CN109846092A - A kind of preparation method of the health care cigarette of mellow in taste - Google Patents
A kind of preparation method of the health care cigarette of mellow in taste Download PDFInfo
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Abstract
The invention discloses a kind of preparation method of the health care cigarette of mellow in taste, include the following steps: that (1) raw material weighs；(2) preparation of flavor component；(3) preparation of pipe tobacco carrier；(4) preparation of mellow instant powder；(5) preparation of finished product.The present invention provides a kind of preparation methods of the health care cigarette of mellow in taste; materials safety; the health-care efficacy that final health care cigarette obtained has calm nerves, mitigates insomnia; help smokers to spend impatient phase in smoking cessation stage, at the same can moistening lung to arrest cough, liver protection of relieving inflammation or internal heat, have protection and curative effect well to the body of smoker; ensure the health of smoker; and mellow in taste is easily received by consumer, has good marketing application value.
Description
Technical field
The invention belongs to product technical fields of giving up smoking, and in particular to a kind of preparation method of the health care cigarette of mellow in taste.
Background technique
Smoking has certain social, has certain social function in social activity, but may induce a variety of diseases again simultaneously
Disease, it is very harmful to individual health.Also just due in this way, smoking cessation is becoming increasingly popular.It is investigated according to the World Health Organization, in industry
In flourishing country, the patients with lung cancer of countries population's a quarter is accounted for, smoking accounts for 90%；Bronchitis is died of, smoking accounts for 75%；
Myocardial infarction is died of, smoking accounts for 25%.Smoking not only brings harm to me, but also brings disaster to children.There is scholar to 5200
Pregnant woman's investigation and analysis, as a result, it has been found that the birth of quantity and the fetus antenatal death rate and Congenital Malformed Children that its husband smokes daily
Rate is directly proportional.Father's non-smoking, the ratio of children's congenital malformation is 0.8%；Smoke daily 1~10 its ratio of father is
1.4%；The ratio for inhaling 10 or more daily is 2.1%.The number of pregnant woman herself's amount of smoking, before also directly influencing baby due
The death rate afterwards.For example, smoking daily, less than a packet, baby death level of significance is 20%；More than one packet of smoking daily, baby
Youngster's death risk rate is 35% or more.It smokes simultaneously as a kind of habituation sexual behaviour, also there is certain mental disease.
The fact that harmfulness of smoking health is generally well known.The chemical substance discharged when different cigarette lighter is not
Together, but mainly the chemical substances such as tar and carbon monoxide are counted, the substance being harmful to the human body is generated after cigarette lighter and is roughly divided into 6 greatly
Class: (1) aldehydes, nitride, olefines, to the irritating effect of respiratory tract；(2) nicotine class can stimulate sympathetic nerve, allow smoking
Person, which is formed, to be relied on；(3) amine, cyanide and heavy metal, category toxicant；(4) Benzpyrene, arsenic, cadmium, methyl hydrazine, amino phenols,
Other radioactive substances, there is carcinogenesis；(5) phenolic compound and formaldehyde etc. have the function of accelerating canceration；(6) one oxygen
Change carbon, lowers the ability that oxygen is transported to whole body by red blood cell.With the continuous improvement of people's health consciousness, more and more people's wills
Know harm of smoking, then various smoking cessation products are ready to appear, such as smoking give-up chewing gum, liquid for giving up smoking, wine for giving off smoking etc., but root
According to market feedback information, that there is mouthfeels is bad for the smoking cessation product of existing market, can not eliminate smoking addiction, the high problem of relapse rate,
And it can not accomplish the effect of playing moistening lung to arrest cough, liver protection of relieving inflammation or internal heat, sterilizing while smoking cessation.
" a kind of smoking cessation Cigarette with traditional Chinese medicines and preparation method thereof " (application No. is 201610049266.4) discloses a kind of ring
Cigarette Cigarette with traditional Chinese medicines and preparation method thereof.The product is made by pure natural Chinese medicine, without containing any additive and toxic
Chemical component, fragrant odour clear away heart-fire and soothe the spirit, other than there is smoking cessation effect well, also have refresh oneself, restoring consciouness, have one's ideas straightened out etc. it is excellent
Point, but bitter taste can be generated after lighting there is traditional Chinese medicine ingredients, mouthfeel is bad, and application value is little.
" a kind of health care cigarette " (application No. is 201610580571.6) discloses a kind of health care cigarette.Although the health care cigarette overcomes
The defect of traditional Chinese medicine smoking cessation product, has effects that moistening lung, liver protection, but mouthfeel is general, has a single function, for thermophilic
The masses of cigarette are simultaneously not suitable for, and can not accomplish calm nerves, relieve stress, thoroughly replace common cigarette, when people in face of pressure or
When person's worry, however it remains the hidden danger relapsed.
Summary of the invention
The purpose of the present invention is providing a kind of preparation method of the health care cigarette of mellow in taste for existing problem,
Materials safety, the health-care efficacy that final health care cigarette obtained has calm nerves, mitigates insomnia, helps smokers to spend smoking cessation rank
Section the impatient phase, while can moistening lung to arrest cough, liver protection of relieving inflammation or internal heat, to the body of smoker have well protection and curative effect, protect
Hinder the health of smoker, and mellow in taste, easily received by consumer, there is good marketing application value.
The present invention is achieved by the following technical solutions:
A kind of preparation method of the health care cigarette of mellow in taste, includes the following steps:
(1) raw material weighs: weigh 6 ~ 10 parts of 12 ~ 16 parts of 10 ~ 14 parts of water chestnut, peppermint, the bamboo shoots of corresponding parts by weight, honeysuckle 11 ~
15 parts, 21 ~ 24 parts of reed root, 6 ~ 9 parts of Siraitia grosvenorii, 7 ~ 11 parts of sweet wormwood, 8 ~ 12 parts of chrysanthemum, 7 ~ 11 parts of rose, 6 ~ 9 parts of carrot,
5 ~ 8 parts of pea, 15 ~ 18 parts of milk；
(2) preparation of flavor component:
A. the weighed peppermint of step (1), honeysuckle, rose, chrysanthemum are put into deep cooling type pulverizer jointly and is carried out at crushing
Reason, it is spare that pulverization process crosses 10 ~ 30 meshes；
B. the powder operated after being sieved in a is added in complex enzyme liquid and is digested, when enzymatic hydrolysis keeps the temperature in enzyme solution to be
It 38 ~ 42 DEG C, filters out that powder is spare after digesting 1 ~ 2h, the ultrasonication of specific frequency is carried out while enzymatic hydrolysis；
C. the powder filtered out in b will be operated to be placed in soxhlet extraction device, using 95% ethyl alcohol as digestion agent, Microwave-assisted firing
It is extracted repeatedly, after extracting 3 ~ 4h, collects leaching liquor and extraction cream is spare；
D. the gained leaching liquor operated in c be concentrated until ethyl alcohol volatilizees to obtain completely flavor component；
(3) preparation of pipe tobacco carrier:
A. extraction cream obtained in the weighed bamboo shoots of step (1), reed root, the same step of sweet wormwood (2) operation c is first cut into cigarette respectively
Then filiform mixes to obtain pipe blend；
B. pipe blend obtained in operation a is placed in white wine and is sufficiently infiltrated, the pipe blend after taking out infiltration is placed in oven
In toasted, toast after 40 ~ 60min up to pipe tobacco carrier；
(4) preparation of mellow instant powder:
A. the weighed water chestnut of step (1), carrot, pea are placed in pulverizer and are tentatively crushed, the revolving speed of pulverizer is
Mixed powder is obtained after 600 ~ 700rpm, 30 ~ 40min of pulverization process；
B. weighed milk, which is put into jointly in microjet high pressure homogenizer, in the same step of mixed powder (1) obtained by operating in a carries out
Homogenization, after 6 ~ 9min of homogenization homogeneous product；
C. Bifidobacterium is inoculated into homogeneous product obtained in operation b, carries out solid state fermentation and obtains tunning；
D. gained tunning in operation c is placed in deep cooling type pulverizer and is crushed, obtained after 35 ~ 45min of pulverization process fast
Molten powder；
(5) preparation of finished product:
A. by the resulting flavor component of step (2), the resulting pipe tobacco carrier of step (3), the resulting mellowness instant powder of step (4)
It is to be put into reaction kettle jointly after 2 ~ 3:10 ~ 14:3 ~ 4 is mixed according to weight ratio, is 100 ~ 120 by the temperature control in reaction kettle
DEG C, the pressure control in reaction kettle is 0.1 ~ 0.2MPa, and the relative air humidity control in reaction kettle is 87 ~ 93%, reaction treatment
After 34 ~ 40min, it is spare to take out mixture；
B. it will operate and be dried in the investment vacuum freeze drier of mixture obtained in a, drying to moisture content is 2 ~ 7%；
C. finished product is made in the mixture investment cigarette machine after will be dry in operation b.
Further, the step (2) operates the specific procedure of pulverization process in a are as follows: the temperature first in holding pulverizer
Degree is -30 ~ -10 DEG C, stirs 20 ~ 30min with the revolving speed of 2000 ~ 4000rpm, then stops crushing, the temperature in machine to be comminuted
When rising to 25 ~ 35 DEG C, start pulverizer, the temperature in pulverizer is down to -20 ~ -10 DEG C, with the revolving speed of 800 ~ 1000rpm into
40 ~ 50min of row pulverization process.
Further, each ingredient and corresponding parts by weight in complex enzyme liquid in the step (2) operation b are as follows: cellulase 3 ~ 4
Part, 2 ~ 3 parts of hemicellulase, 1 ~ 3 part of pectase, 500 ~ 600 parts of sterile water.
Further, the frequency of ultrasonic wave is 50 ~ 60kHz in step (2) the operation b.
Further, the power of microwave is 600 ~ 700W in step (2) the operation c, and heating keeps the temperature in leaching liquor
Degree is 88 ~ 92 DEG C.
Further, temperature control when toasting in step (3) the operation b in oven is 94 ~ 102 DEG C.
Further, in the step (4) operation b when homogenization the operating pressure of microjet high pressure homogenizer be 150 ~
180MPa。
Further, it is 56 ~ 67% that the condition of solid state fermentation, which is relative air humidity, in step (4) the operation c, fermentation
Temperature is 39 ~ 43 DEG C, and fermentation time is 1 ~ 2d.
Further, the revolving speed of pulverizer is 1600 ~ 2000rpm when pulverization process in step (4) the operation d, is crushed
Temperature in machine is -12 ~ -4 DEG C.
Further, when being freeze-dried in the step (5) operation b, the temperature of freezing is -35 ~ -15 DEG C, freezing when
Between be 5 ~ 9min, dry temperature be 55 ~ 65 DEG C.
The present invention provides a kind of preparation method of the health care cigarette of mellow in taste, health care cigarette of the invention mainly includes fragrance
Ingredient, pipe tobacco carrier and mellow instant powder, it is first that peppermint, honeysuckle, rose, chrysanthemum is total in the preparation of flavor component
With being crushed the chemical stability that can not only guarantee effective component in material composition in low temperature environment, additionally it is possible to kill former
Pathogen that may be present in material, has ensured the quality of health care cigarette to a certain extent, during crushing, first with higher
Revolving speed crushed, each raw material is tentatively crushed, due to the structure of the cell wall of powder in every kind of raw material and effectively at
Divide the existence form in cell to have a certain difference, can exist in subsequent processing and extract insufficient phenomenon, at this
In invention, heats up after preliminary crushing, promote to combine closely between different material powder, then carry out separating twice, further
Increase raw material powder between contact area, under the action of similar compatibility principle, promote raw material in effective component synchronize it is molten
Out, it can lay the foundation for subsequent operation.And then resulting powder is placed in enzyme solution and is impregnated, in the auxiliary of ultrasonic wave
It helps under effect, the small vacuole in enzyme solution is activated under sound wave effect, and it includes vacuole that a series of dynamic (dynamical) processes, which occur,
Oscillation, contraction, elongation He Beng Cheongju etc., so that the block layer in enzyme solution between water phase and powder is eliminated, so that mass transfer rate be made to increase
Greatly, enzyme solution acts on powder cell, destroys the structures such as cellulose, hemicellulose, pectin in cell wall, under the assistance of ultrasonic wave,
Cell deforms and ruptures, and cell wall lignin is destroyed, to release content.Then under microwave-assisted effect
It being extracted, effect of the molecule by microwave energy, rotation can be accelerated, and a large amount of thermal energy are immediately generated, cell is further destroyed,
In microwave field, the ability of various material absorbing microwave energies is influenced by the specific heat of substance, shape, dielectric constant and water content,
Therefore the thermal energy of its generation and the thermal energy for passing to ambient enviroment are also different, which causes certain components in extraction system
Or some regions of base matter are selectively heated, and are extracted ingredient to isolate in system or matrix, be allowed into
Enter to microwave absorption capacity in extractant poor, that dielectric constant is small, from the recovery rate for greatly enhancing effective component.Institute
Obtained flavor component has sterilizing, heat-clearing solution fire, moistening lung to arrest cough and other effects, moreover it is possible to assign health care cigarette pure and fresh fragrance.
The raw material that the present invention is prepared using bamboo shoots, reed root, sweet wormwood, the remaining medicinal extract of flavor component as pipe tobacco carrier, mutually twines after chopping
Around, gap mostly close structure is formed, infiltrates and toasts by white wine, the careless fishy smell and astringent taste that removal raw material itself has, and
And under the action of alcohol and high temperature, the surface of pipe blend will form small hole, provide reliably for the combination of other raw materials
Stable carrier.In the preparation of mellow instant powder, preliminary crush obtains water chestnut, carrot, pea powder, then by itself and milk
Mixing carries out the high-pressure homogeneous processing of microjet, the higher-order of oscillation, instantaneous by carrying out high velocity impact to material in oscillating reactions chamber
The effects of pressure drop and intensive shear, cavitation, realizes the fusion that contacts with each other between raw material, by fermentation, is formed mellow
Instant powder easy to use, eliminates the bitter taste of sweet wormwood, reed root etc. and the impact strong to taste bud in raw material, and the instant powder of formation is used
In the raw material of health care, the phenomenon of existing smoking cessation product mouthfeel bitterness is avoided, in addition resulting mellow instant powder, which has, relaxes
Delay effect of nerve, mitigate smoker to the dependence of common cigarette, while health care cigarette moistening lung to arrest cough, clear can be further strengthened
The function and effect of fiery liver protection.Finally resulting raw material is reacted under high-temperature and high-pressure conditions, it is flavor component, mellow instant
Powder uniform close is integrated on pipe tobacco carrier, ultimately forms the health care cigarette of mellow in taste.
The present invention has the advantage that compared with prior art
The present invention provides a kind of preparation method of the health care cigarette of mellow in taste, materials safety, final health care cigarette obtained has
Calm nerves, the health-care efficacy for mitigating insomnia help smokers to spend impatient phase in smoking cessation stage, at the same can moistening lung to arrest cough,
It relieves inflammation or internal heat liver protection, has protection and curative effect well to the body of smoker, ensure the health of smoker, and mellow in taste,
Easily received by consumer, there is good marketing application value.
Specific embodiment
Embodiment 1
A kind of preparation method of the health care cigarette of mellow in taste, includes the following steps:
(1) raw material weighs: weighing 11 ~ 15 parts of 6 parts of 12 parts of 10 parts of water chestnut, peppermint, bamboo shoots, honeysuckle, the reed root of corresponding parts by weight
21 ~ 24 parts, 6 parts of Siraitia grosvenorii, 7 parts of sweet wormwood, 8 parts of chrysanthemum, 7 ~ 11 parts of rose, 6 ~ 9 parts of carrot, 5 ~ 8 parts of pea, milk 15
Part；
(2) preparation of flavor component:
A. the weighed peppermint of step (1), honeysuckle, rose, chrysanthemum are put into deep cooling type pulverizer jointly and is carried out at crushing
Reason, it is spare that pulverization process crosses 10 meshes；
B. the powder operated after being sieved in a is added in complex enzyme liquid and is digested, when enzymatic hydrolysis keeps the temperature in enzyme solution to be
It 38 DEG C, filters out that powder is spare after digesting 1h, the ultrasonication of specific frequency is carried out while enzymatic hydrolysis；
C. the powder filtered out in b will be operated to be placed in soxhlet extraction device, using 95% ethyl alcohol as digestion agent, Microwave-assisted firing
It is extracted repeatedly, after extracting 3h, collects leaching liquor and extraction cream is spare；
D. the gained leaching liquor operated in c be concentrated until ethyl alcohol volatilizees to obtain completely flavor component；
(3) preparation of pipe tobacco carrier:
A. extraction cream obtained in the weighed bamboo shoots of step (1), reed root, the same step of sweet wormwood (2) operation c is first cut into cigarette respectively
Then filiform mixes to obtain pipe blend；
B. pipe blend obtained in operation a is placed in white wine and is sufficiently infiltrated, the pipe blend after taking out infiltration is placed in oven
In toasted, toast after 40min up to pipe tobacco carrier；
(4) preparation of mellow instant powder:
A. the weighed water chestnut of step (1), carrot, pea are placed in pulverizer and are tentatively crushed, the revolving speed of pulverizer is
Mixed powder is obtained after 600rpm, pulverization process 30min；
B. weighed milk, which is put into jointly in microjet high pressure homogenizer, in the same step of mixed powder (1) obtained by operating in a carries out
Homogenization, after homogenization 6min homogeneous product；
C. Bifidobacterium is inoculated into homogeneous product obtained in operation b, carries out solid state fermentation and obtains tunning；
D. gained tunning in operation c is placed in deep cooling type pulverizer and is crushed, obtained after pulverization process 35min instant
Powder；
(5) preparation of finished product:
A. by the resulting flavor component of step (2), the resulting pipe tobacco carrier of step (3), the resulting mellowness instant powder of step (4)
It is to be put into reaction kettle jointly after 2:10:3 is mixed according to weight ratio, is 100 DEG C, in reaction kettle by the temperature control in reaction kettle
Pressure control be 0.1MPa, the relative air humidity control in reaction kettle is 87%, after reaction treatment 34min, takes out mixture
It is spare；
B. it will operate and be dried in the investment vacuum freeze drier of mixture obtained in a, drying to moisture content is 2%；
C. finished product is made in the mixture investment cigarette machine after will be dry in operation b.
Further, the step (2) operates the specific procedure of pulverization process in a are as follows: the temperature first in holding pulverizer
Degree is -30 DEG C, stirs 20min with the revolving speed of 2000rpm, then stops crushing, when the temperature in machine to be comminuted rises to 25 DEG C, open
Dynamic pulverizer, is down to -20 DEG C for the temperature in pulverizer, carries out pulverization process 40min with the revolving speed of 800rpm.
Further, each ingredient and corresponding parts by weight in complex enzyme liquid in the step (2) operation b are as follows: cellulase 3
Part, 2 parts of hemicellulase, 1 part of pectase, 500 parts of sterile water.
Further, the frequency of ultrasonic wave is 50kHz in step (2) the operation b.
Further, the power of microwave is 600W in step (2) the operation c, and the temperature in heating holding leaching liquor is
88℃。
Further, temperature control when toasting in step (3) the operation b in oven is 94 DEG C.
Further, the operating pressure of microjet high pressure homogenizer is when homogenization in step (4) the operation b
150MPa。
Further, it is 56% that the condition of solid state fermentation, which is relative air humidity, in step (4) the operation c, fermentation temperature
It is 39 DEG C, fermentation time 1d.
Further, the revolving speed of pulverizer is 1600rpm when pulverization process in the step (4) operation d, in pulverizer
Temperature is -12 DEG C.
Further, when being freeze-dried in the step (5) operation b, the temperature of freezing is -35 DEG C, and the time of freezing is
5min, dry temperature are 55 DEG C.
Embodiment 2
A kind of preparation method of the health care cigarette of mellow in taste, includes the following steps:
(1) raw material weighs: weighing 13 parts of 8 parts of 14 parts of 12 parts of water chestnut, peppermint, bamboo shoots, honeysuckle, the reed root 22.5 of corresponding parts by weight
Part, 7.5 parts of Siraitia grosvenorii, 9 parts of sweet wormwood, 10 parts of chrysanthemum, 9 parts of rose, 7.5 parts of carrot, 6.5 parts of pea, 16.5 parts of milk；
(2) preparation of flavor component:
A. the weighed peppermint of step (1), honeysuckle, rose, chrysanthemum are put into deep cooling type pulverizer jointly and is carried out at crushing
Reason, it is spare that pulverization process crosses 20 meshes；
B. the powder operated after being sieved in a is added in complex enzyme liquid and is digested, when enzymatic hydrolysis keeps the temperature in enzyme solution to be
It 40 DEG C, filters out that powder is spare after digesting 1.5h, the ultrasonication of specific frequency is carried out while enzymatic hydrolysis；
C. the powder filtered out in b will be operated to be placed in soxhlet extraction device, using 95% ethyl alcohol as digestion agent, Microwave-assisted firing
It is extracted repeatedly, after extracting 3.5h, collects leaching liquor and extraction cream is spare；
D. the gained leaching liquor operated in c be concentrated until ethyl alcohol volatilizees to obtain completely flavor component；
(3) preparation of pipe tobacco carrier:
A. extraction cream obtained in the weighed bamboo shoots of step (1), reed root, the same step of sweet wormwood (2) operation c is first cut into cigarette respectively
Then filiform mixes to obtain pipe blend；
B. pipe blend obtained in operation a is placed in white wine and is sufficiently infiltrated, the pipe blend after taking out infiltration is placed in oven
In toasted, toast after 50min up to pipe tobacco carrier；
(4) preparation of mellow instant powder:
A. the weighed water chestnut of step (1), carrot, pea are placed in pulverizer and are tentatively crushed, the revolving speed of pulverizer is
Mixed powder is obtained after 650rpm, pulverization process 35min；
B. weighed milk, which is put into jointly in microjet high pressure homogenizer, in the same step of mixed powder (1) obtained by operating in a carries out
Homogenization, after homogenization 7.5min homogeneous product；
C. Bifidobacterium is inoculated into homogeneous product obtained in operation b, carries out solid state fermentation and obtains tunning；
D. gained tunning in operation c is placed in deep cooling type pulverizer and is crushed, obtained after pulverization process 40min instant
Powder；
(5) preparation of finished product:
A. by the resulting flavor component of step (2), the resulting pipe tobacco carrier of step (3), the resulting mellowness instant powder of step (4)
It is to be put into reaction kettle jointly after 2.5:12:3.5 is mixed according to weight ratio, is 110 DEG C by the temperature control in reaction kettle, reaction
Pressure control in kettle is 0.15MPa, and the relative air humidity control in reaction kettle is 90%, after reaction treatment 7min, is taken out mixed
It is spare to close object；
B. it will operate and be dried in the investment vacuum freeze drier of mixture obtained in a, drying to moisture content is 4.5%；
C. finished product is made in the mixture investment cigarette machine after will be dry in operation b.
Further, the step (2) operates the specific procedure of pulverization process in a are as follows: the temperature first in holding pulverizer
Degree is -20 DEG C, stirs 25min with the revolving speed of 3000rpm, then stops crushing, when the temperature in machine to be comminuted rises to 30 DEG C, open
Dynamic pulverizer, is down to -15 DEG C for the temperature in pulverizer, carries out pulverization process 45min with the revolving speed of 900rpm.
Further, each ingredient and corresponding parts by weight in complex enzyme liquid in the step (2) operation b are as follows: cellulase 3.5
Part, 2.5 parts of hemicellulase, 2 parts of pectase, 550 parts of sterile water.
Further, the frequency of ultrasonic wave is 55kHz in step (2) the operation b.
Further, the power of microwave is 650W in step (2) the operation c, and the temperature in heating holding leaching liquor is
90℃。
Further, temperature control when toasting in step (3) the operation b in oven is 98 DEG C.
Further, the operating pressure of microjet high pressure homogenizer is when homogenization in step (4) the operation b
165MPa。
Further, it is 61.5% that the condition of solid state fermentation, which is relative air humidity, in step (4) the operation c, fermentation temperature
Degree is 41 DEG C, fermentation time 1.5d.
Further, the revolving speed of pulverizer is 1800rpm when pulverization process in the step (4) operation d, in pulverizer
Temperature is -8 DEG C.
Further, when being freeze-dried in the step (5) operation b, the temperature of freezing is -25 DEG C, and the time of freezing is
7min, dry temperature are 60 DEG C.
Embodiment 3
A kind of preparation method of the health care cigarette of mellow in taste, includes the following steps:
(1) raw material weighs: weighing 15 parts of 10 parts of 16 parts of 14 parts of water chestnut, peppermint, bamboo shoots, honeysuckle, the reed root 24 of corresponding parts by weight
Part, 9 parts of Siraitia grosvenorii, 11 parts of sweet wormwood, 12 parts of chrysanthemum, 11 parts of rose, 9 parts of carrot, 8 parts of pea, 18 parts of milk；
(2) preparation of flavor component:
A. the weighed peppermint of step (1), honeysuckle, rose, chrysanthemum are put into deep cooling type pulverizer jointly and is carried out at crushing
Reason, it is spare that pulverization process crosses 30 meshes；
B. the powder operated after being sieved in a is added in complex enzyme liquid and is digested, when enzymatic hydrolysis keeps the temperature in enzyme solution to be
It 42 DEG C, filters out that powder is spare after digesting 2h, the ultrasonication of specific frequency is carried out while enzymatic hydrolysis；
C. the powder filtered out in b will be operated to be placed in soxhlet extraction device, using 95% ethyl alcohol as digestion agent, Microwave-assisted firing
It is extracted repeatedly, after extracting 4h, collects leaching liquor and extraction cream is spare；
D. the gained leaching liquor operated in c be concentrated until ethyl alcohol volatilizees to obtain completely flavor component；
(3) preparation of pipe tobacco carrier:
A. extraction cream obtained in the weighed bamboo shoots of step (1), reed root, the same step of sweet wormwood (2) operation c is first cut into cigarette respectively
Then filiform mixes to obtain pipe blend；
B. pipe blend obtained in operation a is placed in white wine and is sufficiently infiltrated, the pipe blend after taking out infiltration is placed in oven
In toasted, toast after 60min up to pipe tobacco carrier；
(4) preparation of mellow instant powder:
A. the weighed water chestnut of step (1), carrot, pea are placed in pulverizer and are tentatively crushed, the revolving speed of pulverizer is
Mixed powder is obtained after 700rpm, pulverization process 40min；
B. weighed milk, which is put into jointly in microjet high pressure homogenizer, in the same step of mixed powder (1) obtained by operating in a carries out
Homogenization, after homogenization 9min homogeneous product；
C. Bifidobacterium is inoculated into homogeneous product obtained in operation b, carries out solid state fermentation and obtains tunning；
D. gained tunning in operation c is placed in deep cooling type pulverizer and is crushed, obtained after pulverization process 45min instant
Powder；
(5) preparation of finished product:
A. by the resulting flavor component of step (2), the resulting pipe tobacco carrier of step (3), the resulting mellowness instant powder of step (4)
It is to be put into reaction kettle jointly after 3:14:4 is mixed according to weight ratio, is 120 DEG C, in reaction kettle by the temperature control in reaction kettle
Pressure control be 0.2MPa, the relative air humidity control in reaction kettle is 93%, after reaction treatment 40min, takes out mixture
It is spare；
B. it will operate and be dried in the investment vacuum freeze drier of mixture obtained in a, drying to moisture content is 7%；
C. finished product is made in the mixture investment cigarette machine after will be dry in operation b.
Further, the step (2) operates the specific procedure of pulverization process in a are as follows: the temperature first in holding pulverizer
Degree is -10 DEG C, stirs 30min with the revolving speed of 4000rpm, then stops crushing, when the temperature in machine to be comminuted rises to 35 DEG C, open
Dynamic pulverizer, is down to -10 DEG C for the temperature in pulverizer, carries out pulverization process 50min with the revolving speed of 1000rpm.
Further, each ingredient and corresponding parts by weight in complex enzyme liquid in the step (2) operation b are as follows: cellulase 4
Part, 3 parts of hemicellulase, 3 parts of pectase, 600 parts of sterile water.
Further, the frequency of ultrasonic wave is 60kHz in step (2) the operation b.
Further, the power of microwave is 700W in step (2) the operation c, and the temperature in heating holding leaching liquor is
92℃。
Further, temperature control when toasting in step (3) the operation b in oven is 102 DEG C.
Further, the operating pressure of microjet high pressure homogenizer is when homogenization in step (4) the operation b
180MPa。
Further, it is 67% that the condition of solid state fermentation, which is relative air humidity, in step (4) the operation c, fermentation temperature
It is 43 DEG C, fermentation time 2d.
Further, the revolving speed of pulverizer is 2000rpm when pulverization process in the step (4) operation d, in pulverizer
Temperature is -4 DEG C.
Further, when being freeze-dried in the step (5) operation b, the temperature of freezing is -15 DEG C, and the time of freezing is
9min, dry temperature are 65 DEG C.
Comparative example 1
This comparative example 1 compared with Example 2, saves the whole operation of operation b in step (2), method and step in addition to this
It is all the same.
Comparative example 2
This comparative example 2 changes conventional water-bath into compared with Example 2, by the Microwave-assisted firing in step (2) in operation c
Heating, the temperature after heating in digestion agent is identical, and method and step in addition to this is all the same.
Comparative example 3
This comparative example 3 compared with Example 2, saves the whole operation of step (2), and saves in step (5) operation a
Flavor component, method and step in addition to this are all the same.
Comparative example 4
This comparative example 4 compared with Example 2, saves the whole operation of operation b in step (4), method and step in addition to this
It is all the same.
Comparative example 5
This comparative example 5 compared with Example 2, saves the whole operation of operation c in step (4), method and step in addition to this
It is all the same.
Comparative example 6
This comparative example 6 compared with Example 2, saves the whole operation of step (4), and saves in step (5) operation a
Mellowness instant powder, method and step in addition to this are all the same.
Control group
Application No. is: a kind of health care cigarette disclosed in 201610580571.6.
In order to compare effect of the invention, to embodiment 2, comparative example 1, comparative example 2, comparative example 3, right
Method preparation health care cigarette than embodiment 4, comparative example 5, comparative example 6 and control group carries out aesthetic quality respectively
It smokes panel test, requirement of smokeing panel test: smokeing panel test for each sample needs seven and the above persons' participation, two cigarette country judging panels, and five or more
Provincial judging panel；These judging panels require to pass qualification examinations.It smokes panel test referring to National Standard of the People's Republic of China (GB 5606.4-
2005) " the 4th part of cigarette: sense organ technical requirements " (Cigarettes-Part4:Technical requirements
Forsense-evaluation), 2005-6-17 publication, 2006-1-1 are implemented, and are supervised by People's Republic of China's national quality
Inspection and quarantine general bureau and Standardization Administration of China's publication.
Specific experiment correlation data is as shown in table 1 below:
Table 1
| Gloss (5) | Fragrance (32) | Harmony (6) | Miscellaneous gas (12) | Irritation (20) | Pleasant impression (25) | It is total | |
| Embodiment 2 | 5 | 30 | 6 | 10 | 18 | 23 | 92 |
| Comparative example 1 | 4 | 29 | 5 | 9 | 15 | 18 | 80 |
| Comparative example 2 | 4 | 27 | 6 | 9 | 16 | 21 | 83 |
| Comparative example 3 | 3 | 27 | 4 | 6 | 14 | 14 | 68 |
| Comparative example 4 | 5 | 30 | 5 | 10 | 17 | 20 | 87 |
| Comparative example 5 | 5 | 28 | 6 | 10 | 16 | 21 | 86 |
| Comparative example 6 | 5 | 28 | 6 | 9 | 19 | 20 | 87 |
| Control group | 3 | 28 | 4 | 10 | 13 | 20 | 78 |
Note: each entry value is the average value for having qualified 10 personnel's smoking results of smokeing panel test in upper table 1.
The final obtained health care cigarette mellow in taste of the present invention it can be seen from upper table 1, nonirritant, aftertaste is good, easily by
Consumer is received, and has good marketing application value.
In order to further compare effect of the present invention, this experiment uses voluntary principle, randomly select 400 smoking addiction patients into
Row voluntarily experiment, including the man of 200 25 ~ 70 one full year of life, they are randomly divided into 8 by the Ms of 200 25 ~ 70 one full year of life
Group, every group of 25 men, 25 Mies.Respectively with embodiment 2, comparative example 1, comparative example 2, comparative example 3, right
Method than embodiment 4, comparative example 5, comparative example 6 and control group prepares health care cigarette, then with a 1.5g,
The standard of 20 Zhi Weiyi packets allows patient to test, and exhausts a packet within patient average 3 days, is observed continuously 3 months.Specific experiment comparison
Data are as shown in table 2 below:
Table 2
| Success cure rate (%) | Effective cure rate (%) | |
| Embodiment 2 | 95.9 | 3.7 |
| Comparative example 1 | 93.5 | 3.3 |
| Comparative example 2 | 94.2 | 3.2 |
| Comparative example 3 | 89.4 | 2.5 |
| Comparative example 4 | 94.7 | 3.5 |
| Comparative example 5 | 91.6 | 2.8 |
| Comparative example 6 | 82.1 | 2.4 |
| Control group | 85.2 | 3.1 |
Note: successful cure rate described in upper table 2 specifically refers to be not desired to draw any cigarette there is no any smoking desire；Have
Effect cure rate specifically refers to, and smoking desire gradually weakens.
Health-care efficacy of the health care cigarette with calm nerves, mitigation insomnia produced by the present invention, side it can be seen from upper table 2
Help smokers to spend the impatient phase in smoking cessation stage, at the same can moistening lung to arrest cough, liver protection of relieving inflammation or internal heat, have well to the body of smoker
Protection and curative effect, ensure the health of smoker, have good marketing application value.
Claims (10)
1. a kind of preparation method of the health care cigarette of mellow in taste, which comprises the steps of:
(1) raw material weighs: weigh 6 ~ 10 parts of 12 ~ 16 parts of 10 ~ 14 parts of water chestnut, peppermint, the bamboo shoots of corresponding parts by weight, honeysuckle 11 ~
15 parts, 21 ~ 24 parts of reed root, 6 ~ 9 parts of Siraitia grosvenorii, 7 ~ 11 parts of sweet wormwood, 8 ~ 12 parts of chrysanthemum, 7 ~ 11 parts of rose, 6 ~ 9 parts of carrot,
5 ~ 8 parts of pea, 15 ~ 18 parts of milk；
(2) preparation of flavor component:
A. the weighed peppermint of step (1), honeysuckle, rose, chrysanthemum are put into deep cooling type pulverizer jointly and is carried out at crushing
Reason, it is spare that pulverization process crosses 10 ~ 30 meshes；
B. the powder operated after being sieved in a is added in complex enzyme liquid and is digested, when enzymatic hydrolysis keeps the temperature in enzyme solution to be
It 38 ~ 42 DEG C, filters out that powder is spare after digesting 1 ~ 2h, the ultrasonication of specific frequency is carried out while enzymatic hydrolysis；
C. the powder filtered out in b will be operated to be placed in soxhlet extraction device, using 95% ethyl alcohol as digestion agent, Microwave-assisted firing
It is extracted repeatedly, after extracting 3 ~ 4h, collects leaching liquor and extraction cream is spare；
D. the gained leaching liquor operated in c be concentrated until ethyl alcohol volatilizees to obtain completely flavor component；
(3) preparation of pipe tobacco carrier:
A. extraction cream obtained in the weighed bamboo shoots of step (1), reed root, the same step of sweet wormwood (2) operation c is first cut into cigarette respectively
Then filiform mixes to obtain pipe blend；
B. pipe blend obtained in operation a is placed in white wine and is sufficiently infiltrated, the pipe blend after taking out infiltration is placed in oven
In toasted, toast after 40 ~ 60min up to pipe tobacco carrier；
(4) preparation of mellow instant powder:
A. the weighed water chestnut of step (1), carrot, pea are placed in pulverizer and are tentatively crushed, the revolving speed of pulverizer is
Mixed powder is obtained after 600 ~ 700rpm, 30 ~ 40min of pulverization process；
B. weighed milk, which is put into jointly in microjet high pressure homogenizer, in the same step of mixed powder (1) obtained by operating in a carries out
Homogenization, after 6 ~ 9min of homogenization homogeneous product；
C. Bifidobacterium is inoculated into homogeneous product obtained in operation b, carries out solid state fermentation and obtains tunning；
D. gained tunning in operation c is placed in deep cooling type pulverizer and is crushed, obtained after 35 ~ 45min of pulverization process fast
Molten powder；
(5) preparation of finished product:
A. by the resulting flavor component of step (2), the resulting pipe tobacco carrier of step (3), the resulting mellowness instant powder of step (4)
It is to be put into reaction kettle jointly after 2 ~ 3:10 ~ 14:3 ~ 4 is mixed according to weight ratio, is 100 ~ 120 by the temperature control in reaction kettle
DEG C, the pressure control in reaction kettle is 0.1 ~ 0.2MPa, and the relative air humidity control in reaction kettle is 87 ~ 93%, reaction treatment
After 34 ~ 40min, it is spare to take out mixture；
B. it will operate and be dried in the investment vacuum freeze drier of mixture obtained in a, drying to moisture content is 2 ~ 7%；
C. finished product is made in the mixture investment cigarette machine after will be dry in operation b.
2. a kind of preparation method of the health care cigarette of mellow in taste according to claim 1, which is characterized in that the step (2)
Operate the specific procedure of pulverization process in a are as follows: the temperature first in holding pulverizer is -30 ~ -10 DEG C, with 2000 ~ 4000rpm
Revolving speed stir 20 ~ 30min, then stop crushing, when the temperature in machine to be comminuted rises to 25 ~ 35 DEG C, start pulverizer, by powder
Temperature in broken machine is down to -20 ~ -10 DEG C, carries out 40 ~ 50min of pulverization process with the revolving speed of 800 ~ 1000rpm.
3. a kind of preparation method of the health care cigarette of mellow in taste according to claim 1, which is characterized in that the step (2)
Operate in b each ingredient and corresponding parts by weight in complex enzyme liquid are as follows: 3 ~ 4 parts of cellulase, 2 ~ 3 parts of hemicellulase, pectase 1 ~ 3
Part, 500 ~ 600 parts of sterile water.
4. a kind of preparation method of the health care cigarette of mellow in taste according to claim 1, which is characterized in that the step (2)
The frequency for operating ultrasonic wave in b is 50 ~ 60kHz.
5. a kind of preparation method of the health care cigarette of mellow in taste according to claim 1, which is characterized in that the step (2)
The power for operating microwave in c is 600 ~ 700W, and it is 88 ~ 92 DEG C that heating, which keeps the temperature in leaching liquor,.
6. a kind of preparation method of the health care cigarette of mellow in taste according to claim 1, which is characterized in that the step (3)
The temperature control operated when toasting in b in oven is 94 ~ 102 DEG C.
7. a kind of preparation method of the health care cigarette of mellow in taste according to claim 1, which is characterized in that the step (4)
The operating pressure of microjet high pressure homogenizer is 150 ~ 180MPa when operating homogenization in b.
8. a kind of preparation method of the health care cigarette of mellow in taste according to claim 1, which is characterized in that the step (4)
It is 56 ~ 67% that the condition for operating solid state fermentation in c, which is relative air humidity, and fermentation temperature is 39 ~ 43 DEG C, and fermentation time is 1 ~ 2d.
9. a kind of preparation method of the health care cigarette of mellow in taste according to claim 1, which is characterized in that the step (4)
The revolving speed of pulverizer is 1600 ~ 2000rpm when operating pulverization process in d, and the temperature in pulverizer is -12 ~ -4 DEG C.
10. a kind of preparation method of the health care cigarette of mellow in taste according to claim 1, which is characterized in that the step (5)
When being freeze-dried in operation b, the temperature of freezing is -35 ~ -15 DEG C, and the time of freezing is 5 ~ 9min, and dry temperature is 55 ~ 65
℃。
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111035048A (en) * | 2019-12-26 | 2020-04-21 | 贵州省攀星科技有限公司 | Flower cigarette using folium Eucommiae and flos Lonicerae as base materials and its preparation method |
-
2019
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111035048A (en) * | 2019-12-26 | 2020-04-21 | 贵州省攀星科技有限公司 | Flower cigarette using folium Eucommiae and flos Lonicerae as base materials and its preparation method |
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