CN109925206A - A kind of Non-water washing shampoo and preparation method thereof - Google Patents
A kind of Non-water washing shampoo and preparation method thereof Download PDFInfo
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- CN109925206A CN109925206A CN201910273532.5A CN201910273532A CN109925206A CN 109925206 A CN109925206 A CN 109925206A CN 201910273532 A CN201910273532 A CN 201910273532A CN 109925206 A CN109925206 A CN 109925206A
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- water washing
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Abstract
The invention belongs to daily-use chemical industry technical fields, and in particular to a kind of Non-water washing shampoo and preparation method thereof.The present invention provides a kind of Non-water washing shampoo, which is prepared by methylisothiazolinone, cetyl trimethylammonium bromide, iodine propilolic alcohol butyl mephenesin Carbamate, boric acid, sodium chloride, fatty alcohol polyoxyethylene ether, emulsifier, glycerol, essence and deionized water.The invention also discloses the preparation methods of the Non-water washing shampoo.Non-water washing shampoo of the invention integrates hair nursing, cleaning, removal dandruff, anti-bacterial, anti-itching, fluffy submissive glossy using rear hair, harmless to humans non-stimulated, dimethyl silicone polymer is free of in shampoo, is suitable for various hair qualitys, it is at low cost, stability is good, can be widely applied.
Description
Technical field
The invention belongs to daily-use chemical industry technical fields, and in particular to a kind of Non-water washing shampoo and preparation method thereof.
Background technique
Shampoo is mainly used for cleaning the grease of human secretory being attached on scalp and hair, sweat mixed with dirt, falls off on scalp
Cell and external dust, microorganism and bad smell etc..With the development of modern industry, caused by due to various pollutions
It is dirty that dust causes hair to be easy to, and people almost use shampoo daily, and certain damage is be easy to cause to hair.By
This, apart from cleaning, people to shampoo hair care, in terms of requirement it is higher and higher.
In general, generalling use anionic surfactant when synthesizing existing shampoo, cleaning action is played, is had
When can add the nonionic surfactants of some auxiliary and be used in compounding, these nonionic surfactants mainly play solubilising and cream
Change effect and decontamination, while reducing by surfactant bring to the irritation of eyes.This surfactant needs a large amount of
Water cleaning.In addition, in the market many shampoo manufacturers in order to make hair wash after moisturizing it is smooth, usually add in shampoo
Addition polymerization dimethyl siloxane, but dimethyl silicone polymer is not soluble in water, can not be properly washed, and may increase with access times
More, hair is thick and heavy and gradually loses elasticity, clogging of pores, generates scalp itch, or even dandruff occur, may will affect hair
Health.
Therefore, common shampoo must be cleaned with a large amount of water, and remaining can not may be also properly washed poly-
Dimethyl siloxane is used and is limited by water source and living environment, and may be unfavorable for health.It is for example handicapped old
The groups such as weak person, long-term inpatients patient and weight patient, marine crewman, and in the area of water shortage, the use of common shampoo is
It is restricted.In this context, people have developed Non-water washing shampoo.Chinese patent such as Publication No. CN106074261A is public
Opened it is a kind of by soapberry pericarp, Chinese honey locust (fruit), oil tea be withered, cacumen biotae, mulberry leaf, eclipta, the fleece-flower root, old ginger, peppermint, glossy privet
The disposable shampoo that the medicinal herb components such as son, Folium Apocyni Veneti are prepared, this shampoo medium-height grass survival dose is big, higher cost.
The Chinese patent of Publication No. CN108524325A disclose it is a kind of by the third butane, dehydrated alcohol, cornstarch, the bent chloramines in west,
The disposable hair washing spray that perfume type essence is prepared, which has used a large amount of dehydrated alcohols, although nontoxic, have compared with
Strong irritation, industrially using less.Therefore, it needs to research and develop a kind of with preferable nursing, cleaning, anti-dandruff and antibacterial effect
Fruit and the not high Non-water washing shampoo for being conducive to industrialization production of cost.
Summary of the invention
In view of this, the purpose of the present invention is to provide a kind of stability it is high, at low cost and have nursing, cleaning, antibacterial,
The Non-water washing shampoo and preparation method thereof of antipruritic and anti-dandruff effect.
To achieve the above object, the specific technical solution of the present invention is as follows:
A kind of Non-water washing shampoo, comprising:
Preferably, fatty alcohol polyoxyethylene ether is AEO-9 and/or AEO-7.
Preferably, one of emulsifier Tween-20, Triton-X-100 and OP-10 or several.
Preferably, the mass concentration of methylisothiazolinone is 9.5%~9.9%.
Preferably, Non-water washing shampoo is also containing the essence of 0.05~0.1wt%.
The present invention also provides the preparation methods of Non-water washing shampoo, comprising the following steps:
S1. the deionized water that 45~48wt% is weighed into container is heated to 40~50 DEG C, weighs under keeping warm mode
Stirring in deionized water is added until dissolving in the fatty alcohol polyoxyethylene ether of 0.3~0.5wt% and the glycerol of 3~7wt%；
S2. under stirring conditions, successively into the solution that step S1 is obtained be added 0.5~1.5wt% sodium chloride,
The iodine propilolic alcohol fourth of the boric acid of 0.5~1wt%, the methylisothiazolinone of 0.075~0.1wt%, 0.0075~0.01wt%
The emulsifier of base mephenesin Carbamate and 0.1~0.5wt% all keeps the temperature 10min after dissolution；
S3. 0.05~0.1wt% cetyl trimethylammonium bromide is added into the solution that step S2 is obtained to stir to molten
Solution is added the deionized water of remaining 45~48wt%, stirs evenly, and 0.05~0.1wt% is added after then being cooled to room temperature
Essence to get Non-water washing shampoo.
Technical solution provided by the present invention has the advantages that
1. Non-water washing shampoo component formula provided by the invention is using deionized water as main component, and each component is to human body
It is harmless and nonirritant, it can directly use, exempt a large amount of clear water cleanings, be easy to use quick.
2. Non-water washing shampoo provided by the invention integrates hair nursing, cleaning, removal dandruff, anti-bacterial, anti-itching,
It is fluffy submissive glossy using rear hair, dimethyl silicone polymer is free of in shampoo, is suitable for various hair qualitys, nurse, clean,
The anti-bacterial, anti-itching actual effect time is longer.
3. Non-water washing shampoo component stability provided by the invention is good, can long-term preservation.
4. Non-water washing shampoo provided by the invention is using cetyl trimethylammonium bromide and methylisothiazolinone, iodine
Propilolic alcohol butyl mephenesin Carbamate, boric acid combination, sterilize anti-dandruff and itching-relieving better effect, and play the role of bleeding agent, are conducive to remove head
Dirt is sent out, is cooperated with glycerol, moistening effect is more preferable, and hair is more fluffy submissive glossy.
5. Non-water washing shampoo preparation process provided by the invention is simple, it is not necessarily to complex machines equipment, cost is relatively low, can be big
Large-scale production.
Specific embodiment
A kind of Non-water washing shampoo provided by the invention, comprising: methylisothiazolinone, cetyl trimethyl bromination
Ammonium, iodine propilolic alcohol butyl mephenesin Carbamate, boric acid, sodium chloride, fatty alcohol polyoxyethylene ether, emulsifier, glycerol and deionized water.Its
In, by weight percentage, methylisothiazolinone is preferably 0.075~0.1%；Cetyl trimethylammonium bromide is preferably
0.05~0.1%；Iodine propilolic alcohol butyl mephenesin Carbamate is preferably 0.0075~0.01%；Boric acid is preferably 0.5~1%；Chlorination
Sodium is preferably 0.5~1.5%；Fatty alcohol polyoxyethylene ether is preferably 0.3~0.5%；Emulsifier is preferably 0.1~0.5%；It is sweet
Oil preferably 3~7%；Essence is preferably 0.05~0.1%, and deionized water is surplus.Wherein, the quality of methylisothiazolinone
Concentration is 9.5%~9.9%.
Methylisothiazolinone, cetyl trimethylammonium bromide, iodine propilolic alcohol butyl mephenesin Carbamate and boric acid, which have, to kill
Bacterium antisepsis can make shampoo have stronger stability, can also go while wherein methylisothiazolinone is sterilized
Bits, cetyl trimethylammonium bromide can be cooperateed with glycerol and be played a role, and can effectively be substituted commonly used in the prior art poly-
Dimethyl siloxane keeps hair smooth glossy.In addition, cetyl trimethylammonium bromide also has osmosis, Ke Yiyu
Fatty alcohol polyoxyethylene ether and emulsifier synergistic effect generate preferable clean effect.Fatty alcohol polyoxyethylene ether is
Or mixtures thereof AEO-9, AEO-7, more preferably AEO-7.Emulsifier is preferably Tween-20, Triton-X-100 and OP-10
One of or several, more preferably TX-100.
The preparation method of Non-water washing shampoo, comprising the following steps:
S1. the deionized water that 45~48wt% is weighed into container is heated to 40~50 DEG C, preferably 40 DEG C, is keeping the temperature
It is straight that stirring in deionized water is added in the glycerol of fatty alcohol polyoxyethylene ether and 3~7wt% that 0.3~0.5wt% is weighed under state
To dissolution；
S2. under stirring conditions, successively into the solution that step S1 is obtained be added 0.5~1.5wt% sodium chloride,
The iodine propilolic alcohol fourth of the boric acid of 0.5~1wt%, the methylisothiazolinone of 0.075~0.1wt%, 0.0075~0.01wt%
The emulsifier of base mephenesin Carbamate and 0.1~0.5wt% all keeps the temperature 10min after dissolution；
S3. 0.05~0.1wt% cetyl trimethylammonium bromide is added into the solution that step S2 is obtained to stir to molten
Solution is added the deionized water of remaining 45~48wt%, stirs evenly, and 0.05~0.1wt% is added after then being cooled to room temperature
Essence to get Non-water washing shampoo.
Technical solution of the present invention is clearly and completely described below in conjunction with the specific embodiment of the invention, it is clear that
Described embodiment is a part of the embodiment of the present invention, rather than whole embodiments.It will be appreciated by those skilled in the art that
It modifies to specific embodiments of the present invention or some technical features can be equivalently replaced, without departing from the technology of the present invention
The spirit of scheme should all cover in the scope of protection of the invention.Raw material used by following embodiment of the present invention is commercially available
Commodity.
The formula of 1-3 of the embodiment of the present invention is as shown in table 1, wherein fatty alcohol polyoxyethylene ether used in Example 1 is
AEO-7, emulsifier TX-100；The fatty alcohol polyoxyethylene ether used in embodiment 2 is AEO-7, emulsifier Tween-20；
The fatty alcohol polyoxyethylene ether used in embodiment 3 is AEO-9, emulsifier Triton-X-100.
1 Non-water washing shampoo prescription weight percentage of each component of table
The embodiment of the present invention 1-3's the preparation method comprises the following steps:
S1. a certain amount of deionized water is weighed into container, 40 DEG C of heat preservations is heated to, by fatty alcohol polyoxyethylene ether and sweet
Stirring in deionized water is added for oil until dissolution；
S2. under stirring conditions, sodium chloride, boric acid, methyl-isothiazol are successively added into the solution that step S1 is obtained
Quinoline ketone, iodine propilolic alcohol butyl mephenesin Carbamate and emulsifier all keep the temperature 10min after dissolution；
S3. cetyl trimethylammonium bromide is added into the solution that step S2 is obtained to stir to dissolution, is added remaining
Deionized water stirs evenly, and essence is added after then being cooled to room temperature to get Non-water washing shampoo.
Non-water washing shampoo prepared by Example 1~3 carries out stability experiment, the shampoo of quality such as takes to place respectively
Shampoo is observed in room temperature, high temperature and after ultraviolet environments lower 6 week, observation the results are shown in Table 2
The test of 2 Non-water washing shampoo stability of table
As shown in Table 2, after carrying out 6 weeks Acceleration studies, each index of Examples 1 to 3 is normal, and shampoo of the invention is matched
Fang Wending can be saved for a long time.
Non-water washing shampoo prepared by Example 1~3 carries out functional evaluation, and specific embodiment is as follows:
Tester 60 are chosen, age distribution is 20-50 years old, wherein male 30, women 30.Each sample arrangement
20 testers, tester are to wash hair in the same manner using sample, wash primary head weekly.Each sample continuously makes
With six weeks, tester scored to sample according to the usage experience of oneself.Standards of grading use ten point system, score value higher generation
Table effect is better.Average value finally is calculated to the scoring of every kind of shampoo, it is specific as shown in table 3.
3 Non-water washing shampoo functional evaluation Score Lists of table
Result as shown in table 3 effectively illustrate shampoo of the present invention nursing, cleaning, antibacterial, it is antipruritic and in terms of
With preferable effect.
Better embodiment of the invention is explained in detail above, but the present invention is not limited to above-mentioned embodiment party
Formula within the knowledge of one of ordinary skill in the art can also be without departing from the purpose of the present invention
Various changes can be made.
Claims (6)
1. a kind of Non-water washing shampoo characterized by comprising
2. Non-water washing shampoo according to claim 1, it is characterised in that: the fatty alcohol polyoxyethylene ether is AEO-
9 and/or AEO-7.
3. Non-water washing shampoo according to claim 1, it is characterised in that: the emulsifier is Tween-20, Triton-
One of X-100 and OP-10 are several.
4. Non-water washing shampoo according to claim 1, it is characterised in that: the mass concentration of the methylisothiazolinone
It is 9.5~9.9%.
5. according to claim 1 to Non-water washing shampoo described in 4, it is characterised in that: the Non-water washing shampoo also contains
The essence of 0.05~0.1wt%.
6. the preparation method of Non-water washing shampoo described in claim 5, which comprises the following steps:
S1. the deionized water that 45~48wt% is weighed into container is heated to 40~50 DEG C, weigh 0.3 under keeping warm mode~
Stirring in deionized water is added until dissolving in the fatty alcohol polyoxyethylene ether of 0.5wt% and the glycerol of 3~7wt%；
S2. under stirring conditions, successively into the solution that step S1 is obtained be added 0.5~1.5wt% sodium chloride, 0.5~
The iodine propilolic alcohol butyl ammonia first of the boric acid of 1wt%, the methylisothiazolinone of 0.075~0.1wt%, 0.0075~0.01wt%
The emulsifier of acid esters and 0.1~0.5wt% all keeps the temperature 10min after dissolution；
S3. 0.05~0.1wt% cetyl trimethylammonium bromide is added into the solution that step S2 is obtained to stir to dissolution, adds
The deionized water for entering remaining 45~48wt%, stirs evenly, and the perfume (or spice) of 0.05~0.1wt% is added after then being cooled to room temperature
Essence is to get Non-water washing shampoo.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910273532.5A CN109925206A (en) | 2019-04-05 | 2019-04-05 | A kind of Non-water washing shampoo and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201910273532.5A CN109925206A (en) | 2019-04-05 | 2019-04-05 | A kind of Non-water washing shampoo and preparation method thereof |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107049817A (en) * | 2017-06-19 | 2017-08-18 | 南京福特卡特材料科技有限公司 | A kind of disposable shampoo and preparation method thereof |
| CN107737023A (en) * | 2017-10-30 | 2018-02-27 | 天津司邦适生物科技股份有限公司 | A kind of albumen Non-water washing foaming foam |
| CN108524325A (en) * | 2018-05-29 | 2018-09-14 | 佛山市顺德区香江精细化工实业有限公司 | A kind of Non-water washing hair spray and preparation method thereof |
-
2019
- 2019-04-05 CN CN201910273532.5A patent/CN109925206A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107049817A (en) * | 2017-06-19 | 2017-08-18 | 南京福特卡特材料科技有限公司 | A kind of disposable shampoo and preparation method thereof |
| CN107737023A (en) * | 2017-10-30 | 2018-02-27 | 天津司邦适生物科技股份有限公司 | A kind of albumen Non-water washing foaming foam |
| CN108524325A (en) * | 2018-05-29 | 2018-09-14 | 佛山市顺德区香江精细化工实业有限公司 | A kind of Non-water washing hair spray and preparation method thereof |
Non-Patent Citations (1)
| Title |
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| GOODLUCK09: "碘丙炔正丁胺甲酸酯ipbc抗菌剂", 《HTTPS://WWW.DOC88.COM/P-7456210617933.HTML?R=1》 * |
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Application publication date: 20190625 |