CN109914144A - A kind of face tissue and its method of the preparation of prescriptions worth thousand gold dregs of a decoction resource regeneration - Google Patents
A kind of face tissue and its method of the preparation of prescriptions worth thousand gold dregs of a decoction resource regeneration Download PDFInfo
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Abstract
The present invention relates to the face tissue and its method of a kind of preparation of prescriptions worth thousand gold dregs of a decoction resource regeneration, the technique for disclosing prescriptions worth thousand gold dregs of a decoction slurrying includes Microwave Pretreatment, ethanol pulping, extracts the techniques such as effective component and paper modification.The present invention prepares face tissue with prescriptions worth thousand gold dregs of a decoction raw material, increase expanding treatment process in preparation process, the face tissue being prepared bulk with higher and flexibility, and the durability of fiber is more preferable, paper is still able to maintain preferable water absorbing properties in the case where not being embossed processing；The present invention uses twice sand removing process, while capable of guaranteeing pulp quality, moreover it is possible to guarantee facial tissue product softness, free from admixture；Also extract pharmacological property ingredient in initiative slave pulping and digesting liquid, and be applied to paper itself, the fiber product hygienic characteristic finally obtained is good and nonirritant.
Description
Technical field
The invention belongs to dregs of a decoction resource regeneration technical fields, and in particular, to a kind of prescriptions worth thousand gold dregs of a decoction resource regeneration
Utilize the face tissue and its method of preparation.
Background technique
Face tissue is a kind of paper for daily use, due to its have the characteristics that health, conveniently, it is at low cost, environmentally friendly gradually wide
General universal use, and it is more and more popular with consumers, face tissue can not only be used to wipe water stain, greasy dirt, can also rise
To the effect of cleaning household.Some researches show that, after washing one's hands respectively with face tissue, smear towel, drier hand, then detect
Bacterium residual on hand, the results showed that the bacterium residual of face tissue is minimum.Paper for daily use side, China has been filled up in the appearance of face tissue
One blank in face, currently, big or middle city, hotel, hotel, company and family are used widely face tissue at home.
As the improvement of people's living standards, requirement of the people to face tissue is also higher and higher.In order to improve face tissue
The chemistry such as cationic surfactant, bi ion active agent, silicon emulsion are usually added in flexibility, the prior art in process of production
Softening agent, although this method improves the pliability and bulk of face tissue to a certain extent, due to above-mentioned softening agent
It is chemicals, easily causes allergic reaction.
Chinese medicine slag is Chinese medicine residue remaining after water or organic solvent extraction, wherein containing there are many crude drugs
Ingredient.Currently, only part Chinese medicine slag is used for feed, fertilizer, gardens cultivation matrix, edible fungus culturing, remaining most of Chinese medicine
Slag is concentrated to stack, buries or burn, and not only processing cost is high, and exhaust gas is discharged after processing has pollution to air, and Chinese medicine dreg is dirty
Dye problem has become serious social concern.
Summary of the invention
The present invention provides a kind of prescriptions worth thousand gold dregs of a decoction resource regeneration preparation for the flexible insufficient problem of existing face tissue
The method of face tissue.The method be not only able to solve face tissue flexibility it is poor, easily cause anaphylactoid defect, moreover it is possible to fill
Point using pulping raw material pharmacological property ingredient, be made with antibacterial bacteriostatic function face tissue, be Chinese medicine slag reasonable resourceization again
It makes profits with offer thinking.
Another object of the present invention is to provide a kind of method systems that prescriptions worth thousand gold dregs of a decoction resource regeneration prepares face tissue
Standby face tissue.
The present invention is achieved by the following technical solutions:
A kind of method that prescriptions worth thousand gold dregs of a decoction resource regeneration prepares face tissue, comprising the following steps:
S1. it pre-processes: the prescriptions worth thousand gold dregs of a decoction that water content is 25%~45% is subjected to Micro-wave pretreatment, microwave power
For 900~1500W, microwave irradiation time is 5~10min, for use；
S2. boiling: the prescriptions worth thousand gold dregs of a decoction that step S1 is obtained are placed in boiling vessel, and the second that concentration is 40%~60% is added
After alcoholic solution, liquor ratio is 1:4~5, is rapidly heated to 120~140 DEG C, and blowing after 100~120min of insulation reaction is slightly starched
Material and cooking liquor；
S3. wash: the coarse particles that step S2 is obtained carry out first time desanding processing, are subsequently placed in displacement washing device,
Carries out multistage displacement washing with the ethanol solution that concentration is 55%~70%, cleaning solution ratio is 1:7~8, wash temperature for 40~
60℃；Then it is washed with water completely, obtains fibre semi-finished products after dry；
S4. extruding: the obtained fibre semi-finished products of step S3 are placed in bulking machine and carry out expanding treatment, obtain the extruding dregs of a decoction
Fiber；
S5. the extraction of effective component: concentration is evaporated to the cooking liquor in S2, obtains water after recycling of condensed steam ethyl alcohol
Solution is concentrated, and obtaining has effective component solution；
S6. papermaking: extruding dreg fibers made from step S4 are subjected to second of desanding processing, then manufactures paper with pulp, obtains
To body paper；
S7. the effective component spray solution in S4 is obtained into the face tissue with pharmacological property after dry in the body paper surface of S6.
Preferably, the prescriptions worth thousand gold dregs of a decoction are very heavy group, cherokee rose root, Caulis Spatholobi, single side needle, leatherleaf mahonia, Herba Andrographitis, Radix Angelicae Sinensis
With the dregs of a decoction of the Radix Codonopsis after water or ethyl alcohol extract；
The partial size of the prescriptions worth thousand gold dregs of a decoction is less than 3cm.
Preferably, the preparation method of the prescriptions worth thousand gold dregs of a decoction is prepared with reference to the method for following patent notes: (1)
ZL99115682.X, a kind of manufacture craft of ' Qianjin ' capsule to treat ganopathy；(2) a kind of manufacture of ' Qianjin ' capsule to treat ganopathy of ZL99115683.8
Method；(3) preparation method of ZL98112696.0 compound Chinese medicinal preparation FUKE QIANJIN PIAN.
Preferably, the water content of the prescriptions worth thousand gold dregs of a decoction is 30%~35% in step S1, and microwave power is 1000~1200W,
Microwave irradiation time is 7~8min.
Preferably, in step S2, after the ethanol solution that concentration is 53% is added, liquor ratio 1:4.5 is rapidly heated to 130
DEG C, blowing after insulation reaction 110min obtains coarse particles and cooking liquor.
Preferably, 3 sections of displacement washings are carried out with the ethanol solution that concentration is 60% in step S3, cleaning solution ratio for 1:7~
8, wash temperature is 50 DEG C.
Preferably, the first time desanding processing carries out in sand removing machine, sand in removal；
Second of desanding processing is that dreg fibers made from step S3 are removed spun yarn by gauze.
Preferably, in step S4, the swelling temperature is 110~120 DEG C, and puffing time is 15~20min.
Preferably, the temperature that cooking liquor is concentrated by evaporation in step S5 is 110~120 DEG C, described to have effective component solution
Middle concentration of alcohol is 20%~25%.
Preferably, fiber made from S4 being beaten in step S6, beating degree is 20~30 ° of SR, then manufactures paper with pulp,
Using starch as Cypres, body paper is obtained after dry.The present invention, as sizing agent, can improve paper using starch
Physical property also remains the health of paper, and chemicals bring is avoided to endanger.
Preferably, Cypres concentration is 8%~10%, and coating weight is 0.7~1g/m2。
Preferably, the water content of the body paper is 91%~93%.
Preferably, in step S7, by the effective component spray solution in S4 in the body paper surface of S5, effective component fountain height
It is the 20%~30% of original paper quality, obtains the face tissue with pharmacological property after dry at 60~65 DEG C.
A kind of face tissue for the method preparation preparing face tissue by above-mentioned prescriptions worth thousand gold dregs of a decoction resource regeneration.
Compared with prior art, the invention has the following advantages:
The present invention prepares face tissue by raw material of the prescriptions worth thousand gold dregs of a decoction, increases expanding treatment process in preparation process, is prepared into
The face tissue arrived bulk with higher and flexibility, and the durability of fiber is more preferable, paper be not embossed processing
In the case of be still able to maintain preferable water absorbing properties；The present invention uses twice sand removing process, while capable of guaranteeing pulp quality, also
It can guarantee facial tissue product softness, free from admixture；The present invention extracts effective component in cooking liquor in a creative way, and is applied to body paper
The paper on surface, acquisition has preferable anti-microbial property, avoids the allergic reaction because of caused by addition softening agent.
The method that prescriptions worth thousand gold dregs of a decoction resource regeneration provided by the invention prepares face tissue, simple process, ethyl alcohol can be with
It is recovered by distillation and recycles, to supplement ethyl alcohol for subsequent processing steps, whole preparation process is environmentally protective, has wide
Development prospect.
In conclusion using microwave irradiation technology in conjunction with Ethanol Method, it is residual using the fiber that the prescriptions worth thousand gold dregs of a decoction are prepared as raw material
Stay lignin content low, and pulp preparing process is simple, easy to operate, the time is short.Using the face tissue tool of the method for the present invention preparation
The features such as having pliability good and antibacterial bacteriostatic effect, pliability reach 170mN or more, to shigella dysenteriae, Escherichia coli, S. aureus L-forms,
Streptococcus and Amoeba play the role of effectively inhibiting to kill.
The present invention uses ethanol pulping, and using solvent identical with pharmacy procedure, pulping process does not introduce harmful
Product, it is ensured that the hygienic characteristic of fiber.
Extract pharmacological property ingredient in the also initiative slave pulping and digesting liquid of the present invention, and be applied to fiber itself, it is final to obtain
Fiber product have high functional characteristic and added value.
Specific embodiment
The present invention is further illustrated combined with specific embodiments below.Unless stated otherwise, it is used in the embodiment of the present invention
Raw material and method are the raw material of this field regular market purchase and conventional use of method, used equipment are that this field is routinely set
It is standby.
Embodiment 1
A kind of method that prescriptions worth thousand gold dregs of a decoction resource regeneration prepares face tissue, comprising the following steps:
S1. it pre-processes: the prescriptions worth thousand gold dregs of a decoction that water content is 25% being subjected to Micro-wave pretreatment, microwave power is
900W, microwave irradiation time 5min, for use；
S2. boiling: the prescriptions worth thousand gold dregs of a decoction that step S1 is obtained are placed in boiling vessel, and the ethanol solution that concentration is 40% is added
Afterwards, liquor ratio 1:4 is rapidly heated to 120 DEG C, and blowing after insulation reaction 100min obtains coarse particles and cooking liquor；
S3. it washs: the obtained coarse particles of step S2 being placed in progress first time desanding processing in sand removing machine, in removal after sand
It is placed in displacement washing device, carries out 3 sections of displacement washings with the ethanol solution that concentration is 55%, cleaning solution ratio is 1:7, wash temperature
It is 40 DEG C；Then it is washed with water completely, obtains fibre semi-finished products after dry；
S4. extruding: the obtained fibre semi-finished products of step S3 are placed in bulking machine and carry out expanding treatment, obtain the extruding dregs of a decoction
Fiber；
S5. the extraction of effective component: concentration is evaporated to the cooking liquor in S2, obtains water after recycling of condensed steam ethyl alcohol
Solution is concentrated, and obtaining has effective component solution；Cooking liquor be concentrated by evaporation temperature be 110 DEG C, it is described have drug effect at
Dividing concentration of alcohol in solution is 20%；
S6. papermaking: extruding dreg fibers made from S4 are removed into fine sand by gauze, are then beaten, beating degree is
20 ° of SR, then manufacture paper with pulp, and using starch as Cypres, obtain body paper after dry.The water content of body paper is 91%.
Cypres concentration is 8%, coating weight 0.7g/m2。
S7. by the effective component spray solution in S5 in the body paper surface of S6, effective component fountain height is original paper quality
20%, the face tissue with pharmacological property is obtained after dry at 65 DEG C.
The preparation method of the prescriptions worth thousand gold dregs of a decoction is referred to patent ZL99115682.X, a kind of production work of ' Qianjin ' capsule to treat ganopathy
Skill, the prescriptions worth thousand gold dregs of a decoction are very heavy group, cherokee rose root, Caulis Spatholobi, single side needle, leatherleaf mahonia, Herba Andrographitis, Radix Angelicae Sinensis and Radix Codonopsis pass through water or second
The dregs of a decoction after alcohol extracting.The partial size of the prescriptions worth thousand gold dregs of a decoction is less than 3cm.
Embodiment 2
A kind of method that prescriptions worth thousand gold dregs of a decoction resource regeneration prepares face tissue, comprising the following steps:
S1. it pre-processes: the prescriptions worth thousand gold dregs of a decoction that water content is 45% being subjected to Micro-wave pretreatment, microwave power is
1500W, microwave irradiation time 10min, for use；
S2. boiling: the prescriptions worth thousand gold dregs of a decoction that step S1 is obtained being placed in sand removing machine and carry out first time desanding processing, in removal
Sand is placed in boiling vessel, and after the ethanol solution that concentration is 60% is added, liquor ratio 1:5 is rapidly heated to 140 DEG C, and heat preservation is anti-
Blowing after 120min is answered, coarse particles and cooking liquor are obtained；
S3. wash: the obtained coarse particles of step S2 are placed in displacement washing device, with concentration be 70% ethanol solution into
3 sections of displacement washings of row, cleaning solution ratio are 1:8, and wash temperature is 60 DEG C；Then it is washed with water completely, fiber half is obtained after dry
Finished product；
S4. extruding: the obtained fibre semi-finished products of step S3 are placed in bulking machine and carry out expanding treatment, swelling temperature is
120 DEG C, puffing time 10min obtains extruding dreg fibers；
S5. the extraction of effective component: concentration is evaporated to the cooking liquor in S2, obtains water after recycling of condensed steam ethyl alcohol
Solution is concentrated, and obtaining has effective component solution；Cooking liquor be concentrated by evaporation temperature be 120 DEG C, it is described have drug effect at
Dividing concentration of alcohol in solution is 25%.
S6. papermaking: extruding dreg fibers made from S4 are removed into fine sand by gauze, are then beaten, beating degree is
30 ° of SR, then manufacture paper with pulp, and using starch as Cypres, obtain body paper after dry.The water content of body paper is 93%.
Cypres concentration is 10%, coating weight 1g/m2。
S7. by the effective component spray solution in S5 in the body paper surface of S6, effective component fountain height is original paper quality
30%, the face tissue with pharmacological property is obtained after dry at 60 DEG C.
The preparation method of the prescriptions worth thousand gold dregs of a decoction is referred to a kind of manufacturing method of ' Qianjin ' capsule to treat ganopathy of patent ZL99115683.8,
The prescriptions worth thousand gold dregs of a decoction are very heavy group, cherokee rose root, Caulis Spatholobi, single side needle, leatherleaf mahonia, Herba Andrographitis, Radix Angelicae Sinensis and Radix Codonopsis pass through water or ethyl alcohol
The dregs of a decoction after extraction.The partial size of the prescriptions worth thousand gold dregs of a decoction is less than 2cm.
Embodiment 3
A kind of method that prescriptions worth thousand gold dregs of a decoction resource regeneration prepares face tissue, comprising the following steps:
S1. it pre-processes: the prescriptions worth thousand gold dregs of a decoction that water content is 30% being subjected to Micro-wave pretreatment, microwave power is
1000W, microwave irradiation time 7min, for use；
S2. boiling: the prescriptions worth thousand gold dregs of a decoction that step S1 is obtained being placed in sand removing machine and carry out first time desanding processing, in removal
Sand is placed in boiling vessel, and after the ethanol solution that concentration is 53% is added, liquor ratio 1:4.5 is rapidly heated to 130 DEG C, heat preservation
Blowing after reaction 110min, obtains coarse particles and cooking liquor；
S3. wash: the obtained coarse particles of step S2 are placed in displacement washing device, with concentration be 60% ethanol solution into
3 sections of displacement washings of row, cleaning solution ratio are 1:7, and wash temperature is 50 DEG C；Then it is washed with water completely, fiber half is obtained after dry
Finished product；
S4. extruding: the obtained fibre semi-finished products of step S2 are placed in bulking machine and carry out expanding treatment, swelling temperature is
110 DEG C, puffing time 15min obtains extruding dreg fibers；
S5. the extraction of effective component: concentration is evaporated to the cooking liquor in S2, obtains water after recycling of condensed steam ethyl alcohol
Solution is concentrated, and obtaining has effective component solution；The temperature that cooking liquor is concentrated by evaporation in step S5 is 110 DEG C, the tool
Having concentration of alcohol in effective component solution is 20%；
S6. papermaking: extruding dreg fibers made from S4 are removed into fine sand by gauze, are then beaten, beating degree is
24 ° of SR, then manufacture paper with pulp, and using starch as Cypres, obtain body paper after dry.The water content of body paper is 92%.
Cypres concentration is 9%, coating weight 0.9g/m2。
S7. by the effective component spray solution in S5 in the body paper surface of S6, effective component fountain height is original paper quality
25%, the face tissue with pharmacological property is obtained after dry at 65 DEG C.
The preparation method of the prescriptions worth thousand gold dregs of a decoction refers to matching with patent ZL98112696.0 compound Chinese medicinal preparation FUKE QIANJIN PIAN
Method processed, the prescriptions worth thousand gold dregs of a decoction are very heavy group, cherokee rose root, Caulis Spatholobi, single side needle, leatherleaf mahonia, Herba Andrographitis, Radix Angelicae Sinensis and Radix Codonopsis pass through water
Or the dregs of a decoction after ethyl alcohol extraction.The partial size of the prescriptions worth thousand gold dregs of a decoction is less than 1cm.
Embodiment 4
A kind of method that prescriptions worth thousand gold dregs of a decoction resource regeneration prepares face tissue, comprising the following steps:
S1. it pre-processes: the prescriptions worth thousand gold dregs of a decoction that water content is 35% being subjected to Micro-wave pretreatment, microwave power is
1200W, microwave irradiation time 8min, for use；
S2. boiling: the prescriptions worth thousand gold dregs of a decoction that step S1 is obtained are placed in boiling vessel, and the ethanol solution that concentration is 53% is added
Afterwards, liquor ratio 1:4.5 is rapidly heated to 130 DEG C, and blowing after insulation reaction 110min obtains coarse particles and cooking liquor；
S3. it washs: the obtained coarse particles of step S2 being placed in progress first time desanding processing in sand removing machine, in removal after sand
It is placed in displacement washing device, carries out 3 sections of displacement washings with the ethanol solution that concentration is 60%, cleaning solution ratio is 1:7, wash temperature
It is 50 DEG C；Then it is washed with water completely, obtains fibre semi-finished products after dry；
S4. extruding: the obtained fibre semi-finished products of step S3 are placed in bulking machine and carry out expanding treatment, swelling temperature is
115 DEG C, puffing time 18min obtains extruding dreg fibers；
S5. the extraction of effective component: concentration is evaporated to the cooking liquor in S2, obtains water after recycling of condensed steam ethyl alcohol
Solution is concentrated, and obtaining has effective component solution；The temperature that cooking liquor is concentrated by evaporation in step S5 is 120 DEG C, the tool
Having concentration of alcohol in effective component solution is 25%.
S6. papermaking: extruding dreg fibers made from S4 are removed into fine sand by gauze, are then beaten, beating degree is
28 ° of SR, then manufacture paper with pulp, and using starch as Cypres, obtain body paper after dry.The water content of body paper is 92%.
Cypres concentration is 9%, coating weight 0.8g/m2；
S7. by the body paper surface of effective component spray solution and S6 in S5, effective component fountain height is original paper quality
25%, the face tissue with pharmacological property is obtained after dry at 60 DEG C.
The preparation method of the prescriptions worth thousand gold dregs of a decoction is referred to patent ZL99115682.X, a kind of production work of ' Qianjin ' capsule to treat ganopathy
Skill, the prescriptions worth thousand gold dregs of a decoction are very heavy group, cherokee rose root, Caulis Spatholobi, single side needle, leatherleaf mahonia, Herba Andrographitis, Radix Angelicae Sinensis and Radix Codonopsis pass through water or second
The dregs of a decoction after alcohol extracting.The partial size of the prescriptions worth thousand gold dregs of a decoction is less than 2cm.
Comparative example 1
A kind of method that prescriptions worth thousand gold dregs of a decoction resource regeneration prepares face tissue, comprising the following steps:
S1. boiling: the prescriptions worth thousand gold dregs of a decoction that water content is 35% are placed in boiling vessel, and it is molten that the ethyl alcohol that concentration is 53% is added
After liquid, liquor ratio 1:4.5 is rapidly heated to 130 DEG C, and blowing after insulation reaction 110min obtains coarse particles and cooking liquor；
S2. it washs: the obtained coarse particles of step S1 being placed in progress first time desanding processing in sand removing machine, in removal after sand
It is placed in displacement washing device, carries out 3 sections of displacement washings with the ethanol solution that concentration is 60%, cleaning solution ratio is 1:7, wash temperature
It is 50 DEG C；Then it is washed with water completely, obtains fibre semi-finished products after dry；
S3. extruding: the obtained fibre semi-finished products of step S2 are placed in bulking machine and carry out expanding treatment, swelling temperature is
115 DEG C, puffing time 18min obtains extruding dreg fibers；
S4. the extraction of effective component: concentration is evaporated to the cooking liquor in S1, obtains water after recycling of condensed steam ethyl alcohol
Solution is concentrated, and obtaining has effective component solution；The temperature that cooking liquor is concentrated by evaporation in step S5 is 120 DEG C, the tool
Having concentration of alcohol in effective component solution is 25%.
S5. papermaking: extruding dreg fibers made from S3 are removed into fine sand by gauze, are then beaten, beating degree is
28 ° of SR, then manufacture paper with pulp, and using starch as Cypres, obtain body paper after dry.The water content of body paper is 92%.
Cypres concentration is 9%, coating weight 0.8g/m2；
S6. by the body paper surface of effective component spray solution and S5 in S4, effective component fountain height is original paper quality
25%, the face tissue with pharmacological property is obtained after dry at 60 DEG C.
Comparative example 2
A kind of method that prescriptions worth thousand gold dregs of a decoction resource regeneration prepares face tissue, comprising the following steps:
S1. it pre-processes: the prescriptions worth thousand gold dregs of a decoction that water content is 35% being subjected to Micro-wave pretreatment, microwave power is
1200W, microwave irradiation time 8min, for use；
S2. boiling: the prescriptions worth thousand gold dregs of a decoction that step S1 is obtained are placed in boiling vessel, and the ethanol solution that concentration is 53% is added
Afterwards, liquor ratio 1:4.5 is rapidly heated to 130 DEG C, and blowing after insulation reaction 110min obtains coarse particles and cooking liquor；
S3. it washs: the obtained coarse particles of step S2 being placed in progress first time desanding processing in sand removing machine, in removal after sand
It is placed in displacement washing device, carries out 3 sections of displacement washings with the ethanol solution that concentration is 60%, cleaning solution ratio is 1:7, wash temperature
It is 50 DEG C；Then it is washed with water completely, obtains fibre semi-finished products after dry；
S4. the extraction of effective component: concentration is evaporated to the cooking liquor in S2, obtains water after recycling of condensed steam ethyl alcohol
Solution is concentrated, and obtaining has effective component solution；The temperature that cooking liquor is concentrated by evaporation in step S4 is 120 DEG C, the tool
Having concentration of alcohol in effective component solution is 25%.
S5. papermaking: fibre semi-finished products made from S3 are removed into fine sand by gauze, are then beaten, beating degree is 28 °
Then SR manufactures paper with pulp, using starch as Cypres, obtain body paper after dry.The water content of body paper is 92%.Surface
Sizing agent concentrations are 9%, coating weight 0.8g/m2；
S6. by the body paper surface of effective component spray solution and S5 in S4, effective component fountain height is original paper quality
25%, the face tissue with pharmacological property is obtained after dry at 60 DEG C.
Comparative example 3
A kind of method that prescriptions worth thousand gold dregs of a decoction resource regeneration prepares face tissue, comprising the following steps:
S1. it pre-processes: the prescriptions worth thousand gold dregs of a decoction that water content is 35% being subjected to Micro-wave pretreatment, microwave power is
1200W, microwave irradiation time 8min, for use；
S2. boiling: the prescriptions worth thousand gold dregs of a decoction that step S1 is obtained are placed in boiling vessel, and the ethanol solution that concentration is 53% is added
Afterwards, liquor ratio 1:4.5 is rapidly heated to 130 DEG C, and blowing after insulation reaction 110min obtains coarse particles and cooking liquor；
S3. wash: the obtained coarse particles of step S2 are placed in displacement washing device, with concentration be 60% ethanol solution into
3 sections of displacement washings of row, cleaning solution ratio are 1:7, and wash temperature is 50 DEG C；Then it is washed with water completely, fiber half is obtained after dry
Finished product；
S4. extruding: the obtained fibre semi-finished products of step S3 are placed in bulking machine and carry out expanding treatment, swelling temperature is
115 DEG C, puffing time 18min obtains extruding dreg fibers；
S5. the extraction of effective component: concentration is evaporated to the cooking liquor in S2, obtains water after recycling of condensed steam ethyl alcohol
Solution is concentrated, and obtaining has effective component solution；The temperature that cooking liquor is concentrated by evaporation in step S5 is 120 DEG C, the tool
Having concentration of alcohol in effective component solution is 25%.
S6. papermaking: extruding dreg fibers made from S4 are beaten, and beating degree is 28 ° of SR, are then manufactured paper with pulp, are adopted
It uses starch as Cypres, obtains body paper after dry.The water content of body paper is 92%.Cypres concentration is 9%, is applied
Cloth amount is 0.8g/m2；
S7. by the body paper surface of effective component spray solution and S6 in S5, effective component fountain height is original paper quality
25%, the face tissue with pharmacological property is obtained after dry at 60 DEG C.
Comparative example 4
A kind of method that prescriptions worth thousand gold dregs of a decoction resource regeneration prepares face tissue, comprising the following steps:
S1. it pre-processes: the prescriptions worth thousand gold dregs of a decoction that water content is 35% being subjected to Micro-wave pretreatment, microwave power is
1200W, microwave irradiation time 8min, for use；
S2. boiling: the prescriptions worth thousand gold dregs of a decoction that step S1 is obtained are placed in boiling vessel, and the ethanol solution that concentration is 53% is added
Afterwards, liquor ratio 1:4.5 is rapidly heated to 130 DEG C, and blowing after insulation reaction 110min obtains coarse particles and cooking liquor；
S3. it washs: the obtained coarse particles of step S2 being placed in progress first time desanding processing in sand removing machine, in removal after sand
It is placed in displacement washing device, carries out 3 sections of displacement washings with the ethanol solution that concentration is 60%, cleaning solution ratio is 1:7, wash temperature
It is 50 DEG C；Then it is washed with water completely, obtains fibre semi-finished products after dry；
S4. papermaking: extruding dreg fibers made from S3 are removed into fine sand by gauze, are then beaten, beating degree is
28 ° of SR, then manufacture paper with pulp, and using starch as Cypres, obtain body paper after dry.The water content of body paper is 92%.
Cypres concentration is 9%, coating weight 0.8g/m2。
Comparative example 5~8
The process conditions of comparative example 5~8 are similar to Example 4, the difference is that following technique is respectively adopted in step S1
Condition:
| Prescriptions worth thousand gold dregs of a decoction water content, % | Microwave power, w | Microwave time, min | |
| Comparative example 5 | 24 | 850 | 10 |
| Comparative example 6 | 24 | 1000 | 7 |
| Comparative example 7 | 46 | 1550 | 5 |
| Comparative example 8 | 30 | 850 | 10 |
Comparative example 9~11
The process conditions of comparative example 9~11 are similar to Example 4, the difference is that following technique is respectively adopted in step S4
Condition:
| Swelling temperature, DEG C | Puffing time, min | |
| Comparative example 9 | 90 | 18 |
| Comparative example 10 | 115 | 8 |
| Comparative example 11 | 125 | 10 |
Comparative example 12~14
The process conditions of comparative example 12~14 are similar to Example 4, the difference is that following work is respectively adopted in step S5
Skill condition:
| The temperature of concentration, DEG C | Concentration of alcohol, % | |
| Comparative example 12 | 105 | 20 |
| Comparative example 13 | 125 | 25 |
| Comparative example 14 | 110 | 18 |
Kappa number measurement is carried out to the fiber that the preparation method of Examples 1 to 4 and comparative example 1~14 obtains, wherein Kappa
Value is measured according to standard GB/T/T1546-2004；And the pliability to face tissue, paper strength, Pharmaceutical Compositions content
(being reference with the content of the Berberine hydrochloride in fiber) is measured, wherein pliability is according to standard GB/T/T8942-
1988 are measured, and paper strength is according to national standard
GB/T20808-2006 is measured, and former to shigella dysenteriae, Escherichia coli, S. aureus L-forms, streptococcus and amoeba
The bacteriums such as worm property killed is detected.It the results are shown in Table 1.
Table 1
It is found that the present invention is using the dregs of a decoction as plant material, using microwave irradiation to prescriptions worth thousand gold compared with comparative example 1 and 4~6
The dregs of a decoction are pre-processed, and the lignin components being very beneficial in the dregs of a decoction are separated, and plant cell wall tissue is made to generate micropore knot
Structure is more advantageous to the chemical reaction of subsequent delignification, is prepared using bioanalysis dregs of a decoction pulping process provided by the invention
Paper pulp, residual lignin content is low, and Kappa number is 10% or less.
It is found that the present invention prepares face tissue, preparation process by raw material of the prescriptions worth thousand gold dregs of a decoction compared with comparative example 2 and 9~11
Middle increase expanding treatment process, the face tissue being prepared bulk with higher and flexibility, and the durability of fiber is more
Good, paper is still able to maintain preferable water suction, oil absorbency in the case where not being embossed processing.It is prepared using the method for the present invention
Face tissue have the characteristics that pliability is good and antibacterial bacteriostatic effect, pliability is up to 160mN hereinafter, reaching tissue Grade A
National standard.
It is found that the present invention uses twice sand removing process, while capable of guaranteeing pulp quality compared with comparative example 3, moreover it is possible to
Guarantee facial tissue product softness, free from admixture.
It is found that extracting effective component in the slave cooking liquor of present invention initiative compared with comparative example 4, and it is applied to fiber
On, effectively raise medical value.
It is found that extracting influence of the technique of effective component to effective component in cooking liquor very compared with comparative example 12~14
Greatly, especially influence of the temperature to the viscosity of cooking liquor etc., so that the volatility of effective component is changed.
Dirt count detection
Dirt count measurement is carried out to the paper surface layer that the preparation method of Examples 1 to 4 obtains, dirt count is marked according to country
Quasi- GB/T1541 is measured.It the results are shown in Table 2.
Table 2
Testing result shows that the face tissue paper knot prepared using the method for the present invention is net, without apparent deadfold, incompleteness, hard
The impurity such as mass, raw pulp group.
Skin irritation test
By taking the tender sensitive skin paper of children prepared by the method for Examples 1 to 4 as an example, the tender sensitive skin paper of observation children is to skin
The irritation and allergic reaction of skin provide reference to evaluate its safety.
(1) skin irritation test is carried out using rabbit, divides intact skin group and damage skin group, for 24 hours by rabbit before test
Back backbone diamond wool shaves off, and after being kept in contact 1d, continuous 7d with the tender sensitive skin paper of children and rabbit skin and mucosa respectively, sees
Examining skin, whether there is or not the stimulate the reactions such as erythema, oedema.
(2) skin allergy experiment is carried out using cavy, is kept with the tender sensitive skin paper of children and guinea pig skin mucous membrane weekly
Contact 2 times contacts 4h or more every time, and continuous 3 weeks, whether there is or not the allergic reactions such as erythema, oedema for observation skin.
Experimental result:
The intact skin and damaged skin of rabbit, remove after being intended for single use or be used for multiple times for 24 hours, respectively at 1,24,48,
72h observation, is showed no erythema and oedema, and stimulate the reaction mean scores are < 0.5, nonirritant.
In guinea pig skin allergic experiment, does not occur the cutaneous anaphylaxises such as the obvious erythema of skin, oedema and other are systemic
Allergic reaction.
Clinical trial and result
1, using Examples 1 to 4 preparation face tissue as experimental material, collected pachylosis, pore are coarse, have acne print,
Scar print or volunteer 120 of pigment, wherein male 58, women 62, the age was at 25~40 years old.According to age level in batches after
Four groups are divided at random, respectively the face tissue of Examples 1 to 4 preparation on probation, experimental period 2 months.Trier is conventional clean every night
Behind face, the face tissue that respectively prepared by application Examples 1 to 4,15~20 minutes.
2, result counts
Details photo is clapped as record, as the control after experiment to each angle of face of every trier before experiment.Together
When experiment after ask trier to provide effect assessment, to take statistics.
The results show that test population, which does not occur pore, increases situation, there is 62 skin to belong to sensitivity in test population
Flesh, often because skin care item improper use generates the condition susceptible of erythema, small pox.And in the experimentation, never there is allergy
Symptom, and red blood trace on face phenomenon is obviously improved.
Detailed process equipment and processing step of the invention that the present invention is explained by the above embodiments, those skilled in the art
Member is not it should be appreciated that the present invention is limited by above-described embodiment, and the above embodiments and description only describe the present invention
Principle, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, this is to this field
It is it will be apparent that these changes and improvements all fall within the protetion scope of the claimed invention for technical staff.
Claims (10)
1. a kind of method that prescriptions worth thousand gold dregs of a decoction resource regeneration prepares face tissue, which comprises the following steps:
S1. pre-process: by water content be 25% ~ 45% the prescriptions worth thousand gold dregs of a decoction carry out Micro-wave pretreatment, microwave power be 900 ~
1500W, microwave irradiation time are 5 ~ 10 min, for use；
S2. boiling: the prescriptions worth thousand gold dregs of a decoction that step S1 is obtained are placed in boiling vessel, and the ethanol solution that concentration is 40% ~ 60% is added
Afterwards, liquor ratio is 1:4 ~ 5, is rapidly heated to 120 ~ 140 DEG C, and blowing after 100 ~ 120 min of insulation reaction obtains coarse particles and boiling
Liquid；
S3. wash: the coarse particles that step S2 is obtained carry out first time desanding processing, are subsequently placed in displacement washing device, use is dense
Degree carries out multistage displacement washing for 55% ~ 70% ethanol solution, and cleaning solution ratio is 1:7 ~ 8, and wash temperature is 40 ~ 60 DEG C；Then
It is washed with water completely, obtains fibre semi-finished products after dry；
S4. extruding: the obtained fibre semi-finished products of step S3 being placed in bulking machine and carry out expanding treatment, and it is fine to obtain the extruding dregs of a decoction
Dimension；
S5. the extraction of effective component: concentration is evaporated to the cooking liquor in S2, obtains aqueous solution after recycling of condensed steam ethyl alcohol
It is concentrated, obtaining has effective component solution；
S6. papermaking: extruding dreg fibers made from step S4 are subjected to second of desanding processing, then manufactures paper with pulp, obtains original
Paper；
S7. the effective component spray solution in S4 is obtained into the face tissue with pharmacological property after dry in the body paper surface of S6.
2. the method that prescriptions worth thousand gold dregs of a decoction resource regeneration prepares face tissue according to claim 1, which is characterized in that described
The prescriptions worth thousand gold dregs of a decoction are very heavy group, cherokee rose root, Caulis Spatholobi, single side needle, leatherleaf mahonia, Herba Andrographitis, Radix Angelicae Sinensis and Radix Codonopsis pass through water or ethyl alcohol
The dregs of a decoction after extraction；
The partial size of the prescriptions worth thousand gold dregs of a decoction is less than 3cm.
3. the method that prescriptions worth thousand gold dregs of a decoction resource regeneration prepares face tissue according to claim 1, which is characterized in that step
In rapid S2, after the ethanol solution that concentration is 53% is added, liquor ratio 1:4.5 is rapidly heated to 130 DEG C, 110 min of insulation reaction
Blowing afterwards obtains coarse particles and cooking liquor.
4. the method that prescriptions worth thousand gold dregs of a decoction resource regeneration prepares face tissue according to claim 1, which is characterized in that step
3 sections of displacement washings are carried out with the ethanol solution that concentration is 60% in S3, cleaning solution ratio is 1:7 ~ 8, and wash temperature is 50 DEG C.
5. the method that prescriptions worth thousand gold dregs of a decoction resource regeneration prepares face tissue according to claim 1, which is characterized in that described
First time desanding processing carries out in sand removing machine, sand in removal；
Second of desanding processing is that dreg fibers made from step S3 are removed spun yarn by gauze.
6. the method that prescriptions worth thousand gold dregs of a decoction resource regeneration prepares face tissue according to claim 1, which is characterized in that step
In rapid S4, the swelling temperature is 100 ~ 120 DEG C, and puffing time is 10 ~ 20 min.
7. the method that prescriptions worth thousand gold dregs of a decoction resource regeneration prepares face tissue according to claim 1, which is characterized in that step
In S5 cooking liquor be concentrated by evaporation temperature be 110 ~ 120 DEG C, it is described have effective component solution in concentration of alcohol be 20% ~ 25%.
8. the method that prescriptions worth thousand gold dregs of a decoction resource regeneration prepares face tissue according to claim 1, which is characterized in that step
Fiber made from S4 is beaten in S6, beating degree is 20 ~ 30oThen SR manufactures paper with pulp, using starch as top sizing
Agent obtains body paper after dry.
9. the method that prescriptions worth thousand gold dregs of a decoction resource regeneration prepares face tissue according to claim 1, which is characterized in that step
In S7, by the effective component spray solution in S4 in the body paper surface of S5, effective component fountain height be original paper quality 20% ~
30%, the face tissue with pharmacological property is obtained after dry at 60 ~ 65 DEG C.
10. a kind of face-cloth for the method preparation for preparing face tissue by prescriptions worth thousand gold dregs of a decoction resource regeneration described in claim 1 ~ 9
Paper.
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Citations (5)
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|---|---|---|---|---|
| CN1099827A (en) * | 1994-07-01 | 1995-03-08 | 黄庆文 | Toilet paper with traditional Chinese medicine and making method |
| CN1251763A (en) * | 1998-10-21 | 2000-05-03 | 株洲千金药业股份公司 | Process for preparing Chinese medicine 'Qianjin tablets' for treating gynopathy |
| CN1281074A (en) * | 1999-07-19 | 2001-01-24 | 西北轻工业学院 | Diwei self-catalyzing alcohol process for pulping |
| CN1924187A (en) * | 2006-09-28 | 2007-03-07 | 汤兴然 | Paper making method for straw fiber pulping by 'enzymatic conversion and puffing' |
| CN105484083A (en) * | 2015-11-22 | 2016-04-13 | 北京化工大学 | Green separating process for components of lignocellulose |
-
2017
- 2017-12-12 CN CN201711324453.XA patent/CN109914144A/en not_active Withdrawn
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1099827A (en) * | 1994-07-01 | 1995-03-08 | 黄庆文 | Toilet paper with traditional Chinese medicine and making method |
| CN1251763A (en) * | 1998-10-21 | 2000-05-03 | 株洲千金药业股份公司 | Process for preparing Chinese medicine 'Qianjin tablets' for treating gynopathy |
| CN1281074A (en) * | 1999-07-19 | 2001-01-24 | 西北轻工业学院 | Diwei self-catalyzing alcohol process for pulping |
| CN1924187A (en) * | 2006-09-28 | 2007-03-07 | 汤兴然 | Paper making method for straw fiber pulping by 'enzymatic conversion and puffing' |
| CN105484083A (en) * | 2015-11-22 | 2016-04-13 | 北京化工大学 | Green separating process for components of lignocellulose |
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