CN105331200A - High-pigment-content pure oil non-emulsification cosmetic color paste and preparation method - Google Patents
High-pigment-content pure oil non-emulsification cosmetic color paste and preparation method Download PDFInfo
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Abstract
The invention discloses high-pigment-content pure oil non-emulsification cosmetic color paste and a preparation method. The color paste is prepared from, by weight, 65-85% of pigment, 0.2-2% of a dispersing agent, 0.2-2% of stabilizer and 12-35% of grease. The high-pigment-content pure oil non-emulsification cosmetic color paste is characterized in that the pigment content is high, and the color paste belongs to pure oil non-emulsification color paste. The utilized pigment, the grease, the dispersing agent and the stabilizer are all raw materials which are allowed to be used by a China Cosmetic Ingredient Dictionary, a product is high in solid content, high in covering power, good in stability, high in safety, convenient to use, free of water, easy to add, easy to scatter, simple in preparation process and easy to produce, is the best substitute of traditional powdery pigment and is suitable for the field of cosmetics, food and the like.
Description
Technical field
The present invention relates to cosmetic material field, be specifically related to the pure oil pastes of a kind of makeup.
Background technology
Shortcomings is there is in Traditional makeup level powder pigment in cosmetic formulations uses.The surface level of powder pigment is large, easily reunites between particle, these increased the difficulty of powder dispersion, and particularly in mixing color process, difficult, uneven pigmenting power and the opacifying power of making of dispersion declines, and easily forms color spot and aberration.Powder pigment can produce floating dust in the application simultaneously, not only causes raw material to run off, more has a strong impact on healthy, contaminate environment.
On the market for the pigment of makeup, great majority are still in use powder pigment, and rare paste pigment is in use.The oil pastes had, example: application number 201410457866.5, it discloses a kind of scheme of ferric oxide oil pastes.
The ferric oxide oil pastes that the program provides, wherein the content of pigment is not high, mainly there is following problem in the application:
1. ferric oxide series slurry can only be provided, too dull in color, the slurry oil products such as purple, pink colour, blueness cannot be provided;
2. pigment content is low, and corresponding is grease high-content, thus in use constrains the adjustment of cosmetic formulations and optimize space, will impact the stability of formula.
3. the mill base of low pigment content is reach higher tinting strength, and consumption may increase, and may increase use cost.
4. product is the emulsification system iron oxide color paste of moisture, emulsifying agent and solvent, because emulsification system is kind of a unstable complex system, makes use occasion limited
Summary of the invention
Not high for the content of pigment in existing mill base, affect the problem applied in cosmetic formulations, the object of the invention is to provide a kind of high pigment content makeup pure oil pastes, simultaneously for the pure oil pastes of these high pigment content makeup, provides a kind of preparation method.
In order to achieve the above object, the present invention adopts following technical scheme:
The pure oily non-emulsified makeup mill base of a kind of high pigment content, described mill base is made up of the component of following parts by weight:
In a preferred version of above-mentioned pure oily non-emulsified makeup mill base, described pigment is at least one in ferric oxide, chromic oxide, ultramarine, ferriferro cyanide, titanium dioxide.And ferric oxide is specifically as follows at least one in iron oxide yellow, red iron oxide, iron oxide black, iron oxide brown.
Further, described titanium dioxide is at least one in Rutile type Titanium Dioxide, anatase thpe white powder
In a preferred version of above-mentioned pure oily non-emulsified makeup mill base, described grease is at least one in silicone oil, iso-octyl palmitate, caprylic/capric triglyceride, C12-C15 alcohol benzoic ether, iso-octyl palmitate, Isopropyl myristate.
In a preferred version of above-mentioned pure oily non-emulsified makeup mill base, described dispersion agent is at least one in PEG-30 dimerization hydroxy stearic acid ester, poly-oxystearic acid, the smooth stearate of sorb, the smooth different hard acid esters of sorb, PEG-2 Witconol AL 69-66, PEG/PPG-18/18 polydimethylsiloxane, sucrose fatty ester.
In a preferred version of above-mentioned pure oily non-emulsified makeup mill base, described stablizer is at least one in montmorillonite, organobentonite, silico-aluminate, silicate, aerosil, higher fatty acid.
In a preferred version of above-mentioned pure oily non-emulsified makeup mill base, described thickening material is at least one in cera alba, 80# Microcrystalline Wax, Ka Er ceresine, Magnesium Stearate, carnauba wax.
For the above-mentioned pure oil pastes of high pigment content makeup, its preparation method comprises the following steps:
(1) grease, dispersion agent, thickening material and stablizer that the pure oil pastes of above-mentioned high pigment content makeup comprises proportionally are mixed, heated and stirred, obtain uniform oiliness dispersion medium;
(2), under oiliness dispersion medium heated and stirred step (1) obtained, the colo(u)rant dispersion adding corresponding proportion is mixed into pulpous state;
(3) slurry grinding distribution step (2) obtained 3-4 time, obtains the pure oil pastes of makeup of high pigment content.
In a preferred version of above-mentioned preparation method, the Heating temperature in described step (1) and (2) is 80 ~ 85 DEG C.
In a preferred version of above-mentioned preparation method, adopt grinding distribution equipment to disperse slurry in described step (2), described grinding distribution equipment is at least one in ball mill, colloidal mill, high speed shear dispersion emulsifying machine.
The high pigment content formed according to this programme makeup oil pastes has high solids content, fat content is few, the advantages such as, tinting strength strong, covering power high, water-repellancy excellent, safety non-toxic, easy to use, good stability little on the adjustment impact of formula; Its preparation technology is simple simultaneously, cost is lower, is easy to suitability for industrialized production, replaces traditional powder pigment, be widely used in cosmetic field.
Accompanying drawing explanation
The present invention is further illustrated below in conjunction with the drawings and specific embodiments.
Fig. 1 is that the high-rutile type titanium dioxide content mill base of preparation in this example 4 and commercially available titanium dioxide mill base are according to the comparison diagram of GBT5211.17-1988 white pigment contrast ratio (opacifying power).
Embodiment
The technique means realized to make the present invention, creation characteristic, reaching object and effect is easy to understand, below in conjunction with concrete diagram and example, setting forth the present invention further.
Because in conventional oil-based mill base, pigment content is low, the adjustment of restriction cosmetic formulations and optimization space, thus the stability of formula is impacted.For this problem, this example provides that a kind of pigment content is high, good stability, security are high, strong covering power, the dispersed excellent pure oil pastes of makeup, unnecessary composition can be reduced in the application by the stable mill base of high pigment content to bring into, increase the effect of pigment in cosmetic formulations.
For this reason, the pure oily non-emulsified makeup mill base of this high pigment content, it is made up of the component of following parts by weight:
On this basis, preferred component ratio is:
In the pure oil pastes of high pigment content makeup be made up of upper formula, it uses grease immersion pigment, adds the lipophilicity of pigment, and dispersed, water-repellancy is improved; High pigment content, significantly can reduce the impact of other component in formula application except pigment, improve the opacifying property of pigment simultaneously, reduce consumption, reduce costs.
In addition, use China cosmetic raw material catalogue to allow the raw material used, through speed lapping, pigment changes into pulpous state, can not produce floating dust, and its ease of use and security improve.
Moreover it is more complete that interpolation dispersion agent makes powder pigment disperse, slurry color even, add the viscosity of thickening material and stablizer increase system simultaneously, make it all more stable under high temperature, normal temperature, low temperature.
On this basis, this example additionally provides and has synergistic concrete formula:
Pigment is specially at least one in ferric oxide, chromic oxide, ultramarine, ferriferro cyanide, titanium dioxide.Wherein ferric oxide is at least one in iron oxide yellow, red iron oxide, iron oxide black, iron oxide brown.
Titanium dioxide is at least one in Rutile type Titanium Dioxide, anatase thpe white powder
Grease is at least one in silicone oil, iso-octyl palmitate, caprylic/capric triglyceride, C12-C15 alcohol benzoic ether, iso-octyl palmitate, Isopropyl myristate.
Wherein, silicone oil is at least one in polydimethylsiloxane, octamethylcyclotetrasiloxane, decamethylcyclopentaandoxane, ten diformazan basic ring six siloxanes.
Dispersion agent is at least one in PEG-30 dimerization hydroxy stearic acid ester, poly-oxystearic acid, the smooth stearate of sorb, the smooth different hard acid esters of sorb, PEG-2 Witconol AL 69-66, PEG/PPG-18/18 polydimethylsiloxane, sucrose fatty ester.
Wherein, sucrose fatty ester is at least one in sucrose hard acid esters, Surfhope SE Cosme C 1616, Sugar Ester O 1570, sucrose erucate, Surfhope SE Cosme C 1216.
Stablizer is at least one in montmorillonite, organobentonite, silico-aluminate, silicate, aerosil, higher fatty acid.
Thickening material is at least one in cera alba, 80# Microcrystalline Wax, Ka Er ceresine, Magnesium Stearate, carnauba wax.
The pure oil pastes of high pigment content makeup formed accordingly, its pigment content is up to 65 ~ 85%, and pigment used, grease, dispersion agent, stablizer are all China cosmetic material name catalogues specifies operable raw material, the mill base solid content of working it out is high, good stability, security is high, strong covering power, safety non-toxic are easy to use, add easily dispersion well.
For the pure oil pastes of high pigment content makeup be made up of according to corresponding proportioning above-mentioned each component, this example also provides corresponding preparation method.This preparation method comprises the steps:
(1) each component is taken according to following parts by weight:
By grease, dispersion agent, thickening material, stablizer mixing, heated and stirred, obtains uniform oiliness dispersion medium; Here Heating temperature is 80 ~ 85 DEG C.
(2), under oiliness dispersion medium heated and stirred step (1) obtained, the colo(u)rant dispersion adding 65-85 part is mixed into pulpous state; Here Heating temperature is 80 ~ 85 DEG C.
(3) slurry step (2) obtained, by grinding distribution equipment dispersion 3-4 time, obtains the makeup oil pastes of required high pigment content.Here grinding distribution equipment is at least one in ball mill, colloidal mill, high speed shear dispersion emulsifying machine.
This preparation technology is simple and easy to produce, and is the best substitute of conventional powder pigment, is applicable to the field such as makeup, food.
Below in conjunction with specific embodiment, set forth the present invention further.Should be understood that these embodiments are only not used in for illustration of the present invention to limit the scope of the invention.The experimental technique of unreceipted actual conditions in the following example, measures according to national standard usually.If there is no corresponding national standard, then according to general international standard, normal condition or carry out according to the condition that manufacturer advises.Unless otherwise indicated, otherwise all numbers are weight part, and all per-cent is weight percentage.
Unless otherwise defined or described herein, all specialties used herein and scientific words and those skilled in the art the same meaning be familiar with.In addition any method similar or impartial to described content and material all can be applicable in the inventive method.
Embodiment 1
The formula (by weight percentage) of the pure oil pastes of high pigment content makeup in this example is as follows:
| Red iron oxide | 80％ |
| Isopropyl myristate | 18％ |
| PEG-30 dimerization hydroxy stearic acid ester | 0.9％ |
| Aerosil | 0.65％ |
| 80# Microcrystalline Wax | 0.45％ |
The preparation process of the pure oil pastes of high pigment content makeup in the present embodiment is as follows:
(1) take required Isopropyl myristate, PEG-30 dimerization hydroxy stearic acid ester, aerosil, 80# Microcrystalline Wax in proportion, mixing, heated and stirred at 85 DEG C, obtains homodisperse oil medium.
(2) by the oil medium that obtains under 80 DEG C of heated and stirred, red iron oxide is progressively added in oil medium, stirs and form paste slurry.
(3) by the paste slurry colloidal mill dispersion grinding that obtains 3-4 time, corresponding high pigment content makeup oil pastes is obtained.
The high pigment content red iron oxide mill base prepared according to the method described above takes on a red color paste, and easy to use, color and luster is excellent, does not produce dust, and the contact angle on water droplet and mill base surface is greater than 98 °, and water resistance is better.This mill base is handled as follows, comprises 50 DEG C of heat storages one month, normal temperature places 12 months ,-10 DEG C cold storage 24h, cold storage (-10 DEG C, 24h) is stored up (50 DEG C, 24h) 3 with heat and circulated, all without layering, floating oil, agglomeration.
Embodiment 2
The formula (by weight percentage) of the pure oil pastes of high pigment content makeup of this example is as follows:
| Iron oxide black | 80％ |
| Isopropyl myristate | 16.3％ |
| PEG-30 dimerization hydroxy stearic acid ester | 2.2％ |
| Aerosil | 0.7％ |
| 80# Microcrystalline Wax | 0.8％ |
The preparation method of the high pigment content makeup pure oil colours slurry in the present embodiment is as follows:
(1) take required Isopropyl myristate, PEG-30 dimerization hydroxy stearic acid ester, aerosil, 80# Microcrystalline Wax in proportion, mixing, heated and stirred at 85 DEG C, obtains homodisperse oil medium.
(2) by the oil medium that obtains under 80 DEG C of heated and stirred, iron oxide black is progressively added in oil medium, stirs and form paste slurry.
(3) by the paste slurry sand mill dispersion grinding that obtains 3-4 time, corresponding high pigment content makeup oil pastes is obtained.
The high pigment content iron oxide black mill base color shape darkly prepared according to the method described above, easy to use, color and luster is excellent, does not produce dust, and the contact angle on water droplet and mill base surface is greater than 98 °, and water resistance is better.This mill base is handled as follows, comprises 50 DEG C of heat storages one month, normal temperature places 12 months ,-10 DEG C cold storage 24h, cold storage (-10 DEG C, 24h) is stored up (50 DEG C, 24h) 3 with heat and circulated, all without layering, floating oil, agglomeration.
Embodiment 3
The formula (by weight percentage) of the high pigment content makeup pure oil colours slurry of this example is as follows:
| Iron oxide yellow | 65％ |
| Isopropyl myristate | 17.14％ |
| PEG-30 dimerization hydroxy stearic acid ester | 8.93％ |
| Sugar Ester O 1570 | 8.5％ |
| Magnesium Stearate | 0.43％ |
The preparation method of the high pigment content makeup oil pastes in the present embodiment is as follows:
(1) take required Isopropyl myristate, PEG-30 dimerization hydroxy stearic acid ester, Sugar Ester O 1570, Sugar Ester O 1570, Magnesium Stearate in proportion, mixing, heated and stirred at 85 DEG C, obtains homodisperse oil medium.
(2) by the oil medium that obtains under 80 DEG C of heated and stirred, iron oxide yellow is progressively added in oil medium, stirs and form paste slurry.
(3) by the paste slurry colloidal mill dispersion grinding that obtains 3-4 time, corresponding high pigment content makeup oil pastes is obtained.
The high pigment content iron oxide yellow mill base prepared according to the method described above is yellowish syrup, and easy to use, color and luster is excellent, does not produce dust, and the contact angle on water droplet and mill base surface is greater than 98 °, and water resistance is better.This mill base is handled as follows, comprises 50 DEG C of heat storages one month, normal temperature places 12 months ,-10 DEG C cold storage 24h, cold storage (-10 DEG C, 24h) is stored up (50 DEG C, 24h) 3 with heat and circulated, all without layering, floating oil, agglomeration.
Embodiment 4
The formula (by weight percentage) of the high pigment content makeup pure oil colours slurry of this example is as follows:
| Rutile type Titanium Dioxide | 80％ |
| Isopropyl myristate | 17.4％ |
| PEG-30 dimerization hydroxy stearic acid ester | 0.86％ |
| Aerosil | 0.87％ |
| 80# Microcrystalline Wax | 0.87％ |
The preparation method of the high pigment content makeup pure oil colours slurry of the present embodiment is as follows:
(1) take required Isopropyl myristate, PEG-30 dimerization hydroxy stearic acid ester, aerosil, 80# Microcrystalline Wax in proportion, mixing, heated and stirred at 85 DEG C, obtains homodisperse oil medium.
(2) by the oil medium that obtains under 80 DEG C of heated and stirred, Rutile type Titanium Dioxide is progressively added in oil medium, stirs and form paste slurry.
(3) by the paste slurry sand mill dispersion grinding that obtains 3-4 time, described high-content makeup oil pastes is obtained.
The high pigment content Rutile type Titanium Dioxide mill base prepared according to the method described above is white cream shape, and easy to use, color and luster is excellent, does not produce dust, and water droplet is greater than 98 ° with the contact angle starching surface in vain, and water resistance is better.To this in vain slurry be handled as follows, comprise 50 DEG C of heat storages one month, normal temperature place 12 months ,-10 DEG C cold storage 24h, cold storage (-10 DEG C, 24h) stores up (50 DEG C, 24h) 3 circulate, all without layering, floating oil, agglomeration with hot.
In addition, the performance of this example provides in mill base performance (as strong in tinting strength, covering power is high) existing commercially available mill base of comparing, has great raising.
For high pigment content Rutile type Titanium Dioxide slurry prepared by example 4, carry out the contrast experiment of covering power with commercially available titanium dioxide slurry.
This contrast experiment carries out according to the CNS of GBT5211.17-1988 white pigment contrast ratio (opacifying power).See Fig. 1, the high pigment content Rutile type Titanium Dioxide slurry of preparation in this example 4 shown in it and commercially available titanium dioxide slurry are schemed according to the Experimental comparison of GBT5211.17-1988 white pigment contrast ratio (opacifying power).
As seen from the figure, the high pigment content Rutile type Titanium Dioxide slurry prepared according to this example improves a lot relative to commercially available titanium dioxide slurry tool in covering power, reaches beyond thought excellent effect.
More than show and describe ultimate principle of the present invention, principal character and advantage of the present invention.The technician of the industry should understand; the present invention is not restricted to the described embodiments; what describe in above-described embodiment and specification sheets just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention.Application claims protection domain is defined by appending claims and equivalent thereof.
Claims (9)
1. the pure oily non-emulsified makeup mill base of high pigment content, it is characterized in that, described mill base is made up of the component of following parts by weight:
2. the pure oily non-emulsified makeup mill base of the high pigment content of one according to claim 1, it is characterized in that, described pigment is at least one in ferric oxide, chromic oxide, ultramarine, ferriferro cyanide, titanium dioxide.
3. the pure oily non-emulsified makeup mill base of the high pigment content of one according to claim 1, it is characterized in that, described dispersion agent is at least one in PEG-30 dimerization hydroxy stearic acid ester, poly-oxystearic acid, the smooth stearate of sorb, the smooth different hard acid esters of sorb, PEG-2 Witconol AL 69-66, PEG/PPG-18/18 polydimethylsiloxane, sucrose fatty ester.
4. the pure oily non-emulsified makeup mill base of the high pigment content of one according to claim 1, it is characterized in that, described thickening material is at least one in cera alba, 80# Microcrystalline Wax, Ka Er ceresine, Magnesium Stearate, carnauba wax.
5. the pure oily non-emulsified makeup mill base of the high pigment content of one according to claim 1, it is characterized in that, described stablizer is at least one in montmorillonite, organobentonite, silico-aluminate, silicate, aerosil, higher fatty acid.
6. the pure oily non-emulsified makeup mill base of the high pigment content of one according to claim 1, it is characterized in that, described grease is at least one in silicone oil, iso-octyl palmitate, caprylic/capric triglyceride, C12-C15 alcohol benzoic ether, iso-octyl palmitate, Isopropyl myristate.
7. a preparation method for the pure oily non-emulsified makeup mill base of the high pigment content according to any one of claim 1-6, it is characterized in that, described preparation method comprises the following steps:
(1) grease, dispersion agent, thickening material and stablizer that pure for high pigment content oiling cosmetic mill base comprises proportionally are mixed, heated and stirred, obtain uniform oiliness dispersion medium;
(2), under oiliness dispersion medium heated and stirred step (1) obtained, the colo(u)rant dispersion adding corresponding proportion is mixed into pulpous state;
(3) slurry grinding distribution step (2) obtained 3-4 time, obtains the makeup oil pastes of high pigment content.
8. the pure oily non-emulsified makeup mill base of the high pigment content of one according to claim 7, is characterized in that, the Heating temperature in described step (1) and (2) is 80 ~ 85 DEG C.
9. the preparation method of the pure oily non-emulsified makeup mill base of a kind of high pigment content according to claim 7, it is characterized in that, adopt grinding distribution equipment to disperse slurry in described step (3), described grinding distribution equipment is at least one in ball mill, colloidal mill, high speed shear dispersion emulsifying machine.
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107753303A (en) * | 2017-11-05 | 2018-03-06 | 滁州格锐矿业有限责任公司 | A kind of preparation technology of pigment used for cosmetic |
| CN109602625A (en) * | 2018-12-03 | 2019-04-12 | 广州市嘉菁化妆品有限公司 | A kind of mill base, preparation method and its application |
| CN109908031A (en) * | 2019-03-07 | 2019-06-21 | 浙江纳美新材料股份有限公司 | A kind of edible lipstick mill base and preparation method thereof |
| CN111449988A (en) * | 2020-04-17 | 2020-07-28 | 宁波爱诗化妆品有限公司 | Iron-based water-based pigment color paste for cosmetics, preparation method of iron-based water-based pigment color paste and preparation method of color cosmetic product |
| CN111607837A (en) * | 2019-02-22 | 2020-09-01 | 南亚塑胶工业股份有限公司 | Recycled polyester fiber |
| CN112190491A (en) * | 2020-10-15 | 2021-01-08 | 广州市科能化妆品科研有限公司 | High-dispersity cosmetic inorganic pigment color paste, and preparation method and application thereof |
| CN113230150A (en) * | 2021-03-19 | 2021-08-10 | 上海蔻沣生物科技有限公司 | Toner slurry composition and method of preparing the same |
| WO2024095598A1 (en) * | 2022-11-02 | 2024-05-10 | 日光ケミカルズ株式会社 | Method for producing oily dispersion, and cosmetic material having said oily dispersion blended therein |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107753303A (en) * | 2017-11-05 | 2018-03-06 | 滁州格锐矿业有限责任公司 | A kind of preparation technology of pigment used for cosmetic |
| CN109602625A (en) * | 2018-12-03 | 2019-04-12 | 广州市嘉菁化妆品有限公司 | A kind of mill base, preparation method and its application |
| CN111607837A (en) * | 2019-02-22 | 2020-09-01 | 南亚塑胶工业股份有限公司 | Recycled polyester fiber |
| CN111607837B (en) * | 2019-02-22 | 2022-12-20 | 南亚塑胶工业股份有限公司 | Recycled polyester fiber |
| CN109908031A (en) * | 2019-03-07 | 2019-06-21 | 浙江纳美新材料股份有限公司 | A kind of edible lipstick mill base and preparation method thereof |
| CN111449988A (en) * | 2020-04-17 | 2020-07-28 | 宁波爱诗化妆品有限公司 | Iron-based water-based pigment color paste for cosmetics, preparation method of iron-based water-based pigment color paste and preparation method of color cosmetic product |
| CN111449988B (en) * | 2020-04-17 | 2022-12-27 | 宁波爱诗化妆品有限公司 | Iron-based water-based pigment color paste for cosmetics, preparation method of color paste and preparation method of color cosmetic product |
| CN112190491A (en) * | 2020-10-15 | 2021-01-08 | 广州市科能化妆品科研有限公司 | High-dispersity cosmetic inorganic pigment color paste, and preparation method and application thereof |
| CN112190491B (en) * | 2020-10-15 | 2023-03-31 | 广州市科能化妆品科研有限公司 | High-dispersity cosmetic inorganic pigment color paste and preparation method and application thereof |
| CN113230150A (en) * | 2021-03-19 | 2021-08-10 | 上海蔻沣生物科技有限公司 | Toner slurry composition and method of preparing the same |
| WO2024095598A1 (en) * | 2022-11-02 | 2024-05-10 | 日光ケミカルズ株式会社 | Method for producing oily dispersion, and cosmetic material having said oily dispersion blended therein |
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