CN109908031A - A kind of edible lipstick mill base and preparation method thereof - Google Patents

A kind of edible lipstick mill base and preparation method thereof Download PDF

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Publication number
CN109908031A
CN109908031A CN201910169778.8A CN201910169778A CN109908031A CN 109908031 A CN109908031 A CN 109908031A CN 201910169778 A CN201910169778 A CN 201910169778A CN 109908031 A CN109908031 A CN 109908031A
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China
Prior art keywords
mill base
mill
lipstick
fat
base
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Pending
Application number
CN201910169778.8A
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Chinese (zh)
Inventor
杜慧
赵磊
张涛
何贵平
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Zhejiang Na Mei Novel Material Limited-Liability Co
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Zhejiang Na Mei Novel Material Limited-Liability Co
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Priority to CN201910169778.8A priority Critical patent/CN109908031A/en
Publication of CN109908031A publication Critical patent/CN109908031A/en
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Abstract

A kind of edible lipstick mill base disclosed by the invention and preparation method thereof, including mill base base-material, it is characterized in that, including the following component of mass fraction: the compound pigment of 20-30 parts of fat-soluble plants, 1-3 parts of colorant dispersants, 1-3 parts of moisturizer, 1-5 parts of grinding aids, including following preparation step: (1) by mill base base-material, dispersing agent, moisturizer investment main reaction kettle, heating the mixture that is uniformly dispersed to obtain;(2) by lycopene, curcumin, gardenia blue pigment hybrid modulation to panel tone, the compound pigment of fat-soluble plant and evenly dispersed into mixture is obtained;(3) grinding aid is added, is ground through ball mill;(4) iron shot is sucked out in ox magnet;It is good as materials compatibility to choose the compound pigment of fat-soluble plant, product stability is good, the fine and smooth full multiplicity of color, moisturizer is added in mill base, it ensure that the wettability of lipstick, bead mill technique ensure that the fineness of mill base, shorten the production time, also avoid mill base raw material as filtering and caused by waste.

Description

A kind of edible lipstick mill base and preparation method thereof
Technical field
The present invention relates to cosmetic fields, and in particular to a kind of edible lipstick mill base and preparation method thereof.
Background technique
Pigment toner addition is often directlyed adopt in traditional lipstick colorant manufacturing process, using hand lapping or three-roller into Row hybrid process, method not only dust pollution Datong District when its hybrid process mode certain fineness standard is not achieved so that at There are granular sensation and color and glossiness are all bad for product lipstick.Advantage of the invention is that selecting the other toner of cosmetics-stage and helping Pigment content height, stability, the good lipstick special color of compatibility is made in agent, preferred formula, professional fine bead mill technique Slurry.Mix the lipstick that can be made into function admirable in proportion with lipstick base-material.
Lipstick is as a kind of cosmetics currently popular, and deep to be liked by numerous women, the main component of lipstick includes existing The main component of lipstick is the auxiliary materials such as pigment, surfactant, base starting material (grease wax etc.) and essence in technology Composition, most lipstick raw materials currently on the market contain artificial synthesized ingredient, are readily incorporated in the synthesis process of these ingredients The unsaturated compounds such as aldehyde, ketone and heavy metal classes substance, have potential irritation, and Yi Yinqi skin allergy etc. is bad anti- It answers.
In order to avoid lipstick base-material bring side effect, related personnel has done the replacement of natural component, example to base starting material Chemical industry grease such as is replaced with natural oil, it is then less to the replacement concern of most important pigment composition, such as patent of invention CN201710812567.2 only uses red beet powder as mill base pigment raw material, and color replaces narrow range, only can be controlled to the depth not Same red, the process prior art in addition preparing mill base are mixed generally by raw material at a certain temperature and are obtained, this The mill base of sample preparation is not finer ground, and certain fineness standard is not achieved so that finished product lipstick there are granular sensation and color and Glossiness is all bad.
Therefore while being badly in need of a kind of lipstick mill base and guarantee safety, what can be prepared is rich in color, and mill base is fine and smooth, without particle Sense, color glossiness are good.
Summary of the invention
To solve the above problems, the present invention is novel to provide a kind of edible lipstick mill base and preparation method thereof, mill base is compatible Property high, the fine and smooth full multiplicity of color, no granular sensation, moisturizing degree is high, shortens the production time, also avoids mill base raw material due to mistake Filter and caused by waste.
The technical scheme is that providing a kind of edible lipstick mill base, including mill base base-material, which is characterized in that packet Include the following component of mass fraction: the compound pigment of 20-50 parts of fat-soluble plants, 1-3 parts of colorant dispersants, 1-3 parts of moisturizer, 1- 5 parts of grinding aids.
Preferably, the compound pigment of fat-soluble plant includes one of lycopene, curcumin, gardenia blue pigment Or it is several.
Preferably, the moisturizer is one or more of butter, chamomile caul-fat, vitamin E.
Preferably, the colorant dispersant is beeswax.
Preferably, the grinding aid is iron shot.
Preferably, the iron shot diameter is 0.1-0.5mm.
In addition, also providing a kind of edible lipstick mill base preparation method, which comprises the following steps: (1) by color It starches base-material, dispersing agent, moisturizer to put into main reaction kettle, heats the mixture that is uniformly dispersed to obtain;(2) by lycopene, ginger color Element, gardenia blue pigment hybrid modulation to panel tone obtain the compound pigment of fat-soluble plant and evenly dispersed into mixture;(3) Grinding aid is added, is ground through ball mill;(4) iron shot is sucked out in ox magnet.
Preferably, the ball mill revolving speed is 3000-4000r/min, milling time 30min.
Preferably, the mill base base-material, dispersing agent, moisturizer, the compound pigment of fat-soluble plant, grinding aid component and match Than same as above.
Food grade colorant used in the prior art is for artificial color or comprising water-soluble natural pigment, due to mill base base-material For the liposoluble substances such as esters composition, in order to preferably by pigment dispersion into mill base base-material, according to similar compatibility principle, this For 3 kinds of fat-soluble phytochromes of scheme selection as the raw material for meeting fat-soluble pigment, lycopene is the main of mature tomato Pigment is a kind of oxygen-free carotenoid, and sterling is needle-shaped peony crystal, and fat-soluble, in carotenoid, it has There is the effect of strongest antioxidant activity, lycopene removes free radical to outclass other carotenoid and vitamin E, quenches The rate constant of singlet oxygen of going out is 100 times of vitamin E, be the most powerful antioxidant that is found in nature so far it One;From curcumin refines in ginger, the crystallization of fat-soluble curcumin is orange-yellow powder, has anticancer, anti-inflammatory, anti- The functions such as oxidation;It is raw material by natural pigment made of finishing that natural blue pigment-gardenia blue, which is using gardenia blue pigment,;It chooses The three primary colors that natural fat-soluble phytochrome is blue, red, yellow mixes colours as lipstick, three primary colors can blend institute Some colors, lipstick toning range it is wider, mill base is highly-safe, and due to pigment be it is fat-soluble, the mill base after being adjusted to is steady It is qualitative stronger.
Pigment toner addition is often directlyed adopt in traditional lipstick colorant manufacturing process, using hand lapping or three-roller into Row hybrid process, method not only dust pollution Datong District when its hybrid process mode certain fineness standard is not achieved so that at Product lipstick is there are granular sensation and color and glossiness are all bad, in the present solution, bead mill technique is taken during preparing mill base, and Not only heating stirring or simple grinding have used iron shot as grinding aid in technique, and the grinding operation of ball mill is feeding Pump will be up sent into abrading cylinder by the slurries of pre-dispersed, wet processing by abrading cylinder lower section, in grinding bead, that is, the present embodiment Iron shot specific gravity it is heavier can fall down, make raw material generated in the abrading cylinder with pressure up and down convection current, raw material is between grinding bead During the friendship of pressurized and high speed rotation extends impact in gap, the functions such as emulsification, dispersion, rubbing, grinding are generated, and requirement can be rapidly achieved Fineness, after grinding again by high-speed rotating hard wolfram steel separation slot output abrading cylinder outside, the wolfram steel of the present embodiment separates seam Gap is less than desired fineness, that is, diameter and is no more than 0.5 μm, is one cycle grinding operation, shock is produced between iron shot and raw material And shearing effect, pearl liquid/gas separator is provided in raw material homogenization liquid exit and is detained pearl, makes the separation of pearl liquid is broken can be continuous Carry out, for the safty in use, iron shot omit in the mill base of bead mill or shearing or impact force of the iron shot due to grinding it is too big and Cause iron shot to peel off iron sheet, mill base is adsorbed using this kind of strong magnets of ox magnet, the mill base by bead mill can quickly reach To the fineness of requirement, no longer needs to filtering mill base into removal particle, reduce filtration step, shorten the production time, also avoid Mill base raw material as filtering caused by waste.
The beneficial effects of the present invention are choose that the compound pigment of fat-soluble plant is more preferable as materials compatibility, and product is steady Qualitative good, degree of safety is high, and can arbitrarily mix colours, and color exquisiteness is full, chooses butter, chamomile caul-fat, vitamin E conduct Moisturizer is added in mill base, ensure that the wettability of lipstick, is solved the problems, such as the drying that lipstick is smeared, is avoided using lipstick it Before must first apply lipstick, bead mill technique ensure that the fineness and safety in utilization of mill base, reduce filtration step, shorten production Time, also avoid mill base raw material as filtering and caused by waste.
Specific embodiment
In order to make content of the present invention easily facilitate understanding, With reference to embodiment to of the present invention Technical solution is described further, but the present invention is not limited only to this.
Embodiment 1
By in 100g lanolin oil, 10g beeswax, 10g butter investment beaker, 95 degrees Centigrade half an hour, stir evenly mixed Close object;Lycopene is made as red raw material, curcumin as yellow raw material, gardenia blue pigment according to RGB color model For blue raw material, hybrid modulation takes 10g lycopene, 10g curcumin powder equal to panel tone in the present embodiment in proportion It is even to mix to obtain Chinese red pigment, and be added in beaker;The iron shot that 200 diameters are 0.1mm is added, mixture is put into bead mill Machine, 3000-4000r/min, milling time 30min;The mill base that ball mill is isolated is collected to inhale into beaker, and with ox magnet Iron shot out obtains edible lipstick mill base.
Embodiment 2
By in 100g lanolin oil, 30g beeswax, 30g butter investment beaker, 95 degrees Centigrade half an hour, stir evenly mixed Close object;Lycopene is made as red raw material, curcumin as yellow raw material, gardenia blue pigment according to RGB color model For blue raw material, hybrid modulation takes 15g lycopene, 15g curcumin powder equal to panel tone in the present embodiment in proportion It is even to mix to obtain Chinese red pigment, and be added in beaker;The iron shot that 200 diameters are 0.1mm is added, mixture is put into bead mill Machine, 3000-4000r/min, milling time 30min;The mill base that ball mill is isolated is collected to inhale into beaker, and with ox magnet Iron shot out obtains edible lipstick mill base.
Embodiment 3
By in 100g lanolin oil, 30g beeswax, 30g butter investment beaker, 95 degrees Centigrade half an hour, stir evenly mixed Close object;Lycopene is made as red raw material, curcumin as yellow raw material, gardenia blue pigment according to RGB color model For blue raw material, hybrid modulation takes 12g lycopene, 12g curcumin powder equal to panel tone in the present embodiment in proportion It is even to mix to obtain Chinese red pigment, and be added in beaker;The iron shot that 200 diameters are 0.1mm is added, mixture is put into bead mill Machine, 3000-4000r/min, milling time 30min;The mill base that ball mill is isolated is collected to inhale into beaker, and with ox magnet Iron shot out obtains edible lipstick mill base.
Embodiment 4
By in 100g lanolin oil, 30g beeswax investment beaker, 95 degrees Centigrade half an hour, mixture is stirred evenly to obtain;According to RGB color model is using lycopene as red raw material, curcumin as yellow raw material, gardenia blue pigment as blue raw material Hybrid modulation takes 12g lycopene, 12g curcumin powder uniformly to mix to obtain tangerine to panel tone in the present embodiment in proportion Red pigments, and be added in beaker;The iron shot that 200 diameters are 0.1mm is added, mixture is put into ball mill, 3000- 4000r/min, milling time 30min;It collects the mill base that ball mill is isolated and iron shot is sucked out into beaker, and with ox magnet, Obtain edible lipstick mill base.
Embodiment 5
By in 100g lanolin oil, 30g beeswax, 30g butter investment beaker, 95 degrees Centigrade half an hour, stir evenly mixed Close object;According to RGB color model using food artificial color famille rose as red raw material, food artificial color sunset yellow as Huang Hybrid modulation takes 12g kinds in the present embodiment to panel tone in proportion as blue raw material for chromogen material, food artificial color brilliant blue Lycopene, 12g curcumin powder uniformly mix to obtain Chinese red pigment, and are added in beaker;200 diameters, which are added, is Mixture is put into ball mill, 3000-4000r/min, milling time 30min by the iron shot of 0.1mm;Collect ball mill separation Iron shot is sucked out into beaker, and with ox magnet in mill base out, must compare lipstick mill base 1.
Embodiment 6
By in 100g lanolin oil, 30g beeswax, 30g butter investment beaker, 95 degrees Centigrade half an hour, stir evenly mixed Close object;According to RGB color model using food artificial color famille rose as red raw material, food artificial color sunset yellow as Huang Hybrid modulation takes 12g kinds in the present embodiment to panel tone in proportion as blue raw material for chromogen material, food artificial color brilliant blue Lycopene, 12g curcumin powder uniformly mix to obtain Chinese red pigment, and are added in grinding;After grinding 30min, filtering Grain object, then filtrate is ground into 30min, it filters, examines whether there is or not particle, take filtrate up to comparison lipstick mill base 2.
Embodiment 7
Embodiment 1-6 is used to the sophistication of powder sophistication detection testing sieve detection mill base respectively, the detection of powder sophistication is used Testing sieve can be used for the accurate screening of graininess, the Granularity Structure of granular material, liquid type solid contents and sundries amount, mistake Filter, detection, using vibrating motor as vibration source, vibrating motor vibration drives the vibration of screen(ing) machine pedestal, then is transmitted to by pedestal It is placed on the normal test sieve on pedestal, sieves the material particles less than testing sieve compass screen surface mesh into lower layer's testing sieve, such as This is screened layer by layer, makes the material that same particle sizes are only stayed in every layer of testing sieve, 5 layers of sieve number of plies position, and sieve lattice diameter is 100-500 Mesh;Embodiment 1-5 is subjected to color stability detection respectively, the mill base of embodiment 1-6 kind is stood 15 days at normal temperature, sees and wipes Its sedimentation phenomenon;Embodiment 1-6 is carried out to moisten degree detection respectively, 50 volunteers is chosen and the moist degree of mill base is judged simultaneously It gives a mark (full marks 100 divide), removes average mark;Test result is as follows table:
The foregoing is merely presently preferred embodiments of the present invention, all equivalent changes done according to scope of the present invention patent with repair Decorations, are all covered by the present invention.

Claims (9)

1. a kind of edible lipstick mill base, including mill base base-material, which is characterized in that including the following component of mass fraction: 20-30 The compound pigment of the fat-soluble plant of part, 1-3 parts of colorant dispersants, 1-3 parts of moisturizer, 1-5 parts of grinding aids.
2. a kind of edible lipstick mill base according to claim 1, which is characterized in that the fat-soluble compound pigment of plant Including one or more of lycopene, curcumin, gardenia blue pigment.
3. a kind of edible lipstick mill base according to claim 1, which is characterized in that the moisturizer is butter, ocean is sweet One or more of oil of Flos Chrysanthemi, vitamin E.
4. a kind of edible lipstick mill base according to claim 1, which is characterized in that the colorant dispersant is beeswax.
5. a kind of edible lipstick mill base according to claim 1, which is characterized in that the grinding aid is iron shot.
6. a kind of edible lipstick mill base according to claim 5, which is characterized in that the iron shot diameter is 0.1- 0.5mm。
7. a kind of edible lipstick mill base preparation method, which comprises the following steps: (1) by mill base base-material, dispersion In agent, moisturizer investment main reaction kettle, the mixture that is uniformly dispersed to obtain is heated;(2) by lycopene, curcumin, cape jasmine blue Plain hybrid modulation obtains the compound pigment of fat-soluble plant and evenly dispersed into mixture to panel tone;(3) grinding aid is added, It is ground through ball mill;(4) iron shot is sucked out in ox magnet.
8. a kind of edible lipstick mill base preparation method according to claim 7, which is characterized in that the ball mill revolving speed For 3000-4000r/min, milling time 30min.
9. a kind of edible lipstick mill base preparation method according to claim 7, which is characterized in that the dispersing agent, guarantor Humectant, the compound pigment of fat-soluble plant, the component of grinding aid and with described in such as claim 1-6.
CN201910169778.8A 2019-03-07 2019-03-07 A kind of edible lipstick mill base and preparation method thereof Pending CN109908031A (en)

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CN116660468A (en) * 2023-05-29 2023-08-29 荆州洗涮涮环保科技有限公司 Intelligent monitoring and analyzing method for cosmetic production line
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