CN108498373A - A kind of cosmetic lip and preparation method thereof - Google Patents

A kind of cosmetic lip and preparation method thereof Download PDF

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Publication number
CN108498373A
CN108498373A CN201810419659.9A CN201810419659A CN108498373A CN 108498373 A CN108498373 A CN 108498373A CN 201810419659 A CN201810419659 A CN 201810419659A CN 108498373 A CN108498373 A CN 108498373A
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Prior art keywords
cosmetic
color
lip
cosmetic lip
color material
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CN201810419659.9A
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CN108498373B (en
Inventor
张许昌
钱军
梅杰
邓攀攀
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Shenzhen Orchid Pavilion Science And Technology Co Ltd
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Shenzhen Orchid Pavilion Science And Technology Co Ltd
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Priority to CN201810419659.9A priority Critical patent/CN108498373B/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8105Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
    • A61K8/8111Homopolymers or copolymers of aliphatic olefines, e.g. polyethylene, polyisobutene; Compositions of derivatives of such polymers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/31Hydrocarbons
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/001Preparations for care of the lips

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Dermatology (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a kind of cosmetic lips of offer and preparation method thereof, which includes white oil, polyisobutene, octyl dodecanol, emollients, synthetic wax, beeswax, microwax, antioxidant, preservative, essence, color material.Synthetic wax fusing point is high in the compound system of the present invention, smear is good, cooling is rapid, good toughness, by the adjustment of component, being formed has compared with high-solidification point, can quickly solidify, the cerul system of colour mixture does not occur in the filling postcooling of multiple color, solves the mixed color phenomenon being susceptible in conventional formulation.Clearly, colour mixture, smooth surface, smearing be not uniformly, safe and non-toxic at the cosmetic lip color interface that preparation method through the invention obtains.

Description

A kind of cosmetic lip and preparation method thereof
Technical field
The present invention relates to cosmetic field, more particularly to a kind of cosmetic lip and preparation method thereof.
Background technology
Cosmetic lip is a necessity during we live, and moist, moisturizing and reparation are played to our lip Effect.It is well known that traditional cosmetic lip, based on white or other monochromes.As the development of beauty culture and people are given birth to The flat raising of running water, tone, formula and the function of cosmetic lip all have a greater change, requirement of the people to cosmetic lip It is higher and higher, in its effect, moistens, more pursues innovation in the demands such as color, so some people are the cosmetic lip the effect of Upper carry out reformed AHP, such as some sun compositions are added, make the cosmetic lip with sun-screening function;Some people are grown at it It is innovated above humidity, such as the grease or wax of certain plants property is added, moisten degree height, moistening effect is more preferable;For another example have A little people innovate in its color, such as increasing some shimmering powders keeps its color more gorgeous etc..
But innovation of the cosmetic lip on the market in color is seldom related to the adjustment to its number of colors and type, single The color of a product is all relatively simple on the whole, such as:Red, light pink, yellow etc..And when people need the lip of multiple color When cosmetic, needing to buy branched could meet its demand.But to accomplish a variety of face for occurring not obscuring on cosmetic lip The boundary of color, a variety of colors is clear, and beautiful appearance is very difficult.Also there are many companies and manufacturer to attempt exploitation before this It crosses such product, but usually colour mixture can all occur and the situation that makes product plain, therefore to accomplish that multiple color does not mix Confuse always a technological difficulties for being difficult to break through.
Invention content
A kind of the object of the present invention is to provide color interfaces clear, not colour mixture cosmetic lip and preparation method thereof.
To achieve the above object, the technical solution adopted by the present invention is:
A kind of cosmetic lip includes following components according to weight percent:
Preferably, synthetic wax is modified paraffin, i.e., the cosmetic lip includes following components according to weight percent: The white oil of 25%-50%, 20% polyisobutene, the octyl dodecanol of 8%-10%, the emollients of 5%-10%, 10%- 20% modified paraffin, the beeswax of 1%-5%, the microwax of 4%-8%, the antioxidant of 0.2%-0.6%, 0.1%- The color material of 0.5% preservative, the essence of 0.1%-0.5%, 0-0.5%.
Preferably, synthetic wax is polyethylene wax, i.e., the cosmetic lip includes following components according to weight percent: The white oil of 25%-50%, 20% polyisobutene, the octyl dodecanol of 8%-10%, the emollients of 5%-10%, 10%- 20% polyethylene wax, the beeswax of 1%-5%, the microwax of 4%-8%, the antioxidant of 0.2%-0.6%, 0.1%- The color material of 0.5% preservative, the essence of 0.1%-0.5%, 0-0.5%.
Preferably, synthetic wax includes modified paraffin and polyethylene wax, and modified paraffin accounts for the weight percent of cosmetic lip For 8%-15%, the weight percent that polyethylene wax accounts for cosmetic lip is 5%-8%, i.e., the cosmetic lip is according to weight hundred It includes following components to divide ratio:The white oil of 25%-50%, 20% polyisobutene, the octyl dodecanol of 8%-10%, 5%-10% Emollients, the modified paraffin of 8%-15%, the polyethylene wax of 5%-8%, the beeswax of 1%-5%, 4%-8% microwax, The color material of the antioxidant of 0.2%-0.6%, the preservative of 0.1%-0.5%, the essence of 0.1%-0.5%, 0-0.5%.
It is further preferred that emollients are at least one of ethylhexyl palmitate, Sodium Hyaluronate.
It is further preferred that antioxidant is at least one of tocopherol acetate, dibutyl hydroxy toluene.
It is further preferred that preservative includes at least one of Phenoxyethanol, ethylparaben.
It is further preferred that color material includes at least one of toner, color lake.
The preparation method of above-mentioned cosmetic lip, includes the following steps:
Step 1:White oil, polyisobutene, octyl dodecanol, emollients are added in reaction vessel, agitating and heating, are controlled Warm 95-100 DEG C;
Step 2:Synthetic wax, beeswax and microwax are added into reaction vessel, after being completely dissolved, is cooled to 80-90 DEG C;
Step 3:Antioxidant, antioxidant, essence, stirring is added;
Step 4:Color material is added, it is filling, it is cooling.
Preferably, step 4 includes taking color material, which is the color material of at least one color, and the color material is separately added into Into the different cast feeders of filling machine, control material mouth temperature is filling, cooling.
The beneficial effects of the invention are as follows:Synthetic wax fusing point is high in the compound system of the present invention, smear is good, cooling is rapid, Good toughness, by the adjustment of component, being formed has compared with high-solidification point, can quickly solidify, the filling postcooling of multiple color not The cerul system that colour mixture occurs, solves the mixed color phenomenon being susceptible in conventional formulation.Preparation method through the invention obtains Clearly, colour mixture, smooth surface, smearing be not uniformly, safe and non-toxic at the cosmetic lip color interface obtained.
Specific implementation mode
The technique effect of design and the generation of the present invention is clearly and completely described below with reference to embodiment, with It is completely understood by the purpose of the present invention, feature and effect.
Embodiment 1
A kind of cosmetic lip, gross mass 100kg, including:White oil 34kg, polyisobutene 20kg, octyl 12 Alcohol 10kg, ethylhexyl palmitate 10kg, modified paraffin 15kg, beeswax 3kg, microwax 6.8kg, tocopherol acetate 0.3kg, Phenoxyethanol 0.1kg, essence 0.3kg, toner 0.5kg.
The preparation method of the cosmetic lip, includes the following steps:
Step 1:34kg white oils, 20kg polyisobutene, 10kg octyl dodecanols, 10kg ethylhexyl palmitate are added Into reaction pot, unlatching is slowly stirred and heating equipment, 95-100 DEG C of temperature control;
Step 2:15kg modified paraffins, 3kg beeswaxs, 6.8kg microwaxes are added into reaction vessel, waits for that wax body system is complete Dissolving, unlatching are cooled to 80-90 DEG C;
Step 3:0.3kg tocopherol acetates, 0.1kg Phenoxyethanols and 0.3kg essence is added, stirs evenly;
Step 4:The toner of the color of a variety of needs is allocated according to demand;
Step 5:The total 0.5kg of the toner of different colours is added separately in each cast feeder of screw filler, is controlled Expect the temperature of mouth, starts filling;
Step 6:Filling postcooling is to get to the spiral helicine cosmetic lip of polychrome.
The concrete model of the modified paraffin used in the present embodiment is Polarwachs 30750, and the dropping point of the product is 105-115 DEG C, viscosity under the conditions of 100 DEG C is 7-16mPas.The modified paraffin is that addition polyalphaolefin is modified in paraffin The product of acquisition.Wherein, the monomer C atomicities of polyalphaolefin are more than 10.No. CAS of this modified paraffin be 8002-74-2, 68527-08-2。
Ensureing stabilization that traditional cosmetic lip has not according to product made from formula described in the present embodiment and step Cracking, smear uniformly, moisten lip care under the premise of so that occur multiple color on a product, color interface is clear, and can be with Mashed up different multiple color, color is more gorgeous, compensates for the single defect of traditional cosmetic lip color, meets people For the gorgeous demand of color, pursuit of the people for high-quality innovation life is more met.
Embodiment 2
A kind of cosmetic lip, gross mass 100kg, including:White oil 34kg, polyisobutene 20kg, octyl 12 Alcohol 10kg, ethylhexyl palmitate 10kg, beeswax 3kg, polyethylene wax 15kg, microwax 6.8kg, tocopherol acetate 0.3kg, Phenoxyethanol 0.1kg, essence 0.3kg, toner 0.5kg.
Embodiment 3
A kind of cosmetic lip, gross mass 100kg, including:White oil 34kg, polyisobutene 20kg, octyl 12 Alcohol 10kg, ethylhexyl palmitate 10kg, modified paraffin 10kg, beeswax 3kg, polyethylene wax 5kg, microwax 6.8kg, tocopherol Acetic acid esters 0.3kg, Phenoxyethanol 0.1kg, essence 0.3kg, toner 0.5kg.
The concrete model of the modified paraffin used in the present embodiment is Polarwachs 30919.Polarwachs 30919 Dropping point be 86-91 DEG C, 100 DEG C under the conditions of viscosity be 5-10mPas.This modified paraffin in paraffin also in adding The product of the modified acquisition of polyalphaolefin.Wherein, the monomer C atomicities of polyalphaolefin are more than 10.No. CAS of this modified paraffin be 8002-74-2、68527-08-2。
Embodiment 4
The cosmetic lip of 1. different formulations of table
Component It is formulated 1 (%) It is formulated 2 (%) It is formulated 3 (%) It is formulated 4 (%)
White oil 20-50 20-50 20-50 20-50
Polyisobutene 10-20 10-20 10-20 10-20
Vaseline 8-10 / / /
Octyl dodecanol / 8-10 8-10 8-10
Ethylhexyl palmitate 5-10 5-10 5-10 5-10
Ceresin 8-15 / / /
Modified paraffin / 10-20 8-15
Beeswax 3-5 1-5 1-5 1-5
Polyethylene wax / / 10-20 5-8
Microwax 4-8 4-8 4-8 4-8
Tocopherol acetate 0.3 0.3 0.3 0.3
Phenoxyethanol 0.1 0.1 0.1 0.1
Essence 0.3 0.3 0.3 0.3
Toner 0-0.5 0-0.5 0-0.5 0-0.5
A kind of formula 1 of cosmetic lip exists in the prior art, 1 a kind of cosmetic lip is prepared according to formula, such as with Lower comparative example 1:
Comparative example 1:
A kind of cosmetic lip, gross mass 100kg, including:White oil 34kg, polyisobutene 20kg, vaseline 10kg, ethylhexyl palmitate 10kg, ceresin 15kg, beeswax 3kg, microwax 6.8kg, tocopherol acetate 0.3kg, benzene oxygen Ethyl alcohol 0.1kg, essence 0.3kg, toner 0.5kg.
The fusing point of product made from comparative example 1 is at 62-68 DEG C, the liquid condition of product different colours in preparation process Raw material will appear phenomenon of dissolving each other when filling simultaneously, and cooled and solidified process needs to complete for several minutes, also can in the process So that colour mixture occurs for the raw material of different colours, therefore also there is the case where multiple color is not obscured with regard to extremely difficult in product obtained.
We improve formula 1, obtain formula 2.In formula 2, we have changed ceresin into modified stone Wax.A kind of cosmetic lip such as embodiment 1,30750 fusing points of modified paraffin Polarwachs used are prepared according to the formula Height demoulds, and smear is good, and product multiple color interface made from embodiment 1 is clear, but lotion cooling is still not fast enough Speed, and Individual colours still have slight colour mixture.In addition, product is cracking, toughness and ductility are bad, too crisp.
We further improve formula 2, obtain formula 3.In formula 3, we change modified paraffin into Polyethylene wax.A kind of cosmetic lip such as embodiment 2 is prepared according to the formula, polyethylene wax cooling is rapid, fusing point is high, toughness It is good.Color interface is clear after product made from embodiment 2 is filling, not colour mixture, but product stripping is bad, and smear is poor, and It is harder.
Therefore, we further improve formula 3, and modified paraffin and polyethylene wax are compounded, and obtain Formula 4.Prepare a kind of cosmetic lip such as embodiment 3 according to the formula reduces modified paraffin compared with Example 2 Dosage, modified paraffin can also utilize the Polarwachs30750 in embodiment 1, or will in addition to Polarwachs 30919 The two is used in mixed way.This formula has both the advantages of modified paraffin and polyethylene wax, and product stabilization obtained is not cracked, smeared Even, solidification point is higher, rapid cooling not colour mixture after multiple color is filling.For the fusing point of the formula at 70-75 DEG C, solidification is rapid, system It is 3-5 DEG C higher than the solidification point of product that filling temperature is controlled during standby so that material body solidifies at once upon mixing, makes difference with this The material body of color is difficult to colour mixture situation occur.
Embodiment 3
A kind of cosmetic lip, gross mass 100kg, including:White oil 25.8kg, polyisobutene 20kg, octyl ten Glycol 10kg, ethylhexyl palmitate 10kg, modified paraffin 15kg, beeswax 5kg, polyethylene wax 5kg, microwax 8kg, tocopherol Acetic acid esters 0.3kg, Phenoxyethanol 0.1kg, essence 0.3kg, toner 0.5kg.
Embodiment 4
A kind of cosmetic lip, gross mass 100kg, including:White oil 48kg, polyisobutene 20kg, octyl 12 Alcohol 8kg, ethylhexyl palmitate 5kg, modified paraffin 8kg, beeswax 1kg, polyethylene wax 5kg, microwax 4kg, tocopheryl acetate Ester 0.3kg, Phenoxyethanol 0.2kg, essence 0.3kg, toner 0.2kg.
Embodiment 5
A kind of cosmetic lip, gross mass 100kg, including:White oil 44.45kg, polyisobutene 20kg, octyl ten Glycol 8kg, ethylhexyl palmitate 5kg, modified paraffin 8kg, beeswax 1kg, polyethylene wax 8kg, microwax 4kg, tocopherol second Acid esters 0.03kg, Phenoxyethanol 0.5kg, essence 0.5kg, toner 0.5kg.
Embodiment 6
A kind of cosmetic lip, gross mass 100kg, including:White oil 46.4kg, polyisobutene 10kg, octyl ten Glycol 10kg, ethylhexyl palmitate 10kg, modified paraffin 10kg, beeswax 5kg, microwax 8kg, tocopherol acetate 0.3kg, Phenoxyethanol 0.1kg, essence 0.1kg, toner 0.1kg.
Embodiment 7
A kind of cosmetic lip, gross mass 100kg, including:White oil 46.4kg, polyisobutene 10kg, octyl ten Glycol 10kg, Sodium Hyaluronate 10kg, beeswax 5kg, polyethylene wax 10kg, microwax 8kg, dibutyl hydroxy toluene 0.3kg, Buddhist nun The golden ethyl ester 0.1kg, essence 0.15kg, color lake 0.05kg of pool.
The above description is merely a specific embodiment, but scope of protection of the present invention is not limited thereto, any Belong to those skilled in the art in the technical scope disclosed by the present invention, the change or replacement that can be readily occurred in all are answered It is included within the scope of the present invention.Therefore, protection scope of the present invention should be subject to the protection scope in claims.

Claims (10)

1. a kind of cosmetic lip, which is characterized in that according to weight percent include following components:
2. cosmetic lip according to claim 1, which is characterized in that the synthetic wax is modified paraffin.
3. cosmetic lip according to claim 1, which is characterized in that the synthetic wax is polyethylene wax.
4. cosmetic lip according to claim 1, which is characterized in that the synthetic wax is modified paraffin and polyethylene Wax, the weight percent that the modified paraffin accounts for the cosmetic lip are 8%-15%, and the polyethylene wax accounts for the lip and uses The weight percent of cosmetics is 5%-8%.
5. according to claim 1-4 any one of them cosmetic lips, which is characterized in that the emollients are palm acid ethyl At least one of own ester, Sodium Hyaluronate.
6. according to claim 1-4 any one of them cosmetic lips, which is characterized in that the antioxidant is tocopherol second At least one of acid esters, dibutyl hydroxy toluene.
7. according to claim 1-4 any one of them cosmetic lips, which is characterized in that the preservative be Phenoxyethanol, At least one of ethylparaben.
8. according to claim 1-4 any one of them cosmetic lips, which is characterized in that the color material is in toner, color lake At least one.
9. the preparation method of claim 1-8 any one of them cosmetic lips, which is characterized in that include the following steps:
Step 1:White oil, polyisobutene, octyl dodecanol, emollients are added in reaction vessel, agitating and heating, temperature control 95- 100℃;
Step 2:Synthetic wax, microwax and beeswax are added into reaction vessel, after being completely dissolved, is cooled to 80-90 DEG C;
Step 3:Antioxidant, preservative, essence, stirring is added;
Step 4:Color material is added, it is filling, it is cooling.
10. preparation method according to claim 9, which is characterized in that the step 4 is specially:Take color material, the color Material is the color material of at least one color, and the color material is added separately in the different cast feeders of filling machine, control material mouth temperature, It is filling, it is cooling.
CN201810419659.9A 2018-05-04 2018-05-04 Lip cosmetic and preparation method thereof Active CN108498373B (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110693765A (en) * 2019-10-09 2020-01-17 刘后伟 Technology for producing gradient lipstick by fusing oil wax matrixes with different properties

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Publication number Priority date Publication date Assignee Title
CN1338919A (en) * 1999-12-02 2002-03-06 株式会社资生堂 Composition for lipstick
US20110250151A1 (en) * 2010-04-07 2011-10-13 Jeen International Cold process water soluble wax containing powders
CN102228413A (en) * 2011-06-29 2011-11-02 天津天狮生物发展有限公司 Lipstick and its preparation method
CN107375037A (en) * 2017-08-25 2017-11-24 漳浦彩露华化妆品有限公司 A kind of color-changing lipstick and preparation method thereof
CN107569406A (en) * 2017-08-25 2018-01-12 漳浦彩露华化妆品有限公司 A kind of lip film and preparation method thereof

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1338919A (en) * 1999-12-02 2002-03-06 株式会社资生堂 Composition for lipstick
US20110250151A1 (en) * 2010-04-07 2011-10-13 Jeen International Cold process water soluble wax containing powders
CN102228413A (en) * 2011-06-29 2011-11-02 天津天狮生物发展有限公司 Lipstick and its preparation method
CN107375037A (en) * 2017-08-25 2017-11-24 漳浦彩露华化妆品有限公司 A kind of color-changing lipstick and preparation method thereof
CN107569406A (en) * 2017-08-25 2018-01-12 漳浦彩露华化妆品有限公司 A kind of lip film and preparation method thereof

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110693765A (en) * 2019-10-09 2020-01-17 刘后伟 Technology for producing gradient lipstick by fusing oil wax matrixes with different properties

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