry, obtaining the first dry paper web；
(4) the described first dry paper web is successively subjected to top sizing and the second drying, obtains flowers and fruits odor type cigarette paper.
The present invention successively carries out size degradation and mashing after mixing fiber with water, obtains fibre stuff.In the present invention, described
The mass concentration of fiber is preferably 2~5% in the mixture of fiber and water.The present invention is to the hybrid mode of fiber and water without spy
Different requirement uses hybrid mode well known to those skilled in the art.The present invention is not special to the equipment of the size degradation
It limits, using size degradation equipment well known to those skilled in the art, specially hydrabrusher；The present invention passes through the present invention
Being sufficiently mixed for fiber and water may be implemented in size degradation.
The present invention does not require the operation of the mashing specifically, is operated using mashing well known to those skilled in the art
?.In the present invention, the beating degree of gained fibre stuff is preferably 60~100 ° after the mashing, and more preferably 70~90 °,
Most preferably 80 °.The present invention does not have special requirement to the equipment of mashing, uses beating equipment well known to those skilled in the art
, specific such as mill.The present invention can use physical method by mashing, carries out mechanical or fluid to fiber in water and handles,
Make fiber by shearing force, change the form of fiber, be conducive to wet process and manufacture paper with pulp, half obtained wet web flexibility is good, breathe freely and
Tensile energy is high, to guarantee that finally obtained cigarette paper reaches expected cigarette paper physical index requirement.
After obtaining fibre stuff, the present invention manufactures paper with pulp after mixing the fibre stuff with filler, obtains mixed slurry.
In the present invention, the mass concentration that the fibre stuff mixes filler in gained mixture with filler is preferably 8~20%, more excellent
It is selected as 10~15%.The present invention does not have special requirement to the mode manufactured paper with pulp, and is copied using well known to those skilled in the art
Mode is made, specifically as wet process is manufactured paper with pulp.
After obtaining mixed slurry, the mixed slurry is successively formed, is dehydrated, embossed by the present invention and first is dry,
Obtain the first dry paper web.In the present invention, the molding mode specifically: equably from head box by the mixed slurry
It is ejected into web part of paper machine, is formed after vacuumizing, half wet web is obtained.In the present invention, the humidity of half wet web is preferably
40~60%, more preferably 45~55%, most preferably 45~50%.The present invention is to the mode of the dehydration and embossing without spy
Different requirement uses dehydration well known to those skilled in the art and embossing mode.
In the present invention, the humidity of the described first dry paper web is preferably 3~15%, and more preferably 4~14%, most preferably
It is 5~10%；Described first dry initial temperature is preferably 60~70 DEG C, more preferably 61~69 DEG C, most preferably 65 DEG C；
Described first dry final temperature is preferably 100~110 DEG C, more preferably 101~109 DEG C, most preferably 105 DEG C.This hair
Bright to start to warm up from initial temperature, gradually heat up final temperature.Present invention preferably employs cylinder groups to carry out first dry, the present invention
There is no special restriction for the specific setting condition of the described first dry time and the cylinder group, can guarantee uniformly
The humidity of the dry paper web of dry and gained first is met the requirements.
After obtaining the first dry paper web, the described first dry paper web is successively carried out top sizing and second dry by the present invention
It is dry, obtain flowers and fruits odor type cigarette paper.In the present invention, the top sizing sizing agent includes the group of following mass percentage
Point:
In terms of mass percentage, top sizing sizing agent of the present invention includes 40~60% water, and preferably 45
~55%.
In terms of mass percentage, top sizing sizing agent of the present invention includes 0.05~0.15% flowers and fruits odor type
Essence, preferably 0.08~0.1%.In the present invention, the type of the flowers and fruits flavor essence and above-mentioned flowers and fruits odor type cigarette paper
In flowers and fruits flavor essence type it is identical, details are not described herein.
In terms of mass percentage, top sizing sizing agent of the present invention includes 39.7~59.7% ethyl alcohol, excellent
It is selected as 40~55%.In the present invention, the volumetric concentration of the ethyl alcohol is preferably 95%.
In terms of mass percentage, top sizing sizing agent of the present invention includes 0.25~0.4% combustion adjuvant, excellent
It is selected as 0.3~0.35%.In the present invention, the kind of the type of the combustion adjuvant and the combustion adjuvant in above-mentioned flowers and fruits odor type cigarette paper
Class is identical, and details are not described herein.
In the present invention, the preparation method of the sizing agent preferably includes following steps:
Flowers and fruits flavor essence is dissolved in ethyl alcohol, water is then sequentially added and combustion adjuvant is mixed, obtain sizing agent.
Flowers and fruits flavor essence is preferably dissolved in ethyl alcohol by the present invention under agitation, obtains flowers and fruits odor type solvent.?
In the present invention, the rate of the stirring is preferably 40~70rpm, more preferably 50rpm；The time of the stirring is preferably 30~
60min, more preferably 40~50min；Present invention preferably uses propeller mixers to be stirred；The present invention by stirring so that
Essence is completely dissolved.
After obtaining flowers and fruits odor type solvent, water successively is added to flowers and fruits odor type solvent by the present invention and combustion adjuvant mixes, and obtains
To sizing agent.In the present invention, the hybrid mode of the water, combustion adjuvant and flowers and fruits odor type solvent is preferably stirred；This hair
Water is added in flowers and fruits odor type solvent and is once stirred for bright preferred elder generation, adds combustion adjuvant later and carries out secondary agitation, obtains
Sizing agent.In the present invention, the rate once stirred is preferably 40~70rpm, more preferably 50rpm；It is described once to stir
The time mixed preferably 30~60min, more preferably 40~50min；The rate of the secondary agitation is preferably 80~160rpm, more
Preferably 100~140rpm；The time of the secondary agitation is preferably 30~60min, more preferably 40~50min.The present invention
Using ethyl alcohol as solvent, flowers and fruits flavor essence is first dissolved, then mixed dispersion is made in proportion with water, combustion adjuvant, pass through sizing
Mode is added to flowers and fruits class essential oil in cigarette paper, guarantees the unique suction mouthfeel for assigning cigarette flowers and fruits odor type.In the present invention,
Volatile quantity of flowers and fruits flavor essence durings sizing and drying etc. is ignored.
In the present invention, the mode of the top sizing is preferably two-sided spray, one side coating, intaglio plate coating, comma roller
Coating or the coating of crack squash type；Described second dry initial temperature is preferably 40~50 DEG C, and more preferably 45 DEG C；Described
Two dry final temperatures are preferably 70~80 DEG C, and more preferably 75 DEG C.In the present invention, described second it is dry after paper web it is wet
Degree preferably 4~6%, more preferably 4.5~5%.Present invention preferably employs cylinder groups to carry out the second drying, and the present invention is for institute
The specific setting condition for stating the second dry time and the cylinder group does not have special restriction, can guarantee evenly drying and
The humidity of the dry paper web of gained second is met the requirements after second drying.The present invention is dry by second, can remove flowers and fruits
The impurity such as the ethyl alcohol in moisture, sizing agent in odor type cigarette paper.
After the completion of second is dry, the present invention preferably successively batches the described second dry paper web, rewinding, cutting and beats
Packet, obtains flowers and fruits odor type cigarette paper product.The present invention to it is described batch, rewinding, cutting and packing mode there is no special want
It asks, uses aforesaid operations mode well known to those skilled in the art.
In the present invention, the quantitative target of the flowers and fruits odor type cigarette paper is 26~45g/m2, preferably 28~32g/m2；
Air permeability is 40~70CU, preferably 50~60CU.
Flowers and fruits odor type cigarette paper provided by the invention and preparation method thereof is described in detail below with reference to embodiment,
But they cannot be interpreted as limiting the scope of the present invention.
Embodiment 1
800kg wood pulp cellulose is taken, 23m is added3Water, mashing to beating degree is 83 ° after size degradation, and 350kg is added in the slurry
Calcium carbonate (partial size be 20 μm), mix, manufacture paper with pulp after obtain mixed slurry.
The mixed slurry is successively formed, is dehydrated, is embossed and first is dry, obtains the first dry paper web；Wherein
First dry initial temperature is 65 DEG C, and final temperature is 105 DEG C, and the humidity of the dry paper web of gained first is 8%.
Being added to the ethyl alcohol of 400kg by flowers and fruits class essential oil 1.25kg sweet orange oil, 1.25kg dried orange peel essential oil, (95% volume is dense
Degree) in, it at the uniform velocity stirs 30 minutes, obtains flowers and fruits odor type solvent.In the state of at the uniform velocity stirring, 400kg water is evenly added
Into flowers and fruits odor type solvent, it is configured to the mixed solution that water accounts for solvent volume fraction 50%.It, will be golden in the state of at the uniform velocity stirring
Belong to combustion adjuvant salt 15kg potassium citrate and 7kg sodium citrate is added in mixed solution, at the uniform velocity stirs 30 minutes and obtain sizing agent.
Top sizing and the second drying are successively carried out to the first dry paper web, obtain flowers and fruits odor type cigarette paper；Wherein surface
Resin application methods are two-sided spray, and the second dry initial temperature is 40 DEG C, and final temperature is 79 DEG C, drying time temperature 8s.
This flowers and fruits odor type cigarette paper sample is labeled as 1#, respectively to the quantitative of this sample, air permeability, ventilative variation lines
Number, longitudinal tensile energy, ash content and whiteness are tested, and test result is shown in Table 1；
Aesthetic quality's test is carried out to this sample, test result is shown in Table 2；
Stability test is carried out to this sample, test result is shown in Table 3.
Wherein, corresponding detection method is as follows:
Method for quantitatively determining: GB/T 451.2-2002 " paper and the quantitative measurement of cardboard "；
Air permeability and coefficient of variation measuring method: GB/T 23227-2018 " cigarette paper, forming paper, tipping paper, have between
The measurement of the material and the material gas permeable degree with different air permeable belts of disconnected or continuous ventilating area "；
Ash determination method: GB/T 742-2008 " measurement of paper making raw material, paper pulp, paper and cardboard ash content "；
The measuring method of whiteness: the GB/T 7974-2013 " survey of paper, cardboard and paper pulp blue light diffusing reflection factor D65 brightness
Fixed (diffusion/normal beam technique, outdoor daylight condition) "；
Longitudinal tensile energy measuring method: GB/T 12914-2008 " measurement of paper and cardboard tensile strength "；
Aesthetic quality's test: identical pipe tobacco is used, after identical cigarette mode carries out cigarette, according to standard GB5606.4-
2005 " cigarette sense organ technical requirements " carry out sense organ comparison and smoke panel test；
Stability test: being sealed packaging to cigarette paper using polybag, is placed at backlight and places, when placing different
Between after take out roll into cigarette smoking.
Embodiment 2
It takes 650kg wood pulp cellulose and 150kg ramie pulp fiber to mix, 23m is added3Water, circulation beating is to beating degree after size degradation
Be 83 °, 450kg talcum powder (partial size be 2 μm) be added, mix, manufacture paper with pulp after obtain mixed slurry.
The mixed slurry is successively formed, is dehydrated, is embossed and first is dry, obtains the first dry paper web；Wherein
First dry initial temperature is 60 DEG C, and final temperature is 100 DEG C, time 12s；The humidity of the dry paper web of gained first is
8%.
It is added in the ethyl alcohol (95% volumetric concentration) of 350kg by flowers and fruits class essential oil 3kg vanilla essential oil, at the uniform velocity stirs 60 points
Clock obtains flowers and fruits odor type solvent.In the state of at the uniform velocity stirring, 450kg water is evenly added in flowers and fruits odor type solvent, is matched
It is set to the mixed solution that water accounts for solvent volume fraction 43.75%.In the state of at the uniform velocity stirring, by metal combustion adjuvant salt 20kg lemon
Lemon acid potassium is added in mixed solution, at the uniform velocity stirs 60 minutes and obtains sizing agent.
Top sizing and the second drying are successively carried out to the first dry paper web, obtain flowers and fruits odor type cigarette paper；Wherein surface
Resin application methods are one side coating, and the second dry initial temperature is 45 DEG C, and final temperature is 75 DEG C, drying time temperature 8s.
This flowers and fruits odor type cigarette paper sample is labeled as 2#, using the method for embodiment 1 respectively to the quantitative, saturating of this sample
Manner, the ventilative coefficient of variation, longitudinal tensile energy, ash content and whiteness are tested, and test result is shown in Table 1；
Aesthetic quality's test is carried out to this sample, test result is shown in Table 2；
Stability test is carried out to this sample, test result is shown in Table 3.
Embodiment 3
It takes 650kg wood pulp cellulose and 150kg ramie pulp fiber to mix, 23m is added3Water, circulation beating to beating degree are 83 °,
450kg diatomite (partial size be 10 μm) is added, mix, manufacture paper with pulp after obtain mixed slurry.
The mixed slurry is successively formed, is dehydrated, is embossed and first is dry, obtains the first dry paper web；Wherein
First dry initial temperature is 70 DEG C, and final temperature is 110 DEG C, time 12s；The humidity of the dry paper web of gained first is
10%.
It is added to 450kg's by flowers and fruits class essential oil 0.75kg purple perilla leaf essential oil, 1.75kg vanilla essential oil, 2kg walnut essential oil
In ethyl alcohol (95% volumetric concentration), at the uniform velocity stirs 40 minutes, obtain flowers and fruits odor type solvent.It, will in the state of at the uniform velocity stirring
350kg water is evenly added in flowers and fruits odor type solvent, is configured to the mixed solution that water accounts for solvent volume fraction 56.25%.?
In the state of at the uniform velocity stirring, metal combustion adjuvant salt 7kg potassium citrate and 3kg sodium tartrate are added in mixed solution, at the uniform velocity stirred
It mixes 40 minutes and obtains sizing agent.
Top sizing and the second drying are successively carried out to the first dry paper web, obtain flowers and fruits odor type cigarette paper；Wherein surface
Resin application methods are intaglio plate coating, and the second dry initial temperature is 50 DEG C, and final temperature is 70 DEG C, drying time temperature 8s.
This flowers and fruits odor type cigarette paper sample is labeled as 3#, using the method for embodiment 1 respectively to the quantitative, saturating of this sample
Manner, the ventilative coefficient of variation, longitudinal tensile energy, ash content and whiteness are tested, and test result is shown in Table 1；
Aesthetic quality's test is carried out to this sample, test result is shown in Table 2；
Stability test is carried out to this sample, test result is shown in Table 3.
Comparative example 1
800kg wood pulp cellulose is taken, 23m is added3Water, mashing to beating degree is 83 ° after size degradation, and 350kg is added in the slurry
Calcium carbonate (partial size be 20 μm), mix, manufacture paper with pulp after obtain mixed slurry.
The mixed slurry is successively formed, is dehydrated, is embossed and first is dry, obtains the first dry paper web；Wherein
First dry initial temperature is 65 DEG C, and final temperature is 105 DEG C, and the humidity of the dry paper web of gained first is 8%.
Metal combustion adjuvant salt 15kg potassium citrate and 7kg sodium citrate are added to 800kg in the state of at the uniform velocity stirring
In water, at the uniform velocity stirs 30 minutes and obtain sizing solution.
Top sizing and the second drying are successively carried out to the first dry paper web, obtain normal sample cigarette paper；Wherein surface is applied
Glue mode is two-sided spray, and the second dry initial temperature is 40 DEG C, and final temperature is 79 DEG C, drying time temperature 8s.
This normal sample cigarette paper sample is labeled as 1#, using the method for embodiment 1 respectively to the quantitative, ventilative of this sample
Degree, the ventilative coefficient of variation, longitudinal tensile energy, ash content and whiteness are tested, and test result is shown in Table 1；
Aesthetic quality's test is carried out to this sample, test result is shown in Table 2.
Comparative example 2
It takes 650kg wood pulp cellulose and 150kg ramie pulp fiber to mix, 23m is added3Water, circulation beating is to beating degree after size degradation
Be 83 °, 450kg talcum powder (partial size be 2 μm) be added, mix, manufacture paper with pulp after obtain mixed slurry.
The mixed slurry is successively formed, is dehydrated, is embossed and first is dry, obtains the first dry paper web；Wherein
First dry initial temperature is 60 DEG C, and final temperature is 100 DEG C, time 12s；The humidity of the dry paper web of gained first is
8%.
In the state of at the uniform velocity stirring, metal combustion adjuvant salt 20kg potassium citrate is added in 800kg water, is at the uniform velocity stirred
Obtain sizing agent within 30 minutes.
Top sizing and the second drying are successively carried out to the first dry paper web, obtain normal sample cigarette paper；Wherein surface is applied
Glue mode is one side coating, and the second dry initial temperature is 45 DEG C, and final temperature is 75 DEG C, drying time temperature 8s.
This normal sample cigarette paper sample is labeled as 2#, using the method for embodiment 1 respectively to the quantitative, ventilative of this sample
Degree, the ventilative coefficient of variation, longitudinal tensile energy, ash content and whiteness are tested, and test result is shown in Table 1；
Aesthetic quality's test is carried out to this sample, test result is shown in Table 2.
Comparative example 3
It takes 650kg wood pulp cellulose and 150kg ramie pulp fiber to mix, 23m is added3Water, circulation beating to beating degree are 83 °,
450kg diatomite (partial size be 10 μm) is added, mix, manufacture paper with pulp after obtain mixed slurry.
The mixed slurry is successively formed, is dehydrated, is embossed and first is dry, obtains the first dry paper web；Wherein
First dry initial temperature is 70 DEG C, and final temperature is 110 DEG C, time 12s；The humidity of the dry paper web of gained first is
10%.
Metal combustion adjuvant salt 7kg potassium citrate and 3kg sodium tartrate are added to 800kg water in the state of at the uniform velocity stirring
In, it at the uniform velocity stirs 40 minutes and obtains sizing agent.
Top sizing and the second drying are successively carried out to the first dry paper web, obtain normal sample cigarette paper；Wherein surface is applied
Glue mode is intaglio plate coating, and the second dry initial temperature is 50 DEG C, and final temperature is 70 DEG C, drying time temperature 8s.
This normal sample cigarette paper sample is labeled as 3#, using the method for embodiment 1 respectively to the quantitative, ventilative of this sample
Degree, the ventilative coefficient of variation, longitudinal tensile energy, ash content and whiteness are tested, and test result is shown in Table 1；
Aesthetic quality's test is carried out to this sample, test result is shown in Table 2.
Performance test
1 embodiment of table and comparative example cigarette paper quantitative measurement result
As can be seen from Table 1, the flowers and fruits odor type cigarette paper made of the method for the present invention is quantitative, air permeability, air permeability become
Different coefficient, longitudinal tensile energy, ash content, whiteness are almost unchanged compared with normal sample.Therefore the present invention provides cigarette paper and meets
Requirement of the normal cigarette paper to air permeability, the air permeability coefficient of variation, longitudinal tensile energy, ash content, whiteness.
2 embodiment of table and comparative example cigarette paper aesthetic quality's test result
| Serial number | Sample | Gloss | Fragrance | Harmony | Pleasant impression | Irritation | Miscellaneous gas | Total score |
| 1 | Flowers and fruits odor type cigarette paper 1# | 6 | 30.2 | 6 | 22.5 | 17.5 | 11.0 | 93.2 |
| 2 | Flowers and fruits odor type cigarette paper 2# | 5.8 | 30.1 | 6 | 22.7 | 17.5 | 11.3 | 93.4 |
| 3 | Flowers and fruits odor type cigarette paper 3# | 5.9 | 30.2 | 6 | 22.8 | 17.5 | 11.2 | 93.6 |
| 4 | Normal sample cigarette paper 1# | 5.9 | 30.1 | 6 | 22.4 | 17.2 | 11.0 | 92.6 |
| 5 | Normal sample cigarette paper 2# | 6 | 30.0 | 6 | 22.6 | 16.8 | 10.4 | 91.8 |
| 6 | Normal sample cigarette paper 3# | 6 | 29.9 | 6 | 22.7 | 17.5 | 10.1 | 92.2 |
As can be seen from Table 2, flowers and fruits odor type cigarette paper provided by the invention has good compared with normal sample cigarette paper
Aesthetic quality.Flowers and fruits odor type cigarette pattern during the manufacturing into cigarette paper because be added to flowers and fruits class essence, not only
It will not influence cigarette smoking mouthfeel, in addition to playing promotion cigarette flavor, improve cigarette irritation, cover the effect of miscellaneous gas, may be used also
Assign the unique suction mouthfeel of cigarette.
Cigarette paper stability test result obtained by 3 Examples 1 to 3 of table
In general, the cigarette paper products shelf-life is 1 year, as shown in Table 3, in shelf life of products, use is provided by the invention
Preparation method can effectively keep the fragrance stability of cigarette paper.
As seen from the above embodiment, flowers and fruits odor type cigarette paper provided by the invention can assign cigarette unique suction sense organ,
And fragrance stability is high；Preparation method provided by the invention does not add additional process, energy without changing existing equipment simultaneously
The flavoring cost of cigarette paper is enough effectively reduced.
The above is only a preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, various improvements and modifications may be made without departing from the principle of the present invention, these improvements and modifications are also answered
It is considered as protection scope of the present invention.
Claims (10)
1. a kind of flowers and fruits odor type cigarette paper, which is characterized in that the component including following mass parts:
2. flowers and fruits odor type cigarette paper according to claim 1, which is characterized in that the fiber include wood pulp cellulose and/or
Ramie pulp fiber.
3. flowers and fruits odor type cigarette paper according to claim 1, which is characterized in that the filler includes calcium carbonate, talcum powder
One or more of with diatomite；The partial size of the filler is 2~20 μm.
4. flowers and fruits odor type cigarette paper according to claim 1, which is characterized in that the combustion adjuvant includes citrate, apple
One or more of tartaric acid salt, tartrate and lactate.
5. flowers and fruits odor type cigarette paper according to claim 1, which is characterized in that the flowers and fruits type essence includes sweet orange essence
One in oil, dried orange peel essential oil, purple perilla leaf essential oil, lemon, olive essential oil, vanilla essential oil, spearmint essential oil and walnut essential oil
Kind is several.
6. the preparation method of flowers and fruits odor type cigarette paper described in Claims 1 to 5 any one, which is characterized in that including following step
It is rapid:
(1) size degradation and mashing are successively carried out after mixing fiber with water, obtain fibre stuff；
(2) it manufactures paper with pulp after mixing the fibre stuff with filler, obtains mixed slurry；
(3) mixed slurry successively formed, be dehydrated, being embossed and first is dry, obtaining the first dry paper web；
(4) the described first dry paper web is successively subjected to top sizing and the second drying, obtains flowers and fruits odor type cigarette paper；
The top sizing sizing agent includes the component of following mass percentage:
7. preparation method according to claim 6, which is characterized in that the beating degree of fibre stuff is in the step (1)
60~100 °.
8. preparation method according to claim 6, which is characterized in that the described first dry initial temperature is 60~70
DEG C, final temperature is 100~110 DEG C；Described second dry initial temperature is 40~50 DEG C, and final temperature is 70~80 DEG C.
9. preparation method according to claim 6, which is characterized in that the preparation method of the sizing agent includes following step
It is rapid:
Flowers and fruits flavor essence is dissolved in ethyl alcohol, water is then sequentially added and combustion adjuvant is mixed, obtain sizing agent.
10. preparation method according to claim 6, which is characterized in that the mode of top sizing is double in the step (4)
Face spray, one side coating, intaglio plate coating, comma roller coating or the coating of crack squash type.
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| CN110593007A (en) * | 2019-08-06 | 2019-12-20 | 河南中烟工业有限责任公司 | Preparation method of mint type cigarette paper |
| CN110592995A (en) * | 2019-10-28 | 2019-12-20 | 云南中烟工业有限责任公司 | Hollow double-layer cigarette paper and preparation method thereof |
| CN111074684A (en) * | 2020-01-20 | 2020-04-28 | 中国烟草总公司郑州烟草研究院 | Colored cigarette paper and preparation method thereof |
| CN111778774A (en) * | 2020-07-13 | 2020-10-16 | 河南中烟工业有限责任公司 | Fruity cigarette paper and preparation method thereof |
| CN112796145A (en) * | 2021-02-02 | 2021-05-14 | 云南中烟工业有限责任公司 | Moss scented cigarette paper, its preparation method and use |
| WO2022193351A1 (en) * | 2021-03-15 | 2022-09-22 | 云南中烟工业有限责任公司 | Method for improving aroma of cigarette product by using raspberry ketone glucoside |
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Application publication date: 20190709 |