CN109881488A - A kind of high-strength anti-flaming non-woven fabrics and preparation method thereof - Google Patents
A kind of high-strength anti-flaming non-woven fabrics and preparation method thereof Download PDFInfo
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Abstract
The present invention provides a kind of high-strength anti-flaming non-woven fabrics and preparation method thereof, is related to non-woven fabrics processing technique field.The non-woven fabrics is made of raw material from the following weight: 12-15 parts of polypropylene, 10-12 parts of polyethylene terephthalate, 2-4 parts of polyacrylonitrile, 1-2 parts of Butylated Hydroxytoluene, 4-6 parts of gypsum fiber, 2-4 parts of hydroxyethyl cellulose, 1-3 parts of aluminum phosphate, 0.4-0.8 parts of thioacetamide, 0.2-0.8 parts of casein, 15-20 parts of aqueous polyurethane, 2-3 parts of hydroxy-ethyl acrylate, 1-2 parts of antimony oxide, 1-2 parts of sodium metasilicate, 1-3 parts of triphenyl phosphate, 0.4-0.6 parts of defoaming agent.The present invention overcomes the deficiencies in the prior art, improve the intensity of traditional non-woven cloth, enhance its tensile capacity, and promote flame retardant property by impregnating fire resistant fluid, reinforce the using effect of non-woven fabrics.
Description
Technical field
The present invention relates to non-woven fabrics processing technique fields, and in particular to a kind of high-strength anti-flaming non-woven fabrics and its preparation side
Method.
Background technique
Non-woven fabrics be by include chemical fibre and plant fiber etc. under conditions of using water or air as suspension media
It is made on wet process or dry method paper machine, though without weaving therefore non-woven fabrics is called for cloth.Non-woven fabrics is environment-friendly materials of new generation,
Have many advantages, such as good, the antibacterial waterproof of strength, environmental protection, flexible, non-toxic and tasteless and cheap, and nonwovens markets demand is wide,
The wide modern material industry of coverage, is developing at an amazing speed, is known as " rising industry " of textile limit.
Due to the superior function of nonwoven cloth material, logical produce of non-woven fabrics can be used to prepare some daily necessities, and non-woven fabrics
Product is rich in color, bright-coloured bright and beautiful, Eco-Fashion, widely used, beautiful and generous, and pattern and style are all various, and light, ring
It protects, is recyclable, being the environment-friendly products for ecology of preserving our planet by internationally recognized.Suitable for agricultural film, shoemaking, process hides, bed
Pad, child-mother-covering, decoration, chemical industry, printing, automobile, building materials, the industries such as furniture and dress lining cloth, health care disposable surgical
Clothing, mask, cap, sheet, the disposable tablecloth in hotel, beauty, the gift bag of Saunas or even current fashion, fine work bag, shopping bag, extensively
Accuse bag etc..But bonded fabric product is low compared to the intensity of textile cloth, the field high for some intensity requirements is just no longer suitable
With, it is therefore desirable to a kind of high strength non-woven fabric, and it is also to study now that the flame retardant property for promoting non-woven fabrics, which enhances its safety,
A general orientation.
Summary of the invention
In view of the shortcomings of the prior art, the present invention provides a kind of high-strength anti-flaming non-woven fabrics and preparation method thereof, biography is improved
The intensity of system non-woven fabrics enhances its tensile capacity, and promotes flame retardant property by impregnating fire resistant fluid, reinforces the use of non-woven fabrics
Effect.
In order to achieve the above object, technical solution of the present invention is achieved by the following technical programs:
A kind of high-strength anti-flaming non-woven fabrics, the non-woven fabrics are made of raw material from the following weight: 12-15 parts of polypropylene,
10-12 parts of polyethylene terephthalate, 2-4 parts of polyacrylonitrile, 1-2 parts of Butylated Hydroxytoluene, 4-6 parts of gypsum fiber, ethoxy
2-4 parts of cellulose, 1-3 parts of aluminum phosphate, 0.4-0.8 parts of thioacetamide, 0.2-0.8 parts of casein, aqueous polyurethane 15-20
Part, 2-3 parts of hydroxy-ethyl acrylate, 1-2 parts of antimony oxide, 1-2 parts of sodium metasilicate, 1-3 parts of triphenyl phosphate, defoaming agent 0.4-
0.6 part.
Preferably, the non-woven fabrics is made of raw material from the following weight: 14 parts of polypropylene, polyethylene terephthalate
11 parts of ester, 3 parts of polyacrylonitrile, 1.5 parts of Butylated Hydroxytoluene, 5 parts of gypsum fiber, 3 parts of hydroxyethyl cellulose, 2 parts of aluminum phosphate, thio second
0.6 part of amide, 0.5 part of casein, 18 parts of aqueous polyurethane, 2.5 parts of hydroxy-ethyl acrylate, 1.5 parts of antimony oxide, sodium metasilicate
1.5 parts, 2 parts of triphenyl phosphate, 0.5 part of defoaming agent.
Preferably, the defoaming agent is silicone emulsion, in polyoxyethylene polyoxypropylene glycerin ether, dimethyl silicone polymer
Any one.
The preparation method of the non-woven fabrics the following steps are included:
(1) polypropylene, polyethylene terephthalate, gypsum fiber Hybrid Heating are down to room temperature after mixing evenly
Afterwards, it is spare to obtain mixed-powder at powder for drying and grinding；
(2) it will be sieved after polyacrylonitrile, Butylated Hydroxytoluene, aluminum phosphate, thioacetamide mixed grinding, add 1 times of volume
The deionized water of number, the mixed-powder in above-mentioned steps (1) is added in heating after mixing evenly, adds after high-speed stirred 10-15min
Enter hydroxyethyl cellulose and casein continue to stir mixed resin carries out spinneret processing in machine, it is standby to obtain non-woven fabrics fiber
With；
(3) aqueous polyurethane, hydroxy-ethyl acrylate, antimony oxide, sodium metasilicate, triphenyl phosphate Hybrid Heating are stirred
Defoaming agent is added after a period of time to continue to stir, it is spare to obtain fire resistant fluid；
(4) non-woven fabrics fiber in above-mentioned steps (2) is carried out after being hot pressed into non-woven fabrics, gained nonwoven is distributed in step
(3) heat-insulation soaking is carried out in the fire resistant fluid in, takes out drying afterwards, obtains high-strength anti-flaming non-woven fabrics of the present invention.
Preferably, the temperature that Hybrid Heating stirs in the step (1) is 140-150 DEG C, speed of agitator 200-250r/
Min, mixing time 30-40min.
Preferably, mixed grinding needed 80-100 mesh in the step (2), and the temperature that mixed-powder is added in heating is
100-110 DEG C, the revolving speed of high-speed stirred is 1200-1400r/min, and hydroxyethyl cellulose is added and casein continues turning for stirring
Speed is 600-800r/min, and the time of stirring is 60-80min.
Preferably, the temperature that Hybrid Heating stirs in the step (3) is 60-80 DEG C, speed of agitator 200-400r/
Min, mixing time 10-15min are added defoaming agent and continue the time of stirring as 20-25min.
Preferably, the temperature that step (4) nonwoven is distributed in heat-insulation soaking in fire resistant fluid is 60-65 DEG C, and soaking time is
120-150min。
The present invention provides a kind of high-strength anti-flaming non-woven fabrics and preparation method thereof, and advantage is compared with prior art:
(1) present invention is mixed into fiber base-material using polypropylene, polyethylene terephthalate, gypsum fiber, can have
Effect guarantees to enhance the stability of product while the flexibility and antibiotic property of products obtained therefrom non-woven fabrics, and promotes the strong of product
Degree.
(2) name of the present invention is added the substances such as polyacrylonitrile, Butylated Hydroxytoluene, aluminum phosphate and casein and is effectively promoting product
Enhance the active force between product material while antioxygenic property, promotes the intensity and pull resistance of the product non-woven fabrics.
(3) present invention promotes flame retardant property using in such a way that non-woven fabrics outer layer impregnates fire resistant fluid, and fire resistant fluid use
Aqueous polyurethane, hydroxy-ethyl acrylate, antimony oxide, sodium metasilicate, triphenyl phosphate are mixed with, and are promoting the fire-retardant of product
Product stability is promoted while performance, enhances product using effect.
Specific embodiment
In order to make the object, technical scheme and advantages of the embodiment of the invention clearer, below with reference to the embodiment of the present invention pair
Technical solution in the embodiment of the present invention is clearly and completely described, it is clear that described embodiment is a part of the invention
Embodiment, instead of all the embodiments.Based on the embodiments of the present invention, those of ordinary skill in the art are not making wound
Every other embodiment obtained under the premise of the property made labour, shall fall within the protection scope of the present invention.
Embodiment 1:
A kind of high-strength anti-flaming non-woven fabrics, the non-woven fabrics are made of raw material from the following weight: 12 parts of polypropylene, poly- pair
10 parts of ethylene terephthalate, 2 parts of polyacrylonitrile, 1 part of Butylated Hydroxytoluene, 4 parts of gypsum fiber, 2 parts of hydroxyethyl cellulose, phosphoric acid
1 part of aluminium, 0.4 part of thioacetamide, 0.2 part of casein, 15 parts of aqueous polyurethane, 2 parts of hydroxy-ethyl acrylate, antimony oxide 1
Part, 1 part of sodium metasilicate, 1 part of triphenyl phosphate, 0.4 part of defoaming agent；The defoaming agent is silicone emulsion, polyoxyethylene polyoxypropylene
Any one in glycerin ether, dimethyl silicone polymer.
The preparation method of the non-woven fabrics the following steps are included:
(1) polypropylene, polyethylene terephthalate, gypsum fiber Hybrid Heating are down to room temperature after mixing evenly
Afterwards, it is spare to obtain mixed-powder at powder for drying and grinding；
(2) it will be sieved after polyacrylonitrile, Butylated Hydroxytoluene, aluminum phosphate, thioacetamide mixed grinding, add 1 times of volume
The deionized water of number, the mixed-powder in above-mentioned steps (1) is added in heating after mixing evenly, adds after high-speed stirred 10-15min
Enter hydroxyethyl cellulose and casein continue to stir mixed resin carries out spinneret processing in machine, it is standby to obtain non-woven fabrics fiber
With；
(3) aqueous polyurethane, hydroxy-ethyl acrylate, antimony oxide, sodium metasilicate, triphenyl phosphate Hybrid Heating are stirred
Defoaming agent is added after a period of time to continue to stir, it is spare to obtain fire resistant fluid；
(4) non-woven fabrics fiber in above-mentioned steps (2) is carried out after being hot pressed into non-woven fabrics, gained nonwoven is distributed in step
(3) heat-insulation soaking is carried out in the fire resistant fluid in, takes out drying afterwards, obtains high-strength anti-flaming non-woven fabrics of the present invention.
Wherein, the temperature that Hybrid Heating stirs in the step (1) is 140-150 DEG C, speed of agitator 200-250r/
Min, mixing time 30-40min；Mixed grinding needed 80-100 mesh in the step (2), and mixed-powder is added in heating
Temperature is 100-110 DEG C, and the revolving speed of high-speed stirred is 1200-1400r/min, and hydroxyethyl cellulose is added and casein continues to stir
The revolving speed mixed is 600-800r/min, and the time of stirring is 60-80min；The temperature of Hybrid Heating stirring is in the step (3)
60-80 DEG C, speed of agitator 200-400r/min, mixing time 10-15min, be added defoaming agent continue stirring time be
20-25min；The temperature that step (4) nonwoven is distributed in heat-insulation soaking in fire resistant fluid is 60-65 DEG C, soaking time 120-
150min。
Embodiment 2:
A kind of high-strength anti-flaming non-woven fabrics, the non-woven fabrics are made of raw material from the following weight: 15 parts of polypropylene, poly- pair
12 parts of ethylene terephthalate, 4 parts of polyacrylonitrile, 2 parts of Butylated Hydroxytoluene, 6 parts of gypsum fiber, 4 parts of hydroxyethyl cellulose, phosphoric acid
3 parts of aluminium, 0.8 part of thioacetamide, 0.8 part of casein, 20 parts of aqueous polyurethane, 3 parts of hydroxy-ethyl acrylate, antimony oxide 2
Part, 2 parts of sodium metasilicate, 3 parts of triphenyl phosphate, 0.6 part of defoaming agent；The defoaming agent is silicone emulsion, polyoxyethylene polyoxypropylene
Any one in glycerin ether, dimethyl silicone polymer.
The preparation method of the non-woven fabrics the following steps are included:
(1) polypropylene, polyethylene terephthalate, gypsum fiber Hybrid Heating are down to room temperature after mixing evenly
Afterwards, it is spare to obtain mixed-powder at powder for drying and grinding；
(2) it will be sieved after polyacrylonitrile, Butylated Hydroxytoluene, aluminum phosphate, thioacetamide mixed grinding, add 1 times of volume
The deionized water of number, the mixed-powder in above-mentioned steps (1) is added in heating after mixing evenly, adds after high-speed stirred 10-15min
Enter hydroxyethyl cellulose and casein continue to stir mixed resin carries out spinneret processing in machine, it is standby to obtain non-woven fabrics fiber
With；
(3) aqueous polyurethane, hydroxy-ethyl acrylate, antimony oxide, sodium metasilicate, triphenyl phosphate Hybrid Heating are stirred
Defoaming agent is added after a period of time to continue to stir, it is spare to obtain fire resistant fluid；
(4) non-woven fabrics fiber in above-mentioned steps (2) is carried out after being hot pressed into non-woven fabrics, gained nonwoven is distributed in step
(3) heat-insulation soaking is carried out in the fire resistant fluid in, takes out drying afterwards, obtains high-strength anti-flaming non-woven fabrics of the present invention.
Wherein, the temperature that Hybrid Heating stirs in the step (1) is 140-150 DEG C, speed of agitator 200-250r/
Min, mixing time 30-40min；Mixed grinding needed 80-100 mesh in the step (2), and mixed-powder is added in heating
Temperature is 100-110 DEG C, and the revolving speed of high-speed stirred is 1200-1400r/min, and hydroxyethyl cellulose is added and casein continues to stir
The revolving speed mixed is 600-800r/min, and the time of stirring is 60-80min；The temperature of Hybrid Heating stirring is in the step (3)
60-80 DEG C, speed of agitator 200-400r/min, mixing time 10-15min, be added defoaming agent continue stirring time be
20-25min；The temperature that step (4) nonwoven is distributed in heat-insulation soaking in fire resistant fluid is 60-65 DEG C, soaking time 120-
150min。
Embodiment 3:
A kind of high-strength anti-flaming non-woven fabrics, the non-woven fabrics are made of raw material from the following weight: 14 parts of polypropylene, poly- pair
11 parts of ethylene terephthalate, 3 parts of polyacrylonitrile, 1.5 parts of Butylated Hydroxytoluene, 5 parts of gypsum fiber, 3 parts of hydroxyethyl cellulose, phosphorus
2 parts of sour aluminium, 0.6 part of thioacetamide, 0.5 part of casein, 18 parts of aqueous polyurethane, 2.5 parts of hydroxy-ethyl acrylate, three oxidations two
1.5 parts of antimony, 1.5 parts of sodium metasilicate, 2 parts of triphenyl phosphate, 0.5 part of defoaming agent；The defoaming agent is silicone emulsion, polyoxypropylene is poly-
Any one in ethylene oxide glycerin ether, dimethyl silicone polymer.
The preparation method of the non-woven fabrics the following steps are included:
(1) polypropylene, polyethylene terephthalate, gypsum fiber Hybrid Heating are down to room temperature after mixing evenly
Afterwards, it is spare to obtain mixed-powder at powder for drying and grinding；
(2) it will be sieved after polyacrylonitrile, Butylated Hydroxytoluene, aluminum phosphate, thioacetamide mixed grinding, add 1 times of volume
The deionized water of number, the mixed-powder in above-mentioned steps (1) is added in heating after mixing evenly, adds after high-speed stirred 10-15min
Enter hydroxyethyl cellulose and casein continue to stir mixed resin carries out spinneret processing in machine, it is standby to obtain non-woven fabrics fiber
With；
(3) aqueous polyurethane, hydroxy-ethyl acrylate, antimony oxide, sodium metasilicate, triphenyl phosphate Hybrid Heating are stirred
Defoaming agent is added after a period of time to continue to stir, it is spare to obtain fire resistant fluid；
(4) non-woven fabrics fiber in above-mentioned steps (2) is carried out after being hot pressed into non-woven fabrics, gained nonwoven is distributed in step
(3) heat-insulation soaking is carried out in the fire resistant fluid in, takes out drying afterwards, obtains high-strength anti-flaming non-woven fabrics of the present invention.
Wherein, the temperature that Hybrid Heating stirs in the step (1) is 140-150 DEG C, speed of agitator 200-250r/
Min, mixing time 30-40min；Mixed grinding needed 80-100 mesh in the step (2), and mixed-powder is added in heating
Temperature is 100-110 DEG C, and the revolving speed of high-speed stirred is 1200-1400r/min, and hydroxyethyl cellulose is added and casein continues to stir
The revolving speed mixed is 600-800r/min, and the time of stirring is 60-80min；The temperature of Hybrid Heating stirring is in the step (3)
60-80 DEG C, speed of agitator 200-400r/min, mixing time 10-15min, be added defoaming agent continue stirring time be
20-25min；The temperature that step (4) nonwoven is distributed in heat-insulation soaking in fire resistant fluid is 60-65 DEG C, soaking time 120-
150min。
It should be noted that, in this document, relational terms such as first and second and the like are used merely to a reality
Body or operation are distinguished with another entity or operation, are deposited without necessarily requiring or implying between these entities or operation
In any actual relationship or order or sequence.Moreover, the terms "include", "comprise" or its any other variant are intended to
Non-exclusive inclusion, so that the process, method, article or equipment including a series of elements is not only wanted including those
Element, but also including other elements that are not explicitly listed, or further include for this process, method, article or equipment
Intrinsic element.In the absence of more restrictions, the element limited by sentence "including a ...", it is not excluded that
There is also other identical elements in process, method, article or equipment including the element.
The above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations；Although with reference to the foregoing embodiments
Invention is explained in detail, those skilled in the art should understand that: it still can be to aforementioned each implementation
Technical solution documented by example is modified or equivalent replacement of some of the technical features；And these modification or
Replacement, the spirit and scope for technical solution of various embodiments of the present invention that it does not separate the essence of the corresponding technical solution.
Claims (8)
1. a kind of high-strength anti-flaming non-woven fabrics, which is characterized in that the non-woven fabrics is made of raw material from the following weight: polypropylene
12-15 parts, 10-12 parts of polyethylene terephthalate, 2-4 parts of polyacrylonitrile, 1-2 parts of Butylated Hydroxytoluene, gypsum fiber 4-6
Part, 2-4 parts of hydroxyethyl cellulose, 1-3 parts of aluminum phosphate, 0.4-0.8 parts of thioacetamide, 0.2-0.8 parts of casein, aqueous poly- ammonia
15-20 parts of ester, 2-3 parts of hydroxy-ethyl acrylate, 1-2 parts of antimony oxide, 1-2 parts of sodium metasilicate, 1-3 parts of triphenyl phosphate, defoaming
0.4-0.6 parts of agent.
2. a kind of high-strength anti-flaming non-woven fabrics according to claim 1, which is characterized in that the non-woven fabrics is by following weight
The raw material of part is made: 14 parts of polypropylene, 11 parts of polyethylene terephthalate, 3 parts of polyacrylonitrile, 1.5 parts of Butylated Hydroxytoluene, stone
5 parts of cream fiber, 3 parts of hydroxyethyl cellulose, 2 parts of aluminum phosphate, 0.6 part of thioacetamide, 0.5 part of casein, aqueous polyurethane 18
Part, 2.5 parts of hydroxy-ethyl acrylate, 1.5 parts of antimony oxide, 1.5 parts of sodium metasilicate, 2 parts of triphenyl phosphate, 0.5 part of defoaming agent.
3. a kind of high-strength anti-flaming non-woven fabrics according to claim 1, which is characterized in that it is characterized by: the defoaming
Agent is silicone emulsion, polyoxyethylene polyoxypropylene glycerin ether, any one in dimethyl silicone polymer.
4. a kind of preparation method of high-strength anti-flaming non-woven fabrics, it is characterised in that: the preparation method of the non-woven fabrics includes following
Step:
(1) it after polypropylene, polyethylene terephthalate, gypsum fiber Hybrid Heating being down to room temperature after mixing evenly, does
It is dry to pulverize, it is spare to obtain mixed-powder；
(2) it will be sieved after polyacrylonitrile, Butylated Hydroxytoluene, aluminum phosphate, thioacetamide mixed grinding, add 1 times of volume parts
Deionized water, the mixed-powder in above-mentioned steps (1) is added in heating after mixing evenly, and hydroxyl is added after high-speed stirred 10-15min
Ethyl cellulose and casein continue to stir mixed resin carries out spinneret processing in machine, it is spare to obtain non-woven fabrics fiber；
(3) aqueous polyurethane, hydroxy-ethyl acrylate, antimony oxide, sodium metasilicate, triphenyl phosphate Hybrid Heating are stirred one section
Defoaming agent is added after time to continue to stir, it is spare to obtain fire resistant fluid；
(4) non-woven fabrics fiber in above-mentioned steps (2) is carried out after being hot pressed into non-woven fabrics, gained nonwoven is distributed in step (3)
Fire resistant fluid in carry out heat-insulation soaking, take out drying afterwards, obtain high-strength anti-flaming non-woven fabrics of the present invention.
5. a kind of preparation method of high-strength anti-flaming non-woven fabrics according to claim 4, it is characterised in that: the step
(1) temperature that Hybrid Heating stirs in is 140-150 DEG C, speed of agitator 200-250r/min, mixing time 30-40min.
6. a kind of preparation method of high-strength anti-flaming non-woven fabrics according to claim 4, it is characterised in that: the step
(2) mixed grinding needed 80-100 mesh in, and the temperature that mixed-powder is added in heating is 100-110 DEG C, the revolving speed of high-speed stirred
For 1200-1400r/min, be added hydroxyethyl cellulose and casein to continue the revolving speed of stirring be 600-800r/min, stirring
Time is 60-80min.
7. a kind of preparation method of high-strength anti-flaming non-woven fabrics according to claim 4, it is characterised in that: the step
(3) temperature that Hybrid Heating stirs in is 60-80 DEG C, speed of agitator 200-400r/min, mixing time 10-15min and adds
Enter defoaming agent and continues the time of stirring as 20-25min.
8. a kind of preparation method of high-strength anti-flaming non-woven fabrics according to claim 4, it is characterised in that: the step
(4) it is 60-65 DEG C that nonwoven, which is distributed in the temperature of heat-insulation soaking in fire resistant fluid, soaking time 120-150min.
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Application publication date: 20190614 |
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