CN109832536A - A kind of taste collagen solid beverage and preparation method thereof - Google Patents
A kind of taste collagen solid beverage and preparation method thereof Download PDFInfo
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- CN109832536A CN109832536A CN201811137417.7A CN201811137417A CN109832536A CN 109832536 A CN109832536 A CN 109832536A CN 201811137417 A CN201811137417 A CN 201811137417A CN 109832536 A CN109832536 A CN 109832536A
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Abstract
The present invention discloses a kind of taste collagen solid beverage and preparation method thereof, according to parts by weight includes following components: 0~90 part of ocean fish oligopeptide powder, and 0~90 part of collagen Gly-His-Lys, 1~90 part of Fruit powder.Taste collagen solid beverage is dissolved, and spray drying, it is uniform that the techniques such as fluidized bed granulation obtain color, beautiful, stable prod.The present invention solves single mixing granulation product appearance irregular colour one, is effectively improved the problems such as product mix is uneven using the combined fluidized bed granulation of spray drying is redissolved.The present invention can improve moisture of skin, delay senescence, beauty is crease-resistant, and product colour is uniform, and dissolubility is good, and taste is pleasant.
Description
Technical field
The present invention relates to food, technical field of health care food, and in particular to a kind of taste collagen solid beverage and its
Preparation method.
Background technique
With advancing age, fibroblastic synthesis capability decline, collagen can be gradually lost, and cause skin
If collapsing and lacking collagen in skin, connection solidification will occur for collagenous fibres, reduce iuntercellular mucopolysaccharide, skin will
Soft, elasticity and gloss are lost, aging occurs, while the fibrous fracture of corium, lipoatrophia, sweat gland and smegma subtract
Few, skin just will appear drying, wrinkle, relax the aging phenomenons such as nonelastic.Collagen is boiomacromolecule, animal connective group
Main component in knitting, and the functional protein that content is most in the mammalian body, distribution is most wide, account for total protein
25%~30%, collagen can make skin keep solid and flexible.It is present in human skin, bone, tooth, tendon etc.
Position.In terms of skin, it and elastic fibers resultant force constitute mesh support, provide skin corium firm strong support.Collagen
The distinctive skin repairing of albumen and regeneration effect, can stimulate new collagen to generate, and then Skin Cell is propped up, rise and protect
Effect that is wet and inhibiting wrinkle.The effect of long-term use, which can reach, unfolds coarse groove, desalination microgroove, compact skin.Therefore, collagen egg
The white favor increasingly by the women that likes to be beautiful mostly.Collagen molecules amount is smaller, and molecular weight 1000Da is hereinafter, assimilation effect is got over
It is good, but molecular weight low strap carrys out the bad experience in mouthfeel simultaneously, directly takes and has obvious fishlike smell or bitter taste.Low molecular weight
Collagen is compounded with Fruit powder, and sensory issues are taken in solution, while containing vitamin C and other functional ingredient in Fruit powder, can be promoted
Into the synthesis of collagen, oxidation resistant ability is improved.
About collagen and Fruit powder in presently commercially available collagen product, the pollen compounding such as rose prepares solid beverage
Product it is very much, product be mostly there is the phenomenon that uneven mixing and irregular colour one by mixing between solid, though
Product sensory and mixing uniformity so can be improved by the unified raw material particle size that is sieved, but cannot fundamentally solve product mix
Uniformity.It no matter from product self-view, or is all urgent problem from sense organ angle.Meanwhile passing through wet process system
Grain is used as adhesive for Fruit powder or pollen etc. are soluble in water, pelletizes to collagen, obtained product still exists mixed
The problem of conjunction is uneven, irregular colour one.The present invention mixes between passing through liquid, is spray-dried combined fluidized bed granulation, solves single
One mixing granulation product appearance irregular colour one, is effectively improved the problems such as product mix is uneven.
Summary of the invention
An object of the present invention is to provide a kind of taste collagen solid beverage.
The second object of the present invention is to provide a kind of taste collagen solid beverage and preparation method thereof.
These and other objects of the invention will be come further elucidated above by the following detailed description and explanation.
A kind of taste collagen solid beverage and preparation method thereof, by weight, including ocean fish oligopeptide powder 0~
90 parts, 0~90 part of collagen Gly-His-Lys, 1~90 part of Fruit powder.
Further, a kind of taste collagen solid beverage and preparation method thereof, by weight, including marine fish is oligomeric
0~70 part of Gly-His-Lys, 0~70 part of collagen Gly-His-Lys, 10~30 parts of Fruit powder.
Optimally, a kind of taste collagen solid beverage and preparation method thereof, by weight, including marine fish is oligomeric
40 parts of Gly-His-Lys, 40 parts of collagen Gly-His-Lys, 20 parts of Fruit powder.
A kind of taste collagen solid beverage and preparation method thereof, Fruit powder be Cranberry powder, blueberry powder, blood orange powder,
One or more of orange powder, seabuckthorn fruit powder, pomegranate powder, grape fruit powder.
A kind of taste collagen solid beverage and preparation method thereof, preparation process is as follows:
(1) it ocean fish oligopeptide liquid system: (a) is crushed: fresh cod skin being put into crusher and is crushed；(b) it cleans:
Broken cod skin is put into service sink, cleaned and impregnate 12 with 0.1mol/L~0.5mol/L NaOH solution~
Then 18h is washed till neutrality with clear water；(c) it crushes mashing: broken cod skin being put into colloid mill and is further crushed, is added
Enter purified water, being configured to solid-liquid ratio is 1: 1~1: 3, makes cod skin at slurry condition；(d) it digests: being carried out using composite hydrolytic enzyme
Enzymatic hydrolysis, composite hydrolytic enzyme are acid protease, papain, neutral proteinase, and one or more of bromelain adds
Dosage is 0.5 ‰~the 1.0 ‰ of cod skin quality, and hydrolysis temperature is controlled at 45 DEG C~60 DEG C, and enzymolysis time is in 1h~4h, solution
PH value is controlled 4.0~7.0；(e) enzyme deactivation: after enzymatic hydrolysis, being increased to 70 DEG C~90 DEG C for the temperature of enzymatic vessel, maintain 30min~
60min；(f) separation and purification: the feed liquid after enzyme deactivation is released from enzymatic vessel, is once filtered by plate filter, then
It is filtered by film and carries out secondary filter, by nanofiltration membrane desalination, obtain purification cod skin hydrolyzate；(g) it is concentrated: cod skin hydrolysis
Liquid is by negative pressure inspissator, and control vacuum degree is in 0.5Mpa~1.0Mpa, and when mass concentration is 30%~60%, stopping is concentrated,
It is spare that fish oligopeptide concentrate pump in ocean is transported to intermediate storage tank；
(2) prepared by collagen peptide liquid: (a) being crushed: fresh Java tilapia skin being put into crusher and is crushed；(b) clear
It washes: broken Java tilapia skin being put into service sink, is cleaned with 0.1mol/L~0.5mol/L NaOH solution and impregnates 12
Then~18h is washed till neutrality with clear water, purified water is added, and being configured to solid-liquid ratio is 1: 1~1: 3；(c) it digests: using Compound Water
Solution enzyme is digested, and composite hydrolytic enzyme is acid protease, papain, neutral proteinase, one of bromelain
Or it is several, additive amount is 0.5 ‰~the 1.0 ‰ of Java tilapia skin quality, and hydrolysis temperature is controlled at 45 DEG C~60 DEG C, and enzymolysis time exists
1h~4h, solution ph are controlled 4.0~7.0；(d) enzyme deactivation: after enzymatic hydrolysis, being increased to 70 DEG C~90 DEG C for the temperature of enzymatic vessel,
Maintain 30min~60min；(e) separation and purification: the feed liquid after enzyme deactivation is released from enzymatic vessel, is carried out by plate filter
Primary filtering, filters using film and carries out secondary filter, by nanofiltration membrane desalination, obtains purification Java tilapia skin hydrolyzate；(f) dense
Contracting: Java tilapia skin hydrolyzate by negative pressure inspissator, control vacuum degree in 0.5Mpa~1.0Mpa, when mass concentration 30%~
60%, stop concentration, it is spare that collagen peptide concentrate pump is transported to intermediate storage tank；
(3) fruit powder dissolves: weighing formula ratio fruit powder powder, investment is stirred dissolution, stirs equipped in the material-compound tank of purified water
Mixing rate is 10r/min~30r/min, mixing time 15min~30min, prepares Fruit powder solution solubility 20%~50%；
(4) filter: Fruit powder solution introduces filtering bag filter with pump and is filtered, and filter bag aperture is in 300~600 mesh；
(5) mix: by ocean fish oligopeptide liquid, collagen peptide liquid, Fruit powder solution is proportionally transported to pump mixed
It closes to fill and be mixed, and be uniformly mixing to obtain mixed liquor, mixed liquid concentration is controlled 35%~50%；
(6) filter: mixed liquor is filtered through piping filter into intermediate storage tank；
(7) be spray-dried: setting inlet temperature at 170 DEG C~210 DEG C, outlet temperature at 80 DEG C~100 DEG C, mixed liquor from
Intermediate storage tank is transported to spray drying tower with pump and is spray-dried, and obtains mixed powder；
(8) fluidized bed granulation: mixed powder being put into fluidised bed granulator and is pelletized, and inlet air temperature is controlled at 60 DEG C
~100 DEG C, leaving air temp control at 40 DEG C~70 DEG C, the control of cabin temperature at 50 DEG C~80 DEG C, Granulation time 30min~
50min, moisture control 3%~7%, bulk density is controlled in 0.2g/cm3~0.4g/cm3；
(9) be sieved: the product that fluidized bed granulation is obtained is sieved, control partial size 40 mesh~100 mesh to get at
Product.
Compared with prior art, beneficial effects of the present invention are shown:
1. the present invention is effectively improved existing single hybrid mode using the combined fluidized bed granulating process of spray drying is redissolved,
Make to be sufficiently mixed between raw material, reaches uniformly mixed, color is uniform；
2. improving product mix efficiency, the prior art is mixed with limitation by solid mixing or solid-liquid, by mixing machine,
Certain revolution is kept, improving incorporation time is uniformly mixed raw material as far as possible, and the present invention can allow in a very short period of time raw material to carry out
It is sufficiently mixed, then harvests mixed powder with spray dryer；
3. promoting product quality, product mix is uniform, and material color stable homogeneous brings the promotion of product quality, with biography
System hybrid mode is compared, and product quality has greatly improved.
Specific embodiment
Present invention will be further explained below with reference to specific examples.These embodiments are interpreted as being merely to illustrate this hair
It is bright rather than limit the scope of the invention.After having read the content of the invention recorded, those skilled in the art can
To make various changes or modifications to the present invention, these equivalence changes and modification equally fall into model defined by the claims in the present invention
It encloses.
Embodiment 1
Product mouthfeel validation test
Collagen protein powder (honey peach is good for using collagen solid beverage obtained by embodiment 3 and commercially available soup minister again
Taste), amendment micromolecular collagen powder (acerola concentrate taste) etc. carries out mouthfeel and sense organ is blind comments, and randomly selects 10 people and carries out
Product appearance, smell are investigated in test, and color reconstitutes rear taste, are reconstituted the indexs such as color and are carried out comprehensive score evaluation.
Test index and standard are as follows:
Product appearance: color is uniform, and 20 points；One: 10 point of irregular colour；
Product odour: smell is pleasant, and 20 points；10~15 points of tanginess；Odorlessness 10 divides；Collagen smell, 1~10 point；
Product colour: color is satisfied, and 20 points；Color receives, and 10~15 points；Color does not receive, and 1~10 point；
Reconstitute rear taste: taste is satisfied, and 20 points；Taste receives, and 10~15 points；Taste does not receive, and 1~10 point；
Reconstitute color: color is cordial, and 20 points: color receives, and 10-15 points；Color does not receive, and 1~10 point；
Test result is as follows:
The blind evaluation and test of table 1 examination comprehensive score summarizes
As above-mentioned data it is found that albumen powder obtained by the present invention is compared with commercial like product, taste is pleasant, and breath is certainly
Right feature, mouthfeel degree of recognition are higher than commercial like product.
Embodiment 2
Improve skin moisture Efficacy experiments
1.1 experiment equipment
Laboratory apparatus: SHP88 skin analyzer: German Courage+Khazaka company；
Laboratory sample: 3 sample of embodiment, soup minister are good for collagen protein powder (honey peach taste) again.
1.2 study subject
According to the phase of improvement moisture of skin functional check method in " health food examine with assessment technique specification " 2003 editions
Close regulation, by the principle of voluntariness selection female subjects, the age 30 years old~50 years old, moisture of skin≤12.Subject Exclusion Criteria: 1.
Gestation or breast feeding women, allergic constitution person；2. being associated with cardiovascular and cerebrovascular, liver, kidney, haematopoietic disorder and cyclothymic
Person；3. taking article related with test specimen in a short time, the judgement person to result is influenced；4. not taking sample by test requirements document
Product or midway are detached from, and can not determine that effect or data do not affect the treatment or safety judgement person entirely.
1.3 experimental group
165 female volunteers for meeting the standard of being included in, are randomly divided into test group, positive controls, blank group, and every group each
55.Test group, positive controls, blank group general information no significant difference, are shown in Table 1.
2 testing crew age of table, moisture of skin harmony are examined
1.4 experimental method
Test group takes orally 3 sample of embodiment, one time a day, daily 6g, total 45d；Blank control group takes equivalent pure water；
Positive controls take orally soup minister and are good for collagen protein powder (honey peach taste) again, one time a day, daily 6g, total 45d；Subject is testing
Period stops using drug related with test objective, health food and cosmetics.Do not change original diet during test to practise
It is used, normal diet.
The observation of 1.5 safety indexes
Because this product raw material is food source, body will not be impacted by largely taking, and not consider general symptom, including
Situations such as spirit, sleep, diet, stool and urine；2. blood, urine, feces routine inspection；3. Liver and kidney function inspection；4. electrocardiogram, abdomen B
The index checkings such as super, X-ray chest-fluoroscopy inspection (being checked in on-test primary).
The observation of 1.6 efficiency indexes
Skin moisture content measurement, measurement site are forehead glabella skin.All subjects 30min before survey enters test
It is quiet to be measured in environment.Distilled water is dipped in cleaning cotton balls under rest state and cleans tested position, is dried rear 15min and is carried out moisture
Measurement, test front and back measurement work operated by same instrument, the same person.
1.7 statistical method
Subject uses itself two kinds of control design between group.Own control uses paired t-test, between group control using at
Group t is examined.Data statistics is handled using SPSS statistical software.
2. experimental result and analysis
2.1 determination of moisture results
3 moisture measurement result of table
Note:: * is compared with before test (p < 0.01)；△ is compared with after blank group test (p < 0.01)；Be with it is right
According to group test after compare (p < 0.05)
As shown in Table 2, after 45 days, test group, positive controls test front and back and with blank group comparison among groups, skin water
Dividing has significant difference (p < 0.01).The average value of test group moisture content of skin is increased to by 8.33 ± 1.09 before testing
12.74±1.44.The average value of positive controls moisture content of skin is increased to 10.34 by 8.42 ± 1.11 before testing ±
1.67；Test group test front and back and positive control comparison among groups, moisture of skin are variant (p < 0.05).Thus illustrate, the present invention
Have the function of to improve moisture of skin, and product effect is better than commercial like product.
3. conclusion
The present invention has the function of improving moisture of skin.
Embodiment 3
A kind of taste collagen solid beverage and preparation method thereof, by weight, 40 parts of ocean fish oligopeptide powder, glue
40 parts of former protein peptide powder, 20 parts of Cranberry powder.
Taste collagen solid beverage it is specific the preparation method is as follows:
(1) it ocean fish oligopeptide liquid system: (a) is crushed: fresh cod skin being put into crusher and is crushed；(b) it cleans:
Broken cod skin is put into service sink, 14h is cleaned and impregnated with 0.2mol/L NaOH solution, is then washed with clear water
To neutrality；(c) it crushes mashing: broken cod skin being put into colloid mill and is further crushed, purified water is added, is configured to expect
Liquor ratio is 1: 1, makes cod skin at slurry condition；(d) it digests: being digested using composite hydrolytic enzyme, composite hydrolytic enzyme is acidity
Protease, papain, neutral proteinase, additive amount are the 0.5 ‰ of cod skin quality, and hydrolysis temperature control is at 45 DEG C, enzyme
The time is solved in 2h, solution ph is controlled 5.0；(e) enzyme deactivation: after enzymatic hydrolysis, the temperature of enzymatic vessel is increased to 70 DEG C, is maintained
60min；(f) separation and purification: the feed liquid after enzyme deactivation is released from enzymatic vessel, is once filtered by plate filter, then
It is filtered by film and carries out secondary filter, by nanofiltration membrane desalination, obtain purification cod skin hydrolyzate；(g) it is concentrated: cod skin hydrolysis
Liquid is by negative pressure inspissator, and control vacuum degree is in 0.5Mpa, and when mass concentration is 48%, stopping is concentrated, by ocean fish oligopeptide
It is spare that concentrate pump is transported to intermediate storage tank；
(2) prepared by collagen peptide liquid: (a) being crushed: fresh Rofe skin being put into crusher and is crushed；(b) it cleans:
Broken Java tilapia skin is put into service sink, 14h is cleaned and impregnated with 0.2mol/L NaOH solution, then uses clear water
It is washed till neutrality, purified water is added, being configured to solid-liquid ratio is 1: 1；(c) it digests: being digested using composite hydrolytic enzyme, composite hydrolysis
Enzyme is neutral proteinase and bromelain, and additive amount is the 0.6 ‰ of cod skin quality, and hydrolysis temperature is controlled at 50 DEG C, enzymatic hydrolysis
Time controls in 2h, solution ph 6.0；(d) enzyme deactivation: after enzymatic hydrolysis, the temperature of enzymatic vessel is increased to 80 DEG C, maintains 30min；
(e) separation and purification: the feed liquid after enzyme deactivation is released from enzymatic vessel, is once filtered by plate filter, using film
Filtering carries out secondary filter, by nanofiltration membrane desalination, obtains purification Java tilapia skin hydrolyzate；(f) it is concentrated: Java tilapia skin hydrolyzate
By negative pressure inspissator, vacuum degree is controlled in 0.5Mpa, when mass concentration is 48%, stopping concentration is dense by ocean fish oligopeptide
It is spare that contracting liquid pump is transported to intermediate storage tank；
(3) Cranberry powder dissolves: weighing formula ratio Cranberry powder, investment is stirred equipped in the material-compound tank of purified water
Dissolution, stirring rate 10r/min, mixing time 15min prepare Cranberry powder solution concentration 24%；
(4) filter: Cranberry powder solution introduces filtering bag filter with pump and is filtered, and filter bag aperture is in 600 mesh；
(5) mix: by ocean fish oligopeptide liquid, collagen peptide liquid, Cranberry solution liquid pumps defeated according to formula rate
It is sent to mixing filling to be mixed, and is uniformly mixing to obtain mixed liquor, mixed liquid concentration is controlled 40%；
(6) filter: mixed liquor is filtered through piping filter into intermediate storage tank；
(7) be spray-dried: setting inlet temperature is at 210 DEG C, and at 90 DEG C, mixed liquor pumps defeated outlet temperature from intermediate storage tank
It is sent to spray drying tower to be spray-dried, obtains mixed powder；
(8) fluidized bed granulation: mixed powder being put into fluidised bed granulator and is pelletized, and inlet air temperature is controlled 80
DEG C, leaving air temp control is at 40 DEG C, and the control of cabin temperature is at 55 DEG C, Granulation time 30min, and moisture controls 3.5%, bulk density
Control is in 0.35g/cm3Left and right；
(9) be sieved: the product that fluidized bed granulation is obtained is sieved, control partial size 40 mesh~100 mesh to get at
Product.
Embodiment 4
A kind of taste collagen solid beverage and preparation method thereof, by weight, 50 parts of ocean fish oligopeptide powder, glue
35 parts of former protein peptide powder, 15 parts of blood orange powder.
Taste collagen solid beverage it is specific the preparation method is as follows:
(1) it ocean fish oligopeptide liquid system: (a) is crushed: fresh cod skin being put into crusher and is crushed；(b) it cleans:
Broken cod skin is put into service sink, 16h is cleaned and impregnated with 0.1mol/Lmol/L NaOH solution, then with clear
It is washed to neutrality；(c) it crushes mashing: broken cod skin being put into colloid mill and is further crushed, purified water is added, prepare
It is 1: 1.5 at solid-liquid ratio, makes cod skin at slurry condition；(d) it digests: being digested using composite hydrolytic enzyme, composite hydrolytic enzyme
For acid protease, papain, neutral proteinase, additive amount is the 0.6 ‰ of cod skin quality, and hydrolysis temperature is controlled 50
DEG C, enzymolysis time is controlled in 2.5h, solution ph 5.5；(e) enzyme deactivation: after enzymatic hydrolysis, being increased to 90 DEG C for the temperature of enzymatic vessel,
Maintain 30min；(f) separation and purification: the feed liquid after enzyme deactivation is released from enzymatic vessel, carries out primary mistake by plate filter
Filter filters using film and carries out secondary filter, by nanofiltration membrane desalination, obtains purification cod skin hydrolyzate；(g) it is concentrated: gadus
Skin hydrolyzate is by negative pressure inspissator, and control vacuum degree is in 0.7Mpa, and when mass concentration is 45%, stopping is concentrated, by marine fish
It is spare that oligopeptide concentrate pump is transported to intermediate storage tank；
(2) collagen peptide liquid is standby: (a) being crushed: fresh Java tilapia skin being put into crusher and is crushed；(b) it cleans:
Broken Java tilapia skin is put into service sink, 16h is cleaned and impregnated with 0.1mol/L NaOH solution, then uses clear water
It is washed till neutrality, purified water is added, being configured to solid-liquid ratio is 1: 1.5；(c) it digests: being digested using composite hydrolytic enzyme, Compound Water
Solution enzyme is acid protease, and neutral proteinase, additive amount is the 0.7 ‰ of Java tilapia skin quality, and hydrolysis temperature control is at 60 DEG C, enzyme
The time is solved in 3h, solution ph is controlled 5.5；(d) enzyme deactivation: after enzymatic hydrolysis, the temperature of enzymatic vessel is increased to 90 DEG C, is maintained
30min；(e) separation and purification: the feed liquid after enzyme deactivation is released from enzymatic vessel, is once filtered by plate filter, then
It is filtered by film and carries out secondary filter, by nanofiltration membrane desalination, obtain purification Java tilapia skin hydrolyzate；(f) it is concentrated: Java tilapia skin
Hydrolyzate is by negative pressure inspissator, and control vacuum degree is in 0.7Mpa, and when mass concentration is 45%, stopping is concentrated, by collagen
It is spare that peptide concentrate pump is transported to intermediate storage tank；
(3) blood orange powder dissolves: formula ratio blood orange powder is weighed, investment is stirred dissolution equipped in the material-compound tank of purified water,
Stirring rate is 20r/min, mixing time 20min, prepares blood orange powder solution concentration 30%；
(4) filter: blood orange powder solution introduces filtering bag filter with pump and is filtered, and filter bag aperture is in 300 mesh；
(5) mix: by ocean fish oligopeptide liquid, collagen peptide liquid, blood orange powder solution is proportionally transported to pump mixed
It closes to fill and be mixed, and be uniformly mixing to obtain mixed liquor, mixed liquid concentration is controlled 41%；
(6) filter: mixed liquor is filtered through piping filter into intermediate storage tank；
(7) be spray-dried: setting inlet temperature at 190 DEG C~210 DEG C, outlet temperature at 80 DEG C~90 DEG C, mixed liquor from
Intermediate storage tank is transported to spray drying tower with pump and is spray-dried, and obtains mixed powder；
(8) fluidized bed granulation: mixed powder being put into fluidised bed granulator and is pelletized, and inlet air temperature is controlled 75
DEG C, leaving air temp control is at 45 DEG C, and the control of cabin temperature is at 50 DEG C~60 DEG C, Granulation time 35min, and moisture controls 4.0%, heap
Product density domination is in 0.36g/cm；
(9) be sieved: the product that fluidized bed granulation is obtained is sieved, control partial size 40 mesh~100 mesh to get at
Product.
Embodiment 5
A kind of taste collagen solid beverage and preparation method thereof, by weight, 45 parts of ocean fish oligopeptide powder, glue
35 parts of former protein peptide powder, 20 parts of blueberry powder.
Taste collagen solid beverage it is specific the preparation method is as follows:
(1) it ocean fish oligopeptide liquid system: (a) is crushed: fresh cod skin being put into crusher and is crushed；(b) it cleans:
Broken cod skin is put into service sink, 15h is cleaned and impregnated with 0.25mol/L NaOH solution, is then washed with clear water
To neutrality；(c) it crushes mashing: broken cod skin being put into colloid mill and is further crushed, purified water is added, is configured to expect
Liquor ratio is 1: 2, makes cod skin at slurry condition；(d) it digests: being digested using composite hydrolytic enzyme, composite hydrolytic enzyme is acidity
Protease, neutral proteinase, additive amount are the 0.8 ‰ of cod skin quality, hydrolysis temperature control at 55 DEG C, enzymolysis time in 3h,
Solution ph is controlled 6.0；(e) enzyme deactivation: after enzymatic hydrolysis, the temperature of enzymatic vessel is increased to 85 DEG C, maintains 40min；(f) separation essence
System: the feed liquid after enzyme deactivation being released from enzymatic vessel, is once filtered by plate filter, carries out two using film filtering
Secondary filtering obtains purification cod skin hydrolyzate by nanofiltration membrane desalination；(g) be concentrated: cod skin hydrolyzate is concentrated by negative pressure
Device, control vacuum degree is in 0.8Mpa, and when mass concentration is 46%, ocean fish oligopeptide concentrate is used and pumps conveying by stopping concentration
It is spare to intermediate storage tank；
(2) collagen peptide liquid is standby: (a) being crushed: fresh Java tilapia skin being put into crusher and is crushed；(b) it cleans:
Broken Java tilapia skin is put into service sink, 15h is cleaned and impregnated with 0.25mol/LNaOH solution, then uses clear water
It is washed till neutrality, purified water is added, being configured to solid-liquid ratio is 1: 2；(d) it digests: using neutral proteinase, additive amount is Java tilapia skin
The 0.8 ‰ of quality, at 55 DEG C, enzymolysis time is controlled in 3h, solution ph 7.0 for hydrolysis temperature control；(e) enzyme deactivation: after enzymatic hydrolysis,
The temperature of enzymatic vessel is increased to 80 DEG C, maintains 50min；(f) separation and purification: the feed liquid after enzyme deactivation is released from enzymatic vessel,
It is once filtered by plate filter, is filtered using film and carry out secondary filter, by nanofiltration membrane desalination, obtain purification cod
Fish-skin hydrolyzate；(g) be concentrated: Java tilapia skin hydrolyzate controls vacuum degree in 0.8Mpa, works as mass concentration by negative pressure inspissator
46%, stop concentration, it is spare that collagen peptide concentrate pump is transported to intermediate storage tank；
(3) blueberry powder dissolves: formula ratio blueberry powder is weighed, investment is stirred dissolution equipped in the material-compound tank of purified water,
Stirring rate is 15r/min, mixing time 15min, prepares blueberry powder solution concentration 26%；
(4) filter: blueberry powder solution introduces filtering bag filter with pump and is filtered, and filter bag aperture is in 500 mesh；
(5) mix: by ocean fish oligopeptide liquid, collagen peptide liquid, blueberry powder solution is proportionally transported to pump mixed
It closes to fill and be mixed, and be uniformly mixing to obtain mixed liquor, mixed liquid concentration is controlled 40%；
(6) filter: mixed liquor is filtered through piping filter into intermediate storage tank；
(7) be spray-dried: setting inlet temperature is at 190 DEG C, and at 85 DEG C, mixed liquor pumps defeated outlet temperature from intermediate storage tank
It is sent to spray drying tower to be spray-dried, obtains mixed powder；
(8) fluidized bed granulation: mixed powder being put into fluidised bed granulator and is pelletized, and inlet air temperature is controlled 85
DEG C, leaving air temp control is at 55 DEG C, and the control of cabin temperature is at 60 DEG C, Granulation time 30min, and moisture controls 4.5%, bulk density
Control is in 0.36g/cm3；
(9) be sieved: the product that fluidized bed granulation is obtained is sieved, control partial size 40 mesh~100 mesh to get at
Product.
Embodiment 6
A kind of taste collagen solid beverage and preparation method thereof, by weight, ocean fish collagen oligopeptide powder 45
Part, 45 parts of collagen Gly-His-Lys, 10 parts of seabuckthorn fruit powder.
Taste collagen solid beverage it is specific the preparation method is as follows:
(1) it ocean fish oligopeptide liquid system: (a) is crushed: fresh cod skin being put into crusher and is crushed；(b) it cleans:
Broken cod skin is put into service sink, 13h is cleaned and impregnated with 0.35mol/L NaOH solution, is then washed with clear water
To neutrality；(c) it crushes mashing: broken cod skin being put into colloid mill and is further crushed, purified water is added, is configured to expect
Liquor ratio is 1: 3, makes cod skin at slurry condition；(d) it digests: being digested using composite hydrolytic enzyme, composite hydrolytic enzyme is acidity
Protease, neutral proteinase, additive amount are the 0.8 ‰ of cod skin quality, hydrolysis temperature control at 55 DEG C, enzymolysis time in 4h,
Solution ph is controlled 5.5；(e) enzyme deactivation: after enzymatic hydrolysis, the temperature of enzymatic vessel is increased to 90 DEG C, maintains 40min；(f) separation essence
System: the feed liquid after enzyme deactivation being released from enzymatic vessel, is once filtered by plate filter, carries out two using film filtering
Secondary filtering obtains purification cod skin hydrolyzate by nanofiltration membrane desalination；(g) be concentrated: cod skin hydrolyzate is concentrated by negative pressure
Device, control vacuum degree is in 1.0Mpa, and when mass concentration is 42%, ocean fish oligopeptide concentrate is used and pumps conveying by stopping concentration
It is spare to intermediate storage tank；
(2) prepared by collagen peptide liquid: (a) being crushed: fresh Java tilapia skin being put into crusher and is crushed；(b) clear
It washes: broken cod skin being put into service sink, 12~18h is cleaned and impregnated with 0.35mol/L NaOH solution, then
It is washed till neutrality with clear water, purified water is added, being configured to solid-liquid ratio is 1: 3；(c) it digests: being digested using composite hydrolytic enzyme, it is multiple
Conjunction hydrolase is acid protease, and papain, neutral proteinase, bromelain, additive amount is cod skin quality
0.5 ‰, at 50 DEG C, enzymolysis time is controlled in 2h, solution ph 5.0 for hydrolysis temperature control；(d) it enzyme deactivation: after enzymatic hydrolysis, will digest
The temperature of tank is increased to 70 DEG C, maintains 60min；(e) separation and purification: the feed liquid after enzyme deactivation is released from enzymatic vessel, by plate
Frame filter is once filtered, and is filtered using film and is carried out secondary filter, by nanofiltration membrane desalination, obtains the purification gadus severe edema due to hypofunction of the spleen
Solve liquid；(f) be concentrated: Java tilapia skin hydrolyzate controls vacuum degree in 1.0Mpa, when mass concentration exists by negative pressure inspissator
42%, stop concentration, it is spare that collagen peptide concentrate pump is transported to intermediate storage tank；
(3) seabuckthorn fruit powder dissolves: formula ratio seabuckthorn fruit powder is weighed, investment is stirred dissolution equipped in the material-compound tank of purified water,
Stirring rate is 20r/min, mixing time 30min, prepares seabuckthorn fruit powder solution concentration 28%；
(4) filter: seabuckthorn fruit powder solution introduces filtering bag filter with pump and is filtered, and filter bag aperture is in 500 mesh；
(5) mix: by ocean fish oligopeptide liquid, collagen peptide liquid, seabuckthorn fruit powder solution is proportionally transported to pump mixed
It closes to fill and be mixed, and be uniformly mixing to obtain mixed liquor, mixed liquid concentration is controlled 38%；
(6) filter: mixed liquor is filtered through piping filter into intermediate storage tank；
(7) be spray-dried: setting inlet temperature is at 200 DEG C, and at 80 DEG C, mixed liquor pumps defeated outlet temperature from intermediate storage tank
It is sent to spray drying tower to be spray-dried, obtains mixed powder；
(8) fluidized bed granulation: mixed powder being put into fluidised bed granulator and is pelletized, and inlet air temperature is controlled 80
DEG C, leaving air temp control is at 50 DEG C, and the control of cabin temperature is at 50 DEG C, Granulation time 45min, and moisture controls 4.2%, bulk density
Control is in 0.34g/cm3；
(9) be sieved: the product that fluidized bed granulation is obtained is sieved, control partial size 40 mesh~100 mesh to get at
Product.
Embodiment 7
A kind of taste collagen solid beverage and preparation method thereof, by weight, 50 parts of ocean fish oligopeptide powder, glue
25 parts of former protein peptide powder, 25 parts of pomegranate powder.
Taste collagen solid beverage it is specific the preparation method is as follows:
(1) it ocean fish oligopeptide liquid system: (a) is crushed: fresh cod skin being put into crusher and is crushed；(b) it cleans:
Broken cod skin is put into service sink, 14h is cleaned and impregnated with 0.45mol/L NaOH solution, is then washed with clear water
To neutrality；(c) it crushes mashing: broken cod skin being put into colloid mill and is further crushed, purified water is added, is configured to expect
Liquor ratio is 1: 2, makes cod skin at slurry condition；(d) it digests: being digested using composite hydrolytic enzyme, composite hydrolytic enzyme is acidity
Protease, papain, neutral proteinase, bromelain, additive amount are the 0.5 ‰ of cod skin quality, hydrolysis temperature control
At 45 DEG C, enzymolysis time is controlled in 1.5h, solution ph 5.0 system；(e) enzyme deactivation: after enzymatic hydrolysis, the temperature of enzymatic vessel is increased to
90 DEG C, maintain 30min；(f) separation and purification: the feed liquid after enzyme deactivation is released from enzymatic vessel, carries out one by plate filter
Secondary filtering filters using film and carries out secondary filter, by nanofiltration membrane desalination, obtains purification cod skin hydrolyzate；(g) it is concentrated:
Cod skin hydrolyzate is by negative pressure inspissator, and control vacuum degree is in 0.6Mpa, and when mass concentration is 44%, stopping concentration will be extra large
It is spare that foreign fish oligopeptide concentrate pump is transported to intermediate storage tank；
(2) prepared by collagen peptide liquid: (a) being crushed: fresh Java tilapia skin being put into crusher and is crushed；(b) clear
It washes: broken cod skin being put into service sink, 14h is cleaned and impregnated with 0.45mol/L NaOH solution, then with clear
It is washed to neutrality, purified water is added, being configured to solid-liquid ratio is 1: 2；(c) it digests: being digested using composite hydrolytic enzyme, pawpaw egg
White enzyme, neutral proteinase, bromelain, additive amount are the 0.5 ‰ of Java tilapia skin quality, and hydrolysis temperature control is at 50 DEG C, enzyme
The time is solved in 2h, solution ph is controlled 5.5；(d) enzyme deactivation: after enzymatic hydrolysis, the temperature of enzymatic vessel is increased to 85 DEG C, is maintained
45min；(e) separation and purification: the feed liquid after enzyme deactivation is released from enzymatic vessel, is once filtered by plate filter, then
It is filtered by film and carries out secondary filter, by nanofiltration membrane desalination, obtain purification cod skin hydrolyzate；(f) it is concentrated: the Tilapia mossambica severe edema due to hypofunction of the spleen
Liquid is solved by negative pressure inspissator, control vacuum degree is in 0.6Mpa, and when mass concentration is 44%, stopping is concentrated, by collagen peptide
It is spare that concentrate pump is transported to intermediate storage tank；
(3) pomegranate powder dissolves: formula ratio pomegranate powder is weighed, investment is stirred dissolution equipped in the material-compound tank of purified water,
Stirring rate is 15r/min, mixing time 20min, prepares pomegranate powder solution concentration 27%；
(4) filter: pomegranate powder solution introduces filtering bag filter with pump and is filtered, and filter bag aperture is in 600 mesh；
(5) mix: by ocean fish oligopeptide liquid, collagen peptide liquid, pomegranate powder solution is proportionally transported to pump mixed
It closes to fill and be mixed, and be uniformly mixing to obtain mixed liquor, mixed liquid concentration is controlled 39%；
(6) filter: mixed liquor is filtered through piping filter into intermediate storage tank；
(7) be spray-dried: setting inlet temperature is at 200 DEG C, and at 85 DEG C, mixed liquor pumps defeated outlet temperature from intermediate storage tank
It is sent to spray drying tower to be spray-dried, obtains mixed powder；
(8) fluidized bed granulation: mixed powder being put into fluidised bed granulator and is pelletized, and inlet air temperature is controlled 90
DEG C, leaving air temp control is at 50 DEG C, and the control of cabin temperature is at 60 DEG C, Granulation time 40min, and moisture controls 5%, bulk density control
System is in 0.38g/cm3；
(9) be sieved: the product that fluidized bed granulation is obtained is sieved, control partial size 40 mesh~100 mesh to get at
Product.
Embodiment 8
A kind of taste collagen solid beverage and preparation method thereof, by weight, 48 parts of ocean fish oligopeptide powder, glue
40 parts of former protein peptide powder, 12 parts of grape fruit powder.
Taste collagen solid beverage it is specific the preparation method is as follows:
(1) it ocean fish oligopeptide liquid system: (a) is crushed: fresh cod skin being put into crusher and is crushed；(b) it cleans:
Broken cod skin is put into service sink, 12h is cleaned and impregnated with 0.5mol/L NaOH solution, is then washed with clear water
To neutrality；(c) it crushes mashing: broken cod skin being put into colloid mill and is further crushed, purified water is added, is configured to expect
Liquor ratio is 1: 1, makes cod skin at slurry condition；(d) it digests: being digested using composite hydrolytic enzyme, composite hydrolytic enzyme is acidity
Protease, papain, additive amount are the 1.0 ‰ of cod skin quality, and hydrolysis temperature is controlled at 60 DEG C, and enzymolysis time exists
3.5h, solution ph are controlled 6.5；(e) enzyme deactivation: after enzymatic hydrolysis, the temperature of enzymatic vessel is increased to 90 DEG C, maintains 30min；(f)
Separation and purification: the feed liquid after enzyme deactivation is released from enzymatic vessel, is once filtered by plate filter, is filtered using film
Secondary filter is carried out, by nanofiltration membrane desalination, obtains purification cod skin hydrolyzate；(g) be concentrated: cod skin hydrolyzate passes through negative pressure
Inspissator, control vacuum degree is in 0.8Mpa, and when mass concentration is 47%, stopping concentration pumping ocean fish oligopeptide concentrate
It is spare to be transported to intermediate storage tank；
(2) prepared by collagen peptide liquid: (a) being crushed: fresh Java tilapia skin being put into crusher and is crushed；(b) clear
It washes: broken Java tilapia skin being put into service sink, 12h is cleaned and impregnated with 0.5mol/LNaOH solution, then with clear
It is washed to neutrality, being configured to solid-liquid ratio is 1: 1；(c) it digests: being digested using composite hydrolytic enzyme, composite hydrolytic enzyme is acidity
Protease, papain, neutral proteinase, one or more of bromelain, additive amount are cod skin quality
1.0 ‰, at 60 DEG C, enzymolysis time is controlled in 3.5h, solution ph 6.5 for hydrolysis temperature control；(d) enzyme deactivation: after enzymatic hydrolysis, by enzyme
The temperature of solution tank is increased to 90 DEG C, maintains 30min；(e) separation and purification: the feed liquid after enzyme deactivation is released from enzymatic vessel, is passed through
Plate filter is once filtered, and is filtered using film and is carried out secondary filter, by nanofiltration membrane desalination, obtains purification cod skin
Hydrolyzate；(f) be concentrated: Java tilapia skin hydrolyzate controls vacuum degree in 0.8Mpa, when mass concentration exists by negative pressure inspissator
47%, stop concentration, it is spare that collagen peptide concentrate pump is transported to intermediate storage tank；
(3) grape fruit powder dissolves: formula ratio grape fruit powder is weighed, investment is stirred dissolution equipped in the material-compound tank of purified water,
Stirring rate is 15r/min, mixing time 15min, prepares grape fruit powder solution concentration 20%；
(4) filter: grape fruit powder solution introduces filtering bag filter with pump and is filtered, and filter bag aperture is in 600 mesh；
(5) mix: by ocean fish oligopeptide liquid, collagen peptide liquid, grape fruit powder solution is proportionally transported to pump mixed
It closes to fill and be mixed, and be uniformly mixing to obtain mixed liquor, mixed liquid concentration is controlled 37%；
(6) filter: mixed liquor is filtered through piping filter into intermediate storage tank；
(7) be spray-dried: setting inlet temperature is at 190 DEG C, and at 80 DEG C, mixed liquor pumps defeated outlet temperature from intermediate storage tank
It is sent to spray drying tower to be spray-dried, obtains mixed powder；
(8) fluidized bed granulation: mixed powder being put into fluidised bed granulator and is pelletized, and inlet air temperature is controlled 80
DEG C, leaving air temp control is at 45 DEG C, and the control of cabin temperature is at 55 DEG C, Granulation time 50min, and moisture controls 4.5%, bulk density
Control is in 0.35g/cm3；
(9) be sieved: the product that fluidized bed granulation is obtained is sieved, control partial size 40 mesh~100 mesh to get at
Product.
Claims (5)
1. a kind of taste collagen solid beverage and preparation method thereof, which is characterized in that by weight, including with the following group
Point: 0~90 part of ocean fish oligopeptide powder, 0~90 part of collagen Gly-His-Lys, 1~90 part of Fruit powder.
2. a kind of taste collagen solid beverage according to claim 1 and preparation method thereof, which is characterized in that by weight
Measure part meter, including following components: 0~70 part of ocean fish oligopeptide powder, 0~70 part of collagen Gly-His-Lys, 10~30 parts of Fruit powder.
3. a kind of taste collagen solid beverage according to claim 1 or 2 and preparation method thereof, which is characterized in that
By weight, including following components: 40 parts of ocean fish collagen oligopeptide powder, 40 parts of collagen Gly-His-Lys, 20 parts of Fruit powder.
4. a kind of taste collagen solid beverage according to claim 1 to 3 and preparation method thereof, which is characterized in that institute
The Fruit powder stated is one or more of Cranberry powder, blueberry powder, blood orange powder, orange powder, seabuckthorn fruit powder, pomegranate powder, grape fruit powder.
5. a kind of taste collagen solid beverage according to claim 1 to 3 and preparation method thereof, which is characterized in that institute
The preparation process stated is as follows:
(1) prepared by ocean fish oligopeptide liquid: (a) being crushed: fresh cod skin being put into crusher and is crushed；(b) it cleans: will
Broken cod skin is put into service sink, with 0.1mol/L~0.5mol/L
12~18h is cleaned and impregnated to NaOH solution, is then washed till neutrality with clear water；(c) mashing is crushed: by broken gadus
Skin is put into colloid mill and is further crushed, and purified water is added, and being configured to solid-liquid ratio is 1: 1~1: 3, makes cod skin at slurry
State；(d) it digests: being digested using composite hydrolytic enzyme, composite hydrolytic enzyme is acid protease, papain, neutral protein
Enzyme, one or more of bromelain, additive amount are 0.5 ‰~the 1.0 ‰ of cod skin quality, and hydrolysis temperature is controlled 45
DEG C~60 DEG C, enzymolysis time is controlled in 1h~4h, solution ph 4.0~7.0；(e) enzyme deactivation: after enzymatic hydrolysis, by the temperature of enzymatic vessel
Degree is increased to 70 DEG C~90 DEG C, maintains 30min~60min；(f) separation and purification: the feed liquid after enzyme deactivation is released from enzymatic vessel,
It is once filtered by plate filter, is filtered using film and carry out secondary filter, by nanofiltration membrane desalination, obtain purification cod
Fish-skin hydrolyzate；(g) be concentrated: cod skin hydrolyzate controls vacuum degree in 0.5Mpa~1.0Mpa, works as matter by negative pressure inspissator
Concentration is measured 30%~60%, stops concentration, it is spare that fish oligopeptide concentrate pump in ocean is transported to intermediate storage tank；
(2) prepared by collagen peptide liquid: (a) being crushed: fresh Java tilapia skin being put into crusher and is crushed；(b) it cleans: will
Broken Java tilapia skin is put into service sink, cleaned and impregnate 12 with 0.1mol/L~0.5mol/L NaOH solution~
Then 18h is washed till neutrality with clear water, purified water is added, and being configured to solid-liquid ratio is 1: 1~1: 3；(c) it digests: using composite hydrolysis
Enzyme is digested, and composite hydrolytic enzyme is acid protease, papain, neutral proteinase, one of bromelain or
Several, additive amount is 0.5 ‰~the 1.0 ‰ of Java tilapia skin quality, and hydrolysis temperature is controlled at 45 DEG C~60 DEG C, and enzymolysis time is in 1h
~4h, solution ph are controlled 4.0~7.0；(d) enzyme deactivation: after enzymatic hydrolysis, the temperature of enzymatic vessel is increased to 70 DEG C~90 DEG C, dimension
Hold 30min~60min；(e) separation and purification: the feed liquid after enzyme deactivation is released from enzymatic vessel, carries out one by plate filter
Secondary filtering filters using film and carries out secondary filter, by nanofiltration membrane desalination, obtains purification Java tilapia skin hydrolyzate；(f) dense
Contracting: Java tilapia skin hydrolyzate by negative pressure inspissator, control vacuum degree in 0.5Mpa~1.0Mpa, when mass concentration 30%~
60%, stop concentration and collagen peptide concentrate pumps to be transported to intermediate storage tank spare；
(3) Fruit powder dissolves: weighing formula ratio fruit powder, for investment equipped with dissolution in the material-compound tank of purified water, is stirred, stirring is fast
Rate is 10r/min~30r/min, mixing time 15min~30min, prepares fruit powder solution concentration 20%~50%；
(4) filter: Fruit powder solution introduces filtering bag filter with pump and is filtered, and filter bag aperture is in 300 mesh~600 mesh；
(5) mix: by ocean fish oligopeptide liquid, collagen peptide liquid, Fruit powder solution is proportionally transported to mixing with pump and fills
It is mixed, and is uniformly mixing to obtain mixed liquor, mixed liquid concentration is controlled 35%~50%；
(6) filter: mixed liquor is filtered through piping filter into intermediate storage tank；
(7) be spray-dried: setting inlet temperature is at 170 DEG C~210 DEG C, and outlet temperature is at 80 DEG C~100 DEG C, and mixed liquor is from centre
Storage tank is transported to spray drying tower with pump and is spray-dried, and obtains mixed powder；
(8) fluidized bed granulation: mixed powder being put into fluidised bed granulator and is pelletized, inlet air temperature control 60 DEG C~
100 DEG C, at 40 DEG C~70 DEG C, cabin temperature is controlled at 50 DEG C~80 DEG C, Granulation time 30min~50min for leaving air temp control,
Moisture control 3%~7%, bulk density is controlled in 0.2g/cm3~0.4g/cm3；
(9) be sieved: the product that fluidized bed granulation is obtained is sieved, and controls partial size in 40 mesh~100 mesh to get finished product.
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| CN110279054A (en) * | 2019-07-26 | 2019-09-27 | 北京姿美堂生物技术有限公司 | A kind of collagen solid beverage and preparation method thereof improving " screen flesh " |
| WO2020258585A1 (en) * | 2019-06-27 | 2020-12-30 | 杭州妇帮医疗科技有限公司 | Health food for improvement of female fertility and preparation method thereof |
| CN112715815A (en) * | 2021-01-28 | 2021-04-30 | 海南省胜鑫生物科技有限责任公司 | Cod micromolecular collagen peptide solid beverage |
| CN112715959A (en) * | 2021-01-28 | 2021-04-30 | 海南省胜鑫生物科技有限责任公司 | Cod small-molecule collagen peptide vitamin C powder |
| CN112956703A (en) * | 2021-04-09 | 2021-06-15 | 果畅(苏州)健康科技有限公司 | Collagen peptide health food and production method thereof |
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