CN109914129A - A kind of clean fabric dyeing and printing process - Google Patents
A kind of clean fabric dyeing and printing process Download PDFInfo
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- CN109914129A CN109914129A CN201910208100.6A CN201910208100A CN109914129A CN 109914129 A CN109914129 A CN 109914129A CN 201910208100 A CN201910208100 A CN 201910208100A CN 109914129 A CN109914129 A CN 109914129A
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Abstract
The present invention discloses a kind of clean fabric dyeing and printing process, including pretreatment procedure, dyeing process and postprocessing working procedures.The present invention carries out pre-treating technology to fabric using the solution that dehydrated alcohol organic solvent and desizing agent and dehydrated alcohol organic solvent and bleaching agent mix, solve the problems, such as in conventional fabrics pre-treating technology big water consumption and difficult recycling and seriously polluted, and with the decomposition and removing of the substances such as pectic substance in fiber, Inter-fiber voids increase, fibrous inside channel is opened, fabric exhibits go out the feel and uniform capillary effect of fluffy softness, it is more advantageous to subsequent dyeing and finishing processing, dehydrated alcohol organic solvent is added, slurry and natural impurity are preferably contacted with desizing liquid and bleaching liquid, to achieve the purpose that remove in a short time, the water consumption of pre-treating technology can also be greatly reduced, it is energy saving.
Description
Technical field
The present invention discloses a kind of clean fabric dyeing and printing process, belongs to technical field of textile printing.
Background technique
Textile industry is that parts, the fabrics such as China traditional pillar industry, including weaving, printing and dyeing, chemical fibre and clothes refer to
The textile made of natural fiber or synthetic fibers can be divided into woven fabric, knitted fabric and non-woven by different processing methods
Cloth is the raw material for making the articles for daily use such as clothing, curtain, and printing and dyeing, which refer to, shows fabric needed for people by dyeing
The various colors wanted keeps fabric more beautiful, however is dyed using existing dyeing to fabric, dyeing quality compared with
Difference is easy to influence using effect.
Summary of the invention
The purpose of the present invention is just providing a kind of clean fabric dyeing and printing process to solve the problem above-mentioned.
The present invention is achieved through the following technical solutions above-mentioned purpose, a kind of clean fabric dyeing and printing process, including pre-treatment
Process, dyeing process and postprocessing working procedures, the pretreatment procedure include desizing process and bleaching process, and the desizing process is
Fabric is immersed in desizing liquid and carries out desizing, the desizing liquid is organic molten by the dehydrated alcohol that volume fraction is 50%-95%
The aliphatic alcohol polyethenoxy that the desizing agent and concentration that water that agent, volume fraction are 5%-50%, concentration are 1-10g/L are 1-2g/L
Ether mixes, and the bleaching process, which refers to immerse fabric in bleaching liquid, to be bleached, and the bleaching liquid is by volume fraction
Bleaching agent that water that the dehydrated alcohol organic solvent of 50%-95%, volume fraction are 5%-50%, concentration are 2-5g/L, concentration
The hydrogen peroxide bleaching stabilizer NCS-PB that fatty alcohol polyoxyethylene ether and concentration for 1-3g/L are 3-7g/L is mixed, in the dyeing
In processes, selection reactive dye are required according to different colours, the fabric after pretreatment procedure is put into 45 DEG C of bath raio 1:10-1:
In 20 water, the levelling agent that concentration the is 1-1.5g/L, softening agent that carrier auxiliary agent, concentration are 1.5-2.5g/L, dense is then added
It spends the bleeding agent for being 1.5-2.5g/L, the diffusant that concentration is 0.8-1.2g/L, then utilizes Acetic acid-sodium acetate buffer by pH
Value is adjusted to 4.5-5, and reactive dye are added, and heating rate is 1 DEG C/min, and temperature rises to 40-50 DEG C, and heat preservation 30min is subsequent
Temperature of continuing rising, heating rate are 1 DEG C/min, and temperature rises to 95-100 DEG C, start to cool down after keeping the temperature 60min, cooling rate 1.5
DEG C/dyestuff water is discharged and injected clear water again when temperature is down to 50 DEG C, rinses 15min with clear water, locate after described by min
Science and engineering sequence includes soap washing and laking procedure, and soap washing is that the fabric after dyeing rinses 15 with 50 DEG C of liquid soap
Min, then 15min is rinsed with 60 DEG C of clear water, laking procedure is that the fabric after cleaning is put into fixation liquid to carry out fixation, described
Fixation liquid contains the salt that concentration is 15-25g/L and the citric acid that concentration is 5-10g/L, and color fixing temperature is 75 DEG C, the fixation time
For 60min, fabric, and dewatered drying are cleaned with clear water after fixation.
Preferably, the desizing liquid bath raio in the desizing process be 1:20-1:40, desizing temperature be under room temperature state with
1 DEG C/min is to slowly warm up to 70 DEG C, keeps the temperature 45 minutes, is then slowly dropped to 40 DEG C hereinafter, after desizing with 2 DEG C/min again
It discharges water.
Preferably, the bleaching liquid bath raio in the bleaching process is 1:20-1:30, and bleaching temperature is slow with 1.5 DEG C/min
85 DEG C are warming up to, bleaching time is 120 minutes, is then slowly dropped to 40 DEG C hereinafter, discharging water after bleaching with 2 DEG C/min again.
Preferably, the bleaching agent is hydrogen peroxide.
Preferably, the sodium bicarbonate group that the anhydrous sodium sulphate and concentration that the carrier auxiliary agent is 1-2g/L by concentration are 1-1.5g/L
At.
Preferably, the reactive dye are KN type, the phosphine of the X-type of dichloro s-triazine, the K-type of a chloro-s-triazine, vinyl sulfone(RemzaolHuo Xingranliaohuoxingjituan)
One of F type of one chlorine pyrimidine of p-type and difluoro of sour rouge is a variety of.
Preferably, the softening agent in the dyeing process is ester based quaternary ammonium salt softening agent, and bleeding agent is fatty alcohol polyoxy second
Alkene ether, diffusant are dispersing agent NNO.
Preferably, the levelling agent is stearyl dimethyl benzyl ammonium chloride.
Compared with prior art, the beneficial effects of the present invention are:
The present invention mixed with desizing agent and dehydrated alcohol organic solvent and bleaching agent using dehydrated alcohol organic solvent and
At solution pre-treating technology is carried out to fabric, solve water consumption in conventional fabrics pre-treating technology big and difficult recycling and pollution be tight
The problem of weight, and with the decomposition and removing of the substances such as pectic substance in fiber, Inter-fiber voids increase, fibrous inside channel quilt
It opens, fabric exhibits go out the feel and uniform capillary effect of fluffy softness, are more advantageous to subsequent dyeing and finishing processing, anhydrous second is added
Alcohol organic solvent enables slurry and natural impurity preferably to contact with desizing liquid and bleaching liquid, to reach in the short time
The purpose of interior removing, moreover it is possible to greatly reduce the water consumption of pre-treating technology, it is energy saving, and be not added in dyeing process
PH value is adjusted to 4.5-5 by Acetic acid-sodium acetate buffer by the alkaline matters such as soda ash, required appropriate when meeting dyeing
Acidic environment avoids leading to dyestuff because temperature increases so that dyeing effect is excellent, and is added high temperature levelling agent in dyeing process
Heat-resistant stability reduces and then leads to dye aggregation, influences level dyeing and contaminates effect thoroughly, or even can also lead to the problem of color dot, color stain,
So that dyeing effect is more preferable, and in dyeing process, temperature rises at the progressive mode of staged, and strict control heats up
Rate of temperature fall and dyeing time, so that textile dyeing firmness height, even dyeing, dye stability are good, while in dyer
It is added and soaps and color fixing process after skill, so that dyeing firmness is more preferable.
Specific embodiment
The following is a clear and complete description of the technical scheme in the embodiments of the invention, it is clear that described embodiment
Only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, the common skill in this field
Art personnel every other embodiment obtained without making creative work belongs to the model that the present invention protects
It encloses.
A kind of clean fabric dyeing and printing process, including pretreatment procedure, dyeing process and postprocessing working procedures, pretreatment procedure packet
Desizing process and bleaching process are included, desizing process is to immerse fabric in desizing liquid to carry out desizing, and desizing liquid is by volume fraction
Desizing agent that water that the dehydrated alcohol organic solvent of 50%-95%, volume fraction are 5%-50%, concentration are 1-10g/L and dense
Degree is that the fatty alcohol polyoxyethylene ether of 1-2g/L mixes, and bleaching process, which refers to immerse fabric in bleaching liquid, to be bleached,
Water that dehydrated alcohol organic solvent that bleaching liquid is 50%-95% by volume fraction, volume fraction are 5%-50%, concentration 2-
The hydrogen peroxide bleaching stabilizer NCS-PB that the fatty alcohol polyoxyethylene ether and concentration that the bleaching agent of 5g/L, concentration are 1-3g/L are 3-7g/L
Mix, hydrogen peroxide bleaching stabilizer NCS-PB have excellent chelating, complexing, can in aqueous solution iron, copper, aluminium, magnesium,
Calcium binding guarantees that fabric is smoothly bleached to alleviate the decomposition rate of hydrogen peroxide, so that semi-finished product are with particularly good
Whiteness and capillary effect, and hydrogen peroxide bleaching stabilizer NCS-PB also has stronger cleaning to act on to undesired water, while collecting alkaline-resisting and resistance to height
Temperature is integrated, significant effect.
According to the above technical scheme: using dehydrated alcohol organic solvent and desizing agent and dehydrated alcohol organic solvent and drift
The white dose of solution mixed carries out pre-treating technology to fabric, solves water consumption in conventional fabrics pre-treating technology big and difficult time
Receipts and seriously polluted problem, and with the decomposition and removing of the substances such as pectic substance in fiber, Inter-fiber voids increase, fiber
Inner passage is opened, and fabric exhibits go out the feel and uniform capillary effect of fluffy softness, is more advantageous to subsequent dyeing and finishing processing,
Dehydrated alcohol organic solvent is added, slurry and natural impurity are preferably contacted with desizing liquid and bleaching liquid, to reach
To the purpose removed in a short time, moreover it is possible to greatly reduce the water consumption of pre-treating technology, it is energy saving.
In dyeing process, selection reactive dye are required according to different colours, the fabric after pretreatment procedure is put into 45
In the water of DEG C bath raio 1:10-1:20, the levelling agent that concentration is 1-1.5g/L, carrier auxiliary agent, concentration 1.5-2.5g/ is then added
Then the diffusant that bleeding agent that the softening agent of L, concentration are 1.5-2.5g/L, concentration are 0.8-1.2g/L utilizes acetic acid-vinegar
PH value is adjusted to 4.5-5 by sour sodium buffer, and reactive dye are added, and heating rate is 1 DEG C/min, and temperature rises to 40-50 DEG C,
The subsequent temperature of continuing rising of 30min is kept the temperature, heating rate is 1 DEG C/min, and temperature rises to 95-100 DEG C, starts to cool down after keeping the temperature 60min, is dropped
Warm speed is 1.5 DEG C/min, when temperature is down to 50 DEG C, dyestuff water is discharged and injected clear water again, is rinsed with clear water
15min, postprocessing working procedures include soap washing and laking procedure, and soap washing is the fabric after dyeing with 50 DEG C of liquid soap
15min is rinsed, then rinses 15min with 60 DEG C of clear water, laking procedure is that the fabric after cleaning is put into fixation liquid to be consolidated
Color, fixation liquid contain the salt that concentration is 15-25g/L and the citric acid that concentration is 5-10g/L, and color fixing temperature is 75 DEG C, fixation
Time is 60min, cleans fabric, and dewatered drying with clear water after fixation.
According to the above technical scheme: slow by Acetic acid-sodium acetate that the alkaline matters such as soda ash are not added in dyeing process
PH value is adjusted to 4.5-5 by fliud flushing, and required proper sourness environment, so that dyeing effect is excellent, and is contaminating when meeting dyeing
High temperature levelling agent is added in color process, avoiding increasing because of temperature causes dyestuff heat-resistant stability to reduce and then leads to dye aggregation,
It influences level dyeing and contaminates effect thoroughly, or even can also lead to the problem of color dot, color stain, so that dyeing effect is more preferable, and in dyeing process
In, temperature rises at the progressive mode of staged, and strict control heating rate of temperature fall and dyeing time, so that fabric contaminates
Color firmness height, even dyeing, dye stability are good, while being added and soaping and color fixing process after dyeing, so that dyeing
Firmness is more preferable.
Desizing liquid bath raio in desizing process is 1:20-1:40, and desizing temperature is slow with 1 DEG C/min under room temperature state
Slowly 70 DEG C are warming up to, 45 minutes is kept the temperature, is then slowly dropped to 40 DEG C hereinafter, discharging water after desizing with 2 DEG C/min again.
Bleaching liquid bath raio in bleaching process is 1:20-1:30, and bleaching temperature is to slowly warm up to 85 DEG C with 1.5 DEG C/min,
Bleaching time is 120 minutes, is then slowly dropped to 40 DEG C hereinafter, discharging water after bleaching with 2 DEG C/min again.
Bleaching agent is hydrogen peroxide.
According to the above technical scheme: hydrogen peroxide can carry out oxidation to the slurry on fabric, make slurry by macromolecular
Amount oxidative degradation becomes small-molecular-weight, is easy to remove from fabric, the bleaching efficiency of fabric is improved, so that the whiteness of fabric increases
Greatly.
The sodium bicarbonate that the anhydrous sodium sulphate and concentration that carrier auxiliary agent is 1-2g/L by concentration are 1-1.5g/L forms.
According to the above technical scheme: since fiber and dyestuff are all negatively charged in the solution, repulsion can be generated between the two
Power can ionize out cation, Cation adsorption connects in fiber surface, dye anion by the way that anhydrous sodium sulphate and sodium bicarbonate is added
Suffered repulsive force just can weaken significantly when nearly fiber surface, and what reduction was generated due to Coulomb force can hinder, and improve dyestuff dye-uptake,
And the solubility of dyestuff in water can be reduced, promote dyestuff in conjunction with fiber, the dye-uptake of dyestuff is further increased, to reduce
The dosage of dyestuff deepens color, thus improves level-dyeing property, keeps dyestuff good to the spreadability of fiber, and every fastness ability is excellent
Good, degree of fixation improves, and anhydrous sodium sulphate and sodium bicarbonate are used cooperatively, and effect is more significant.
Reactive dye be the X-type of dichloro s-triazine, the K-type of a chloro-s-triazine, the KN type of vinyl sulfone(RemzaolHuo Xingranliaohuoxingjituan), the p-type of phosphonates and
One of F type of one chlorine pyrimidine of difluoro is a variety of.
Softening agent in dyeing process is ester based quaternary ammonium salt softening agent, and bleeding agent is fatty alcohol polyoxyethylene ether, diffusant
For dispersing agent NNO.
According to the above technical scheme: dispersing agent NNO has excellent diffusivity and protecting colloid performance, improves using effect
Fruit.
Levelling agent is stearyl dimethyl benzyl ammonium chloride.
According to the above technical scheme: stearyl dimethyl benzyl ammonium chloride can significantly improve dye aggregation degree, to dye
The affinity of material is greater than dyestuff to the affinity of fiber, and before contaminating on dyestuff, the levelling agent first generation with dyestuff ining conjunction with is stable to gather
Collective delays dyeing time to reduce the diffusion rate of dyestuff, and with the change of condition, dyestuff progressively disengages levelling agent,
And in conjunction with fiber, but levelling agent still has certain affinity to dyestuff at this time, therefore has slow dye and move dye effect.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims
Variation is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiments being understood that.
Claims (8)
1. a kind of clean fabric dyeing and printing process, which is characterized in that including pretreatment procedure, dyeing process and postprocessing working procedures, institute
Stating pretreatment procedure includes desizing process and bleaching process, and the desizing process is to immerse fabric in desizing liquid to carry out desizing,
Water that dehydrated alcohol organic solvent that the desizing liquid is 50%-95% by volume fraction, volume fraction are 5%-50%, concentration
The fatty alcohol polyoxyethylene ether that desizing agent and concentration for 1-10g/L are 1-2g/L mixes, the bleaching process refer to by
Fabric, which immerses in bleaching liquid, to be bleached, dehydrated alcohol organic solvent, the body that the bleaching liquid is 50%-95% by volume fraction
Fatty alcohol polyoxyethylene ether that bleaching agent that water that fraction is 5%-50%, concentration are 2-5g/L, concentration are 1-3g/L and dense
Degree is that the hydrogen peroxide bleaching stabilizer NCS-PB of 3-7g/L is mixed, and in the dyeing process, requires selection to live according to different colours
Property dyestuff, the fabric after pretreatment procedure is put into the water of 45 DEG C of bath raio 1:10-1:20, then be added concentration be 1-1.5g/L
Levelling agent, carrier auxiliary agent, concentration be 1.5-2.5g/L softening agent, concentration be 1.5-2.5g/L bleeding agent, concentration be
Then pH value is adjusted to 4.5-5 using Acetic acid-sodium acetate buffer, and reactive dye is added by the diffusant of 0.8-1.2g/L,
Heating rate is 1 DEG C/min, and temperature rises to 40-50 DEG C, keeps the temperature the subsequent temperature of continuing rising of 30min, and heating rate is 1 DEG C/min, temperature
95-100 DEG C is risen to, starts to cool down after keeping the temperature 60min, cooling rate is 1.5 DEG C/min, when temperature is down to 50 DEG C, by dyestuff
Water discharge and again injected clear water rinse 15min with clear water, and the postprocessing working procedures include soap washing and laking procedure, soap
Washing process is that the fabric after dyeing rinses 15min with 50 DEG C of liquid soap, then rinses 15min with 60 DEG C of clear water, described solid
Color process is that the fabric after cleaning is put into fixation liquid to carry out fixation, and the fixation liquid contains the salt that concentration is 15-25g/L
The citric acid for being 5-10g/L with concentration, color fixing temperature are 75 DEG C, and the fixation time is 60min, are cleaned and are knitted with clear water after fixation
Object, and dewatered drying.
2. a kind of clean fabric dyeing and printing process according to claim 1, which is characterized in that the desizing in the desizing process
Liquid bath ratio is 1:20-1:40, and desizing temperature is to be to slowly warm up to 70 DEG C under room temperature state with 1 DEG C/min, keeps the temperature 45 minutes, so
40 DEG C are slowly dropped to hereinafter, discharging water after desizing with 2 DEG C/min again afterwards.
3. a kind of clean fabric dyeing and printing process according to claim 1, which is characterized in that the bleaching in the bleaching process
Liquid bath ratio is 1:20-1:30, and bleaching temperature is to slowly warm up to 85 DEG C with 1.5 DEG C/min, and bleaching time is 120 minutes, then again
40 DEG C are slowly dropped to hereinafter, discharging water after bleaching with 2 DEG C/min.
4. a kind of clean fabric dyeing and printing process according to claim 1, which is characterized in that the bleaching agent is peroxidating
Hydrogen.
5. a kind of clean fabric dyeing and printing process according to claim 1, which is characterized in that the carrier auxiliary agent is by concentration
The sodium bicarbonate that the anhydrous sodium sulphate and concentration of 1-2g/L is 1-1.5g/L forms.
6. a kind of clean fabric dyeing and printing process according to claim 1, which is characterized in that the reactive dye are that dichloro is equal
One of the X-type of triazine, the K-type of a chloro-s-triazine, F type of one chlorine pyrimidine of the KN type of vinyl sulfone(RemzaolHuo Xingranliaohuoxingjituan), the p-type of phosphonates and difluoro
Or it is a variety of.
7. a kind of clean fabric dyeing and printing process according to claim 1, which is characterized in that the softness in the dyeing process
Agent is ester based quaternary ammonium salt softening agent, and bleeding agent is fatty alcohol polyoxyethylene ether, and diffusant is dispersing agent NNO.
8. a kind of clean fabric dyeing and printing process according to claim 1, which is characterized in that the levelling agent is octadecyl
Dimethyl benzyl ammonium chloride.
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Cited By (1)
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CN111733588A (en) * | 2020-06-11 | 2020-10-02 | 台州同兴印染有限公司 | Knitted fabric printing and dyeing pretreatment liquid, preparation method and knitted fabric dyeing process |
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CN103255609A (en) * | 2013-06-08 | 2013-08-21 | 武汉纺织大学 | Pretreatment method of cotton fabric |
CN103952923A (en) * | 2014-05-21 | 2014-07-30 | 太仓市宝明化纤有限公司 | High-efficiency and environment-friendly chemical fiber dyeing technology |
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