CN109602625A - A kind of mill base, preparation method and its application - Google Patents
A kind of mill base, preparation method and its application Download PDFInfo
- Publication number
- CN109602625A CN109602625A CN201811467622.XA CN201811467622A CN109602625A CN 109602625 A CN109602625 A CN 109602625A CN 201811467622 A CN201811467622 A CN 201811467622A CN 109602625 A CN109602625 A CN 109602625A
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- CN
- China
- Prior art keywords
- mill base
- toner
- preparation
- parts
- weight
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 239000002537 cosmetic Substances 0.000 claims abstract description 17
- WWZKQHOCKIZLMA-UHFFFAOYSA-M octanoate Chemical compound CCCCCCCC([O-])=O WWZKQHOCKIZLMA-UHFFFAOYSA-M 0.000 claims abstract description 9
- TXBCBTDQIULDIA-UHFFFAOYSA-N 2-[[3-hydroxy-2,2-bis(hydroxymethyl)propoxy]methyl]-2-(hydroxymethyl)propane-1,3-diol Chemical group OCC(CO)(CO)COCC(CO)(CO)CO TXBCBTDQIULDIA-UHFFFAOYSA-N 0.000 claims abstract description 8
- 150000001875 compounds Chemical class 0.000 claims abstract description 8
- 239000000203 mixture Substances 0.000 claims abstract description 8
- GKAVWWCJCPVMNR-UHFFFAOYSA-N tridecyl octadecanoate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCCCCCCCCCCCCC GKAVWWCJCPVMNR-UHFFFAOYSA-N 0.000 claims abstract description 6
- PDYOTPOJFZAOIS-UHFFFAOYSA-N decanoic acid;2,2-dimethylpropane-1,3-diol;octanoic acid Chemical compound OCC(C)(C)CO.CCCCCCCC(O)=O.CCCCCCCCCC(O)=O PDYOTPOJFZAOIS-UHFFFAOYSA-N 0.000 claims abstract description 5
- 238000009417 prefabrication Methods 0.000 claims abstract description 4
- 239000000654 additive Substances 0.000 claims description 10
- 230000000996 additive effect Effects 0.000 claims description 10
- 150000002148 esters Chemical class 0.000 claims description 2
- 239000002253 acid Substances 0.000 claims 1
- GHVNFZFCNZKVNT-UHFFFAOYSA-N decanoic acid Chemical compound CCCCCCCCCC(O)=O GHVNFZFCNZKVNT-UHFFFAOYSA-N 0.000 abstract description 3
- WFXHUBZUIFLWCV-UHFFFAOYSA-N (2,2-dimethyl-3-octanoyloxypropyl) octanoate Chemical group CCCCCCCC(=O)OCC(C)(C)COC(=O)CCCCCCC WFXHUBZUIFLWCV-UHFFFAOYSA-N 0.000 abstract 1
- 239000006185 dispersion Substances 0.000 description 7
- 239000002270 dispersing agent Substances 0.000 description 6
- 239000000463 material Substances 0.000 description 5
- 239000004615 ingredient Substances 0.000 description 4
- 229940049920 malate Drugs 0.000 description 4
- BJEPYKJPYRNKOW-UHFFFAOYSA-L malate(2-) Chemical compound [O-]C(=O)C(O)CC([O-])=O BJEPYKJPYRNKOW-UHFFFAOYSA-L 0.000 description 4
- 239000002994 raw material Substances 0.000 description 4
- 238000000034 method Methods 0.000 description 3
- 238000009736 wetting Methods 0.000 description 3
- WNWHHMBRJJOGFJ-UHFFFAOYSA-N 16-methylheptadecan-1-ol Chemical compound CC(C)CCCCCCCCCCCCCCCO WNWHHMBRJJOGFJ-UHFFFAOYSA-N 0.000 description 2
- 238000005119 centrifugation Methods 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 125000003636 chemical group Chemical group 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- UIVPNOBLHXUKDX-UHFFFAOYSA-N 3,5,5-trimethylhexyl 3,5,5-trimethylhexanoate Chemical compound CC(C)(C)CC(C)CCOC(=O)CC(C)CC(C)(C)C UIVPNOBLHXUKDX-UHFFFAOYSA-N 0.000 description 1
- OQILCOQZDHPEAZ-UHFFFAOYSA-N Palmitinsaeure-octylester Natural products CCCCCCCCCCCCCCCC(=O)OCCCCCCCC OQILCOQZDHPEAZ-UHFFFAOYSA-N 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000004359 castor oil Substances 0.000 description 1
- 235000019438 castor oil Nutrition 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000006471 dimerization reaction Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- GJQLBGWSDGMZKM-UHFFFAOYSA-N ethylhexyl palmitate Chemical compound CCCCCCCCCCCCCCCC(=O)OC(CC)CCCCC GJQLBGWSDGMZKM-UHFFFAOYSA-N 0.000 description 1
- 239000012847 fine chemical Substances 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 1
- 229940100554 isononyl isononanoate Drugs 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 150000004701 malic acid derivatives Chemical class 0.000 description 1
- 239000002480 mineral oil Substances 0.000 description 1
- 235000010446 mineral oil Nutrition 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 210000004906 toe nail Anatomy 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Emergency Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a kind of mill base, preparation method and its application, mill base includes component by weight: 5-75 parts of tridecanol trimellitate；1-20 parts of tridecanol stearate；Six caprylate of dipentaerythritol/1-15 parts of six decylate；Neopentyl glycol dicaprylate/5-40 parts of dicaprate；20-85 parts of toner；Preparation method includes: prefabrication step: tridecanol trimellitate, tridecanol stearate, six caprylate of dipentaerythritol/six decylates and neopentyl glycol dicaprylate/dicaprate being mixed, compound lard is obtained；Toner adds step: toner being added in compound lard, mill base is obtained after homogeneous；Mill base is applied in cosmetic composition, and stability is good, deposited phenomenon does not occur, and mobility is good.
Description
Technical field
The present invention relates to a kind of mill base, preparation method and its applications, belong to cosmetics additive technical field.
Background technique
Cosmetics refer to any position that human body surface is interspersed among with smearing, sprinkling or other similar method, such as skin
Skin, hair refer to toenail, lips and teeth etc., to reach cleaning, maintenance, beauty, modification and change appearance, or amendment human scent, it protects
Hold the chemical industrial product or fine chemical product for the purpose of kilter.Therefore, cosmetics usually unavoidably add toner, color
Slurry etc., to adjust the color of cosmetics, plays better modification.
Existing mill base used for cosmetic is with mineral oil, ethylhexyl palmitate, isononyl isononanoate, castor oil, two mostly
The monomer or mixture combination toner of the greases such as isooctadecanol malate, obtain the finely dispersed mill base of toner.But this point
Scattered mill base has the disadvantage that: first is that stability is insufficient, it may appear that deposit clumps phenomenon；Second is that poor fluidity, is unfavorable for being added to
In the various base-materials for needing to colour；Third is that the content of toner cannot be excessively high, excessively high then poor dispersion, therefore usually 20-
40%, cause the amount for the dispersion pulp being added in base-material can be larger, influences the use feeling of cosmetics finished product, intractable, easily floating powder,
Shedding etc..
Summary of the invention
For overcome the deficiencies in the prior art, the first purpose of this invention is to provide a kind of mill base, which stablizes
Property it is good, do not occur deposited phenomenon, and mobility is good, can be used as additive and be added in various cosmetics.
Second object of the present invention is to provide a kind of preparation method of above-mentioned mill base.
Third object of the present invention is to provide a kind of application of above-mentioned mill base.
Realize that the first purpose of this invention can reach by adopting the following technical scheme that: a kind of mill base, including by weight
Measure the following components of part meter:
Further, including following components by weight:
Further, including following components by weight:
Further, including following components by weight:
Further, toner is organic toner.
Further, toner is inorganic toner.
Further, the viscosity of mill base is less than 20000cps.
Realize that second object of the present invention can reach by adopting the following technical scheme that: a kind of mill base as described above
Preparation method, comprising:
Prefabrication step: by tridecanol trimellitate, tridecanol stearate, six caprylate of dipentaerythritol/
Six decylates and neopentyl glycol dicaprylate/dicaprate mixing, obtain compound lard；
Toner adds step: toner being added in compound lard, mill base is obtained after homogeneous.
Realize that third object of the present invention can reach by adopting the following technical scheme that: a kind of mill base as described above
Application, for by mill base be applied to cosmetic composition in.
Further, the additive amount of mill base is the 5-15% of cosmetic combinations amount of substance.
Compared with prior art, the beneficial effects of the present invention are:
1, stability of pigment paste of the present invention is good, is not in deposited phenomenon；
2, mill base good dispersion of the present invention, good fluidity can be used as additive and be added in various base material of cosmetics, preparation
Cosmetics, it is easy to use；
3, mill base of the present invention is still able to maintain good dispersibility in the case where fat content is low, toner content is high, is concentrated
Degree is high, then can substantially reduce the adding ingredient in base material of cosmetics, reduces influence of the mill base to the use feeling of base-material.
Detailed description of the invention
Fig. 1 is the picture after mill base centrifugation；
Fig. 2 is the picture of mill base smear；
Fig. 3 is the spreadable picture of embodiment lipstick；
Fig. 4 is the spreadable picture of comparative example lipstick.
Specific embodiment
In the following, being described further in conjunction with specific embodiment to the present invention:
A kind of mill base, including following components by weight:
Mill base is prepared by the following method to obtain:
Prefabrication step: by tridecanol trimellitate, tridecanol stearate, six caprylate of dipentaerythritol/
Six decylates and neopentyl glycol dicaprylate/dicaprate mixing, obtain compound lard；
Toner adds step: toner being added in compound lard, mill base is obtained after homogeneous.
The usage mode of mill base are as follows: can be used as additive and be added in cosmetic composition, additive amount is cosmetic composition
The 5-15% of quality.
Play the role of the ingredient of aid dispersion: tridecanol trimellitate, tridecanol stearate, dimerization in mill base
Six caprylate of pentaerythrite/six decylates and neopentyl glycol dicaprylate/dicaprate, the stability of mill base mainly with toner and
The energy of dispersing agent is related, and the chemical group of toner surface is consistent with the matching of the chemical group power in dispersing agent, if point
Powder is bad to the degree of wetting of toner surface, and dispersant group is inadequate to the adhesive force of toner surface, and dispersing agent is from toner surface
It falls off, that mill base loses stability just to deposited phenomenon occur.Six caprylate of dipentaerythritol/six decylates are a kind of
Mixed ester has the characteristic of dispersion, attachment, by can ensure that dispersing agent can be uniform with the synergy of other three kinds of ingredients
The surface of toner is covered on to reach sufficiently wetting and toner does not reassociate, stability is good, mill base of good dispersion to be formed.?
In the case that other three kinds of Ingredient Amounts are constant, when six caprylate of dipentaerythritol/six decylate additive amounts are less than 1 part,
The mill base of preparation has unstable phenomenon；When six caprylate of dipentaerythritol/six decylate additive amounts are greater than 15 parts, system
Standby mill base also has unstable phenomenon.It is optimal to the dispersion of toner, stable effect between additive amount 1-15.
Embodiment 1:
A kind of mill base, including following components by weight:
Mill base is prepared by the preparation step in specific embodiment.
Embodiment 2:
A kind of mill base, including following components by weight:
Mill base is prepared by the preparation step in specific embodiment.
The viscosity of mill base is 7500cps in embodiment 1, and the viscosity of mill base is 18000cps in embodiment 2, is carried out to mill base
Centrifugal test carries out centrifugation test in 1 hour with the revolving speed of 3000rpm, and observation result does not have deposited phenomenon, and mill base is stablized (such as
Shown in Fig. 1)；Observed with glass slide: toner is evenly distributed in dispersing agent, without clustering phenomena (as shown in Figure 2).
Embodiment 1, embodiment 2 are distinguished in its raw material that lipstick is added, additional amount is the 12% of total raw material quality, is made into
Lipstick finished product.
Mill base is prepared as a comparison case with diisooctadecanol malate+toner, due to diisooctadecanol malate point
The ability for dissipating toner is poor, so 30 parts of diisooctadecanol malate cannot can not be prepared 70 parts of toner complete wetting
At mill base, therefore uses 60 parts of diisooctadecanol malates instead and 40 parts of toner is added to prepare mill base.By conversion scale, it is added into
In the raw material of lipstick, needing additional amount is the 21% of total mass of raw material, the addition 12% that can be just made into mill base of the present invention
Toner amount is consistent.
The product of the closer former lipstick formula of embodiment 1, the lipstick color development degree more preferable (as shown in Figure 3) of embodiment 2, use feeling
Matter；And then color development degree is poor (as shown in Figure 4) for comparative example 1, and greasy feeling is heavier, influences the use feeling of original formulation lipstick.
For those skilled in the art, it can make other each according to the above description of the technical scheme and ideas
Kind is corresponding to be changed and deforms, and all these change and deform the protection model that all should belong to the claims in the present invention
Within enclosing.
Claims (10)
1. a kind of mill base, which is characterized in that including following components by weight:
2. mill base as described in claim 1, which is characterized in that including following components by weight:
3. mill base as described in claim 1, which is characterized in that including following components by weight:
4. mill base as described in claim 1, which is characterized in that including following components by weight:
5. mill base as described in claim 1, which is characterized in that the toner is organic toner.
6. mill base as described in claim 1, which is characterized in that the toner is inorganic toner.
7. mill base as described in claim 1, which is characterized in that the viscosity of the mill base is less than 20000cps.
8. a kind of preparation method of mill base as described in claim 1, characterized by comprising:
Prefabrication step: by tridecanol trimellitate, tridecanol stearate, six caprylate of dipentaerythritol/six last of the ten Heavenly stems
Acid esters and neopentyl glycol dicaprylate/dicaprate mixing, obtain compound lard；
Toner adds step: toner being added in compound lard, mill base is obtained after homogeneous.
9. a kind of application of mill base as described in claim 1, which is characterized in that for mill base is applied to cosmetic composition
In.
10. the application of mill base as claimed in claim 9, which is characterized in that the additive amount of the mill base is cosmetic composition
The 5-15% of quality.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811467622.XA CN109602625A (en) | 2018-12-03 | 2018-12-03 | A kind of mill base, preparation method and its application |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811467622.XA CN109602625A (en) | 2018-12-03 | 2018-12-03 | A kind of mill base, preparation method and its application |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109602625A true CN109602625A (en) | 2019-04-12 |
Family
ID=66006287
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811467622.XA Pending CN109602625A (en) | 2018-12-03 | 2018-12-03 | A kind of mill base, preparation method and its application |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109602625A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112274444A (en) * | 2020-11-23 | 2021-01-29 | 雅纯(广州)生物技术有限公司 | Toner for color cosmetics and preparation method thereof |
| CN116327619A (en) * | 2023-01-10 | 2023-06-27 | 娇时日化（杭州）股份有限公司 | Moisturizing lipstick and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105331200A (en) * | 2015-11-13 | 2016-02-17 | 上海联锴日用化工有限公司 | High-pigment-content pure oil non-emulsification cosmetic color paste and preparation method |
| CN107903718A (en) * | 2017-12-01 | 2018-04-13 | 常德金德新材料科技股份有限公司 | A kind of aqueous color paste and preparation method thereof |
| CN108272648A (en) * | 2018-03-26 | 2018-07-13 | 上海蔻沣生物科技有限公司 | Cosmetics powder, oil pastes and preparation method thereof |
-
2018
- 2018-12-03 CN CN201811467622.XA patent/CN109602625A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105331200A (en) * | 2015-11-13 | 2016-02-17 | 上海联锴日用化工有限公司 | High-pigment-content pure oil non-emulsification cosmetic color paste and preparation method |
| CN107903718A (en) * | 2017-12-01 | 2018-04-13 | 常德金德新材料科技股份有限公司 | A kind of aqueous color paste and preparation method thereof |
| CN108272648A (en) * | 2018-03-26 | 2018-07-13 | 上海蔻沣生物科技有限公司 | Cosmetics powder, oil pastes and preparation method thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112274444A (en) * | 2020-11-23 | 2021-01-29 | 雅纯(广州)生物技术有限公司 | Toner for color cosmetics and preparation method thereof |
| CN116327619A (en) * | 2023-01-10 | 2023-06-27 | 娇时日化（杭州）股份有限公司 | Moisturizing lipstick and preparation method thereof |
| CN116327619B (en) * | 2023-01-10 | 2024-02-13 | 娇时日化（杭州）股份有限公司 | Moisturizing lipstick and preparation method thereof |
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| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20190412 |
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| RJ01 | Rejection of invention patent application after publication |