CN1793500A - Cigarette paper and preparation method thereof - Google Patents
Cigarette paper and preparation method thereof Download PDFInfo
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- CN1793500A CN1793500A CN 200510048641 CN200510048641A CN1793500A CN 1793500 A CN1793500 A CN 1793500A CN 200510048641 CN200510048641 CN 200510048641 CN 200510048641 A CN200510048641 A CN 200510048641A CN 1793500 A CN1793500 A CN 1793500A
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Abstract
The invention discloses cigarette paper and its manufacturing method. The cigarette paper is used working of paper as carrier, plant alcohol extract cream body with 1.2000+/-0.0050 relative density as additive. The quality of the working of paper is used as criterion. Thus the mass percent of the additive is 0.01%-0.05%. the relative density of additive cream body is 1.2000+/-0.0050. The plant is one of aromatic tobacco, burley tobacco, Maryland, drying tobacco, Pu'er tea, golden buckwheat rhizome, pseudo-ginseng, or Broadleaf Herb leaf, or their mixture. The invention can obviously improve cigarette sucking aftertaste, reduce sting, and coordinate cigarette smoke.
Description
Technical field
The present invention relates to a kind of cigarette paper, more particularly, is a kind of cigarette paper that contains plant extracts.
Background technology
Tobacco enterprise owing to face identical problem-lifting cigarette quality, all needs to develop corresponding cigarette odor-absorbing compensation technique in suction quality that improves cigarette product and reduction tar process.On the one hand, improving the cigarette smoking quality is cigarette enterprise unremitting effort direction.Why tobacco becomes people's the product of sucking, and reason is to contain in the tobacco nicotine and various natural materials with fragrance, can give the smoker with fragrance and excited sensation when suction.But,, thereby influence the quality of formulation product because these compositions make material quality fluctuate because of a series of variations such as natural conditions, cultivation technique and modulation techniques in the tobacco.In addition,, also need to be corrected, strengthen or the original fragrance of compensation tobacco leaf itself by perfuming even select sound tobacco fully for use.When raw tobacco material fragrance not enough or flat, jealous not good enoughly just need remedy by perfuming.On the other hand, current low-coke tar cigarette development trend is irreversible, and along with growing to even greater heights of world's anti-smoking campaign, various countries' tobacco business reduces the tar content of cigarette one after another, the continuous low tarization of cigarette.Cigarette smoke mainly is grouped into by one-tenth such as tar, nicotine, moisture, cigarette smoke gaseous substances, and wherein tar, nicotine are the sources of smoker's sense organ impression.The suction quality that the tar content that cigarette is low is become reconciled is a pair of contradiction.The result that ordinary circumstance, tar content and being proportionate property of cigarette smoking quality, low tarization bring the cigarette smoking quality to descend.For when reducing tar, can obtain the cigarette odor-absorbing compensation technique that higher suction quality just needs development to match with reducing tar and reducing harm.
The suction flavor compensation technique means that can obtain better suction quality cigarette are diversified, mainly comprise low tar leaf group suction flavor compensation technique, cigarette flavors is inhaled the flavor compensation technique, three paper, one rod is inhaled the flavor compensation technique, means such as the compensation technique of other types, therefore the current situation of number of ways suction flavor compensation technique shows, the suction flavor compensation technique of low-coke tar cigarette is an integrated technology.But the suction flavor compensation effect of existing cigarette paper is desirable not enough, and pending further investigation is arranged.
Summary of the invention
It mainly is to carry out the work around the screening of cigarette paper functional additive that cigarette paper is inhaled the flavor compensation technique.Cigarette paper is inhaled flavor compensation additive and is comprised three types.First type is functional form plant extracts additive; Second type is that microcapsules are inhaled flavor compensation additive; The third type is the perfumery matter additive of diving.This additive of three types has different separately characteristics, can effectively improve the low-coke tar cigarette suction quality from different perspectives.The present invention carries out the work from plant extracts additive aspect.
Purpose of the present invention is exactly the actual needs at production of cigarettes, and a kind of cigarette paper that can improve the cigarette smoking pleasant impression, reduce excitant and coordinate cigarette smoke is provided, to reach the suction flavor that improves the fragrant jealous quality of low and middle-grade cigarette, compensation low-coke tar cigarette.
Purpose of the present invention is achieved by following technical proposals.
The invention provides a kind of cigarette paper, it is carrier with the finished paper, is that 1.2000 ± 0.0050 plant alcohol extracts lotion is an additive with relative density; Quality with finished paper is a benchmark, and described additive mass percent is 0.01%-0.05%, and the relative density of additive lotion is 1.2000 ± 0.0050; Described plant is selected from a kind of in Turkish tobaccos, burley tobaccos, Maryland, airing cigarette, Pu'er tea, cymose buckwheat rhizome, pseudo-ginseng or the Folium Ilicis or their mixture.
The invention provides a kind of preparation method of cigarette paper, this method comprises the step of following order:
(1) respectively with a kind of in Turkish tobaccos, burley tobaccos, Maryland, airing cigarette, Pu'er tea, cymose buckwheat rhizome, pseudo-ginseng or the Folium Ilicis be raw material, it is crushed to 20～40 orders;
(2) with the edible ethanol of 10 times of weight 70 ℃ of following reflux twice, refluxed 2 hours at every turn, merging filtrate, standing over night, getting supernatant, to be evaporated to relative density be 1.2000 ± 0.0050 lotion;
(3) adopt macroreticular resin that the lotion that ethanol extract concentrates is carried out column chromatography for separation, collect the ethanol elution thing, concentrating and being prepared as relative density is 1.2000 ± 0.0050 lotion, has promptly obtained 8 kinds of fragrant class additives of diving respectively;
(4) method is routinely added calcium carbonate in the process of slurrying, adds combustion adjuvant and the fragrant class additive of diving in machine hand's program process, promptly makes required cigarette paper; Wherein, be benchmark with the quality of finished paper, the mass percent of calcium carbonate addition is 20%～40%; The mass percent of combustion adjuvant addition is 6%～10%; Described combustion adjuvant is selected from a kind of in citric acid sylvite, sodium citrate salt, malic acid sylvite or the malic acid sodium salt or their mixture; The mass percent of latent fragrant class additive addition is 0.01%-0.05%.
Compared with prior art, the present invention has following beneficial effect:
The present invention select for use first in the plants such as Turkish tobaccos, burley tobaccos, Maryland, airing cigarette, Pu'er tea, cymose buckwheat rhizome, pseudo-ginseng, Folium Ilicis the edible ethanol extract alone or in combination the cigarette paper additive of preferred for preparation add in the cigarette paper, can reach the obvious effect that improves the cigarette smoking pleasant impression, reduces excitant and coordinate cigarette smoke.Simultaneously, the solid sense of low-coke tar cigarette suction quality is strengthened, enrich cigarette smoke.
2. the present invention develops the fragrant class cigarette paper additive series of diving, and is benchmark with the quality of finished paper, and addition is a 0.01%-0.05% alcohol extract lotion, and addition is extremely low, and the additive cost is expected to be controlled at about 450 yuan of/ton paper.If a large amount of the use, cost has the space of decline, has industrial application value.
The specific embodiment
Below by specific embodiment the present invention is done explanation in further detail, but content of the present invention be not limited to for embodiment.
With regard to the technical scheme that the present invention proposes, carried out the experimental study of following system:
1. the edible ethanol extract of single plant adds experiment
In the process that conventional cigarette paper is produced, in machine hand's preface section, adopt the ethanol extract of Turkish tobaccos, burley tobaccos, Maryland, airing cigarette, Pu'er tea, cymose buckwheat rhizome, pseudo-ginseng or Folium Ilicis plant, carry out single plant edible food ethanol extract respectively, by the mode of spray, spray is compared with coating method, desired concn is low, add more evenly, finish and add experiment, other explained hereafter steps are carried out routinely.By smoking result and cigarette smoke index analysis data, finish the edible ethanol extract optimization experiment of single plant at last.
2. several edible ethanol extract combination are added experiment
In the scope of eight kind of plant edible ethanol extracts, method by orthogonal experiment, finish the combination experiment of eight kinds of additives, in the process that conventional cigarette paper is produced, in machine hand's preface section, adopt the ethanol extract combined additive of plants such as Turkish tobaccos, burley tobaccos, Maryland, airing cigarette, Pu'er tea, cymose buckwheat rhizome, pseudo-ginseng, Folium Ilicis, by the mode of spray, finish and add experiment, other explained hereafter steps are carried out routinely.By smoking result and cigarette smoke index analysis data, finish the ethanol extract combined additive optimization experiment of eight kind of plant at last.
By the influence of additive, confirmed the effect of cigarette paper additive series of the present invention to cigarette conventional index and cigarette sensory evaluating smoking result.In following all embodiment, except that additive therefor and addition change, all the other parameters and process conditions are all identical.
Embodiment 1
A. the preparation of cigarette paper and respective sample cigarette
1. determine the related physical index of sample cigarette paper: air permeance for cigarette paper 60 Ke Shi, cigarette paper grammes per square metre 28 gram/square centimeters.2. determine cigarette paper filling kind and addition: calcium carbonate is used in inorganic filler; Addition 30% (addition is that the quality with finished paper is the mass percent of benchmark).3. determine the kind and the addition of cigarette paper combustion adjuvant: what combustion adjuvant used is the composition of combustion-supporting salt such as citric acid sylvite, sodium citrate salt, malic acid sylvite, malic acid sodium salt; The addition of this combustion adjuvant is 8% (mass percent).4, described cigarette paper is all used conventional paper machine production, in tankman's preface section that cigarette paper is produced, adds inorganic filler in paper pulp; Combustion adjuvant adds with the spray mode in machine hand's preface; Equally in machine hand's preface section, (the additive addition is 0.05% of a finished paper quality to the cymose buckwheat rhizome ethanol extract as additive, described additive quality is that relative density is 1.2000 ± 0.0050 ethanol extract lotion quality), by the mode of spray, finish and add experiment.Then cigarette paper is cut into the cigarette paper of 27 mm wides.Adopt conventional cigarette producing process to produce sample 1, the additive parameter sees Table 1.
B. conventional cigarette smoke analysis of sample cigarette and sensory evaluating smoking
1. test the preparation that cigarette propped up and captured cigarette smoke composition filter disc.The cigarette sample cigarette propped up be placed on temperature (22 ± 1) ℃ equably, balance is 48 hours in the environmental condition of relative humidity (60 ± 2) %, selects experiment and props up with cigarette by average quality ± 0.02g and average resistance to suction ± 49Pa scope.Cambridge filter is placed on temperature (22 ± 1) ℃, and balance is 48 hours under the environmental condition of relative humidity (60 ± 2) %.
2. main flume analysis.Smoking machine is pressed YC/29-1996 standard suction cigarette and is measured cigarette mainstream smoke total particulate matter, measures carbonomonoxide concentration in the cigarette smoke with non-diffusion type infrared gas analyser.The main flume analysis result sees Table 2.
3. sample cigarette sensory evaluating smoking.The cigarette aesthetic quality smokes panel test and smokes panel test by the method for GB 5606.4-1996 " specification requirement of cigarette sense organ " regulation, and the scoring form designs according to requirement of experiment.Sample cigarette sensory evaluating smoking the results are shown in Table 3.
Result of the test shows cymose buckwheat rhizome: ethanol extract is as the cigarette sample 1 of the functional cigarette paper preparation of Additive Production, abideing by conventional flue gas analysis data of sample cigarette that national standard method obtains and the cigarette aesthetic quality data of smokeing panel test shows, it is little that sample 1 conventional flue gas analysis data contrast cigarette difference, and contrast cigarette by a relatively large margin lifting is arranged in the sample 1 cigarette aesthetic quality data of smokeing panel test.The cymose buckwheat rhizome ethanol extract can significantly improve cigarette sense organ comfort level as the functional cigarette paper additive, and elegance, assorted gas, stimulation, several in the pleasant impression index of smokeing panel test has all obtained bigger raising.
Embodiment 2
Repeat embodiment 1, following difference is arranged: the functional cigarette paper additive is an airing cigarette edible ethanol extract, and be prepared into cigarette paper and corresponding cigarette sample 2 (the additive addition is 0.05% of a finished paper quality, and described additive quality is that relative density is 1.2000 ± 0.0050 ethanol extract lotion quality).Additive parameter and testing result see Table 4～table 6.
Ethanol extract is as the cigarette sample 1 of the functional cigarette paper of Additive Production preparation, abides by conventional flue gas analysis data of sample cigarette that national standard method obtains and cigarette aesthetic quality and smokes panel test that data see Table 5, table 6.It is little that sample 1 conventional flue gas analysis data contrast cigarette difference, and contrast cigarette by a relatively large margin lifting is arranged in the sample 1 cigarette aesthetic quality data of smokeing panel test.Airing cigarette ethanol extract is as the functional cigarette paper additive, can significantly increase the fragrant and pure and mild degree of old cigarette, and elegance, perfume quantity, assorted several in the gas index of smokeing panel test obtains bigger raising.
Embodiment 3
Repeat embodiment 1, following difference is arranged: the functional cigarette paper additive is two kinds of additive packages that (airing cigarette, cymose buckwheat rhizome) is combined in proportion in eight kinds of natural plants edible ethanol extracts, and be prepared into cigarette paper and corresponding cigarette sample 3 (the additive addition is 0.05% of a finished paper quality, and described additive quality is that relative density is two kinds of mixed quality of ethanol extract lotion of 1.2000 ± 0.0050).Additive parameter and testing result see Table 7～table 9.
Airing cigarette and cymose buckwheat rhizome ethanol extract mix the cigarette sample 3 of back as the functional cigarette paper preparation of Additive Production in proportion, abide by conventional flue gas analysis data of sample cigarette that national standard method obtains and cigarette aesthetic quality and smoke panel test that data see Table 8, table 9, these data show that the sample 3 cigarette aesthetic qualities data (elegance, assorted gas, stimulation) of smokeing panel test contrast cigarette by a relatively large margin lifting is arranged, and it is little to contrast cigarette difference in sample 3 conventional flue gas analysis data.
Embodiment 4
Repeat embodiment 1, following difference is arranged: the functional cigarette paper additive is the additive package that in eight kinds of natural plants edible ethanol extracts two kinds (Turkish tobaccos, Maryland) are combined in proportion, and be prepared into cigarette paper and corresponding cigarette sample 4 (the additive addition is 0.05% of a finished paper quality, and described additive quality is that relative density is two kinds of mixed quality of ethanol extract lotion of 1.2000 ± 0.0050).Additive parameter and testing result see Table 10～table 12.
Turkish tobaccos and Maryland ethanol extract mix the cigarette sample 4 of back as the functional cigarette paper preparation of Additive Production in proportion, abide by conventional flue gas analysis data of sample cigarette that national standard method obtains and cigarette aesthetic quality and smoke panel test that data see Table 11, table 12, these data show that the sample 4 cigarette aesthetic qualities data of smokeing panel test contrast cigarette by a relatively large margin lifting is arranged, especially on cigarette elegance, assorted gas, several sensory evaluating smoking's indexs of pleasant impression, obtain bigger raising, and it is little to contrast cigarette difference in sample 4 conventional flue gas analysis data.
Embodiment 5
Repeat embodiment 1, following difference is arranged: the functional cigarette paper additive is two kinds of additive packages that (burley tobaccos, cymose buckwheat rhizome) is combined in proportion in eight kinds of natural plants edible ethanol extracts, and be prepared into cigarette paper and corresponding cigarette sample 5 (the additive addition is 0.05% of a finished paper quality, and described additive quality is that relative density is two kinds of mixed quality of ethanol extract lotion of 1.2000 ± 0.0050).Additive parameter and testing result see Table 13～table 15.
Burley tobaccos and cymose buckwheat rhizome ethanol extract mix the cigarette sample 5 of back as the functional cigarette paper preparation of Additive Production in proportion, abide by conventional flue gas analysis data of sample cigarette that national standard method obtains and cigarette aesthetic quality and smoke panel test that data see Table 14, table 15, it is little that these data show that sample 5 conventional flue gas analysis data contrast cigarette difference, and contrast cigarette by a relatively large margin lifting is arranged in the sample 5 cigarette aesthetic qualities data of smokeing panel test, especially on cigarette richness, assorted gas, stimulation, several sensory evaluating smokings of pleasant impression, obtain bigger raising.
Embodiment 6
Repeat embodiment 1:, following difference is arranged: the functional cigarette paper additive is two kinds of additive packages that (airing cigarette, Folium Ilicis) is combined in proportion in eight kinds of natural plants edible ethanol extracts, and be prepared into cigarette paper and corresponding cigarette sample 6 (the additive addition is 0.02% of a finished paper quality, and described additive quality is that relative density is two kinds of mixed quality of ethanol extract lotion of 1.2000 ± 0.0050).Additive parameter and testing result see Table 16～table 18.
Abideing by conventional flue gas analysis data (table 17) of sample cigarette that national standard method obtains and the cigarette aesthetic quality data (table 18) of smokeing panel test from the cigarette sample of above-mentioned functions cigarette paper preparation can find out, airing cigarette and Folium Ilicis ethanol extract mix the cigarette sample 6 of back as the functional cigarette paper preparation of Additive Production in proportion, it is little that its conventional flue gas analysis data contrast cigarette difference, data contrast cigarette and the cigarette aesthetic quality smokes panel test by a relatively large margin lifting, and especially elegance, perfume quantity, strength, stimulation, several indexs of pleasant impression have all obtained higher scoring.Additive parameter and testing result see Table 4～table 6.
Embodiment 7
Repeat embodiment 1:, following difference is arranged: the functional cigarette paper additive is three kinds of additive packages that (Maryland, cymose buckwheat rhizome, pseudo-ginseng) is combined in proportion in eight kinds of natural plants edible ethanol extracts, and be prepared into cigarette paper and corresponding cigarette sample 7 (the additive addition is 0.02% of a finished paper quality, and described additive quality is that relative density is two kinds of mixed quality of ethanol extract lotion of 1.2000 ± 0.0050).Additive parameter and testing result see Table 19～table 21.
Abideing by conventional flue gas analysis data (table 20) of sample cigarette that national standard method obtains and the cigarette aesthetic quality data (table 21) of smokeing panel test from the cigarette sample of above-mentioned functions cigarette paper preparation can find out, Maryland, cymose buckwheat rhizome and pseudo-ginseng ethanol extract mix the cigarette sample 7 of back as the functional cigarette paper preparation of Additive Production in proportion, it is little that its conventional flue gas analysis data contrast cigarette difference, data contrast cigarette and the cigarette aesthetic quality smokes panel test by a relatively large margin lifting, sample 7 sense organ comfort levels have obtained fine improvement, mouthfeel Hui Tian promotes the production of body fluid, elegance, assorted gas, stimulate, several indexs of pleasant impression have all obtained higher scoring, and be significantly increased compared with the control (〉=1.0).
Embodiment 8
Repeat embodiment 1:, following difference is arranged: the functional cigarette paper additive is three kinds of additive packages that (airing cigarette, Pu'er tea, Folium Ilicis) is combined in proportion in eight kinds of natural plants edible ethanol extracts, and be prepared into cigarette paper and corresponding cigarette sample 8 (the additive addition is 0.02% of a finished paper quality, and described additive quality is that relative density is two kinds of mixed quality of ethanol extract lotion of 1.2000 ± 0.0050).Additive parameter and testing result see Table 22～table 24.
Airing cigarette, Pu'er tea and Folium Ilicis ethanol extract mix the cigarette sample 8 of back as the functional cigarette paper preparation of Additive Production in proportion, above-mentioned table 23 and table 24 have provided sample 8 respectively and have abideed by conventional flue gas analysis data of sample cigarette that national standard method obtains and the cigarette aesthetic quality data of smokeing panel test, it is little that these data show that sample 8 conventional flue gas analysis data contrast cigarette difference, and contrast cigarette by a relatively large margin lifting is arranged in the sample 8 cigarette aesthetic qualities data (assorted gas, stimulation, pleasant impression) of smokeing panel test.
Table 1 additive parameter
| The additive title | Cymose buckwheat rhizome |
| Addition (quality with finished paper is the mass percent of benchmark) | 0.05％ |
The conventional flue gas analysis data of table 2 sample cigarette
| The sample title | Puff number | Tar content | Average resistance to suction | Moisture content | Nicotine content in smoke | CO content |
| Sample 1 | 8.1 | 11.84 | 1194 | 1.72 | 1.12 | 14.4 |
| Contrast | 8.2 | 11.94 | 1243 | 1.82 | 1.20 | 14.8 |
The table 3 sample cigarette aesthetic quality data of smokeing panel test
| The sample sequence number | Fragrance richness 10 | Elegance 10 | Perfume quantity 10 | Concentration 10 | Strength 10 | Assorted gas 10 | Stimulate 10 | Pleasant impression 10 | Total points |
| Sample 1 | 8 | 7.5 | 8 | 8.0 | 9 | 8 | 8.5 | 8.5 | 65.5 |
| Contrast | 7.5 | 6.5 | 8.0 | 8.0 | 8.5 | 6.5 | 7.0 | 7.5 | 59.5 |
| Remarks: mouth rod length 20cm | |||||||||
Table 4.
| The additive title | The airing cigarette |
| Addition (quality with finished paper is the mass percent of benchmark) | 0.05％ |
Table 5.
| The sample title | Puff number | Tar content | Average resistance to suction | Moisture content | Nicotine content in smoke | CO content |
| Sample 2 | 8.5 | 12.54 | 1204 | 1.93 | 1.32 | 15.4 |
| Contrast | 8.2 | 11.94 | 1243 | 1.82 | 1.20 | 14.8 |
Table 6.
| The sample sequence number | Fragrance richness 10 | Elegance 10 | Perfume quantity 10 | Concentration 10 | Strength 10 | Assorted gas 10 | Stimulate 10 | Pleasant impression 10 | Total points |
| Sample 2 | 8 | 8 | 8 | 8 | 9 | 8 | 8 | 8 | 65 |
| Contrast | 7.5 | 6.5 | 7.5 | 8.0 | 8.5 | 7 | 7.0 | 7.5 | 59.5 |
| Remarks: mouth rod length 20cm | |||||||||
Table 7.
| The additive title | The airing cigarette | Cymose buckwheat rhizome |
| Additive mixed proportion (%) | 50％ | 50％ |
| Total addition level (quality with finished paper is the mass percent of benchmark) | 0.05％ | |
Table 8.
| The sample title | Puff number | Tar content | Average resistance to suction | Moisture content | Nicotine content in smoke | CO content |
| Sample 3 | 8.7 | 13.54 | 1144 | 1.96 | 1.32 | 15.4 |
| Contrast | 8.9 | 13.94 | 1151 | 1.92 | 1.40 | 15.8 |
Table 9.
| The sample sequence number | Fragrance master full scale 10 | Elegance 10 | Perfume quantity 10 | Concentration 10 | Strength 10 | Assorted gas 10 | Stimulate 10 | Pleasant impression 10 | Total points |
| Sample 3 | 8.0 | 8.0 | 8.0 | 8 | 8.5 | 8 | 8 | 8 | 64.5 |
| Contrast | 7.5 | 6.5 | 8.5 | 8.0 | 8.5 | 6.5 | 7.0 | 7.5 | 60.0 |
| Remarks: mouth rod length 20cm | |||||||||
Table 10.
| The additive title | Turkish tobaccos | Maryland |
| Additive mixed proportion (%) | 30％ | 70％ |
| Total addition level (quality with finished paper is the mass percent of benchmark) | 0.05％ | |
Table 11.
| The sample title | Puff number | Tar content | Average resistance to suction | Moisture content | Nicotine content in smoke | CO content |
| Sample 4 | 9.0 | 14.54 | 1134 | 1.97 | 1.32 | 15.4 |
| Contrast | 8.7 | 13.94 | 1173 | 1.92 | 1.30 | 14.8 |
Table 12.
| The sample sequence number | Fragrance richness 10 | Elegance 10 | Perfume quantity 10 | Concentration 10 | Strength 10 | Assorted gas 10 | Stimulate 10 | Pleasant impression 10 | Total points |
| Sample 4 | 8 | 8.0 | 8 | 8 | 9 | 8 | 7.5 | 8.5 | 65 |
| Contrast | 7.5 | 7.0 | 8.0 | 8.0 | 8.5 | 6.5 | 7.0 | 7.5 | 60 |
| Remarks: mouth rod length 20cm | |||||||||
Table 13.
| The additive title | Burley tobaccos | Cymose buckwheat rhizome |
| Additive mixed proportion (%) | 40％ | 60％ |
| Total addition level (quality with finished paper is the mass percent of benchmark) | 0.05％ | |
Table 14.
| The sample title | Puff number | Tar content | Average resistance to suction | Moisture content | Nicotine content in smoke | CO content |
| Sample 5 | 8.5 | 13.54 | 1204 | 1.73 | 1.32 | 14.4 |
| Contrast | 8.2 | 13.64 | 1243 | 1.72 | 1.30 | 14.2 |
Table 15.
| The sample sequence number | Fragrance richness 10 | Elegance 10 | Perfume quantity 10 | Concentration 10 | Strength 10 | Assorted gas 10 | Stimulate 10 | Pleasant impression 10 | Total points |
| Sample 5 | 8.0 | 8.0 | 8.0 | 8.0 | 9.0 | 8.0 | 8.0 | 8.5 | 65.5 |
| Contrast | 7.0 | 7.5 | 8.0 | 8.0 | 8.5 | 6.5 | 7.0 | 7.5 | 60.0 |
| Remarks: mouth rod length 20cm | |||||||||
Table 16.
| The additive title | The airing cigarette | Folium Ilicis |
| Additive mixed proportion (%) | 80％ | 20％ |
| Total addition level (quality with finished paper is the mass percent of benchmark) | 0.02％ | |
Table 17.
| The sample title | Puff number | Tar content | Average resistance to suction | Moisture content | Nicotine content in smoke | CO content |
| Sample 6 | 8.5 | 13.84 | 1204 | 1.93 | 1.32 | 14.4 |
| Contrast | 8.2 | 13.94 | 1243 | 1.87 | 1.24 | 14.6 |
Table 18.
| The sample sequence number | Fragrance richness 10 | Elegance 10 | Perfume quantity 10 | Concentration 10 | Strength 10 | Assorted gas 10 | Stimulate 10 | Pleasant impression 10 | Total points |
| Sample 6 | 8.0 | 8.5 | 8.0 | 8.0 | 9.0 | 8.0 | 8.0 | 8.5 | 66.0 |
| Contrast | 8.0 | 7.5 | 7.0 | 8.0 | 8.0 | 7.5 | 7.0 | 7.5 | 60.5 |
| Remarks: mouth rod length 20cm | |||||||||
Table 19.
| The additive title | Maryland | Cymose buckwheat rhizome | Pseudo-ginseng |
| Additive mixed proportion (%) | 40％ | 40％ | 20％ |
| Total addition level (quality with finished paper is the mass percent of benchmark) | 0.02％ | ||
Table 20.
| The sample title | Puff number | Tar content | Average resistance to suction | Moisture content | Nicotine content in smoke | CO content |
| Sample 7 | 8.8 | 13.54 | 1199 | 1.73 | 1.28 | 14.24 |
| Contrast | 8.6 | 13.74 | 1192 | 1.81 | 1.30 | 14.28 |
Table 21.
| The sample sequence number | Fragrance richness 10 | Elegance 10 | Perfume quantity 10 | Concentration 10 | Strength 10 | Assorted gas 10 | Stimulate 10 | Pleasant impression 10 | Total points |
| Sample 7 | 8.0 | 7.5 | 8.0 | 8.0 | 8.5 | 8.0 | 8.0 | 8.5 | 64.5 |
| Contrast | 8.0 | 6.5 | 8.0 | 8.0 | 8.0 | 6.5 | 7.0 | 7.5 | 59.5 |
| Remarks: mouth rod length 20cm | |||||||||
Table 22.
| The additive title | The airing cigarette | Green tea | Folium Ilicis |
| Additive mixed proportion (%) | 60％ | 20％ | 20％ |
| Total addition level (quality with finished paper is the mass percent of benchmark) | 0.02％ | ||
Table 23.
| The sample title | Puff number | Tar content | Average resistance to suction | Moisture content | Nicotine content in smoke | CO content |
| Sample 8 | 8.5 | 13.96 | 1169 | 1.93 | 1.19 | 14.7 |
| Contrast | 8.2 | 14.01 | 1163 | 1.82 | 1.23 | 14.9 |
Table 24.
| The sample sequence number | Fragrance richness 10 | Elegance 10 | Perfume quantity 10 | Concentration 10 | Strength 10 | Assorted gas 10 | Stimulate 10 | Pleasant impression 10 | Total points |
| Sample 8 | 8.0 | 8.0 | 8.0 | 8.0 | 9.0 | 8.0 | 8.5 | 8.5 | 66 |
| Contrast | 7.5 | 7.5 | 8.0 | 8.0 | 8.5 | 6.5 | 7.0 | 7.5 | 60.5 |
| Remarks: mouth rod length 20cm | |||||||||
Claims (2)
1. a cigarette paper is characterized in that with the finished paper being carrier, is that 1.2000 ± 0.0050 plant alcohol extracts lotion is an additive with relative density; Quality with finished paper is a benchmark, and the mass percent of described additive is 0.01%-0.05%, and the relative density of additive lotion is 1.2000 ± 0.0050; Described plant is selected from a kind of in Turkish tobaccos, burley tobaccos, Maryland, airing cigarette, Pu'er tea, cymose buckwheat rhizome, pseudo-ginseng or the Folium Ilicis or their mixture.
2. the preparation method of the described cigarette paper of claim 1 is characterized in that adopting the step of following order:
(1) respectively with a kind of in Turkish tobaccos, burley tobaccos, Maryland, airing cigarette, Pu'er tea, cymose buckwheat rhizome, pseudo-ginseng or the Folium Ilicis be raw material, it is crushed to 20～40 orders;
(2) with the edible ethanol of 10 times of weight 70 ℃ of following reflux twice, refluxed 2 hours at every turn, merging filtrate, standing over night, getting supernatant, to be evaporated to relative density be 1.2000 ± 0.0050 lotion;
(3) adopt macroreticular resin that the lotion that ethanol extract concentrates is carried out column chromatography for separation, collect the ethanol elution thing, concentrating and being prepared as relative density is 1.2000 ± 0.0050 lotion, has promptly obtained 8 kinds of fragrant class additives of diving respectively;
(4) method is routinely added calcium carbonate in the process of slurrying, adds combustion adjuvant and the fragrant class additive of diving in machine hand's program process, promptly makes required cigarette paper; Wherein, be benchmark with the quality of finished paper, the mass percent of calcium carbonate addition is 20%～40%; The mass percent of combustion adjuvant addition is 6%～10%; Described combustion adjuvant is selected from a kind of in citric acid sylvite, sodium citrate salt, malic acid sylvite or the malic acid sodium salt or their mixture; The mass percent of latent fragrant class additive addition is 0.01%-0.05%.
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| CN 200510048641 CN1793500A (en) | 2005-11-23 | 2005-11-23 | Cigarette paper and preparation method thereof |
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| CN 200510048641 CN1793500A (en) | 2005-11-23 | 2005-11-23 | Cigarette paper and preparation method thereof |
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| CN (1) | CN1793500A (en) |
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| CN101858044A (en) * | 2010-06-23 | 2010-10-13 | 牡丹江恒丰纸业股份有限公司 | Preparation method of cigarette paper additive |
| CN102021860A (en) * | 2010-06-01 | 2011-04-20 | 云南恩典科技产业发展有限公司 | Water-based paint containing Puerh tea extracts for cigarette shaping paper |
| CN101629399B (en) * | 2008-07-17 | 2012-12-12 | 红塔烟草(集团)有限责任公司 | Cigarette paper containing Chinese medicinal herb additive and preparation method thereof |
| CN103362033A (en) * | 2013-07-31 | 2013-10-23 | 广州市澳键丰泽生物科技有限公司 | Cigarette paper |
| CN105200857A (en) * | 2015-08-20 | 2015-12-30 | 嘉兴景程生物科技有限公司 | Fresh-scent cigarette paper and preparation method thereof |
| CN108251216A (en) * | 2018-01-18 | 2018-07-06 | 云南中烟工业有限责任公司 | A kind of preparation method and application of the Pu'er tea absolute oil containing the fragrant component of Viscμm articulatum Burm f cause |
| CN109989298A (en) * | 2019-05-10 | 2019-07-09 | 云南红塔蓝鹰纸业有限公司 | A kind of flowers and fruits odor type cigarette paper and preparation method thereof |
| CN112064406A (en) * | 2020-09-07 | 2020-12-11 | 云南中烟工业有限责任公司 | Special aroma forming paper prepared from jatropha roots of Dai nationality traditional edible spice plants of Xishuangbanna, method and application thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101629399B (en) * | 2008-07-17 | 2012-12-12 | 红塔烟草(集团)有限责任公司 | Cigarette paper containing Chinese medicinal herb additive and preparation method thereof |
| CN102021860A (en) * | 2010-06-01 | 2011-04-20 | 云南恩典科技产业发展有限公司 | Water-based paint containing Puerh tea extracts for cigarette shaping paper |
| CN102021860B (en) * | 2010-06-01 | 2012-07-18 | 云南恩典科技产业发展有限公司 | Water-based paint containing Puerh tea extracts for cigarette shaping paper |
| CN101858044A (en) * | 2010-06-23 | 2010-10-13 | 牡丹江恒丰纸业股份有限公司 | Preparation method of cigarette paper additive |
| CN101858044B (en) * | 2010-06-23 | 2011-07-06 | 牡丹江恒丰纸业股份有限公司 | Preparation method of cigarette paper additive |
| CN103362033A (en) * | 2013-07-31 | 2013-10-23 | 广州市澳键丰泽生物科技有限公司 | Cigarette paper |
| CN105200857A (en) * | 2015-08-20 | 2015-12-30 | 嘉兴景程生物科技有限公司 | Fresh-scent cigarette paper and preparation method thereof |
| CN105200857B (en) * | 2015-08-20 | 2017-04-19 | 嘉兴景程生物科技有限公司 | Fresh-scent cigarette paper and preparation method thereof |
| CN108251216A (en) * | 2018-01-18 | 2018-07-06 | 云南中烟工业有限责任公司 | A kind of preparation method and application of the Pu'er tea absolute oil containing the fragrant component of Viscμm articulatum Burm f cause |
| CN109989298A (en) * | 2019-05-10 | 2019-07-09 | 云南红塔蓝鹰纸业有限公司 | A kind of flowers and fruits odor type cigarette paper and preparation method thereof |
| CN112064406A (en) * | 2020-09-07 | 2020-12-11 | 云南中烟工业有限责任公司 | Special aroma forming paper prepared from jatropha roots of Dai nationality traditional edible spice plants of Xishuangbanna, method and application thereof |
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