CN109942192A - Grey colour cosmetic soil glaze and preparation method thereof and potlery tile - Google Patents
Grey colour cosmetic soil glaze and preparation method thereof and potlery tile Download PDFInfo
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- CN109942192A CN109942192A CN201910388114.0A CN201910388114A CN109942192A CN 109942192 A CN109942192 A CN 109942192A CN 201910388114 A CN201910388114 A CN 201910388114A CN 109942192 A CN109942192 A CN 109942192A
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- cosmetic soil
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Abstract
The invention discloses a kind of preparation method of grey colour cosmetic soil glaze, the preparation method of the ash colour cosmetic soil glaze is the following steps are included: weigh following raw materials: 50~90 parts of low temperature frits and 10~40 parts of antimony tin ash colorants according to poidometer；High-temperature fusion is carried out after the weighed raw material is mixed；Product after the completion of high-temperature fusion is directly poured into water to obtain grey frit；Then water for ball milling is added to obtain grey colour cosmetic soil glaze using the grey frit, low temperature mud, dispersing agent and degumming agent.The present invention also provides a kind of grey colour cosmetic soil glaze and potlery tiles.The present invention has carried out color development and colour stable since the antimony tin ash colorant in the grey colour cosmetic soil glaze that is prepared has first passed through high temperature in advance, the color of grey colour cosmetic soil glaze layer is influenced smaller by sintering temperature in potlery tile sintering process, to reduce the color difference of the grey colour cosmetic soil glaze layer for the grey potlery tile being fired into, the quality of grey potlery tile is improved.
Description
Technical field
The present invention relates to ceramic technology field, more particularly to grey colour cosmetic soil glaze and preparation method thereof and potlery tiles.
Background technique
Colour cosmetic soil glaze is the common raw material for preparing coloured potlery tile, will have the charity of colour cosmetic soil glaze in potlery tile green body
On, the cosmetic soil glaze layer obtained after firing can not only cover color, rough surface and defect of idiosome etc., and can also obtain
The color needed has good decoration function.Wherein, grey colour cosmetic soil glaze is a kind of wherein more common coloured makeup
Clay glaze material.
The firing range of potlery tile is 1000 DEG C~1180 DEG C, and firing range is wider, therefore is sintered the kiln (example of potlery tile
Such as tunnel oven or roller kilns) furnace body in temperature uniformity it is poor.However, due to the hair of chromophore component in grey colour cosmetic soil glaze
Color is very sensitive to firing temperature, and the minor deviations of firing temperature may cause the inclined of the cosmetic soil glaze layer color being fired into
Difference, therefore the grey colour cosmetic soil glaze layer for the grey potlery tile being fired into is easy to appear color difference, has seriously affected the ash being prepared
The quality of color potlery tile.
Above content is only used to facilitate the understanding of the technical scheme, and is not represented and is recognized that above content is existing skill
Art.
Summary of the invention
The main purpose of the present invention is to provide a kind of grey colour cosmetic soil glaze and preparation method thereof and potlery tiles, it is intended to solve
Certainly the color development of chromophore component is very sensitive to firing temperature in grey colour cosmetic soil glaze at present, the ash for the grey potlery tile being fired into
The technical issues of colour cosmetic soil glaze layer is easy to appear color difference, has seriously affected the quality of grey potlery tile.
To achieve the above object, the present invention provides a kind of preparation method of grey colour cosmetic soil glaze, the ash colour cosmetic soil
The preparation method of glaze the following steps are included:
Following raw materials: 50~90 parts of low temperature frits and 10~40 parts of antimony tin ash colorants are weighed according to poidometer；
After the weighed low temperature frit and the antimony tin ash coloring material for mixing, high-temperature fusion is carried out, wherein the high temperature
The firing temperature of melting is 1000 DEG C~1400 DEG C, when soak a length of 10min~60min；
Product after the completion of high-temperature fusion is directly poured into water to obtain grey frit；
According to poidometer weigh 10~70 parts of grey frits, 30~90 parts of low temperature mud, 0~1 part of dispersing agent and 0~
0.3 part of degumming agent adds water for ball milling to obtain grey colour cosmetic soil glaze.
Preferably, the low temperature frit includes one of lead frit, lead boron frit and low-temperature transparent frit.
Preferably, the fineness of the low temperature frit is 10 mesh or more.
Preferably, the low temperature mud drum includes one of black mud, kaolin, ball clay, red soil and feldspar.
Preferably, the dispersing agent includes one of sodium carboxymethylcellulose, dextrin and guar gum.
Preferably, the degumming agent includes one of sodium tripolyphosphate, sodium metasilicate and sodium humate.
Preferably, during adding water for ball milling to obtain grey colour cosmetic soil glaze, the fineness of the grey colour cosmetic soil glaze is controlled
For 325 mesh full by.
In addition, to achieve the above object, the present invention also provides a kind of grey colour cosmetic soil glaze, the ash colour cosmetic soil glaze
It is prepared by the preparation method of as above described in any item grey colour cosmetic soil glaze.
In addition, to achieve the above object, the present invention also provides a kind of potlery tile, the potlery tile includes idiosome layer and makeup clay glaze
Layer, wherein the cosmetic soil glaze layer is prepared using grey colour cosmetic soil glaze as described above.
Grey frit that the embodiment of the present invention proposes and preparation method thereof, grey colour cosmetic soil glaze and preparation method thereof and pottery
Watt, following raw materials: 50~90 parts of low temperature frits and 10~40 parts of antimony tin ash colorants are weighed first, in accordance with poidometer；By weighed institute
After stating low temperature frit, the grey color development oxide and antimony tin ash mixing, high-temperature fusion is carried out, wherein the high temperature melting
The firing temperature melted is 1000 DEG C~1400 DEG C, when soak a length of 10min~60min；By the production after the completion of high-temperature fusion
Object is directly poured into water to obtain grey frit；Then low temperature mud, dispersing agent, degumming agent and the grey frit are utilized, water polo is added
Mill obtains grey colour cosmetic soil glaze.The present invention due in the cosmetic soil glaze that is prepared antimony tin ash colorant first pass through height in advance
Temperature has carried out color development and colour stable, and the color of cosmetic soil glaze is influenced smaller by sintering temperature in potlery tile sintering process, from
And the color difference phenomenon of the grey colour cosmetic soil glaze layer for the grey potlery tile being fired into is reduced, improve the quality of grey potlery tile.
The realization, the function and the advantages of the object of the present invention will be described further in conjunction with the embodiments.
Specific embodiment
It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not intended to limit the present invention.
Firstly, preparation method to grey frit provided in an embodiment of the present invention, grey colour cosmetic soil glaze and potlery tile and
The potlery tile ash colour cosmetic soil glaze layer color difference method of inspection is summarized.
The preparation of grey frit:
(1) following raw materials: 50~90 parts of low temperature frits and 10~40 parts of antimony tin ashs are weighed according to poidometer.Wherein, described
Low temperature frit is the frit that melting temperature is less than or equal to 1200 DEG C, it is preferable that the low temperature frit includes lead frit, lead boron frit
One of with low-temperature transparent frit, the fineness of the low temperature frit is that (mesh number is bigger, and frit partial size is smaller, melts for 10 mesh or more
Block is thinner).The main component of the antimony tin ash colorant is antimony oxide and tin oxide.
(2) by after the weighed low temperature frit, the cobalt oxide and the antimony tin ash coloring material for mixing, high temperature melting is carried out
Melt, wherein the firing temperature (i.e. maximum temperature) of the high-temperature fusion is 1000 DEG C~1400 DEG C, and soak duration is (i.e. most
Heat preservation duration under high-temperature) it is 10min~60min.Preferably, when carrying out the high-temperature fusion, in the feelings of conditions permit
Under condition, raising heating rate (such as being heated up using the maximum heating rate of fusion apparatus) as far as possible was heated up with reducing
The different bring Color influences of antimony tin ash colorant colour developing under different temperatures in journey.
(3) product after the completion of high-temperature fusion is directly poured into water, carries out water quenching and obtains grey frit.
The grey frit being prepared according to the above method prepare raw material by weight and include 50~90 parts of low temperature frits and
10~40 parts of antimony tin ash colorants, wherein the low temperature frit includes one in lead frit, lead boron frit and low-temperature transparent frit
Kind.
Grey colour cosmetic soil glaze preparation:
According to poidometer weigh 10~70 parts of grey frits, 30~90 parts of low temperature mud, 0~1 part of dispersing agent and 0~
0.3 part of degumming agent adds water for ball milling to obtain grey colour cosmetic soil glaze.Preferably, the grey colour cosmetic soil glaze that control ball milling obtains
Fineness be 325 meshes full by.Preferably, the low temperature mud drum includes one of black mud, kaolin, ball clay, red soil and feldspar.
Being added with for the dispersing agent is evenly dispersed conducive to each component in the grey colour glaze being prepared, it is preferable that the dispersing agent packet
Include one of sodium carboxymethylcellulose, dextrin and guar gum.The degumming agent is used for the grey colour cosmetic soil glaze for preventing from generating
Colloid is formed, the preferably described degumming agent includes one of sodium tripolyphosphate, sodium metasilicate and sodium humate.
The raw material for preparing for the grey colour cosmetic soil glaze being prepared according to above scheme includes 10~70 parts of above method systems
The standby obtained grey frit, 30~90 parts of low temperature mud, 0~1 part of dispersing agent and 0~0.3 part of degumming agent.
Potlery tile preparation:
The grey colour cosmetic soil glaze charity being prepared according to above scheme is formed into grey colour cosmetic soil on potlery tile green body
Glaze layer, being then sintered can be obtained potlery tile.It is understood that the blank raw material of the potlery tile, grey colour cosmetic soil glaze
Charity thickness, the sintering condition of potlery tile etc. normal condition can be used, be not particularly limited herein.
It include green body layer and grey colour cosmetic soil glaze layer according to the potlery tile that above scheme is prepared, wherein the ashing color
Adornment clay glaze layer is prepared using the grey colour cosmetic soil glaze that the above method is prepared.
Potlery tile ash colour cosmetic soil glaze layer color difference is examined: extracting the same cosmetic soil of different riding positions, different kiln discharge times
Its ash colour cosmetic soil glaze layer is placed in together upward, the ash of each potlery tile is observed apart from potlery tile 2m by the potlery tile of glaze preparation
Colour cosmetic soil glaze layer color whether there is obvious color difference.
Technical solution provided by the present application, will be used to prepare first the low temperature frit of grey colour cosmetic soil glaze, cobalt oxide and
Antimony tin ash colorant first passes through the prefabricated grey frit of high temperature, carries out the color development of cobalt oxide in advance and stablizes pigment color.Then sharp again
Grey colour cosmetic soil glaze is prepared with grey frit.Due in grey colour cosmetic soil glaze cobalt oxide and cobalt ash colorant it is pre- advanced
Gone color development and stablize pigment color, color no longer change or changes and is smaller when being fired again, thus reduce potlery tile burn
The color difference problem of the ash colour cosmetic soil glaze layer as caused by furnace chamber temperature unevenness when knot.
Embodiment 1
Following raw materials: 50 parts of lead frits and 10 parts of antimony tin ash colorants are weighed according to poidometer.Weighed above-mentioned raw materials are mixed
After conjunction, be put into crucible, carry out high-temperature fusion under the following conditions: melting temperature is 1250 DEG C, and when soak is a length of
Then obtained fusant is directly poured into and carries out water quenching in the water of room temperature by 30min, obtain grey frit 1.
Weigh following raw materials according to poidometer: 10 parts of grey frits, 1,90 part of black mud, 0.3 part of sodium carboxymethylcellulose and
0.1 part of sodium tripolyphosphate adds water polo to be milled to 325 meshes full by obtaining grey colour cosmetic soil glaze 1.
Grey 1 charity of colour cosmetic soil glaze is formed into grey colour cosmetic soil glaze layer on potlery tile green body, grey colour cosmetic soil will be included
The potlery tile green body of glaze layer 1 stacks firing in tunnel oven and obtains potlery tile 1.
Different riding positions in tunnel oven, the potlery tile 1 of different kiln discharge times are extracted, upward by its grey colour cosmetic soil glaze layer
It is placed in together, observes that uniform grey is presented in the grey colour cosmetic soil glaze layer of each potlery tile apart from potlery tile 2m, without obvious color difference,
Reach high-class product color difference acceptance criteria in national standard (sintered tiles).
Embodiment 2
Following raw materials: 60 parts of lead boron frits and 20 parts of antimony tin ash colorants are weighed according to poidometer.By weighed above-mentioned raw materials
It after mixing, is put into crucible, carry out high-temperature fusion under the following conditions: melting temperature is 1400 degrees Celsius, soak duration
Then directly obtained fusant is poured into and carries out water quenching in the water of room temperature for 10min, obtains grey frit 2.
Weigh following raw materials according to poidometer: 25 parts of grey frit 2 and 75 part kaolin add water polo to be milled to 325 meshes complete
By obtaining grey colour cosmetic soil glaze 2.
Grey 2 charity of colour cosmetic soil glaze is formed into grey colour cosmetic soil glaze layer on potlery tile green body, grey colour cosmetic soil will be included
The potlery tile green body of glaze layer 2 stacks firing in tunnel oven and obtains potlery tile 2.
Different riding positions in tunnel oven, the potlery tile 2 of different kiln discharge times are extracted, upward by its grey colour cosmetic soil glaze layer
It is placed in together, observes that uniform grey is presented in the grey colour cosmetic soil glaze layer of each potlery tile apart from potlery tile 2m, without obvious color difference,
Reach high-class product color difference acceptance criteria in national standard (sintered tiles).
Embodiment 3
Following raw materials: 70 parts of low-temperature transparent frits and 30 parts of antimony tin ash colorants are weighed according to poidometer.It will be weighed above-mentioned
It after raw material mixing, is put into crucible, carry out high-temperature fusion under the following conditions: melting temperature is 1300 DEG C, soak duration
Then directly obtained fusant is poured into and carries out water quenching in the water of room temperature for 20min, obtains grey frit 3.
Following raw materials: 40 parts of grey frits, 3,60 parts of ball clays, 0.5 part of dextrin and 0.2 part of sodium metasilicate are weighed according to poidometer,
Water polo is added to be milled to 325 meshes full by obtaining grey colour cosmetic soil glaze 3.
Grey 3 charity of colour cosmetic soil glaze is formed into grey colour cosmetic soil glaze layer on potlery tile green body, grey colour cosmetic soil will be included
The potlery tile green body of glaze layer 3 stacks firing in tunnel oven and obtains potlery tile 3.
Different riding positions in tunnel oven, the potlery tile 3 of different kiln discharge times are extracted, upward by its grey colour cosmetic soil glaze layer
It is placed in together, observes that uniform grey is presented in the grey colour cosmetic soil glaze layer of each potlery tile apart from potlery tile 2m, without obvious color difference,
Reach high-class product color difference acceptance criteria in national standard (sintered tiles).
Embodiment 4
Following raw materials: 80 parts of lead frits and 40 parts of antimony tin ash colorants are weighed according to poidometer.Weighed above-mentioned raw materials are mixed
After conjunction, be put into crucible, carry out high-temperature fusion under the following conditions: melting temperature is 1100 DEG C, and when soak is a length of
Then obtained fusant is directly poured into and carries out water quenching in the water of room temperature by 45min, obtain grey frit 4.
Weigh following raw materials according to poidometer: 55 parts of grey frits, 4,45 parts of red soil, 0.7 part of sodium carboxymethylcellulose and
0.3 part of sodium tripolyphosphate adds water polo to be milled to 325 meshes full by obtaining grey colour cosmetic soil glaze 4.
Grey 4 charity of colour cosmetic soil glaze is formed into grey colour cosmetic soil glaze layer on potlery tile green body, grey colour cosmetic soil will be included
The potlery tile green body of glaze layer 4 stacks firing in tunnel oven and obtains potlery tile 4.
Different riding positions in tunnel oven, the potlery tile 4 of different kiln discharge times are extracted, upward by its grey colour cosmetic soil glaze layer
It is placed in together, observes that uniform grey is presented in the grey colour cosmetic soil glaze layer of each potlery tile apart from potlery tile 2m, without obvious color difference,
Reach high-class product color difference acceptance criteria in national standard (sintered tiles).
Embodiment 5
Following raw materials: 90 parts of lead boron frits and 50 parts of antimony tin ash colorants are weighed according to poidometer.By weighed above-mentioned raw materials
It after mixing, is put into crucible, carry out high-temperature fusion under the following conditions: melting temperature is 1000 degrees Celsius, soak duration
Then directly obtained fusant is poured into and carries out water quenching in the water of room temperature for 60min, obtains grey frit 5.
Following raw materials: 70 parts of grey frits, 5,30 parts of feldspars, 1 part of guar gum and 0.2 part of humic acid are weighed according to poidometer
Sodium adds water polo to be milled to 325 meshes full by obtaining grey colour cosmetic soil glaze 5.
Grey 5 charity of colour cosmetic soil glaze is formed into grey colour cosmetic soil glaze layer on potlery tile green body, grey colour cosmetic soil will be included
The potlery tile green body of glaze layer 5 stacks firing in tunnel oven and obtains potlery tile 5.
Different riding positions in tunnel oven, the potlery tile 5 of different kiln discharge times are extracted, upward by its grey colour cosmetic soil glaze layer
It is placed in together, observes that uniform grey is presented in the grey colour cosmetic soil glaze layer of each potlery tile apart from potlery tile 2m, without obvious color difference,
Reach high-class product color difference acceptance criteria in national standard (sintered tiles).
The grey colour cosmetic soil glaze charity that any of the above-described embodiment obtains it can be seen from above embodiments result is in potlery tile
On be fired into potlery tile when, present between different riding positions, the potlery tile of different kiln discharge times in tunnel oven uniform
Grey reaches high-class product color difference acceptance criteria in national standard (sintered tiles) without obvious color difference.To reduce the ash being fired into
The color difference phenomenon of the grey colour cosmetic soil glaze layer of color potlery tile, improves the quality of grey potlery tile.
It should be noted that, in this document, the terms "include", "comprise" or its any other variant are intended to non-row
His property includes, so that the process, method, article or the system that include a series of elements not only include those elements, and
And further include other elements that are not explicitly listed, or further include for this process, method, article or system institute it is intrinsic
Element.In the absence of more restrictions, the element limited by sentence " including ... ", it is not excluded that including the element
Process, method, there is also other identical elements in article or system.
In addition, the description for being related to " first ", " second " etc. in this application is used for description purposes only, and should not be understood as referring to
Show or imply its relative importance or implicitly indicates the quantity of indicated technical characteristic." first ", " are defined as a result,
Two " feature can explicitly or implicitly include at least one of the features.
The above is only a preferred embodiment of the present invention, is not intended to limit the scope of the invention, all to utilize this hair
Equivalent article or equivalent process transformation made by bright description are applied directly or indirectly in other relevant technology necks
Domain is included within the scope of the present invention.
Claims (9)
1. a kind of preparation method of ash colour cosmetic soil glaze, which is characterized in that the preparation method packet of the ash colour cosmetic soil glaze
Include following steps:
Following raw materials: 50~90 parts of low temperature frits and 10~40 parts of antimony tin ash colorants are weighed according to poidometer；
After the weighed low temperature frit and the antimony tin ash coloring material for mixing, high-temperature fusion is carried out, wherein the high-temperature fusion
Firing temperature be 1000 DEG C~1400 DEG C, when soak a length of 10min~60min；
Product after the completion of high-temperature fusion is directly poured into water to obtain grey frit；
10~70 parts of grey frits, 30~90 parts of low temperature mud, 0~1 part of dispersing agent and 0~0.3 part are weighed according to poidometer
Degumming agent adds water for ball milling to obtain grey colour cosmetic soil glaze.
2. the preparation method of ash colour cosmetic soil glaze as described in claim 1, which is characterized in that the low temperature frit includes lead
One of frit, lead boron frit and low-temperature transparent frit.
3. the preparation method of ash colour cosmetic soil glaze as described in claim 1, which is characterized in that the fineness of the low temperature frit
More than 10 mesh.
4. the preparation method of ash colour cosmetic soil glaze as described in claim 1, which is characterized in that the low temperature mud drum includes black
One of mud, kaolin, ball clay, red soil and feldspar.
5. the preparation method of ash colour cosmetic soil glaze as described in claim 1, which is characterized in that the dispersing agent includes carboxylic first
One of base sodium cellulosate, dextrin and guar gum.
6. the preparation method of ash colour cosmetic soil glaze as described in claim 1, which is characterized in that the degumming agent includes trimerization
One of sodium phosphate, sodium metasilicate and sodium humate.
7. the preparation method of ash colour cosmetic soil glaze as claimed in any one of claims 1 to 6, which is characterized in that water for ball milling is added to obtain
To during grey colour cosmetic soil glaze, the fineness for controlling the grey colour cosmetic soil glaze be 325 mesh full by.
8. a kind of ash colour cosmetic soil glaze, which is characterized in that the ash colour cosmetic soil glaze passes through such as any one of claim 1-7
The preparation method of the grey colour cosmetic soil glaze is prepared.
9. a kind of potlery tile, which is characterized in that the potlery tile includes idiosome layer and cosmetic soil glaze layer, wherein the cosmetic soil glaze layer
It is prepared using grey colour cosmetic soil glaze as claimed in claim 8.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910388114.0A CN109942192A (en) | 2019-05-09 | 2019-05-09 | Grey colour cosmetic soil glaze and preparation method thereof and potlery tile |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910388114.0A CN109942192A (en) | 2019-05-09 | 2019-05-09 | Grey colour cosmetic soil glaze and preparation method thereof and potlery tile |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN116354746A (en) * | 2023-04-03 | 2023-06-30 | 景德镇市望龙陶瓷有限公司 | Ceramic clay cosmetic soil for ceramic glaze surface decoration and use method thereof |
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| CN101255067A (en) * | 2007-12-28 | 2008-09-03 | 冼金源 | Preparation method of metal-imitation glaze |
| KR100891360B1 (en) * | 2008-12-15 | 2009-04-01 | 주식회사 한일세라믹 | Aseok, pigment-particle, absorbency-particle and it uses this to form on the surface of the brick to design and color |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN116354746A (en) * | 2023-04-03 | 2023-06-30 | 景德镇市望龙陶瓷有限公司 | Ceramic clay cosmetic soil for ceramic glaze surface decoration and use method thereof |
| CN116354746B (en) * | 2023-04-03 | 2024-03-26 | 景德镇市望龙陶瓷有限公司 | Ceramic clay cosmetic soil for ceramic glaze surface decoration and use method thereof |
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Application publication date: 20190628 |