CN105213359A - Women's secret conditioning liquid and preparation method thereof - Google Patents
Women's secret conditioning liquid and preparation method thereof Download PDFInfo
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- CN105213359A CN105213359A CN201510621087.9A CN201510621087A CN105213359A CN 105213359 A CN105213359 A CN 105213359A CN 201510621087 A CN201510621087 A CN 201510621087A CN 105213359 A CN105213359 A CN 105213359A
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Abstract
The invention discloses a kind of women's secret conditioning liquid, comprise the raw material of following weight portion: A expects: hibitane 0.05 ~ 0.5 part, Borneolum Syntheticum 0.05 ~ 1 part, triclosan 0.01 ~ 0.3 part, ethanol 1 ~ 25 part, Tween 80? 0.5 ~ 5 part, 0.1 ~ 0.5 part, essence, pure water 66-98 part; B expects: antiseptic 0.1 ~ 0.5 part, citric acid 0.1 ~ 0.5 part.Present invention also offers a kind of preparation method of women's secret conditioning liquid.The present invention effectively can clean privates dirt, anti-bacteria grows, protect privates mucosa injury-free, and heat-clearing and toxic substances removing, keeps good privates environment.
Description
Technical field
The present invention relates to feminine care products, be specifically related to a kind of women's secret conditioning liquid and preparation method thereof.
Background technology
Conditioning liquid is requisite clean skin care item in female life.Only on pudendum cleaning, most of women also follows the out-of-date methods of decades, cleans with clear water.But investigation shows: women is trichomonas, mycotic, senile vaginitis are high incidence gynaecopathia, these diseases can be prevented by improving individual topical health in fact.Many women clean pudendum can use other cleaning supplies such as bath gel or fancy soap, and life-time service can cause pudendum sour environment to be destroyed, and changes and guides pH value, make dysbacteriosis, and local resistance declines, and brings out gynaecopathia.
Therefore, need badly at present a kind ofly effectively can clean privates dirt, anti-bacteria grows, women's secret conditioning liquid of protecting privates mucosa injury-free.
Summary of the invention
An object of the present invention is to solve at least the problems referred to above and/or defect, and the advantage will illustrated at least is below provided.
A further object of the invention is to provide a kind of women's secret conditioning liquid, and it effectively can clean privates dirt, anti-bacteria grows, protect privates mucosa injury-free, and heat-clearing and toxic substances removing, keeps good privates environment.
A further object of the invention is to provide a kind of U-shaped extractor, and it can process simultaneously process respectively two kinds of Chinese crude drugs, and extract active substance in enclosed space, extraction efficiency is high, and intensive degree is high, to prepare women's secret conditioning liquid.
In order to realize, according to these objects of the present invention and other advantage, providing a kind of women's secret conditioning liquid, comprise the raw material of following weight portion:
A expects: hibitane 0.05 ~ 0.5 part, Borneolum Syntheticum 0.05 ~ 1 part, triclosan 0.01 ~ 0.3 part, ethanol 1 ~ 25 part, Tween 80 0.5 ~ 5 part, 0.1 ~ 0.5 part, essence, pure water 66-98 part;
B expects: antiseptic 0.1 ~ 0.5 part, citric acid 0.1 ~ 0.5 part.
Preferably, described women's secret conditioning liquid, also comprise: C expects, it is: mass ratio be 6 ~ 8: 3 ~ 6: 3 ~ 6: 8 ~ 10: 6 ~ 8: 3 ~ 6: 2 ~ 4: 2 ~ 4: 3 Cortex Phellodendri, Herba Taraxaci, Herba Houttuyniae, Radix Scutellariae, Radix Ophiopogonis, Herba Dendrobii, Semen Sesami Nigrum, Semen Nelumbinis and Fructus Lycii, through extracting the Chinese medicine extract obtained, the weight ratio of described Chinese medicine extract and described citric acid is 10: 1.
A preparation method for women's secret conditioning liquid, comprises the following steps:
Step one, A is expected in the pure water of 2/3 amount add reaction pot, hibitane, Borneolum Syntheticum and triclosan are added reaction container, add ethanol and mix, stirring and dissolving, then adds Tween 80 and essence in reaction container, after all material dissolution mixing, reaction pot described in suction, stirs 15min;
Step 2, in advance by A expect in 1/3 amount pure water dissolve B material in antiseptic, the reaction pot in step one adds the antiseptic and citric acid that have dissolved successively, stirring 20min, 240 mesh filter screens filtrations, to obtain final product.
Preferably, the preparation method of described women's secret conditioning liquid, also comprises:
Step 3, one U-shaped extractor is provided, it comprises the first hollow box body that side is cylindrical shape, 3rd hollow box body of opposite side to be the second hollow box body of cylindrical shape and bottom be arc, the top of described first hollow box body and described second hollow box body is provided with can the first lid of On/Off, described first hollow box body is connected with nitrogen cylinder with the top of described second hollow box body, the inside of described first hollow box body and described second hollow box body is provided with rotatable leakage cylinder, the bottom of described first hollow box body and described second hollow box body is provided with screen cloth and slide valve successively, the top of described 3rd hollow box body is provided with can the second lid of On/Off, described first hollow box body and described second hollow box body external rings are provided with the first electric heating tube, and the bottom of described 3rd hollow box body is provided with the second electric heating tube,
Step 4, get the Cortex Phellodendri that mass ratio is 6 ~ 8: 3 ~ 6: 3 ~ 6: 8 ~ 10: 6 ~ 8: 3 ~ 6: 2 ~ 4: 2 ~ 4: 3, Herba Taraxaci, Herba Houttuyniae, Radix Scutellariae, Radix Ophiopogonis, Herba Dendrobii, Semen Sesami Nigrum, Semen Nelumbinis and Fructus Lycii, by the Cortex Phellodendri of above-mentioned mass ratio, Radix Scutellariae, Radix Ophiopogonis and Herba Dendrobii are placed in the leakage cylinder in described first hollow box body, and close the first lid being positioned at top, by the Herba Taraxaci of above-mentioned mass ratio, Herba Houttuyniae, Semen Sesami Nigrum, Semen Nelumbinis and Fructus Lycii are placed in the leakage cylinder of described second hollow box body, and close the first lid being positioned at top, ethanol are placed in described 3rd hollow box body, and close described second lid, open the slide valve be positioned at below screen cloth, make described first hollow box body, described second hollow box body is communicated with described 3rd hollow box body, but material does not wherein contact with each other, control two rotating speeds leaking cylinder and be 60r/min, start described second electric heating tube, described in electrical heating, the 3rd hollow box body is to the whole evaporate to dryness of ethanol, in described U-shaped extractor, pass into nitrogen, keep 1 ~ 2h, return back to atmospheric pressure,
Step 5, close the slide valve be positioned at below screen cloth, make described first hollow box body, described second hollow box body is not communicated with described 3rd hollow box body, deionized water is passed in described first hollow box body and described second hollow box body, liquid level is made to exceed the surface of the material of described first hollow box body and described second hollow box body inside, close the first lid being positioned at top, control two rotating speeds leaking cylinder and be 60r/min, start described first electric heating tube, first hollow box body described in electrical heating and described second hollow box body, to the surface of liquid level lower than the material of described first hollow box body and described second hollow box body inside, open described slide valve, medicinal liquid after filtering is imported described 3rd hollow box body, repeat 2 ~ 3 times, the medicinal liquid that described 3rd hollow box body is collected is derived, obtain Chinese medicine extract,
Step 6, Chinese medicine extract step 5 obtained, 240 mesh filter screens filter, and after radiation sterilizing, be mix at 10: 1 with the citric acid in step 2 according to mass ratio, stirring 30min, obtains described women's secret conditioning liquid.
Preferably, the preparation method of described women's secret conditioning liquid, the aperture of described leakage cylinder is 1mm, and described screen cloth is provided with 1.5 × 1.5mm squared mesh.
Preferably, the preparation method of described women's secret conditioning liquid, in step 4, the temperature of the third hollow box body described in electrical heating is 70 ~ 75 DEG C, in step 5, and the temperature of the first hollow box body described in electrical heating and described second hollow box body is 95 ~ 98 DEG C.
Preferably, the preparation method of described women's secret conditioning liquid, in step 4, the pressure passing into nitrogen in described U-shaped extractor is 2 ~ 3MPa.
The present invention at least comprises following beneficial effect:
The first, hibitane and triclosan are wide-spectrum bactericide, Borneolum Syntheticum heat-clearing and toxic substances removing, convenient and swift, sterilization good effect; The basis of above formula is added the Chinese medicine extract that multiple Chinese medicinal components is obtained, heat-clearing and toxic substances removing on the one hand, avoid and suppress triclosan to the side effect of human body, on the other hand, the generation of effective suppression privates antibacterial, the dirt that cleaning fold place conceals, forms moist, healthy local environment, antibacterial, antiviral, raising immunity of organisms; Preparation method of the present invention is simple and convenient, strictly sterilizes to each process cleaning by factory's cleaning and sterilizing technique;
The second, Cortex Phellodendri, bitter cold sedimentation, heat clearing and damp drying, eliminating fire and detoxication power is strong; Herba Taraxaci, heat-clearing and toxic substances removing, diuresis eliminating stagnation, prevents and treats urinary tract infection; Herba Houttuyniae, heat-clearing and toxic substances removing, detumescence treat skin ulcer; Radix Scutellariae, heat clearing and damp drying, eliminating fire and detoxication; Replenishing YIN and removing heat Radix Ophiopogonis, treatment yin asthenia generating intrinsic heat; Herba Dendrobii, nourishing YIN and clearing away heat, loses for cloudy impairment of body fluid; Semen Sesami Nigrum, nourishing of invigorating blood circulation; Semen Nelumbinis, antidiarrheal leukorrhagia stopping, tranquilizing by nourishing the heart; Fructus Lycii, tonify deficiency benefit essence, nourishing YIN and clearing away heat, improves immunity; Each taste Chinese medicine monarch, bactericidal antiphlogistic, privates of releiving skin, avoids the diseases such as urinary tract infection;
3rd, the invention provides a kind of U-shaped extractor, pretreatment is carried out to Chinese medicine, by being separated into three independently casings, when opening slide valve, the material being positioned at the leakage cylinder of the first hollow box body and the leakage cylinder of the second hollow box body is positioned at above screen cloth, do not contact with the ethanol of the 3rd hollow box body, steam ethanol to all volatilizations, penetrate into medical material inside, sterilization is stripping active substance also, by applying high-pressure inert gas, promote the stripping of active substance, when closing slide valve, the material being arranged in the leakage cylinder of the first hollow box body and the second hollow box body decocts at rotary course, then slide valve is opened, export to the 3rd hollow box body, merge medicinal liquid repeatedly, obtain Chinese medicine extract,
Four, the present invention is according to physical factors such as Chinese medicine form, hardness, Chinese medicine is divided into two groups, throw in the leakage cylinder in the first hollow box body and the second hollow box body respectively, carry out successively steaming, suppress and decocting at seal cavity, active substance dissolution is maximized; The aperture of leaking cylinder is less than the aperture of screen cloth, and the Chinese crude drug in anti-leak-stopping cylinder enters the 3rd hollow box body; Step 4, electricity heating degree 70 ~ 75 DEG C, reaches the boiling point of ethanol, makes whole evaporation, to steam Chinese crude drug, in step 5, electrical heating temperature is 95 ~ 98 DEG C, and high temperature makes deionized water seethe with excitement, with decocting herb material, in step 4, pressure is 2 ~ 3MPa, promotes the stripping of active substance.
Part is embodied by explanation below by other advantage of the present invention, target and feature, part also will by research and practice of the present invention by those skilled in the art is understood.
Accompanying drawing explanation
Fig. 1 is the structural representation of U-shaped extractor of the present invention.
Detailed description of the invention
Below in conjunction with drawings and Examples, the present invention is described in further detail, can implement according to this with reference to description word to make those skilled in the art.
< embodiment 1>
A kind of women's secret conditioning liquid, comprises the raw material of following weight portion:
A expects: hibitane 0.05 part, Borneolum Syntheticum 0.05 part, triclosan 0.01 part, ethanol 1 part, Tween 80 0.5 part, 0.1 part, essence, pure water 66 parts;
B expects: antiseptic 0.1 part, citric acid 0.1 part.
A preparation method for women's secret conditioning liquid, comprises the following steps:
Step one, A is expected in the pure water of 2/3 amount add reaction pot, hibitane, Borneolum Syntheticum and triclosan are added reaction container, add ethanol and mix, stirring and dissolving, then adds Tween 80 and essence in reaction container, after all material dissolution mixing, reaction pot described in suction, stirs 15min;
Step 2, in advance by A expect in 1/3 amount pure water dissolve B material in antiseptic, the reaction pot in step one adds the antiseptic and citric acid that have dissolved successively, stirring 20min, 240 mesh filter screens filtrations, to obtain final product.
< embodiment 2>
A kind of women's secret conditioning liquid, comprises the raw material of following weight portion:
A expects: hibitane 0.5 part, Borneolum Syntheticum 1 part, triclosan 0.3 part, ethanol 25 parts, Tween 80 5 parts, 0.5 part, essence, pure water 98 parts;
B expects: antiseptic 0.5 part, citric acid 0.5 part.
A preparation method for women's secret conditioning liquid, comprises the following steps:
Step one, A is expected in the pure water of 2/3 amount add reaction pot, hibitane, Borneolum Syntheticum and triclosan are added reaction container, add ethanol and mix, stirring and dissolving, then adds Tween 80 and essence in reaction container, after all material dissolution mixing, reaction pot described in suction, stirs 15min;
Step 2, in advance by A expect in 1/3 amount pure water dissolve B material in antiseptic, the reaction pot in step one adds the antiseptic and citric acid that have dissolved successively, stirring 20min, 240 mesh filter screens filtrations, to obtain final product.
< embodiment 3>
A kind of women's secret conditioning liquid, comprises the raw material of following weight portion:
A expects: hibitane 0.25 part, Borneolum Syntheticum 0.07 part, triclosan 0.15 part, ethanol 14 parts, Tween 80 3 parts, 0.3 part, essence, pure water 72 parts;
B expects: antiseptic 0.3 part, citric acid 0.3 part.
A preparation method for women's secret conditioning liquid, comprises the following steps:
Step one, A is expected in the pure water of 2/3 amount add reaction pot, hibitane, Borneolum Syntheticum and triclosan are added reaction container, add ethanol and mix, stirring and dissolving, then adds Tween 80 and essence in reaction container, after all material dissolution mixing, reaction pot described in suction, stirs 15min;
Step 2, in advance by A expect in 1/3 amount pure water dissolve B material in antiseptic, the reaction pot in step one adds the antiseptic and citric acid that have dissolved successively, stirring 20min, 240 mesh filter screens filtrations, to obtain final product.
< embodiment 4>
A kind of women's secret conditioning liquid, comprises the raw material of following weight portion:
A expects: hibitane 0.05 part, Borneolum Syntheticum 0.05 part, triclosan 0.01 part, ethanol 1 part, Tween 80 0.5 part, 0.1 part, essence, pure water 66 parts;
B expects: antiseptic 0.1 part, citric acid 0.1 part;
C expects: its for mass ratio be 6: 3: 3: 8: 6: 3: 2: 2: 3 Cortex Phellodendri, Herba Taraxaci, Herba Houttuyniae, Radix Scutellariae, Radix Ophiopogonis, Herba Dendrobii, Semen Sesami Nigrum, Semen Nelumbinis and Fructus Lycii, through extracting the Chinese medicine extract obtained, the weight ratio of described Chinese medicine extract and described citric acid is 10: 1.
A preparation method for women's secret conditioning liquid, comprises the following steps:
Step one, A is expected in the pure water of 2/3 amount add reaction pot, hibitane, Borneolum Syntheticum and triclosan are added reaction container, add ethanol and mix, stirring and dissolving, then adds Tween 80 and essence in reaction container, after all material dissolution mixing, reaction pot described in suction, stirs 15min;
Step 2, in advance by A expect in 1/3 amount pure water dissolve B material in antiseptic, the reaction pot in step one adds the antiseptic and citric acid that have dissolved successively, stirring 20min, 240 mesh filter screens filtrations, to obtain final product;
Step 3, one U-shaped extractor is provided, it comprises the first hollow box body 1 that side is cylindrical shape, 3rd hollow box body 3 of opposite side to be the second hollow box body 2 of cylindrical shape and bottom be arc, the top of described first hollow box body 1 and described second hollow box body 2 is provided with can the first lid 4 of On/Off, described first hollow box body 1 is connected with nitrogen cylinder 5 with the top of described second hollow box body 2, the inside of described first hollow box body 1 and described second hollow box body 2 is provided with rotatable leakage cylinder 6, the aperture of described leakage cylinder 6 is 1mm, the bottom of described first hollow box body 1 and described second hollow box body 2 is provided with screen cloth 7 and slide valve 8 successively, described screen cloth 7 is provided with 1.5 × 1.5mm squared mesh, the top of described 3rd hollow box body 3 is provided with can the second lid 9 of On/Off, described first hollow box body 1 and described second hollow box body 2 external rings are provided with the first electric heating tube 10, and the bottom of described 3rd hollow box body 3 is provided with the second electric heating tube,
Step 4, get the Cortex Phellodendri of above-mentioned mass ratio, Herba Taraxaci, Herba Houttuyniae, Radix Scutellariae, Radix Ophiopogonis, Herba Dendrobii, Semen Sesami Nigrum, Semen Nelumbinis and Fructus Lycii, by the Cortex Phellodendri of above-mentioned mass ratio, Radix Scutellariae, Radix Ophiopogonis and Herba Dendrobii are placed in the leakage cylinder 6 in described first hollow box body 1, and close the first lid 4 being positioned at top, by the Herba Taraxaci of above-mentioned mass ratio, Herba Houttuyniae, Semen Sesami Nigrum, Semen Nelumbinis and Fructus Lycii are placed in the leakage cylinder 6 of described second hollow box body 2, and close the first lid 4 being positioned at top, ethanol is placed in described 3rd hollow box body 3, and closes described second lid 9, open the slide valve 8 be positioned at below screen cloth 7, make described first hollow box body 1, described second hollow box body 2 is communicated with described 3rd hollow box body 3, but material does not wherein contact with each other, control two rotating speeds leaking cylinder 6 and be 60r/min, start described second electric heating tube, the temperature of the third hollow box body described in electrical heating is 70 DEG C, the whole evaporate to dryness of the 3rd hollow box body 3 to ethanol described in electrical heating, nitrogen is passed in described U-shaped extractor, the pressure of nitrogen is 2MPa, keeps 1h, returns back to atmospheric pressure,
Step 5, close the slide valve 8 be positioned at below screen cloth 7, make described first hollow box body 1, described second hollow box body 2 is not communicated with described 3rd hollow box body 3, deionized water is passed in described first hollow box body 1 and described second hollow box body 2, liquid level is made to exceed the surface of the material of described first hollow box body 1 and described second hollow box body 2 inside, close the first lid 4 being positioned at top, control two rotating speeds leaking cylinder 6 and be 60r/min, start described first electric heating tube 10, the temperature of the first hollow box body 1 described in electrical heating and described second hollow box body 2 is 95 DEG C, to the surface of liquid level lower than the material of described first hollow box body 1 and described second hollow box body 2 inside, open described slide valve 8, medicinal liquid after filtering is imported described 3rd hollow box body 3, repeat 2 times, the medicinal liquid collected by described 3rd hollow box body 3 is derived, obtain Chinese medicine extract,
Step 6, Chinese medicine extract step 5 obtained, 240 mesh filter screens filter, and after radiation sterilizing, be mix at 10: 1 with the citric acid in step 2 according to mass ratio, stirring 30min, obtains described women's secret conditioning liquid.
< embodiment 5>
A kind of women's secret conditioning liquid, comprises the raw material of following weight portion:
A expects: hibitane 0.5 part, Borneolum Syntheticum 1 part, triclosan 0.3 part, ethanol 25 parts, Tween 80 5 parts, 0.5 part, essence, pure water 98 parts;
B expects: antiseptic 0.5 part, citric acid 0.5 part;
C expects: its for mass ratio be 8: 6: 6: 10: 8: 6: 4: 4: 3 Cortex Phellodendri, Herba Taraxaci, Herba Houttuyniae, Radix Scutellariae, Radix Ophiopogonis, Herba Dendrobii, Semen Sesami Nigrum, Semen Nelumbinis and Fructus Lycii, through extracting the Chinese medicine extract obtained, the weight ratio of described Chinese medicine extract and described citric acid is 10: 1.
A preparation method for women's secret conditioning liquid, comprises the following steps:
Step one, A is expected in the pure water of 2/3 amount add reaction pot, hibitane, Borneolum Syntheticum and triclosan are added reaction container, add ethanol and mix, stirring and dissolving, then adds Tween 80 and essence in reaction container, after all material dissolution mixing, reaction pot described in suction, stirs 15min;
Step 2, in advance by A expect in 1/3 amount pure water dissolve B material in antiseptic, the reaction pot in step one adds the antiseptic and citric acid that have dissolved successively, stirring 20min, 240 mesh filter screens filtrations, to obtain final product;
Step 3, one U-shaped extractor is provided, it comprises the first hollow box body 1 that side is cylindrical shape, 3rd hollow box body 3 of opposite side to be the second hollow box body 2 of cylindrical shape and bottom be arc, the top of described first hollow box body 1 and described second hollow box body 2 is provided with can the first lid 4 of On/Off, described first hollow box body 1 is connected with nitrogen cylinder 5 with the top of described second hollow box body 2, the inside of described first hollow box body 1 and described second hollow box body 2 is provided with rotatable leakage cylinder 6, the aperture of described leakage cylinder 6 is 1mm, the bottom of described first hollow box body 1 and described second hollow box body 2 is provided with screen cloth 7 and slide valve 8 successively, described screen cloth 7 is provided with 1.5 × 1.5mm squared mesh, the top of described 3rd hollow box body 3 is provided with can the second lid 9 of On/Off, described first hollow box body 1 and described second hollow box body 2 external rings are provided with the first electric heating tube 10, and the bottom of described 3rd hollow box body 3 is provided with the second electric heating tube,
Step 4, get the Cortex Phellodendri of above-mentioned mass ratio, Herba Taraxaci, Herba Houttuyniae, Radix Scutellariae, Radix Ophiopogonis, Herba Dendrobii, Semen Sesami Nigrum, Semen Nelumbinis and Fructus Lycii, by the Cortex Phellodendri of above-mentioned mass ratio, Radix Scutellariae, Radix Ophiopogonis and Herba Dendrobii are placed in the leakage cylinder 6 in described first hollow box body 1, and close the first lid 4 being positioned at top, by the Herba Taraxaci of above-mentioned mass ratio, Herba Houttuyniae, Semen Sesami Nigrum, Semen Nelumbinis and Fructus Lycii are placed in the leakage cylinder 6 of described second hollow box body 2, and close the first lid 4 being positioned at top, ethanol is placed in described 3rd hollow box body 3, and closes described second lid 9, open the slide valve 8 be positioned at below screen cloth 7, make described first hollow box body 1, described second hollow box body 2 is communicated with described 3rd hollow box body 3, but material does not wherein contact with each other, control two rotating speeds leaking cylinder 6 and be 60r/min, start described second electric heating tube, the temperature of the third hollow box body described in electrical heating is 75 DEG C, the whole evaporate to dryness of the 3rd hollow box body 3 to ethanol described in electrical heating, nitrogen is passed in described U-shaped extractor, the pressure of nitrogen is 3MPa, keeps 2h, returns back to atmospheric pressure,
Step 5, close the slide valve 8 be positioned at below screen cloth 7, make described first hollow box body 1, described second hollow box body 2 is not communicated with described 3rd hollow box body 3, deionized water is passed in described first hollow box body 1 and described second hollow box body 2, liquid level is made to exceed the surface of the material of described first hollow box body 1 and described second hollow box body 2 inside, close the first lid 4 being positioned at top, control two rotating speeds leaking cylinder 6 and be 60r/min, start described first electric heating tube 10, the temperature of the first hollow box body 1 described in electrical heating and described second hollow box body 2 is 98 DEG C, to the surface of liquid level lower than the material of described first hollow box body 1 and described second hollow box body 2 inside, open described slide valve 8, medicinal liquid after filtering is imported described 3rd hollow box body 3, repeat 3 times, the medicinal liquid collected by described 3rd hollow box body 3 is derived, obtain Chinese medicine extract,
Step 6, Chinese medicine extract step 5 obtained, 240 mesh filter screens filter, and after radiation sterilizing, be mix at 10: 1 with the citric acid in step 2 according to mass ratio, stirring 30min, obtains described women's secret conditioning liquid.
< embodiment 6>
A kind of women's secret conditioning liquid, comprises the raw material of following weight portion:
A expects: hibitane 0.25 part, Borneolum Syntheticum 0.07 part, triclosan 0.15 part, ethanol 14 parts, Tween 80 3 parts, 0.3 part, essence, pure water 72 parts;
B expects: antiseptic 0.3 part, citric acid 0.3 part;
C expects: its for mass ratio be 7: 5: 5: 9: 7: 5: 3: 3: 3 Cortex Phellodendri, Herba Taraxaci, Herba Houttuyniae, Radix Scutellariae, Radix Ophiopogonis, Herba Dendrobii, Semen Sesami Nigrum, Semen Nelumbinis and Fructus Lycii, through extracting the Chinese medicine extract obtained, the weight ratio of described Chinese medicine extract and described citric acid is 10: 1.
A preparation method for women's secret conditioning liquid, comprises the following steps:
Step one, A is expected in the pure water of 2/3 amount add reaction pot, hibitane, Borneolum Syntheticum and triclosan are added reaction container, add ethanol and mix, stirring and dissolving, then adds Tween 80 and essence in reaction container, after all material dissolution mixing, reaction pot described in suction, stirs 15min;
Step 2, in advance by A expect in 1/3 amount pure water dissolve B material in antiseptic, the reaction pot in step one adds the antiseptic and citric acid that have dissolved successively, stirring 20min, 240 mesh filter screens filtrations, to obtain final product;
Step 3, one U-shaped extractor is provided, it comprises the first hollow box body 1 that side is cylindrical shape, 3rd hollow box body 3 of opposite side to be the second hollow box body 2 of cylindrical shape and bottom be arc, the top of described first hollow box body 1 and described second hollow box body 2 is provided with can the first lid 4 of On/Off, described first hollow box body 1 is connected with nitrogen cylinder 5 with the top of described second hollow box body 2, the inside of described first hollow box body 1 and described second hollow box body 2 is provided with rotatable leakage cylinder 6, the aperture of described leakage cylinder 6 is 1mm, the bottom of described first hollow box body 1 and described second hollow box body 2 is provided with screen cloth 7 and slide valve 8 successively, described screen cloth 7 is provided with 1.5 × 1.5mm squared mesh, the top of described 3rd hollow box body 3 is provided with can the second lid 9 of On/Off, described first hollow box body 1 and described second hollow box body 2 external rings are provided with the first electric heating tube 10, and the bottom of described 3rd hollow box body 3 is provided with the second electric heating tube,
Step 4, get the Cortex Phellodendri of above-mentioned mass ratio, Herba Taraxaci, Herba Houttuyniae, Radix Scutellariae, Radix Ophiopogonis, Herba Dendrobii, Semen Sesami Nigrum, Semen Nelumbinis and Fructus Lycii, by the Cortex Phellodendri of above-mentioned mass ratio, Radix Scutellariae, Radix Ophiopogonis and Herba Dendrobii are placed in the leakage cylinder 6 in described first hollow box body 1, and close the first lid 4 being positioned at top, by the Herba Taraxaci of above-mentioned mass ratio, Herba Houttuyniae, Semen Sesami Nigrum, Semen Nelumbinis and Fructus Lycii are placed in the leakage cylinder 6 of described second hollow box body 2, and close the first lid 4 being positioned at top, ethanol is placed in described 3rd hollow box body 3, and closes described second lid 9, open the slide valve 8 be positioned at below screen cloth 7, make described first hollow box body 1, described second hollow box body 2 is communicated with described 3rd hollow box body 3, but material does not wherein contact with each other, control two rotating speeds leaking cylinder 6 and be 60r/min, start described second electric heating tube, the temperature of the third hollow box body described in electrical heating is 72 DEG C, the whole evaporate to dryness of the 3rd hollow box body 3 to ethanol described in electrical heating, nitrogen is passed in described U-shaped extractor, the pressure of nitrogen is 2.5MPa, keeps 1h, returns back to atmospheric pressure,
Step 5, close the slide valve 8 be positioned at below screen cloth 7, make described first hollow box body 1, described second hollow box body 2 is not communicated with described 3rd hollow box body 3, deionized water is passed in described first hollow box body 1 and described second hollow box body 2, liquid level is made to exceed the surface of the material of described first hollow box body 1 and described second hollow box body 2 inside, close the first lid 4 being positioned at top, control two rotating speeds leaking cylinder 6 and be 60r/min, start described first electric heating tube 10, the temperature of the first hollow box body 1 described in electrical heating and described second hollow box body 2 is 96 DEG C, to the surface of liquid level lower than the material of described first hollow box body 1 and described second hollow box body 2 inside, open described slide valve 8, medicinal liquid after filtering is imported described 3rd hollow box body 3, repeat 3 times, the medicinal liquid collected by described 3rd hollow box body 3 is derived, obtain Chinese medicine extract,
Step 6, Chinese medicine extract step 5 obtained, 240 mesh filter screens filter, and after radiation sterilizing, be mix at 10: 1 with the citric acid in step 2 according to mass ratio, stirring 30min, obtains described women's secret conditioning liquid.
< antibacterial experiment in vitro >
Get Clinical isolation staphylococcus aureus, Candida albicans and B-mode micrococcus scarlatinae, be incubated at respectively in culture medium, women's secret conditioning liquid that Example 1 ~ 6 obtains makes experimental example, get certain gynaecologic washing lotion commercially available to do ratio, adopt test tube method to measure minimum inhibitory concentration, experimental result is as follows:
As seen from the above table, embodiment 1 ~ 6 pair of staphylococcus aureus, Candida albicans and B-mode micrococcus scarlatinae all have stronger bacteriostasis, and wherein the minimum inhibitory concentration of embodiment 4 ~ 6 is minimum, illustrate that in-vitro antibacterial effect is best.
< clinical practice experiment >
Zheng, female, 46 years old, pudendal pruritus was red and swollen, profuse leukorrhea, used women's secret conditioning liquid that embodiment 6 is obtained, every day washing vagina, symptom alleviated on 3rd, and 7 again without sense of discomfort.
Zhang, female, 52 years old, vagina drying, yellowish urine constipation, uses women's secret conditioning liquid that embodiment 6 is obtained, every day washing vagina, symptom alleviated on 4th, and 8 again without sense of discomfort.
King so-and-so, female, 41 years old, body jock itch, used women's secret conditioning liquid that embodiment 6 is obtained, every day rinsing vulva and anus, symptom alleviated on 5th, and 12 again without sense of discomfort.
Although embodiment of the present invention are open as above, but it is not restricted to listed in description and embodiment utilization, it can be applied to various applicable the field of the invention completely, for those skilled in the art, can easily realize other amendment, therefore do not deviating under the general concept that claim and equivalency range limit, the present invention is not limited to specific details and illustrates here and the legend described.
Claims (7)
1. women's secret conditioning liquid, is characterized in that, comprises the raw material of following weight portion:
A expects: hibitane 0.05 ~ 0.5 part, Borneolum Syntheticum 0.05 ~ 1 part, triclosan 0.01 ~ 0.3 part, ethanol 1 ~ 25 part, Tween 80 0.5 ~ 5 part, 0.1 ~ 0.5 part, essence, pure water 66-98 part;
B expects: antiseptic 0.1 ~ 0.5 part, citric acid 0.1 ~ 0.5 part.
2. women's secret conditioning liquid as claimed in claim 1, it is characterized in that, also comprise: C expects, it is: mass ratio be 6 ~ 8: 3 ~ 6: 3 ~ 6: 8 ~ 10: 6 ~ 8: 3 ~ 6: 2 ~ 4: 2 ~ 4: 3 Cortex Phellodendri, Herba Taraxaci, Herba Houttuyniae, Radix Scutellariae, Radix Ophiopogonis, Herba Dendrobii, Semen Sesami Nigrum, Semen Nelumbinis and Fructus Lycii, through extracting the Chinese medicine extract obtained, the weight ratio of described Chinese medicine extract and described citric acid is 10: 1.
3. a preparation method for women's secret conditioning liquid as claimed in claim 1, is characterized in that, comprise the following steps:
Step one, A is expected in the pure water of 2/3 amount add reaction pot, hibitane, Borneolum Syntheticum and triclosan are added reaction container, add ethanol and mix, stirring and dissolving, then adds Tween 80 and essence in reaction container, after all material dissolution mixing, reaction pot described in suction, stirs 15min;
Step 2, in advance by A expect in 1/3 amount pure water dissolve B material in antiseptic, the reaction pot in step one adds the antiseptic and citric acid that have dissolved successively, stirring 20min, 240 mesh filter screens filtrations, to obtain final product.
4. the preparation method of women's secret conditioning liquid as claimed in claim 3, is characterized in that, also comprise:
Step 3, one U-shaped extractor is provided, it comprises the first hollow box body that side is cylindrical shape, 3rd hollow box body of opposite side to be the second hollow box body of cylindrical shape and bottom be arc, the top of described first hollow box body and described second hollow box body is provided with can the first lid of On/Off, described first hollow box body is connected with nitrogen cylinder with the top of described second hollow box body, the inside of described first hollow box body and described second hollow box body is provided with rotatable leakage cylinder, the bottom of described first hollow box body and described second hollow box body is provided with screen cloth and slide valve successively, the top of described 3rd hollow box body is provided with can the second lid of On/Off, described first hollow box body and described second hollow box body external rings are provided with the first electric heating tube, and the bottom of described 3rd hollow box body is provided with the second electric heating tube,
Step 4, get the Cortex Phellodendri that mass ratio is 6 ~ 8: 3 ~ 6: 3 ~ 6: 8 ~ 10: 6 ~ 8: 3 ~ 6: 2 ~ 4: 2 ~ 4: 3, Herba Taraxaci, Herba Houttuyniae, Radix Scutellariae, Radix Ophiopogonis, Herba Dendrobii, Semen Sesami Nigrum, Semen Nelumbinis and Fructus Lycii, by the Cortex Phellodendri of above-mentioned mass ratio, Radix Scutellariae, Radix Ophiopogonis and Herba Dendrobii are placed in the leakage cylinder in described first hollow box body, and close the first lid being positioned at top, by the Herba Taraxaci of above-mentioned mass ratio, Herba Houttuyniae, Semen Sesami Nigrum, Semen Nelumbinis and Fructus Lycii are placed in the leakage cylinder of described second hollow box body, and close the first lid being positioned at top, ethanol are placed in described 3rd hollow box body, and close described second lid, open the slide valve be positioned at below screen cloth, make described first hollow box body, described second hollow box body is communicated with described 3rd hollow box body, but material does not wherein contact with each other, control two rotating speeds leaking cylinder and be 60r/min, start described second electric heating tube, described in electrical heating, the 3rd hollow box body is to the whole evaporate to dryness of ethanol, in described U-shaped extractor, pass into nitrogen, keep 1 ~ 2h, return back to atmospheric pressure,
Step 5, close the slide valve be positioned at below screen cloth, make described first hollow box body, described second hollow box body is not communicated with described 3rd hollow box body, deionized water is passed in described first hollow box body and described second hollow box body, liquid level is made to exceed the surface of the material of described first hollow box body and described second hollow box body inside, close the first lid being positioned at top, control two rotating speeds leaking cylinder and be 60r/min, start described first electric heating tube, first hollow box body described in electrical heating and described second hollow box body, to the surface of liquid level lower than the material of described first hollow box body and described second hollow box body inside, open described slide valve, medicinal liquid after filtering is imported described 3rd hollow box body, repeat 2 ~ 3 times, the medicinal liquid that described 3rd hollow box body is collected is derived, obtain Chinese medicine extract,
Step 6, Chinese medicine extract step 5 obtained, 240 mesh filter screens filter, and after radiation sterilizing, be mix at 10: 1 with the citric acid in step 2 according to mass ratio, stirring 30min, obtains described women's secret conditioning liquid.
5. the preparation method of women's secret conditioning liquid as claimed in claim 4, it is characterized in that, the aperture of described leakage cylinder is 1mm, and described screen cloth is provided with 1.5 × 1.5mm squared mesh.
6. the preparation method of women's secret conditioning liquid as claimed in claim 5, it is characterized in that, in step 4, the temperature of the third hollow box body described in electrical heating is 70 ~ 75 DEG C, in step 5, the temperature of the first hollow box body described in electrical heating and described second hollow box body is 95 ~ 98 DEG C.
7. the preparation method of women's secret conditioning liquid as claimed in claim 6, it is characterized in that, in step 4, the pressure passing into nitrogen in described U-shaped extractor is 2 ~ 3MPa.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106085751A (en) * | 2016-06-28 | 2016-11-09 | 盐城工学院 | A kind of cordyceps militaris liquor leaching device and extraction separation method |
| CN109125705A (en) * | 2018-09-05 | 2019-01-04 | 国之祥健康产业有限公司 | A kind of women privates conditioning liquid and its preparation method and application |
| CN110652541A (en) * | 2018-06-28 | 2020-01-07 | 黄玉兰 | Female bacteriostatic lotion and preparation method thereof |
| CN113396904A (en) * | 2021-06-21 | 2021-09-17 | 福州大学 | Preparation method of borneol-triclosan composite antibacterial agent |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101623251A (en) * | 2009-08-11 | 2010-01-13 | 湖北穆兰同大科技有限公司 | Gynecological antibacterial gel bionic propellant |
| CN103655908A (en) * | 2013-11-21 | 2014-03-26 | 山东东阿阿胶股份有限公司 | Novel compound colla corii asini pulp and preparation technology thereof |
| CN104920499A (en) * | 2015-05-15 | 2015-09-23 | 金维元 | Compound disinfectant, and preparation method and application thereof |
-
2015
- 2015-09-25 CN CN201510621087.9A patent/CN105213359B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101623251A (en) * | 2009-08-11 | 2010-01-13 | 湖北穆兰同大科技有限公司 | Gynecological antibacterial gel bionic propellant |
| CN103655908A (en) * | 2013-11-21 | 2014-03-26 | 山东东阿阿胶股份有限公司 | Novel compound colla corii asini pulp and preparation technology thereof |
| CN104920499A (en) * | 2015-05-15 | 2015-09-23 | 金维元 | Compound disinfectant, and preparation method and application thereof |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106085751A (en) * | 2016-06-28 | 2016-11-09 | 盐城工学院 | A kind of cordyceps militaris liquor leaching device and extraction separation method |
| CN106085751B (en) * | 2016-06-28 | 2023-04-25 | 盐城工学院 | Cordyceps sinensis wine leaching device and leaching separation method |
| CN110652541A (en) * | 2018-06-28 | 2020-01-07 | 黄玉兰 | Female bacteriostatic lotion and preparation method thereof |
| CN109125705A (en) * | 2018-09-05 | 2019-01-04 | 国之祥健康产业有限公司 | A kind of women privates conditioning liquid and its preparation method and application |
| CN113396904A (en) * | 2021-06-21 | 2021-09-17 | 福州大学 | Preparation method of borneol-triclosan composite antibacterial agent |
| CN113396904B (en) * | 2021-06-21 | 2022-06-21 | 福州大学 | Preparation method of borneol-triclosan composite antibacterial agent |
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