CN109984953A - A kind of protein peptides take a shower, clean skin gel and preparation method thereof - Google Patents
A kind of protein peptides take a shower, clean skin gel and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/046—Aerosols; Foams
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/645—Proteins of vegetable origin; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/736—Chitin; Chitosan; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/85—Polyesters
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/14—Preparations for removing make-up
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/596—Mixtures of surface active compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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Abstract
The present invention relates to a kind of showers of protein peptides, clean skin gel and preparation method thereof, including 8~12 parts of plant fat acyl hydrolyzed vegetable protein salt, 1.2~2.5 parts of lauryl alcohol lactate, 1~10 part of plant fat acylsarcosine salt, 0.5~1 part of lauroyl arginine ethyl ester hydrochloride, ten 0.5~1 part of polyglycerol mono fat acid esters, 0.00008~0.0001 part of N- succinyl-chitosan, 1~5 part of polyalcohol, 67.5~87.6 parts of water；For transparent material, then in each transparent material of mixture, shower, clean skin gel is made after aged in elder generation's group system when preparation.Bath sense silk cunning is pleasant, washing effect is powerful, consistency is ideal, sterilizing, moisturizing and nourishing skin, foam exquisiteness are enriched, it is convenient to rinse and safe and non-toxic naturalization hydrolyzed vegetable protein peptide is taken a shower, clean skin gel.
Description
Technical field
The present invention relates to daily personal care technical fields, refer specifically to the shower of one kind naturalization hydrolyzed vegetable protein peptide, clean skin is coagulated
Glue and preparation method thereof.
Background technique
Disclose application No. is the Chinese patent application of CN201611050731 " a kind of silk peptide shower cream of skin care moisturizing and
Preparation method ", it is prepared from the following raw materials: 30-50 parts of silk peptide powder, 15-20 parts of gelatin, 5-12 parts of sodium alginate, bletilla striata powder
3-8 parts, poly- sub- 6-9 parts of carboxyl carbonic ester, 3-7 parts of ethyl acetate, 10-20 parts of fortune firethorn fruit extract, 11-14 parts of rhizoma typhonii powder,
2-5 parts of glutamic acid, 3-6 parts of sebum amino acid, 3-8 parts of mulberry leaf rosemary, 3-5 parts of hirudin, polyethylene glycol mono stearate 5-
10 parts, 2-8 parts of saualane, 10-15 parts of procyanidine, 5-8 parts of hirudin and 50-60 parts of water.
Application No. is the Chinese patent applications of CN201810911850 to disclose " a kind of plant polypeptide shampoo ", with quality
Part meter, which includes: 2-4 parts of the tuber of multiflower knotweed, and 10-14 parts of cacumen biotae, 3-5 parts of mulberry leaf, 4-6 parts of Radix Glycyrrhizae, 2-4 parts of ganoderma lucidum, kuh-seng
2-4 parts, 0.5-2 parts of rhizome of chuanxiong, 1-2 parts of the root of Dahurain angelica, 1-2 parts of ramulus cinnamomi, 0.5-2 parts of ginseng, 1-3 parts of folium artemisiae argyi, 2-4 parts of rhizoma cyperi, gleditsia sinensis 4-6
Part, 5-7 parts of soapberry, 2-4 parts of grandmother's fourth, 1-3 parts of dried peppermint leaf, 1-3 parts of Ilex Latifolia Thunb, 0.5-2 parts of Radix Angelicae Sinensis, 2-4 parts of lopseed, ginger
8-10 parts of powder, 10-20 parts of tea seed powder, 0.5-2 parts of cloves, 1-3 parts of lycopodium calvatum, 0.5-2 parts of radix rehmanniae preparata, 2-4 parts of fructus lycii, PORIA ALBA 5-
9 parts, BA-90018-12 parts of Ge Mandi, anti-dandruff peptide 3-7 parts, 8-12 parts of myristyl glutamic acid, 4-6 parts of sodium lauroyl sarcosine.
Above-mentioned technical proposal is when in use without sliding skin sense of relaxing, and nourishing skin is not comprehensive, and component is excessively complicated, is easily mixed into chemistry
The sensitization pathogenic factors such as synthetic residual, some also use non-natural object.
Another exploration that industry is made is to develop and promote to be with the final decomposition product of protein peptides-amino acid table work
The so-called amino acid shower cream of major ingredient, but such product price is higher, washes rear skin and shrinks tight and have astringent sense, moistens degree not
Foot, moisturizing timeliness are not grown, and some even irritates conjunctive bulbi, need to mix traditional chemical detergent and the chemical synthesis of larger dose
Rouge agent is assigned to cover its deficiency.Although the olive oil acylamino- hydrochlorate series raw material moistness developed recently improves to some extent, valence
Lattice are expensive, and clean skin power is weak, and foam is rare, be not suitable for making major ingredient and the breakthrough that makes product generate matter.
When and so far, the protein peptides bath for meeting above-mentioned naturalization requirement washes that clean skin product are popular not yet, and technos sums up
Formula and preparation process present on many bottlenecks, concentrate the following:
1. though repeatedly washing after protein peptides type anion table clean skin living, still there is the greasy stagnant evil of viscous hand in skin quick-drying
Sense is difficult to make bath lotion major ingredient so that protein peptides type anion table is living；
2. prior art can not make naturalization amino acid and protein peptides type bathe lotion and draw into high thick pleasant type gel (natural height
The gel products skin sense of molecule thickener modulation is greasy stagnant not well), because of the thickener with surfactant properties naturally changed
It could not still succeed in developing；
3. the intrinsic extremely difficult removal of bad smell living of protein peptides type anion table；
4. albumen peptides product is easily putrid and deteriorated, the screening of naturalization preservative is difficult, causes product stability poor；
5. albumen peptides table is living could not still to be eliminated bath and washes ends, though repeatedly rinsing still has contraction tight feeling and puckery to skin
The defect of sense.
Summary of the invention
The technical problem to be solved by the invention for the present situation of prior art is to provide a kind of bath sense silk it is sliding it is pleasant, wash
Wash that effect is powerful, consistency is ideal, sterilizing, moisturizing and nourishing skin, foam exquisiteness are enriched, rinse convenient and safe and non-toxic day
The shower of rightization hydrolyzed vegetable protein peptide, clean skin gel.
Another technical problem to be solved by this invention is the status for the prior art, and it is sliding easypro to provide a kind of bath sense silk
It feels well, washing effect is powerful, consistency is ideal, sterilizing, moisturizing and nourishing skin, foam exquisiteness are enriched, rinses convenient and safe nothing
The preparation method of the malicious shower of naturalization hydrolyzed vegetable protein peptide, clean skin gel.
The technical scheme of the invention to solve the technical problem is: a kind of shower, clean skin gel, feature exist
In: in parts by weight, including following components
Above-mentioned each component is selected from cosmetics-stage raw material.
It is also preferable to include the natural perfume materials of 0.2~1 parts by weight.
The plant fat acyl hydrolyzed vegetable protein salt is for by can actually change production made from operating procedure condition as follows
Product:
Well known organic synthesis technique (thionyl chloride method or phosphorus trichloride are first used from seven to 20 natural carbon fatty acids
Method) chloride fat acyl chloride, then with plant protein peptide obtained by vegetable protein enzymatic hydrolysis and purification process through amidation, then pass through
Carbonate neutralizes to obtain product.Specifically, being enzymatic hydrolysis type plant protein peptide through centrifugation-UF membrane-taste removal technique, i.e., with double enzyme water
(1500~1800Ug of basic protein enzyme dosage, 1 1000~1600Ug of Papain enzyme dosage), enzyme hydrolysis condition pH is
7.2~8.5,45~48 DEG C of temperature, substrate (vegetable protein) concentration 8~12%, the time 3~5 hours.It terminates hydrolysis and uses temperature
85~88 DEG C, enzymatic hydrolysis type plant protein peptide takes through 1000~1500rpm centrifugal treating obtained by 10~15 minutes duration
Supernatant, in conjunction with nanofiltration membrane (rolled film, hollow-fibre membrane, plate and frame film and tubular membrane etc., preferred rolled film, cross-flow stage die
Formula) isolation technics, Scientific application space bit former type and Donnan arrange negative effect, intercept the low of 200~500 dalton of molecular weight
Poly- peptide accounts for 92~93wt%, amino acid account for 0.5~1wt% vegetable protein peptide mixer (first it is multistage retention component concentration
Mixed liquor, then through coconut husk type deodorization active carbon in 50~55 DEG C of " dispersion-stirring-filtering " method deodorizations known to industry operate to
Less more than three times, low-temperature vacuum drying to anhydrous state), with fat acyl chloride in 60~85 DEG C of amidation process in atent solvent
At least 3 hours, vacuum desolvation agent added deionized water or purifying water dispersion, then neutralizes through potassium carbonate or sodium carbonate, and active carbon is deodorized
Removal of impurities, vacuum concentration dehydration products therefrom.
Preferably, the plant fat acyl hydrolyzed vegetable protein salt is by enzymatic hydrolysis type oat protein peptide and cocounut oil acyl chlorides and carbon
Sour potassium hydrolyzes avenin potassium according to the cosmetics-stage cocounut oil acyl that the above method is prepared, by enzymatic hydrolysis type oat protein peptide and olive
The cosmetics-stage olive oleoyl that olive oleoyl chloride and potassium carbonate are prepared according to the above method hydrolyzes avenin potassium or by digesting
The cosmetics-stage lauroyl hydrolysis oat egg that type oat protein peptide and lauroyl chloride and potassium carbonate are prepared according to the above method
White potassium etc..
The lauryl alcohol lactate is the esterification products from natural laruyl alcohol and lactic acid, preferred cosmetics-stage laurel
Alcohol lactate.
The plant fat acylsarcosine salt is from 12 to 16 natural carbon fatty acid elder generation chloride system fat
Acyl chlorides, and is originated from natural sarcosine amidation, then neutralized products therefrom.It is preferred that cosmetics-stage cocoyl sarcosine sodium, change
Cosmetic grade sodium lauroyl sarcosine, cosmetics-stage myristoyl sodium sarcosinate etc..More it is selected as cosmetics-stage myristoyl sodium sarcosinate
The mixed system for being 1~6:1 with cocoyl sarcosine sodium weight ratio.
The lauroyl arginine ethyl ester hydrochloride is from natural lauric acid elder generation chloride fat acyl chloride, with source
It is esterified from natural arginine amide, then with ethyl alcohol.With hydrochloric acid at salt products therefrom.It is preferred that commercially available pharmaceutical grade or cosmetics-stage
Lauroyl arginine ethyl ester hydrochloride.
The N- succinyl-chitosan is first to be dehydrated succinic anhydride processed from natural succinic acid, molten in anhydrous food grade
In agent and from natural chitosan amidation products therefrom.It is preferred that pharmaceutical grade or cosmetics-stage N- succinyl-chitosan sterling,
The polyalcohol is from or mixtures thereof natural glycerol, xylitol, sorbierite etc..It is preferred that pharmaceutical grade or change
Cosmetic grade glycerol.
The natural perfume material is natural essential oil, can according to need and selects any one of existing natural essential oil or more
Kind, preferably, select at least one of refined jasmine oil, the rare essential oil of Min, chamomile essential oil and Cananga odorata quintessence oil.
The ten polyglycerol mono fat esters are ten polyglycereol and the mono-esterification from eight to 12 natural carbon fatty acids
Ten polyglycereol list caprylate of product, preferably pharmaceutical grade or cosmetics-stage.
In above-mentioned each scheme, preferably the water is deionized water or purified water.
Above-mentioned naturalization hydrolyzed vegetable protein peptide takes a shower, the preparation method of clean skin gel, comprising the following steps:
(1) pre- ingredient is prepared
Under agitation, according to formula ratio by plant fat acyl hydrolyzed vegetable protein salt, plant fat acylsarcosine salt
It is added to and has been heated to 60~75 DEG C and accounts in the water of total amount 3/4ths, stirring obtains A phase materials to fully transparent；
Under agitation, ten polyglycerol mono fat acid esters are added to according to formula ratio and have been heated to 60~75 DEG C and account for
In the water of total amount a quarter, lauroyl arginine ethyl ester hydrochloride is added to fully transparent in stirring, stirring to fully transparent,
Obtain B phase materials；
Under agitation, N- succinyl-chitosan is added to according to formula ratio and has been heated to 60~75 DEG C of polyalcohol
In, stirring obtains C phase materials to fully transparent；
(2) gel material is modulated
A phase materials are put into impregnation pot, 60~75 DEG C of stringent temperature control, 100~150rpm of revolving speed is controlled, by B phase materials
In pouring into A phase materials in 30 minutes, constant temperature stirring 15 minutes fully transparent to material system；Then it is dripped in 30 minutes
C phase materials continue 60~75 DEG C of temperature control, control 100~150rpm of revolving speed, and stirring 15 minutes fully transparent to material system；It will
Material is cooled to 55~65 DEG C, in lauryl alcohol lactate is added portionwise in above-mentioned material in 30 minutes, control revolving speed 80~
100rpm, stirring at least 45 minutes are in fully transparent low thick gel state to material system, then control 30~40rpm of revolving speed, side
Cooling side is stirred at least 20 minutes, until material is up to 35 DEG C hereinafter, addition natural perfume material, is stirred at least 20 minutes, until material is in saturating
Until the bright thick cohesion colloidal state of height；
(3) it is aged
Step (2) resulting material is placed in and is aged 20~30 hours at room temperature to get transparent thick naturalization of height is arrived
The shower of hydrolyzed vegetable protein peptide, clean skin gel.
Compared with the prior art, the advantages of the present invention are as follows:
1. amino acid and protein peptides type can not be made to bathe the awkward situation that lotion draws into the pleasant thick gel preparations of height for prior art,
It originally visits and arrives lauryl alcohol lactate/myristoyl sarcosinate thickened systems, micro-emulsion technology is dexterously utilized and passes through cream
Liquid thickening prepares the transparent thick gel of height, avoids the greasy stagnant detest skin sense of product caused by being thickened with natural polymer sizing material；
2. (oligopeptide of control 200~500 dalton of molecular weight accounts for 92 to molecular weight adjustment when being hydrolyzed by vegetable protein
~93%, amino acid accounts for 0.5~1% vegetable protein peptide mixer) resulting protein peptides type anion table is living, with cationic
Lauroyl arginine ethyl ester hydrochloride is ingenious, and at salt, resulting molecular weight is relatively large, and hydrophily is good, is firmly adsorbed on flesh
The intermediary of skin surface and the sliding effect brilliance of silk, cooperates with generation to subtract friction effect with succinyl-chitosan), creatively eliminate
The protein peptides type anion table intrinsic greasy stagnant unhappiness of hand of gluing in skin quick-drying living is felt, the sliding pleasant bath of egg white silk is built
Sense.This cationic lauroyl arginine ethyl ester hydrochloride subtracts with living cooperate at salt system/succinyl-chitosan of anion table
Friction mode in the industry cycle belongs to pioneering；
3. vegetable protein obtains 200~500 dalton of molecular weight through complex enzyme zymohydrolysis-centrifugation-UF membrane-taste removal technique
Oligopeptide account for 92~93%, amino acid accounts for 0.5~1% oligopeptide mixture, and fat acyl chloride amidation, then through potassium carbonate
Or live in sodium carbonate with resulting anion table, pole ease-of-use and high efficiency cocoanut active charcoal, which is deodorized, to clean (at least three times) and obtains free from extraneous odour
Type product, such molecular weight of albumen science screening de-taste the technique combined with active carbon and completely eliminate protein type anion table
Bad smell living washes product convenient for bath and assigns fragrant operation, originally solve long-standing problem industry the bath of albumen peptides wash it is clean
The serious technical problem of skin strange smell；
4. cationic lauroyl arginine ethyl ester hydrochloride/protein peptides anion table work/succinyl-chitosan synergic agent
System eliminates the bath of amino acid table living body system because showing fabulous affinity and permeability to skin when washing end and rinsing: to skin
The contraction tight feeling and astringent sense of skin；
5. the foam that protein peptides anion table work/succinyl-chitosan collaboration system builds lasting exquisiteness；
6. with that can make the lauroyl arginine ethyl ester hydrochloride of food group material and itself just have the amino acid table of bacteriostasis
The work of living and polyglycereol esters table is constructed from protective system, and chemical preservative is avoided；
It exterminates most of fungies, bacterium and virus 7. lauroyl arginine ethyl ester hydrochloride can press down and so that bath is washed skin detergents and show
Good disinfection function is shown；
8. having both the functions such as moisturizing, tender skin, compact, pore refining and nutrition skin-protection；
9. washing power is powerful, light make-up effect brilliance is unloaded, foam gos deep into pore, takes away the dirts such as deep layer makeup material, while moderate
Except grease, it is dry and cracked to avoid washing rear skin, so that skin is kept smooth, restores the normal barrier function of skin；
10. bath avoids tradition and assigns greasy sliding oiling malice caused by rouge agent when washing, exfoliating is facilitated to operate；
11. easily rinsing, maximum one skin of organ of human body area is remained without chemical harmful substance；
12. real salt-free formula；
13. mother and baby is dedicated, stimulus data is less than the similar products of amino acid table modulation living；
14. removing the necessary solubilizer of fragrance essential oil from, the agent is reduced to the sensitization of skin；
15. the thickened systems that successfully protein peptides table is living are newly opened up, it is a variety of from natural function to be added in this system
Property component lay the foundation, convenient for exploitation whitening, remove the series of products such as wrinkle, anti-aging.
16. component itself or each group of component are derived from naturally, and are decomposed into natural products, details are as follows:
Plant fat acyl hydrolyzed vegetable protein salt by fatty acid (naturally occurring) chloride, then with plant protein peptide (day
So exist) amidated, it is obtained with (naturally occurring) neutralization of carbonate, and be decomposed into fatty acid (naturally occurring), vegetable protein
Peptide (naturally occurring) and salt (naturally occurring)；
Lauryl alcohol lactate is obtained by (naturally occurring) esterification of laruyl alcohol (naturally occurring) and lactic acid, and is decomposed into the moon
Cinnamic alcohol (naturally occurring) and lactic acid (naturally occurring)；
Plant fat acylsarcosine salt by fatty acid (naturally occurring) chloride, then with sarcosine (naturally occurring) acyl ammonia
Change, is obtained with (naturally occurring) neutralization of carbonate, and be decomposed into fatty acid (naturally occurring), sarcosine (naturally occurring) and salt
(naturally occurring)；
Lauroyl arginine ethyl ester hydrochloride by lauric acid (naturally occurring) chloride, then with arginine (naturally occurring)
It with the esterification products arginine ethyl ester amidated of ethyl alcohol (naturally occurring), is obtained with (naturally occurring) neutralization of hydrochloric acid, and decomposable
At fatty acid (naturally occurring), arginine (naturally occurring), ethyl alcohol (naturally occurring) and hydrochloric acid (naturally occurring)；
Ten polyglycerol mono fat acid esters polymerize to obtain ten polyglycereol by glycerol (naturally occurring), then (naturally deposit with fatty acid
) esterification and obtain, and be decomposed into fatty acid (naturally occurring) and glycerol (naturally occurring)；
N- succinyl-chitosan is dehydrated into succinic anhydride by succinic acid (naturally occurring), then with chitosan (naturally occurring)
It is esterified and obtains, and be decomposed into succinic acid (naturally occurring) and chitosan (naturally occurring)；
The naturally occurring glycerol of polyalcohol system, xylitol or sorbierite etc., or it is also possible to their mixture.
The naturally occurring essential oil of natural perfume material system.
The above-mentioned combination rich in innovative technical solution builds unexpected effect for product, i.e. bath is washed
What pleasant silk was sliding after process and bath are washed feels to be better than a so-called natural type skin detergents to appear on the market any up to now, even
More than the soft and smooth skin sense of organic silicone oil, while the thickening process for amino acid and albumen peptides skin detergents creates a road Tiao Xin.
The present invention elicites lauryl alcohol lactate and plant fat acyl hydrolyzed vegetable protein salt/plant fat acylsarcosine salt is multiple
Zoarium, which ties up in water phase, can draw the growth stage stable thick clear microemulsion liquid system of height, and elicite cationic lauroyl arginine second
Ester hydrochloride subtracts friction mode with living cooperate at salt system/succinyl-chitosan of protein peptides anion table, creatively eliminates
The protein peptides type anion table intrinsic greasy stagnant unhappiness of hand of gluing in skin quick-drying living is felt, the sliding pleasant bath of egg white silk is built
Sense.Final products raw material is naturally changed completely, non-stimulated, and appearance is pleasing, fragrant, consistency ideal, sterilizing, moisturizing and nourishing
Skin, foam exquisiteness are abundant, washing effect is powerful, and it is convenient and safe and non-toxic to rinse, and have both moisturizing, tender skin, compact, pore refining
And the functions such as nutrition skin-protection, and lay the foundation to add a variety of functional components naturally that are originated from this system, convenient for exploitation
The series of products such as wrinkle, anti-aging are removed in whitening.Meanwhile naturalization hydrolyzed vegetable protein peptide is taken a shower, clean skin gel is safe and non-toxic, i.e.,
Make to eat by mistake once in a while and does not also hinder health.
Specific embodiment
Present invention is further described in detail with reference to embodiments.
It is as follows that the present invention addresses " naturalization albumen peptide product " concept defining:
1. product major ingredient is protein peptides surfactant；
2. raw material selected by product is nature natural products, alternatively, raw material selected by product is to be with nature natural products
It is (i.e. artificial synthesized not introduce non-natural formation through environmentally protective chemical reaction process combination of sciences (with chemical bonds) for raw material
And it is non-naturally occurring) group, product core group be all it is natural, can by nature decompose or by the biological enzyme of human body
And other biological decomposing system resolves into the identical structured product of natural products existing for nature, and its intermediary for decomposing without
Damage the environmentally protective product of human health；
3. raw material selected by product meets cosmetics code requirement, non-stimulated allergy, no chemical synthesis preservative.
Embodiment 1 (naturalization hydrolyzed vegetable protein peptide face cleaning gel)
The naturalization hydrolyzed vegetable protein peptide of the present embodiment is taken a shower, clean skin gel (face cleaning gel) includes following components:
The 99.8% cocounut oil acyl hydrolyzes avenin potassium, is for by product made from following process conditions:
Avenin with double enzyme water (1500~1800Ug of basic protein enzyme dosage, 1 Papain enzyme dosage 1000~
1600Ug), enzyme hydrolysis condition pH is 7.2~8.5,45~48 DEG C of temperature, substrate (vegetable protein) concentration 8~12%, time 3
~5h.Hydrolysis is terminated using enzymatic hydrolysis type oat protein peptide obtained by 85~88 DEG C of temperature, 10~15min of duration, through 1000
~1500rpm centrifugal treating, takes supernatant, and in conjunction with nanofiltration membrane (rolled film, cross-flow transition mode) isolation technics, Scientific application is empty
Meta position former type and Donnan arrange negative effect, and the oligopeptide of interception 200~500 dalton of molecular weight accounts for 92~93wt%, amino
Acid account for 0.5~1wt% avenin peptide mixer (first multistage retention component concentration mixed liquor, then deodorize through coconut husk type
At least three times in 50~55 DEG C of operations of " dispersion-stirring-filtering " the method deodorization known to industry, low-temperature vacuum drying is extremely for active carbon
Anhydrous state), with cocounut oil acyl chlorides in ethyl acetate in 60~85 DEG C amidation process 3 hours, vacuum desolvation agent adds deionization
Water or purifying water dispersion, then neutralized through potassium carbonate or sodium carbonate, active carbon, which is deodorized, to clean, and vacuum concentration dehydration gained 99.8% contains
Volume production object.
Also the cocounut oil acyl that optional Shanghai is Mild COP30 along the trade mark of brightness Chemical Co., Ltd. hydrolyzes avenin potassium water
Agent product, vacuum concentration dehydration to 99.8% content product.
Naturally change the shower of hydrolyzed vegetable protein peptide in the present embodiment, clean skin gel (face cleaning gel) preparation method includes following
Step:
(1) pre- ingredient is prepared
Under agitation, control 100~150rpm of revolving speed, by 99.8% cocounut oil acyl hydrolyze 95 kilograms of avenin potassium,
99.8% 20 kilogram 99.8% of cocoyl sarcosine sodium and 85 kilograms of myristoyl sodium sarcosinate, which are added to, has been heated to 60~75 DEG C
548 kilograms of water in, obtain A phase materials to fully transparent within stirring at least 30 minutes；
Under agitation, 100~150rpm of revolving speed is controlled, 8 kilograms of ten polyglycereol monolaurates are added to and has been added
In 182.8 kilograms of water of heat to 60~75 DEG C, at least 30 minutes are stirred to extremely fully transparent, 99.8% lauroyl arginine of addition
8 kilograms of carbethoxy hydrochloride, B phase materials are obtained to fully transparent within stirring at least 30 minutes；
Under agitation, 100~150rpm of revolving speed is controlled, according to formula ratio by 0.0009 kilogram of N- succinyl-chitosan
It is added in 35 kilograms of 99.9% glycerol for being heated to 60~75 DEG C, stirs at least 3 hours to obtain C up to fully transparent
Phase materials；
(2) gel material is modulated
A phase materials are put into the high-quality stainless steel impregnation pot of 1000 liters, 60~75 DEG C of stringent temperature control, controls revolving speed 100
~150rpm, by B phase materials in pouring into A phase materials in 30 minutes, constant temperature stirring 15 minutes fully transparent to material system；It connects
In dripping C phase materials in 30 minutes, continue 60~75 DEG C of temperature control, control 100~150rpm of revolving speed, stirring 15 minutes to object
Material is fully transparent；Material is cooled to 55~65 DEG C, in 30 minutes by 20 kilograms of 99.8% lauryl alcohol lactate in batches
It is added in above-mentioned material, controls 80~100rpm of revolving speed, stirring at least 45 minutes to material system in fully transparent moderate consistency
Then gel state controls 30~40rpm of revolving speed, stir at least 20 minutes while cooling, until material is up to 35 DEG C hereinafter, addition Min is rare
It 3 kilograms of essential oil, stirs at least 20 minutes, until the thick cohesion colloidal state of the transparent height of material；
(3) it is aged
Step (2) resulting material is placed in and is aged 20~30 hours at room temperature to get transparent thick naturalization of height is arrived
Hydrolyzed vegetable protein peptide face cleaning gel.
Embodiment 2 (naturalization hydrolyzed vegetable protein peptide bath gels)
The naturalization hydrolyzed vegetable protein peptide of the present embodiment is taken a shower, clean skin gel (bath gels) includes following components:
Above-mentioned each component is selected from cosmetics-stage, and wherein associated core raw material selection approach is as follows:
30% cocoyl sarcosine sodium water solution is provided by Guangzhou Tianci Advanced Materials Co., Ltd；
99.8% lauroyl arginine ethyl ester hydrochloride is provided by Zhengzhou pleasant virtue Biotechnology Co., Ltd；
N- succinyl-chitosan is provided by Beijing Onlystar Technology Co., Ltd..
The 30% cocounut oil acyl hydrolyzes avenin potassium, is for by product made from following process conditions:
Avenin with double enzyme water (1500~1800Ug of basic protein enzyme dosage, 1 Papain enzyme dosage 1000~
1600Ug), enzyme hydrolysis condition pH is 7.2~8.5,45~48 DEG C of temperature, substrate (vegetable protein) concentration 8~12%, time 3
~5h.Hydrolysis is terminated using enzymatic hydrolysis type oat protein peptide obtained by 85~88 DEG C of temperature, 10~15min of duration, through 1000
~1500rpm centrifugal treating, takes supernatant, and in conjunction with nanofiltration membrane (rolled film, cross-flow transition mode) isolation technics, Scientific application is empty
Meta position former type and Donnan arrange negative effect, and the oligopeptide of interception 200~500 dalton of molecular weight accounts for 92~93wt%, amino
Acid account for 0.5~1wt% avenin peptide mixer (first multistage retention component concentration mixed liquor, then deodorize through coconut husk type
At least three times in 50~55 DEG C of operations of " dispersion-stirring-filtering " the method deodorization known to industry, low-temperature vacuum drying is extremely for active carbon
Anhydrous state), with cocounut oil acyl chlorides in ethyl acetate in 60~85 DEG C amidation process 3 hours, vacuum desolvation agent adds deionization
Water or purifying water dispersion, then neutralized through potassium carbonate or sodium carbonate, active carbon, which is deodorized, to clean, and vacuum concentration dehydration gained 99.8% contains
Volume production object.
Also the 30% cocounut oil acyl that optional Shanghai is Mild COP30 along the trade mark of brightness Chemical Co., Ltd. hydrolyzes avenin
Potassium aqua product.
Naturally change the shower of hydrolyzed vegetable protein peptide in the present embodiment, clean skin gel (bath gels) preparation method includes following
Step:
(1) pre- ingredient is prepared
Under agitation, 100~150rpm of revolving speed is controlled, 30% cocounut oil acyl is hydrolyzed into avenin aqueous solutions of potassium 350
Kilogram, 32 kilograms of 30% cocoyl sarcosine sodium water solution, 30% 35 kilograms of myristoyl sodium sarcosinate aqueous solution, which is added to, have been added
In 303 kilograms of water of heat to 60~75 DEG C (input amount of water has been 594.7 kilograms at this time, accounts for total amount 3/4ths), stirring is extremely
To fully transparent, A phase materials are obtained within few 30 minutes；
Under agitation, 100~150rpm of revolving speed is controlled, ten 10 kilograms of polyglycereol list caprylates are added to and have been heated
Into 198 kilograms of water of 60~75 DEG C, at least 30 minutes are stirred to extremely fully transparent, 99.8% lauroyl arginine ethyl ester of addition
8 kilograms of hydrochloride, B phase materials are obtained to fully transparent within stirring at least 30 minutes；
Under agitation, 100~150rpm of revolving speed is controlled, according to formula ratio by 0.001 kilogram of N- succinyl-chitosan
It is added in 50 kilograms of 99.9% glycerol for being heated to 60~75 DEG C, stirs at least 3 hours to obtain C up to fully transparent
Phase materials；
(2) gel material is modulated
A phase materials are put into the high-quality stainless steel impregnation pot of 1000 liters, 60~75 DEG C of stringent temperature control, controls revolving speed 100
~150rpm, by B phase materials in pouring into A phase materials in 30 minutes, constant temperature stirring 15 minutes fully transparent to material system；It connects
In dripping C phase materials in 30 minutes, continue 60~75 DEG C of temperature control, control 100~150rpm of revolving speed, stirring 15 minutes to object
Material is fully transparent；Material is cooled to 55~65 DEG C, in 30 minutes by 15 kilograms of 99.8% lauryl alcohol lactate in batches
It is added in above-mentioned material, controls 80~100rpm of revolving speed, stirring at least 45 minutes to material system in fully transparent moderate consistency
Then gel state controls 30~40rpm of revolving speed, stir at least 20 minutes while cooling, until material is up to 35 DEG C hereinafter, being added foreign sweet
It 2 kilograms of chrysanthemum essential oil, stirs at least 20 minutes, until the thick cohesion colloidal state of the transparent height of material；
(3) it is aged
Step (2) resulting material is placed in and is aged 20~30 hours at room temperature to get transparent thick naturalization of height is arrived
Hydrolyzed vegetable protein peptide bath gels.
Embodiment 3 (naturalization hydrolyzed vegetable protein peptide makeup removing gel)
The naturalization hydrolyzed vegetable protein peptide of the present embodiment is taken a shower, clean skin gel (makeup removing gel) includes following components:
Above-mentioned each component is selected from cosmetics-stage in addition to pharmaceutical grade
99.8% lauroyl hydrolyzes avenin potassium, is for by product made from following process conditions:
Avenin with double enzyme water (1500~1800Ug of basic protein enzyme dosage, 1 Papain enzyme dosage 1000~
1600Ug), enzyme hydrolysis condition pH is 7.2~8.5,45~48 DEG C of temperature, substrate (vegetable protein) concentration 8~12%, time 3
~5h.Hydrolysis is terminated using enzymatic hydrolysis type oat protein peptide obtained by 85~88 DEG C of temperature, 10~15min of duration, through 1000
~1500rpm centrifugal treating, takes supernatant, and in conjunction with nanofiltration membrane (rolled film, cross-flow transition mode) isolation technics, Scientific application is empty
Meta position former type and Donnan arrange negative effect, and the oligopeptide of interception 200~500 dalton of molecular weight accounts for 92~93wt%, amino
Acid account for 0.5~1wt% avenin peptide mixer (first multistage retention component concentration mixed liquor, then deodorize through coconut husk type
At least three times in 50~55 DEG C of operations of " dispersion-stirring-filtering " the method deodorization known to industry, low-temperature vacuum drying is extremely for active carbon
Anhydrous state), with lauroyl chloride in ethyl acetate in 60~85 DEG C amidation process 3 hours, vacuum desolvation agent adds deionization
Water or purifying water dispersion, then neutralized through potassium carbonate or sodium carbonate, active carbon, which is deodorized, to clean, and vacuum concentration dehydration gained 99.8% contains
Volume production object.
Naturally change the shower of hydrolyzed vegetable protein peptide in the present embodiment, clean skin gel (makeup removing gel) preparation method includes following
Step:
(1) pre- ingredient is prepared
Under agitation, control 100~150rpm of revolving speed, by 99.8% lauroyl hydrolyze 86 kilograms of avenin potassium,
99.8% 40 kilogram 99.8% of sodium lauroyl sarcosine and 40 kilograms of myristoyl sodium sarcosinate, which are added to, has been heated to 60~75 DEG C
569 kilograms of water in, obtain A phase materials to fully transparent within stirring at least 30 minutes；
Under agitation, 100~150rpm of revolving speed is controlled, 10 kilograms of ten polyglycereol monolaurates are added to and has been added
In 189 kilograms of water of heat to 60~75 DEG C, at least 30 minutes are stirred to fully transparent, 99.8% lauroyl arginine ethyl ester of addition
6 kilograms of hydrochloride, B phase materials are obtained to fully transparent within stirring at least 30 minutes；
Under agitation, 100~150rpm of revolving speed is controlled, according to formula ratio by N- succinyl-chitosan 0.00085 thousand
In gram being added in 30 kilograms of the 99.9% glycerol mixed alcohols with 2 kilograms of 99.9% sorbierite for be heated to 60~75 DEG C, stir
At least 3 hours are mixed to obtain C phase materials up to fully transparent；
(2) gel material is modulated
A phase materials are put into the high-quality stainless steel impregnation pot of 1000 liters, 60~75 DEG C of stringent temperature control, controls revolving speed 100
~150rpm, by B phase materials in pouring into A phase materials in 30 minutes, constant temperature stirring 15 minutes fully transparent to material system；It connects
In dripping C phase materials in 30 minutes, continue 60~75 DEG C of temperature control, control 100~150rpm of revolving speed, stirring 15 minutes to object
Material is fully transparent；Material is cooled to 55~65 DEG C, in 30 minutes by 25 kilograms of 99.8% lauryl alcohol lactate in batches
It is added in above-mentioned material, controls 80~100rpm of revolving speed, stirring at least 45 minutes solidifying in fully transparent low consistency to material system
Then colloidal state controls 30~40rpm of revolving speed, stir at least 20 minutes while cooling, until material is up to 35 DEG C hereinafter, jasmine essence is added
3 kilograms of oil stirs at least 20 minutes, until the transparent moderate thick cohesion colloidal state of material；
(3) it is aged
Step (2) resulting material is placed in and is aged 20~30 hours at room temperature to get transparent thick naturalization of height is arrived
Hydrolyzed vegetable protein peptide makeup removing gel.
It is solidifying with regard to this naturalization hydrolyzed vegetable protein peptide shower clean skin of the invention referring to the countries concerned's standard and professional standard
Glue is measured with commercially available amino acid shower cream contrast sample for the basic performance in terms of skin care, and see Table 1 for details.
Table 1
1 related data of table shows that naturalization hydrolyzed vegetable protein peptide shower clean skin gel of the invention relaxes in pH value, skin sense
May just as well, more excellent than commercially available ammonia shower cream on the skin cares core index such as moistening effect.
Referring to GBZ/T240.2-2011 chemicals toxicological evaluation program and test method part 2 acute oral toxicity
The correlation step of test measures above-mentioned naturalization hydrolyzed vegetable protein peptide shower clean skin gel to the acute oral toxicity of big white mouse
LD50 is greater than 16000mg/kg, it was demonstrated that product line of the invention belongs to nontoxic grade range, thus the indirect proof present invention naturalization
Hydrolyzed vegetable protein peptide shower clean skin gel is strayed into human body also because its body metabolism centre and final product belong to nontoxic grade model once in a while
It encloses and lossless health.
The present invention naturally changes hydrolyzed vegetable protein peptide shower clean skin gel and other commercially available amino acids shower cream irritations
Comparison
Test method: zeins method
Method And Principle: zeins (zein) and surfactant almost not soluble in water interacts,
Water solubility increases, zein more more soluble than weak stimulation surfactant compared with the surfactant of strong and stimulating.Therefore according to water-soluble
The situation of change of Action of Surfactant front and back nitrogen content in liquid, the solubility after determining zein and Action of Surfactant,
And skin irritation caused by the nitrogen content (zein value unit is in terms of g/L) in the zein dissolved and surfactant is at just
Than it will therefore be appreciated that the irritating size of surfactant.
Judgment basis: Zein > semi-finals irritation；2 < Zein <, 4 low irritant；Zein < 2 is nonirritant.
Testing result related data such as table 2.
Table 2
From the data in table 2, it can be seen that the irritation of naturalization hydrolyzed vegetable protein peptide shower clean skin gel of the invention to skin
It is more much smaller without the amino acid table work class shower cream irritated than being known as, it is only the 1/30 to 1/210 of the series.
Claims (10)
1. a kind of protein peptides are taken a shower, clean skin gel, it is characterised in that formed including following weight:
The plant fat acyl hydrolyzed vegetable protein salt is by product made from following process conditions:
By enzymatic hydrolysis type plant protein peptide after centrifugation-UF membrane-taste removal, vegetable protein peptide mixer is obtained；The plant egg
Molecular weight in white peptide mixer containing 92~93wt% is the oligopeptide of 200~500 dalton and the amino of 0.5~1wt%
Acid；
The vegetable protein peptide mixer and fat acyl chloride are subjected to amidation process, product is neutralized through potassium carbonate or sodium carbonate
Afterwards, it is deodorized and is cleaned using active carbon, obtain the plant fat acyl hydrolyzed vegetable protein salt.
2. protein peptides according to claim 1 are taken a shower, clean skin gel, it is characterised in that it further include natural perfume material, the day
The dosage of right fragrance is 0.2~1 parts by weight.
3. protein peptides according to claim 1 are taken a shower, clean skin gel, it is characterised in that the plant fat acyl hydrolyzing plant
Protein salt is that the cocounut oil acyl of cosmetics-stage hydrolyzes avenin potassium, the olive oleoyl of cosmetics-stage hydrolyzes avenin potassium or makeup
The lauroyl of grade hydrolyzes avenin potassium.
4. protein peptides according to claim 1 are taken a shower, clean skin gel, it is characterised in that the lauryl alcohol lactate be from
The esterification products of natural laruyl alcohol and lactic acid, preferred cosmetics-stage lauryl alcohol lactate.
5. protein peptides according to claim 1 are taken a shower, clean skin gel, it is characterised in that: the plant fat acyl flesh ammonia
Hydrochlorate is the mixture of the cocoyl sarcosine sodium of cosmetics-stage myristoyl sodium sarcosinate and cosmetics-stage, and the weight ratio of the two is
1~6:1.
6. protein peptides according to claim 1 are taken a shower, clean skin gel, it is characterised in that: the lauroyl arginine second
Ester hydrochloride is by product made from following process conditions:
From natural lauric acid elder generation chloride fat acyl chloride, it is esterified with from natural arginine amide, then with ethyl alcohol,
With hydrochloric acid at salt products therefrom；
Preferred commercially available pharmaceutical grade or cosmetics-stage lauroyl arginine ethyl ester hydrochloride.
7. protein peptides according to claim 1 are taken a shower, clean skin gel, it is characterised in that: the N- succinyl-chitosan
For pharmaceutical grade or the sterling of cosmetics-stage.
8. protein peptides according to claim 1 are taken a shower, clean skin gel, it is characterised in that: the polyalcohol is selected from natural
The glycerol of cosmetics-stage, xylitol, or mixtures thereof sorbierite；The ten polyglycerol mono fat esters gather sweet for pharmaceutical grade ten
Oily list caprylate.
9. protein peptides according to claim 2 are taken a shower, clean skin gel, it is characterised in that: the natural perfume material is selected from jasmine
At least one of the rare essential oil of jasmine essential oil, Min, chamomile essential oil and Cananga odorata quintessence oil.
10. the protein peptides as described in any one of claim 1~9 are taken a shower, the preparation method of clean skin gel, it is characterised in that including under
State step:
(1) pre- ingredient is prepared
Under agitation, plant fat acyl hydrolyzed vegetable protein salt, plant fat acylsarcosine salt are added according to formula ratio
It is accounted in the water of total amount 3/4ths to being heated to 60~75 DEG C, stirring obtains A phase materials to fully transparent；
Under agitation, ten polyglycerol mono fat acid esters are added to according to formula ratio and have been heated to 60~75 DEG C and account for total amount
In the water of a quarter, lauroyl arginine ethyl ester hydrochloride is added to fully transparent in stirring, and stirring obtains B to fully transparent
Phase materials；
Under agitation, N- succinyl-chitosan is added to according to formula ratio in the polyalcohol for being heated to 60~75 DEG C,
Stirring obtains C phase materials to fully transparent；
(2) gel material is modulated
By A phase materials put into impregnation pot in, at 60~75 DEG C, 100~150rpm, by B phase materials in 20~50 minutes fall
Enter in A phase materials, constant temperature stirring 10~20 minutes fully transparent to material system；Then in dripping C phase in 20~50 minutes
Material, continue temperature control stirred at 60~75 DEG C, under 100~150rpm 10~20 minutes it is fully transparent to material system；By material
55~65 DEG C are cooled to, in lauryl alcohol lactate is added portionwise in above-mentioned material in 20~50 minutes, is stirred under 80~100rpm
It mixes to material system in fully transparent low thick gel state；Then it at 30~40rpm, is stirred at least 20 minutes while cooling, until
When material is up to 35 DEG C or less, natural perfume material is added, stirs at least 20 minutes, until the thick cohesion colloidal state of the transparent height of material；
(3) it is aged
Step (2) resulting material is placed in be aged at room temperature 20~30 hours and is hydrolyzed to get to thick naturalization of transparent height
Plant protein peptide shower, clean skin gel.
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| Publication number | Publication date |
|---|---|
| CN109984953B (en) | 2022-08-19 |
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