CN109914154A - A kind of face tissue and its method of the preparation of dreg fibers material - Google Patents
A kind of face tissue and its method of the preparation of dreg fibers material Download PDFInfo
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- CN109914154A CN109914154A CN201711324454.4A CN201711324454A CN109914154A CN 109914154 A CN109914154 A CN 109914154A CN 201711324454 A CN201711324454 A CN 201711324454A CN 109914154 A CN109914154 A CN 109914154A
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- face tissue
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Abstract
The present invention relates to the face tissue and its method of a kind of preparation of dreg fibers material, the technique for disclosing prescriptions worth thousand gold dregs of a decoction papermaking includes bioanalysis slurrying, extruding, extracts the techniques such as effective component, papermaking and paper modification.The present invention prepares face tissue with prescriptions worth thousand gold dregs of a decoction raw material, increase expanding treatment process in preparation process, the face tissue being prepared bulk with higher and flexibility, and the durability of fiber is more preferable, paper is still able to maintain preferable water suction, oil absorbency in the case where not being embossed processing；The present invention uses twice sand removing process, while capable of guaranteeing pulp quality, moreover it is possible to guarantee facial tissue product softness, free from admixture；The also initiative extraction pharmacological property ingredient from slurrying filtrate, and be applied to fiber itself, the fiber product hygienic characteristic finally obtained is good and nonirritant.
Description
Technical field
The invention belongs to pulp and paper technology fields, and in particular, to a kind of face tissue of dreg fibers material preparation and
Its method.
Background technique
Face tissue is a kind of paper for daily use, due to its have the characteristics that health, conveniently, it is at low cost, environmentally friendly gradually wide
General universal use, and it is more and more popular with consumers, face tissue can not only be used to wipe water stain, greasy dirt, can also rise
To the effect of cleaning household.Some researches show that, after washing one's hands respectively with face tissue, smear towel, drier hand, then detect
Bacterium residual on hand, the results showed that the bacterium residual of face tissue is minimum.Paper for daily use side, China has been filled up in the appearance of face tissue
One blank in face, currently, big or middle city, hotel, hotel, company and family are used widely face tissue at home.
As the improvement of people's living standards, requirement of the people to face tissue is also higher and higher.In order to improve face tissue
The chemistry such as cationic surfactant, bi ion active agent, silicon emulsion are usually added in flexibility, the prior art in process of production
Softening agent, although this method improves the pliability and bulk of face tissue to a certain extent, due to above-mentioned softening agent
It is chemicals, easily causes allergic reaction.
Chinese medicine slag is the Chinese medicine dregs of a decoction remaining after water or organic solvent extraction, wherein containing there are many crude drugs
Ingredient.Currently, only part Chinese medicine slag is used for feed, fertilizer, gardens cultivation matrix, edible fungus culturing, remaining most of Chinese medicine
Slag is concentrated to stack, buries or burn, and not only processing cost is high, and exhaust gas is discharged after processing has pollution to air, and Chinese medicine dreg is dirty
Dye problem has become serious social concern.
Summary of the invention
The present invention provides a kind of prescriptions worth thousand gold dregs of a decoction resource regeneration preparation for the flexible insufficient problem of existing face tissue
The method of face tissue.The method be not only able to solve face tissue flexibility it is poor, easily cause anaphylactoid defect, moreover it is possible to fill
Point using pulping raw material pharmacological property ingredient, be made with antibacterial bacteriostatic function face tissue, be Chinese medicine slag reasonable resourceization again
It makes profits with offer thinking.
Another object of the present invention is to provide the face tissues that a kind of dreg fibers material prepares the method preparation of face tissue.
The present invention is achieved by the following technical solutions:
A kind of method that dreg fibers material prepares face tissue, comprising the following steps:
S1. it pre-processes: the prescriptions worth thousand gold dregs of a decoction that water content is 25%~45% is subjected to Micro-wave pretreatment, microwave power
For 400~700W, the microwave time is 20~40min, for use；
S2. ferment: the prescriptions worth thousand gold dregs of a decoction deionized water that step S1 is obtained is impregnated and washing, in washing water is
Property, it is dehydrated, dispersed, then placed it in fermentation vat, biological complex enzyme is added, after mixing evenly, under aerobic conditions,
Fermentation process is carried out to prescriptions worth thousand gold dregs of a decoction material, is filtered after fermentation, obtains filtrate and filtrate；
S3. it washs: the filtrate in step S2 is subjected to first time desanding processing, then impregnated, divided repeatedly with water
It dissipates and washs, until dehydration seals after washing water is neutral, obtain fibre semi-finished products after dry；
S4. extruding: the obtained fibre semi-finished products of step S3 are placed in bulking machine and carry out expanding treatment, obtain the extruding dregs of a decoction
Fiber；
S5. the extraction of effective component: concentration is evaporated to the filtrate in step S2, obtaining has effective component solution；
S6. papermaking: extruding dreg fibers made from step S4 are subjected to second of desanding processing, then manufactures paper with pulp, obtains
To body paper；
S7. the effective component spray solution in S5 is obtained into the face tissue with pharmacological property after dry in the body paper surface of S6.
Preferably, the prescriptions worth thousand gold dregs of a decoction are very heavy group, cherokee rose root, Caulis Spatholobi, single side needle, leatherleaf mahonia, Herba Andrographitis, Radix Angelicae Sinensis
With Radix Codonopsis after water or ethyl alcohol extract the remaining dregs of a decoction；
The partial size of the prescriptions worth thousand gold dregs of a decoction is less than 3cm.
Preferably, the preparation method of the prescriptions worth thousand gold dregs of a decoction is prepared with reference to the method for following patent notes: (1)
ZL99115682.X, a kind of manufacture craft of ' Qianjin ' capsule to treat ganopathy；(2) a kind of manufacture of ' Qianjin ' capsule to treat ganopathy of ZL99115683.8
Method；(3) preparation method of ZL98112696.0 compound Chinese medicinal preparation FUKE QIANJIN PIAN.
Preferably, the water content of the prescriptions worth thousand gold dregs of a decoction is 30%~35% in step S1, and the power of the microwave radiation is 600
~700W, time are 20~30min.
Preferably, biological complex enzyme described in step S2 is prepared by the raw material of following weight percent: whiterot fungi 6~
12%, Ficus virens 12~20%, zytase 24~30% and laccase 10~20%.
Preferably, in step S2, the biological complex enzyme additional amount is 2~4 kg/ton of material.
Preferably, fermentation process temperature described in step S2 is 55~65 DEG C, and the time is 3~4h.
Preferably, the first time desanding processing carries out in sand removing machine, sand in removal；
Second of desanding processing is that dreg fibers made from step S3 are removed spun yarn by gauze.
Preferably, in step S4, the swelling temperature is 100~120 DEG C, and puffing time is 10~20min.
Preferably, the temperature that filtrate is concentrated by evaporation in step S5 is 100~110 DEG C, time of evaporation and concentration is 30~
40min。
Preferably, fiber made from S4 being beaten in step S6, beating degree is 20~30 ° of SR, then manufactures paper with pulp,
Using starch as Cypres, body paper is obtained after dry.The present invention, as sizing agent, can improve paper using starch
Physical property also remains the health of paper, and chemicals bring is avoided to endanger.
Preferably, the water content of the body paper is 91%~93%.
Preferably, in step S7, by the effective component spray solution in S5 in the body paper surface of S6, effective component fountain height
It is the 20%~30% of original paper quality, obtains the face tissue with pharmacological property after dry at 60~65 DEG C.
A kind of face tissue prepared by the method that above-mentioned dreg fibers material prepares face tissue.
Compared with prior art, the method that dreg fibers material provided by the invention prepares face tissue has the advantage that
The present invention carries out bioanalysis slurrying by raw material of the prescriptions worth thousand gold dregs of a decoction for the first time, exists simultaneously draft according to the prescriptions worth thousand gold dregs of a decoction
Plant and shrub raw material this characteristic, the biology using whiterot fungi, Ficus virens, zytase and laccase composition are multiple
Synthase, the effect coordinated using reasonable compatibility between each strain and enzyme, jointly, a variety of lignins is same in the effectively degradation dregs of a decoction
When, additionally it is possible to the chromophoric group in paper pulp is removed, the whiteness of face tissue is effectively promoted.
The present invention prepares face tissue by raw material of the prescriptions worth thousand gold dregs of a decoction, increases expanding treatment process in preparation process, is prepared into
The face tissue arrived bulk with higher and flexibility, and the durability of fiber is more preferable, paper be not embossed processing
In the case of be still able to maintain preferable water absorbing properties；The present invention uses twice sand removing process, while capable of guaranteeing pulp quality, also
It can guarantee facial tissue product softness, free from admixture；The present invention extracts effective component in filtrate in a creative way, and is applied to base paper sheet
The paper in face, acquisition has preferable anti-microbial property, avoids the allergic reaction because of caused by addition softening agent.
The method provided by the invention for preparing face tissue using prescriptions worth thousand gold dregs of a decoction resource regeneration, simple process, ethyl alcohol
It can be recovered by distillation and recycle, to supplement ethyl alcohol for subsequent processing steps, whole preparation process is environmentally protective, has
Broad based growth prospect.
The method that dreg fibers material provided by the invention prepares face tissue, pulp preparing process is simple, is not only reacting
Any harmful substance will not be generated to environment in the process, easy to operate, the time is short.
In conclusion the present invention solves the problems, such as that existing microwave irradiation technology pulping process is complicated；And focus on solving life
The object legal system slurry situation that treatment effeciency is low, effect is poor has pliability good and antibacterial using the face tissue of the method for the present invention preparation
The features such as fungistatic effect, pliability is in 160mN hereinafter, to shigella dysenteriae, Escherichia coli, S. aureus L-forms, streptococcus and amoeba
Protozoon plays the role of effectively inhibiting to kill.
The present invention uses bioanalysis slurrying, and pulping process does not introduce harmful chemicals, it is ensured that the hygienic characteristic of fiber.
The also initiative extraction pharmacological property ingredient from slurrying filtrate of the present invention, and be applied to fiber itself, finally obtain
Fiber product has high functional characteristic and added value.
Specific embodiment
The present invention is further illustrated combined with specific embodiments below.Unless stated otherwise, it is used in the embodiment of the present invention
Raw material and method are the raw material of this field regular market purchase and conventional use of method, used equipment are that this field is routinely set
It is standby.
Embodiment 1
The present embodiment provides a kind of methods that dreg fibers material prepares face tissue, specific steps are as follows:
S1. it pre-processes: the prescriptions worth thousand gold dregs of a decoction that water content is 25% being subjected to Micro-wave pretreatment, microwave power is
400W, microwave time are 40min, for use；
S2. ferment: the prescriptions worth thousand gold dregs of a decoction deionized water that step S1 is obtained is impregnated and washing, in washing water is
Property, it is dehydrated, dispersed, then placed it in fermentation vat, 2 kg/ton of biological complex enzyme material are added, after mixing evenly,
Under aerobic conditions, fermentation process is carried out to prescriptions worth thousand gold dregs of a decoction material, fermentation process temperature is 55 DEG C, time 4h, fermentation ends
After be filtered, obtain filtrate and filtrate；
S3. it washs: the filtrate in step S2 being placed in progress first time desanding processing in sand removing machine, is used after sand in removal
Water is impregnated repeatedly, dispersed and is washed, until after washing water is neutral, dehydration, sealing obtain fibre semi-finished products after dry；
S4. extruding: the obtained fibre semi-finished products of step S3 are placed in bulking machine and carry out expanding treatment, swelling temperature is
100 DEG C, puffing time 20min obtains extruding dreg fibers；
S5. the extraction of effective component: being evaporated concentration to the filtrate in step S2, and evaporating temperature is 100 DEG C, is evaporated dense
The time of contracting is 30min, and obtaining has effective component solution；
S6. papermaking: extruding dreg fibers made from S4 are removed into fine sand by gauze, are then beaten, beating degree is
30 ° of SR, then manufacture paper with pulp, and using starch as Cypres, obtain body paper after dry.The water content of body paper is 93%.
Cypres concentration is 10%, coating weight 1g/m2。
S7. by the effective component spray solution in S5 in the body paper surface of S6, effective component fountain height is original paper quality
20%, the face tissue with pharmacological property is obtained after dry at 65 DEG C.
The preparation method of the prescriptions worth thousand gold dregs of a decoction is referred to patent ZL99115682.X, a kind of production work of ' Qianjin ' capsule to treat ganopathy
Skill, the prescriptions worth thousand gold dregs of a decoction are very heavy group, cherokee rose root, Caulis Spatholobi, single side needle, leatherleaf mahonia, Herba Andrographitis, Radix Angelicae Sinensis and Radix Codonopsis pass through water or second
Dregs of a decoction mixing after alcohol extracting.The partial size of the prescriptions worth thousand gold dregs of a decoction is less than 3cm.
Wherein, biological complex enzyme is prepared by the raw material of following weight percent: whiterot fungi 6%, yellow archespore Mao Pingcao
Bacterium 20%, zytase 24% and laccase 20%.
Embodiment 2
The present embodiment provides a kind of methods that dreg fibers material prepares face tissue, specific steps are as follows:
S1. it pre-processes: the prescriptions worth thousand gold dregs of a decoction that water content is 45% being subjected to Micro-wave pretreatment, microwave power is
700W, microwave time are 20min, for use；
S2. ferment: the prescriptions worth thousand gold dregs of a decoction deionized water that step S1 is obtained is impregnated and washing, in washing water is
Property, it is dehydrated, dispersed, then placed it in fermentation vat, 4 kg/ton of biological complex enzyme material are added, after mixing evenly,
Under aerobic conditions, fermentation process temperature is 65 DEG C, and time 3h is filtered after fermentation, obtains filtrate and filtrate；
S3. it washs: the filtrate in step S2 being placed in progress first time desanding processing in sand removing machine, is used after sand in removal
Water is impregnated repeatedly, dispersed and is washed, until after washing water is neutral, dehydration, sealing obtain fibre semi-finished products after dry；
S4. extruding: the obtained fibre semi-finished products of step S3 are placed in bulking machine and carry out expanding treatment, swelling temperature is
120 DEG C, puffing time 10min obtains extruding dreg fibers；
S5. the extraction of effective component: being evaporated concentration to the filtrate in step S2, and evaporating temperature is 110 DEG C, is evaporated dense
The time of contracting is 30min, and obtaining has effective component solution；
S6. papermaking: extruding dreg fibers made from S4 are removed into fine sand by gauze, are then beaten, beating degree is
30 ° of SR, then manufacture paper with pulp, and using starch as Cypres, obtain body paper after dry.The water content of body paper is 91%.
Cypres concentration is 10%, coating weight 1g/m2。
S7. by the body paper surface of effective component spray solution and S6 in S5, effective component fountain height is original paper quality
30%, the face tissue with pharmacological property is obtained after dry at 60 DEG C.
The preparation method of the prescriptions worth thousand gold dregs of a decoction refers to matching with patent ZL98112696.0 compound Chinese medicinal preparation FUKE QIANJIN PIAN
Method processed, the prescriptions worth thousand gold dregs of a decoction are very heavy group, cherokee rose root, Caulis Spatholobi, single side needle, leatherleaf mahonia, Herba Andrographitis, Radix Angelicae Sinensis and Radix Codonopsis pass through water
Or the dregs of a decoction mixing after ethyl alcohol extraction.The partial size of the prescriptions worth thousand gold dregs of a decoction is less than 2cm.
Wherein, biological complex enzyme is prepared by the raw material of following weight percent: whiterot fungi 12%, yellow archespore Mao Pingcao
Bacterium 12%, zytase 30% and laccase 10%.
Embodiment 3
The present embodiment provides a kind of methods that dreg fibers material prepares face tissue, specific steps are as follows:
S1. it pre-processes: the prescriptions worth thousand gold dregs of a decoction that water content is 35% being subjected to Micro-wave pretreatment, microwave power is
600W, microwave time are 30min, for use；
S2. ferment: the prescriptions worth thousand gold dregs of a decoction deionized water that step S1 is obtained is impregnated and washing, in washing water is
Property, it is dehydrated, dispersed, then placed it in fermentation vat, 1 kg/ton of biological complex enzyme material is added, after mixing evenly,
Under aerobic conditions, fermentation process temperature is 58 DEG C, and time 3.5h is filtered after fermentation, obtains filtrate and filtrate；
S3. it washs: the filtrate in step S2 being placed in progress first time desanding processing in sand removing machine, is used after sand in removal
Water is impregnated repeatedly, dispersed and is washed, until after washing water is neutral, dehydration, sealing obtain fibre semi-finished products after dry；
S4. extruding: the obtained fibre semi-finished products of step S3 are placed in bulking machine and carry out expanding treatment, swelling temperature is
110 DEG C, puffing time 15min obtains extruding dreg fibers；
S5. the extraction of effective component: being evaporated concentration to the filtrate in step S2, and evaporating temperature is 105 DEG C, is evaporated dense
The time of contracting is 35min, and obtaining has effective component solution；
S6. papermaking: extruding dreg fibers made from S4 are removed into fine sand by gauze, are then beaten, beating degree is
24 ° of SR, then manufacture paper with pulp, and using starch as Cypres, obtain body paper after dry.The water content of body paper is 92%.
Cypres concentration is 9%, coating weight 0.9g/m2。
S7. by the effective component spray solution in S5 in the body paper surface of S6, effective component fountain height is original paper quality
25%, the face tissue with pharmacological property is obtained after dry at 60 DEG C.
The preparation method of the prescriptions worth thousand gold dregs of a decoction is referred to a kind of manufacturing method of ' Qianjin ' capsule to treat ganopathy of patent ZL99115683.8,
The prescriptions worth thousand gold dregs of a decoction are very heavy group, cherokee rose root, Caulis Spatholobi, single side needle, leatherleaf mahonia, Herba Andrographitis, Radix Angelicae Sinensis and Radix Codonopsis pass through water or ethyl alcohol
Dregs of a decoction mixing after extraction.The partial size of the prescriptions worth thousand gold dregs of a decoction is less than 1cm.
Biological complex enzyme is prepared by the raw material of following weight percent: whiterot fungi 8%, Ficus virens
18%, zytase 26% and laccase 18%.
Embodiment 4
The present embodiment provides a kind of methods that dreg fibers material prepares face tissue, specific steps are as follows:
S1. it pre-processes: the prescriptions worth thousand gold dregs of a decoction that water content is 35% being subjected to Micro-wave pretreatment, microwave power is
500W, microwave time are 35min, for use；
S2. ferment: the prescriptions worth thousand gold dregs of a decoction deionized water that step S1 is obtained is impregnated and washing, in washing water is
Property, it is dehydrated, dispersed, then placed it in fermentation vat, 2 kg/ton of biological complex enzyme material are added, after mixing evenly,
Under aerobic conditions, fermentation process temperature is 60 DEG C, and time 3h is filtered after fermentation, obtains filtrate and filtrate；
S3. it washs: the filtrate in step S2 being placed in progress first time desanding processing in sand removing machine, is used after sand in removal
Water is impregnated repeatedly, dispersed and is washed, until after washing water is neutral, dehydration, sealing obtain fibre semi-finished products after dry；
S4. extruding: the obtained fibre semi-finished products of step S3 are placed in bulking machine and carry out expanding treatment, swelling temperature is
115 DEG C, puffing time 18min obtains extruding dreg fibers；
S5. the extraction of effective component: being evaporated concentration to the filtrate in step S2, and evaporating temperature is 105 DEG C, is evaporated dense
The time of contracting is 38min, and obtaining has effective component solution；
S6. papermaking: extruding dreg fibers made from S4 are removed into fine sand by gauze, are then beaten, beating degree is
28 ° of SR, then manufacture paper with pulp, and using starch as Cypres, obtain body paper after dry.The water content of body paper is 92%.
Cypres concentration is 9%, coating weight 0.8g/m2；
S7. by the effective component spray solution in S5 in the body paper surface of S6, effective component fountain height is original paper quality
25%, the face tissue with pharmacological property is obtained after dry at 65 DEG C.
The preparation method of the prescriptions worth thousand gold dregs of a decoction is referred to a kind of manufacturing method of ' Qianjin ' capsule to treat ganopathy of patent ZL99115683.8,
The prescriptions worth thousand gold dregs of a decoction are very heavy group, cherokee rose root, Caulis Spatholobi, single side needle, leatherleaf mahonia, Herba Andrographitis, Radix Angelicae Sinensis and Radix Codonopsis pass through water or ethyl alcohol
Dregs of a decoction mixing after extraction.The partial size of the prescriptions worth thousand gold dregs of a decoction is less than 3cm.
Biological complex enzyme is prepared by the raw material of following weight percent: whiterot fungi 10%, Ficus virens
15%, zytase 24% and laccase 15%.
Comparative example 1
The present embodiment provides a kind of methods that dreg fibers material prepares face tissue, specific steps are as follows:
S1. it ferments: the prescriptions worth thousand gold dregs of a decoction deionized water that water content is 35% being impregnated and washed, in washing water is
Property, it is dehydrated, dispersed, then placed it in fermentation vat, 2 kg/ton of biological complex enzyme material are added, after mixing evenly,
Under aerobic conditions, fermentation process temperature is 60 DEG C, and time 3h is filtered after fermentation, obtains filtrate and filtrate；
S2. it washs: the filtrate in step S1 being placed in progress first time desanding processing in sand removing machine, is used after sand in removal
Water is impregnated repeatedly, dispersed and is washed, until after washing water is neutral, dehydration, sealing obtain fibre semi-finished products after dry；
S3. extruding: the obtained fibre semi-finished products of step S2 are placed in bulking machine and carry out expanding treatment, swelling temperature is
115 DEG C, puffing time 18min obtains extruding dreg fibers；
S4. the extraction of effective component: being evaporated concentration to the filtrate in step S1, and evaporating temperature is 105 DEG C, is evaporated dense
The time of contracting is 38min, and obtaining has effective component solution；
S5. papermaking: extruding dreg fibers made from S3 are removed into fine sand by gauze, are then beaten, beating degree is
28 ° of SR, then manufacture paper with pulp, and using starch as Cypres, obtain body paper after dry.The water content of body paper is 92%.
Cypres concentration is 9%, coating weight 0.8g/m2；
S6. by the effective component spray solution in S4 in the body paper surface of S5, effective component fountain height is original paper quality
25%, the face tissue with pharmacological property is obtained after dry at 65 DEG C.
Comparative example 2
The present embodiment provides a kind of methods that dreg fibers material prepares face tissue, specific steps are as follows:
S1. it pre-processes: the prescriptions worth thousand gold dregs of a decoction that water content is 35% being subjected to Micro-wave pretreatment, microwave power is
500W, microwave time are 35min, for use；
S2. ferment: the prescriptions worth thousand gold dregs of a decoction deionized water that step S1 is obtained is impregnated and washing, in washing water is
Property, it is dehydrated, dispersed, then placed it in fermentation vat, 2 kg/ton of biological complex enzyme material are added, after mixing evenly,
Under aerobic conditions, fermentation process temperature is 60 DEG C, and time 3h is filtered after fermentation, obtains filtrate and filtrate；
S3. it washs: the filtrate in step S2 being placed in progress first time desanding processing in sand removing machine, is used after sand in removal
Water is impregnated repeatedly, dispersed and is washed, until after washing water is neutral, dehydration, sealing obtain fibre semi-finished products after dry；
S4. the extraction of effective component: being evaporated concentration to the filtrate in step S2, and evaporating temperature is 105 DEG C, is evaporated dense
The time of contracting is 38min, and obtaining has effective component solution；
S5. papermaking: extruding dreg fibers made from S3 are removed into fine sand by gauze, are then beaten, beating degree is
28 ° of SR, then manufacture paper with pulp, and using starch as Cypres, obtain body paper after dry.The water content of body paper is 92%.
Cypres concentration is 9%, coating weight 0.8g/m2；
S6. by the effective component spray solution in S4 in the body paper surface of S5, effective component fountain height is original paper quality
25%, the face tissue with pharmacological property is obtained after dry at 65 DEG C.
Comparative example 3
The present embodiment provides a kind of methods that dreg fibers material prepares face tissue, specific steps are as follows:
S1. it pre-processes: the prescriptions worth thousand gold dregs of a decoction that water content is 35% being subjected to Micro-wave pretreatment, microwave power is
500W, microwave time are 35min, for use；
S2. ferment: the prescriptions worth thousand gold dregs of a decoction deionized water that step S1 is obtained is impregnated and washing, in washing water is
Property, it is dehydrated, dispersed, then placed it in fermentation vat, 2 kg/ton of biological complex enzyme material are added, after mixing evenly,
Under aerobic conditions, fermentation process temperature is 60 DEG C, and time 3h is filtered after fermentation, obtains filtrate and filtrate；
S3. it washs: the filtrate in step S2 being placed in progress first time desanding processing in sand removing machine, is used after sand in removal
Water is impregnated repeatedly, dispersed and is washed, until after washing water is neutral, dehydration, sealing obtain fibre semi-finished products after dry；
S4. extruding: the obtained fibre semi-finished products of step S3 are placed in bulking machine and carry out expanding treatment, swelling temperature is
115 DEG C, puffing time 18min obtains extruding dreg fibers；
S5. papermaking: extruding dreg fibers made from S4 are removed into fine sand by gauze, are then beaten, beating degree is
28 ° of SR, then manufacture paper with pulp, and using starch as Cypres, obtain body paper after dry.The water content of body paper is 92%.
Cypres concentration is 9%, coating weight 0.8g/m2；
Comparative example 4
The present embodiment provides a kind of methods that dreg fibers material prepares face tissue, specific steps are as follows:
S1. it pre-processes: the prescriptions worth thousand gold dregs of a decoction that water content is 35% being subjected to Micro-wave pretreatment, microwave power is
500W, microwave time are 35min, for use；
S2. ferment: the prescriptions worth thousand gold dregs of a decoction deionized water that step S1 is obtained is impregnated and washing, in washing water is
Property, it is dehydrated, dispersed, then placed it in fermentation vat, 2 kg/ton of biological complex enzyme material are added, after mixing evenly,
Under aerobic conditions, fermentation process temperature is 60 DEG C, and time 3h is filtered after fermentation, obtains filtrate and filtrate；
S3. it washs: the filtrate in step S2 is impregnated repeatedly, disperses and washed with water, in washing water is
Property after, dehydration, sealing obtain fibre semi-finished products after dry；
S4. extruding: the obtained fibre semi-finished products of step S3 are placed in bulking machine and carry out expanding treatment, swelling temperature is
115 DEG C, puffing time 18min obtains extruding dreg fibers；
S5. the extraction of effective component: being evaporated concentration to the filtrate in step S2, and evaporating temperature is 105 DEG C, is evaporated dense
The time of contracting is 38min, and obtaining has effective component solution；
S6. papermaking: extruding dreg fibers made from S4 are beaten, and beating degree is 28 ° of SR, are then manufactured paper with pulp, are adopted
It uses starch as Cypres, obtains body paper after dry.The water content of body paper is 92%.Cypres concentration is 9%, is applied
Cloth amount is 0.8g/m2；
S7. by the effective component spray solution in S5 in the body paper surface of S6, effective component fountain height is original paper quality
25%, the face tissue with pharmacological property is obtained after dry at 65 DEG C.
Comparative example 5~8
The process conditions of comparative example 5~8 are similar to Example 4, the difference is that following technique is respectively adopted in step S1
Condition:
| Prescriptions worth thousand gold dregs of a decoction water content, % | Microwave power, w | Microwave time, min | |
| Comparative example 5 | 24 | 350 | 40 |
| Comparative example 6 | 24 | 600 | 30 |
| Comparative example 7 | 46 | 850 | 20 |
| Comparative example 8 | 30 | 350 | 40 |
Comparative example 9~11
The process conditions of comparative example 9~11 are similar to Example 4, the difference is that following technique is respectively adopted in step S4
Condition:
Comparative example 12~14
The process conditions of comparative example 12~14 are similar to Example 4, the difference is that following work is respectively adopted in step S5
Skill condition:
The whiteness of the face tissue obtained to the preparation method of Examples 1 to 4 and comparative example 1~14, pliability, paper are strong
Degree, Pharmaceutical Compositions content (being reference with the content of the Berberine hydrochloride in fiber) are measured, wherein whiteness is marked according to country
Quasi- GB/T 8940.2-1988 is measured, and pliability is measured according to standard GB/T/T8942-1988, paper strength root
It is measured according to standard GB/T/T20808-2006, and to shigella dysenteriae, Escherichia coli, S. aureus L-forms, streptococcus and amoeba
The bacteriums such as protozoon property killed is detected.It the results are shown in Table 1.
Table 1
It is found that the present invention is using the dregs of a decoction as plant material compared with comparative example 1 and 5~8, directly made using microwave irradiation technology
Standby bleached pulp is not only able to a variety of lignins in the degradation dregs of a decoction in conjunction with the synergistic effect between strain each in biological complex enzyme and enzyme,
The chromophoric group in paper pulp can also be removed, bleaching efficiency is improved；The present invention solves existing in a creative way from the angle of environmental protection
Bioanalysis slurrying handles the low problem of whiteness, and whiteness can reach 80% or more.
It is found that the present invention prepares face tissue, preparation process by raw material of the prescriptions worth thousand gold dregs of a decoction compared with comparative example 2 and 9~11
Middle increase expanding treatment process, the face tissue being prepared bulk with higher and flexibility, and the durability of fiber is more
Good, paper is still able to maintain preferable water absorbing properties in the case where not being embossed processing.The face prepared using the method for the present invention
Towel paper has the characteristics that pliability is good and antibacterial bacteriostatic effect, and pliability is in 160mN or less.
It is found that the present invention uses twice sand removing process, while capable of guaranteeing pulp quality compared with to Billy 3, moreover it is possible to
Guarantee facial tissue product softness, free from admixture.
It is found that present invention initiative extracts effective component from filtrate compared with comparative example 4, and it is applied to fiber
On, effectively raise medical value.
It is found that influence of the technique to effective component for extracting effective component in filtrate is very big compared with comparative example 12~14,
Especially influence of the temperature to the viscosity of filtrate etc., so that the volatility of effective component is changed.
Dirt count detection
Dirt count measurement is carried out to the paper surface layer that the preparation method of Examples 1 to 4 obtains, dirt count is marked according to country
Quasi- GB/T1541 is measured.It the results are shown in Table 2.
Table 2
Testing result shows that the face tissue paper knot prepared using the method for the present invention is net, without apparent deadfold, incompleteness, hard
The impurity such as mass, raw pulp group.
Skin irritation test
By taking the tender sensitive skin paper of children prepared by the method for Examples 1 to 4 as an example, the tender sensitive skin paper of observation children is to skin
The irritation and allergic reaction of skin provide reference to evaluate its safety.
(1) skin irritation test is carried out using rabbit, divides intact skin group and damage skin group, for 24 hours by rabbit before test
Back backbone diamond wool shaves off, and after being kept in contact 1d, continuous 7d with the tender sensitive skin paper of children and rabbit skin and mucosa respectively, sees
Examining skin, whether there is or not the stimulate the reactions such as erythema, oedema.
(2) skin allergy experiment is carried out using cavy, is kept with the tender sensitive skin paper of children and guinea pig skin mucous membrane weekly
Contact 2 times contacts 4h or more every time, and continuous 3 weeks, whether there is or not the allergic reactions such as erythema, oedema for observation skin.
Experimental result:
The intact skin and damaged skin of rabbit, remove after being intended for single use or be used for multiple times for 24 hours, respectively at 1,24,48,
72h observation, is showed no erythema and oedema, and stimulate the reaction mean scores are < 0.5, nonirritant.
In guinea pig skin allergic experiment, does not occur the cutaneous anaphylaxises such as the obvious erythema of skin, oedema and other are systemic
Allergic reaction.
Clinical trial and result
1, using Examples 1 to 4 preparation face tissue as experimental material, collected pachylosis, pore are coarse, have acne print,
Scar print or volunteer 120 of pigment, wherein male 45, women 75, the age was at 25~40 years old.According to age level in batches after
Two groups are divided at random, respectively the face tissue of Examples 1 to 4 preparation on probation, experimental period 2 months.Trier is conventional clean every night
Behind face, the face tissue that respectively prepared by application Examples 1 to 4,15~20 minutes.
2, result counts
Details photo is clapped as record, as the control after experiment to each angle of face of every trier before experiment.Together
When experiment after ask trier to provide effect assessment, to take statistics.
The results show that test population, which does not occur pore, increases situation, there is 75 skin to belong to sensitivity in test population
Flesh, often because skin care item improper use generates erythema, small pox all condition susceptibles.And in the experimentation, never there is allergy
Symptom, and red blood trace on face phenomenon is obviously improved.
Detailed process equipment and processing step of the invention that the present invention is explained by the above embodiments, those skilled in the art
Member is not it should be appreciated that the present invention is limited by above-described embodiment, and the above embodiments and description only describe the present invention
Principle, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, this is to this field
It is it will be apparent that these changes and improvements all fall within the protetion scope of the claimed invention for technical staff.
Claims (10)
1. a kind of method that dreg fibers material prepares face tissue, which comprises the following steps:
S1. pre-process: by water content be 25% ~ 45% the prescriptions worth thousand gold dregs of a decoction carry out Micro-wave pretreatment, microwave power be 400 ~
700W, microwave time are 20 ~ 40 min, for use；
S2. ferment: the prescriptions worth thousand gold dregs of a decoction deionized water that step S1 is obtained is impregnated and washing, until washing water is neutrality, into
Row dehydration, dispersion, then place it in fermentation vat, biological complex enzyme are added, after mixing evenly, under aerobic conditions, to thousand
Golden recipe slag material carries out fermentation process, is filtered after fermentation, obtains filtrate and filtrate；
S3. wash: by step S2 filtrate carry out first time desanding processing, then impregnated repeatedly with water, disperse and
Washing, until after washing water is neutral, dehydration, sealing obtain fibre semi-finished products after dry；
S4. extruding: the obtained fibre semi-finished products of step S3 being placed in bulking machine and carry out expanding treatment, and it is fine to obtain the extruding dregs of a decoction
Dimension；
S5. the extraction of effective component: concentration is evaporated to the filtrate in step S2, obtaining has effective component solution；
S6. papermaking: extruding dreg fibers made from step S4 are subjected to second of desanding processing, then manufactures paper with pulp, obtains original
Paper；
S7. the effective component spray solution in S5 is obtained into the face tissue with pharmacological property after dry in the body paper surface of S6.
2. the method that dreg fibers material prepares face tissue according to claim 1, which is characterized in that the prescriptions worth thousand gold dregs of a decoction
It is remaining after water or ethyl alcohol extract for very heavy group, cherokee rose root, Caulis Spatholobi, single side needle, leatherleaf mahonia, Herba Andrographitis, Radix Angelicae Sinensis and Radix Codonopsis
The dregs of a decoction；
The partial size of the prescriptions worth thousand gold dregs of a decoction is less than 3cm.
3. the method that dreg fibers material prepares face tissue according to claim 1, which is characterized in that raw described in step S2
Object complex enzyme is prepared by the raw material of following weight percent: whiterot fungi 6 ~ 12%, Ficus virens 12 ~ 20%, wood are poly-
Carbohydrase 24 ~ 30% and laccase 10 ~ 20%.
4. the method that dreg fibers material prepares face tissue according to claim 1, which is characterized in that described in step S2
Fermentation process temperature is 55 ~ 65 DEG C, and the time is 3 ~ 4 h.
5. the method that dreg fibers material prepares face tissue according to claim 1, which is characterized in that the first time desanding
Processing carries out in sand removing machine, sand in removal；
Second of desanding processing is that dreg fibers made from step S3 are removed spun yarn by gauze.
6. the method that dreg fibers material prepares face tissue according to claim 1, which is characterized in that described in step S4
Swelling temperature is 100 ~ 120 DEG C, and puffing time is 10 ~ 20 min.
7. the method that dreg fibers material prepares face tissue according to claim 1, which is characterized in that filtrate in step S5
The temperature of evaporation and concentration is 100 ~ 110 DEG C, and the time of evaporation and concentration is 30 ~ 40 min.
8. the method that dreg fibers material prepares face tissue according to claim 1, which is characterized in that by S4 system in step S6
The fiber obtained is beaten, and beating degree is 20 ~ 30oThen SR manufactures paper with pulp, using starch as Cypres, after dry
Obtain body paper.
9. the method that dreg fibers material prepares face tissue according to claim 1, which is characterized in that in step S7, by S5
In effective component spray solution in the body paper surface of S6, effective component fountain height is the 20% ~ 30% of original paper quality, in 60 ~ 65
The face tissue with pharmacological property is obtained at DEG C after drying.
10. a kind of face tissue for the method preparation for preparing face tissue by any one of the claim 1 ~ 9 dreg fibers material.
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| CN1099827A (en) * | 1994-07-01 | 1995-03-08 | 黄庆文 | Toilet paper with traditional Chinese medicine and making method |
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| CN1924187A (en) * | 2006-09-28 | 2007-03-07 | 汤兴然 | Paper making method for straw fiber pulping by 'enzymatic conversion and puffing' |
| CN104005247A (en) * | 2014-05-15 | 2014-08-27 | 昆明理工大学 | Microwave-assisted preparation method of bagasse bleached pulp |
| CN104179055A (en) * | 2014-07-18 | 2014-12-03 | 刘秀平 | Grass fiber bio-separation compound preparation and application method thereof |
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2017
- 2017-12-12 CN CN201711324454.4A patent/CN109914154A/en not_active Withdrawn
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1099827A (en) * | 1994-07-01 | 1995-03-08 | 黄庆文 | Toilet paper with traditional Chinese medicine and making method |
| CN1251763A (en) * | 1998-10-21 | 2000-05-03 | 株洲千金药业股份公司 | Process for preparing Chinese medicine 'Qianjin tablets' for treating gynopathy |
| CN1924187A (en) * | 2006-09-28 | 2007-03-07 | 汤兴然 | Paper making method for straw fiber pulping by 'enzymatic conversion and puffing' |
| CN104005247A (en) * | 2014-05-15 | 2014-08-27 | 昆明理工大学 | Microwave-assisted preparation method of bagasse bleached pulp |
| CN104179055A (en) * | 2014-07-18 | 2014-12-03 | 刘秀平 | Grass fiber bio-separation compound preparation and application method thereof |
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Application publication date: 20190621 |