CN103483913B - A kind of oiliness purple blue paste and preparation method thereof - Google Patents
A kind of oiliness purple blue paste and preparation method thereof Download PDFInfo
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- CN103483913B CN103483913B CN201210193216.5A CN201210193216A CN103483913B CN 103483913 B CN103483913 B CN 103483913B CN 201210193216 A CN201210193216 A CN 201210193216A CN 103483913 B CN103483913 B CN 103483913B
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- Prior art keywords
- oiliness
- dispersant
- purple
- alkyd resin
- product
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- 238000002360 preparation method Methods 0.000 title description 12
- 239000002270 dispersing agent Substances 0.000 claims abstract description 19
- 229920000180 alkyd Polymers 0.000 claims abstract description 11
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 8
- 239000000203 mixture Substances 0.000 claims abstract description 8
- DKPFZGUDAPQIHT-UHFFFAOYSA-N Butyl acetate Natural products CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 claims abstract description 6
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 claims abstract description 6
- LLHKCFNBLRBOGN-UHFFFAOYSA-N propylene glycol methyl ether acetate Chemical compound COCC(C)OC(C)=O LLHKCFNBLRBOGN-UHFFFAOYSA-N 0.000 claims abstract description 5
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 2
- IPHJYJHJDIGARM-UHFFFAOYSA-M copper phthalocyaninesulfonic acid, dioctadecyldimethylammonium salt Chemical group [Cu+2].CCCCCCCCCCCCCCCCCC[N+](C)(C)CCCCCCCCCCCCCCCCCC.C=1C(S(=O)(=O)[O-])=CC=C(C(=NC2=NC(C3=CC=CC=C32)=N2)[N-]3)C=1C3=NC([C]1C=CC=CC1=1)=NC=1N=C1[C]3C=CC=CC3=C2[N-]1 IPHJYJHJDIGARM-UHFFFAOYSA-M 0.000 claims description 2
- 150000002333 glycines Chemical class 0.000 claims description 2
- NLZUEZXRPGMBCV-UHFFFAOYSA-N Butylhydroxytoluene Chemical group CC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 NLZUEZXRPGMBCV-UHFFFAOYSA-N 0.000 claims 1
- 235000010354 butylated hydroxytoluene Nutrition 0.000 claims 1
- 239000002002 slurry Substances 0.000 abstract description 6
- 238000010790 dilution Methods 0.000 abstract description 5
- 239000012895 dilution Substances 0.000 abstract description 5
- 239000000843 powder Substances 0.000 abstract 1
- CGLVZFOCZLHKOH-UHFFFAOYSA-N 8,18-dichloro-5,15-diethyl-5,15-dihydrodiindolo(3,2-b:3',2'-m)triphenodioxazine Chemical compound CCN1C2=CC=CC=C2C2=C1C=C1OC3=C(Cl)C4=NC(C=C5C6=CC=CC=C6N(C5=C5)CC)=C5OC4=C(Cl)C3=NC1=C2 CGLVZFOCZLHKOH-UHFFFAOYSA-N 0.000 description 6
- 239000006185 dispersion Substances 0.000 description 6
- 238000000034 method Methods 0.000 description 5
- 239000000463 material Substances 0.000 description 4
- 235000011837 pasties Nutrition 0.000 description 4
- 230000008569 process Effects 0.000 description 4
- 239000004576 sand Substances 0.000 description 4
- 230000008901 benefit Effects 0.000 description 3
- 238000000576 coating method Methods 0.000 description 3
- XCJYREBRNVKWGJ-UHFFFAOYSA-N copper(II) phthalocyanine Chemical compound [Cu+2].C12=CC=CC=C2C(N=C2[N-]C(C3=CC=CC=C32)=N2)=NC1=NC([C]1C=CC=CC1=1)=NC=1N=C1[C]3C=CC=CC3=C2[N-]1 XCJYREBRNVKWGJ-UHFFFAOYSA-N 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 239000011248 coating agent Substances 0.000 description 2
- 230000007812 deficiency Effects 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 238000010422 painting Methods 0.000 description 2
- 229920002126 Acrylic acid copolymer Polymers 0.000 description 1
- 241001597008 Nomeidae Species 0.000 description 1
- 235000003140 Panax quinquefolius Nutrition 0.000 description 1
- 240000005373 Panax quinquefolius Species 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- YENIOYBTCIZCBJ-UHFFFAOYSA-N acetic acid;1-methoxypropan-2-ol Chemical compound CC(O)=O.COCC(C)O YENIOYBTCIZCBJ-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000004816 latex Substances 0.000 description 1
- 229920000126 latex Polymers 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
Landscapes
- Compositions Of Macromolecular Compounds (AREA)
- Paints Or Removers (AREA)
- Developing Agents For Electrophotography (AREA)
Abstract
The invention provides a kind of oiliness purple blue paste.It is characterized in that being made up of following composition and percentage by weight: alkyd resin, propylene glycol methyl ether acetate, anti skinning agent, dispersant, collaborative dispersant, purple/blueness powder, the milled mixtures of butyl acetate.A kind of oiliness purple slurry of the present invention, has anti-loose colour, grows dim, and improves storage stability and the feature of dilution stability simultaneously.
Description
Technical field
The invention belongs to the technical field of coating, the present invention relates to a kind of oiliness purple blue paste and preparation method thereof.
Background technology
Now the oiliness purple blue paste of commercial type is all that to use alkyd resin or synthctic fat acid resin be raw material,
Add the product that wetting dispersing agent is formed to improve the dispersibility of toner.It has the advantages such as tinting strength, tinting power is good, covering power is good.Existing
It is very serious generally to there is loose colour, situation of growing dim in some oiliness purple blue paste, the drawback such as storage stability and dilution stability difference.
Summary of the invention
It is an object of the invention to, it is provided that a kind of oiliness purple blue paste.
It is an object of the invention to, it is provided that the preparation method of a kind of oiliness purple blue paste, to overcome existing for prior art
Disadvantages mentioned above and deficiency.The loose colour existed such as existing purple blue paste, situation of growing dim are serious, store process and dilution
The technological deficiency of precipitation occurs.
The present invention designs a kind of oiliness purple blue paste, it is characterised in that be made up of following composition and percentage by weight:
Alkyd resin 40%-60%,
Propylene glycol monomethyl ether acetic acid 15%-25%,
Anti skinning agent 0.05%-0.2%,
Dispersant 2%-5%,
Collaborative dispersant 0.5%-3%,
Purple/blue powder 10%-20%,
Butyl acetate 5%-15%.
Wherein, described alkyd resin is Oleum Glycines modified alkyd resin, can use the JD11-65H product of Zhan Chen coating group.
Wherein, described anti skinning agent is 2,6-di-tert-butyl-4-methy phenol, and the trade mark that can use bright Sheng chemical industry is BHT
Product.
Wherein, described dispersant is the acrylic acid copolymer soln of structure, can use the BYK2025 product of Bi Ke company.
Wherein, described collaborative dispersant is the derivant of pigment purple, blue, and the Solsperse 5000 of Lu Borun can be used to produce
Product.
The preparation method of a kind of oiliness purple blue paste, it is characterised in that comprise the steps of:
(1) various materials proportionally mix also high speed dispersion, and preparation becomes pasty product,
(2) then cross the fineness of sand mill extremely regulation, i.e. obtain qualified product.It is characterized in that: in step (1), institute
State is 1500 ~ 2000rpm at a high speed.It is characterized in that: in step (2), described fineness is 10 ~ 15 μm.
It is an advantage of the invention that the collaborative dispersant of employing, play and prevent from painting loose colour, growing dim and aid dispersion effect, have
Anti-loose colour, grow dim, stable storing and the feature of dilution stability.
Detailed description of the invention
Below in conjunction with specific embodiment, the invention will be further described.Should be understood that following example are merely to illustrate this
Invent not for limiting the scope of the present invention.
The experimental technique of unreceipted actual conditions in the following example, generally according to normal condition, or the bar that manufacturer provides
Part is carried out.
Embodiment 1
A kind of oiliness purple slurry formula (weight), oiliness permanent violet mill base.
Oiliness permanent violet mill base component and weight proportion are as follows:
Alkyd resin 40 kilograms, propylene glycol methyl ether acetate 25 kilograms, anti skinning agent 0.1 kilogram, dispersant 4 kilograms, association
With dispersant 0.9 kilogram, permanent violet toner 20 kilograms, butyl acetate 10 kilograms.
Preparation method:
(1) it is the most conventional physical mixing processes, will proportionally mix and 1800rpm high speed dispersion by various materials,
Preparation becomes pasty product,
(2) then sand mill excessively, to fineness 15 μm, i.e. obtains the product that double centner is qualified.
Embodiment 2
A kind of oiliness blueness slurry formula (weight): oiliness phthalocyanine blue mill base.
Oiliness phthalocyanine blue mill base component and weight proportion are as follows:
Alkyd resin 55 kilograms, propylene glycol methyl ether acetate 15 kilograms, anti skinning agent 0.1 kilogram, dispersant 4 kilograms, association
With dispersant 1.9 kilograms, phthalocyanine blue toner 20 kilograms, butyl acetate 5 kilograms.
Preparation method:
(1) it is the most conventional physical mixing processes, will proportionally mix and 2000rpm high speed dispersion by various materials,
Preparation becomes pasty product,
(2) then sand mill excessively, to fineness 15 μm, i.e. obtains the product that double centner is qualified.
Embodiment 3
A kind of oiliness purple slurry formula (weight), oiliness permanent violet mill base.
Oiliness permanent violet mill base component and weight proportion are as follows:
Alkyd resin 60 kilograms, propylene glycol methyl ether acetate 15 kilograms, anti skinning agent 0.1 kilogram, dispersant 4 kilograms, association
With dispersant 2.9 kilograms, permanent violet toner 11 kilograms, butyl acetate 9 kilograms.
Preparation method:
(1) it is the most conventional physical mixing processes, will proportionally mix and 1800rpm high speed dispersion by various materials,
Preparation becomes pasty product,
(2) then sand mill excessively, to fineness 15 μm, i.e. obtains the product that double centner is qualified.
Employing refers to grind experimental technique, GB/T21090-2007 " color-adjustable base latex coatings "-compatibility test method-refer to grind
The method characteristic whether having aberration, the product preparing the present invention is detected, and comparison uses Guangzhou, commercially available prod Ke Dise
Color company limited general oiliness purple slurry, general oiliness cyanic colours slurry.Result is as shown in table 1.
The detection of table 1 product
Can draw from each index of table 1, the present invention uses collaborative dispersant, plays and prevents from painting loose colour, growing dim also
The effect of aid dispersion.The present invention significantly improves than comparison effect.The oiliness purple blue paste of the present invention, has anti-loose colour, sends out
Flower, stable storing, tinting strength, tinting power be good and the feature of dilution stability.
The ultimate principle of the present invention, principal character and advantages of the present invention have more than been shown and described.The technology of the industry
Personnel, it should be appreciated that the present invention is not restricted to the described embodiments, simply illustrating this described in above-described embodiment and description
The principle of invention, the present invention also has various changes and modifications without departing from the spirit and scope of the present invention, and these become
Change and improvement both falls within scope of the claimed invention.Claimed scope by appending claims and
Equivalent defines.
Claims (1)
1. an oiliness purple blue paste, it is characterised in that be made up of following composition and percentage by weight:
Alkyd resin 40%-60%,
Propylene glycol methyl ether acetate 15%-25%,
Anti skinning agent 0.05%-0.2%,
Dispersant 2%-5%,
Collaborative dispersant 0.5%-3%,
Purple/blue powder 10%-20%,
Butyl acetate 5%-15%；
Described alkyd resin is Oleum Glycines modified alkyd resin；
Described anti skinning agent is 2,6 di tert butyl 4 methyl phenol；
Described dispersant is the BYK2025 product of Bi Ke company；
Described collaborative dispersant is Solsperse 5000 product of Lu Borun.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210193216.5A CN103483913B (en) | 2012-06-12 | 2012-06-12 | A kind of oiliness purple blue paste and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210193216.5A CN103483913B (en) | 2012-06-12 | 2012-06-12 | A kind of oiliness purple blue paste and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103483913A CN103483913A (en) | 2014-01-01 |
| CN103483913B true CN103483913B (en) | 2016-12-14 |
Family
ID=49824530
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210193216.5A Active CN103483913B (en) | 2012-06-12 | 2012-06-12 | A kind of oiliness purple blue paste and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103483913B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104865359A (en) * | 2015-05-11 | 2015-08-26 | 刘俊平 | Meal residue liquid regenerated oil dyeing agent |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1161437C (en) * | 2001-03-15 | 2004-08-11 | 海洋化工研究院 | Acrylic acid modified high-performance water-thinned alkyd enamal |
| US6736892B2 (en) * | 2001-07-19 | 2004-05-18 | Ethox Chemicals Llc | Pigment dispersions containing styrenated and sulfated phenol alkoxylates |
| JP4963031B2 (en) * | 2006-03-15 | 2012-06-27 | 花王株式会社 | Non-aqueous pigment dispersant |
| CN102120910B (en) * | 2011-01-24 | 2013-06-26 | 嘉宝莉化工集团股份有限公司 | Environmentally-friendly solvent type woodware coating with formaldehyde-absorbing function and preparation method thereof |
-
2012
- 2012-06-12 CN CN201210193216.5A patent/CN103483913B/en active Active
Also Published As
| Publication number | Publication date |
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| CN103483913A (en) | 2014-01-01 |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C53 | Correction of patent for invention or patent application | ||
| CB02 | Change of applicant information |
Address after: 8555 No. 201707 Shanghai city Qingpu District Songze Avenue Applicant after: Shanghai Zhanchen Paint Co., Ltd. Applicant after: Zhanchen Coatings Group Co., Ltd. Applicant after: Beijing Zhanchen Chemical Industry Co., Ltd. Applicant after: Qingdao Zhan Chen novel material company limited Applicant after: Chengdu Zhanchen Chemical Co., Ltd. Address before: 8555 No. 201707 Shanghai city Qingpu District Songze Avenue Applicant before: Shanghai Fuchen Chemical Co., Ltd. Applicant before: Zhanchen Coatings Group Co., Ltd. Applicant before: Beijing Zhanchen Chemical Industry Co., Ltd. Applicant before: Qingdao Fuchen Chemical Co., Ltd. Applicant before: Chengdu Zhanchen Chemical Co., Ltd. |
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| COR | Change of bibliographic data |
Free format text: CORRECT: APPLICANT; FROM: SHANGHAI FUCHEN CHEMICAL CO. LTD. TO: SHANGHAI ZHANCHEN PAINT CO., LTD. Free format text: CORRECT: APPLICANT; FROM: ZHANCHEN COATINGS GROUP CO., LTD. BEIJING ZHANCHEN CHEMICAL INDUSTRY CO., LTD. QINGDAO VISION CHEMICAL CO., LTD. CHENGDU ZHANCHEN CHEMICAL CO., LTD. TO: ZHANCHEN COATINGS GROUP CO., LTD. BEIJING ZHANCHEN CHEMICAL INDUSTRY CO., LTD. QINGDAO ZHANCHEN NEW MATERIAL CO., LTD. CHENGDU ZHANCHEN CHEMICAL CO., LTD. |
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| CB02 | Change of applicant information |
Address after: 8555 No. 201707 Shanghai city Qingpu District Songze Avenue Applicant after: Shanghai Zhanchen Paint Co., Ltd. Applicant after: CHINA ZHANCHEN PAINTS GROUP LTD. Applicant after: Beijing Zhan Chen novel material company limited Applicant after: Qingdao Zhan Chen novel material company limited Applicant after: Chengdu Zhan Chen coating company limited Address before: 8555 No. 201707 Shanghai city Qingpu District Songze Avenue Applicant before: Shanghai Zhanchen Paint Co., Ltd. Applicant before: Zhanchen Coatings Group Co., Ltd. Applicant before: Beijing Zhanchen Chemical Industry Co., Ltd. Applicant before: Qingdao Zhan Chen novel material company limited Applicant before: Chengdu Zhanchen Chemical Co., Ltd. |
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Effective date of registration: 20200513 Address after: 201799 8555 Songze Avenue, Qingpu District, Shanghai Co-patentee after: Zhuhai zhanchen New Material Co., Ltd Patentee after: SHANGHAI ZHANCHEN PAINT Co.,Ltd. Co-patentee after: QINGDAO ZHANCHEN NEW MATERIAL Co.,Ltd. Co-patentee after: CHENGDU ZHANCHEN PAINTS Co.,Ltd. Address before: 8555 No. 201707 Shanghai city Qingpu District Songze Avenue Co-patentee before: ZHANCHEN NEW MATERIAL GROUP Co.,Ltd. Patentee before: SHANGHAI ZHANCHEN PAINT Co.,Ltd. Co-patentee before: BEIJING ZHANCHEN NEW MATERIAL Co.,Ltd. Co-patentee before: QINGDAO ZHANCHEN NEW MATERIAL Co.,Ltd. Co-patentee before: CHENGDU ZHANCHEN PAINTS Co.,Ltd. |