CN109758059A - A kind of stain removal bactericidal floor wet tissue and its preparation process - Google Patents
A kind of stain removal bactericidal floor wet tissue and its preparation process Download PDFInfo
- Publication number
- CN109758059A CN109758059A CN201910033463.0A CN201910033463A CN109758059A CN 109758059 A CN109758059 A CN 109758059A CN 201910033463 A CN201910033463 A CN 201910033463A CN 109758059 A CN109758059 A CN 109758059A
- Authority
- CN
- China
- Prior art keywords
- parts
- wet tissue
- added
- stirred
- minutes
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of stain removal bactericidal floor wet tissue and its preparation processes, including the wet tissue liquid that spunlace non-woven cloth and spunlace non-woven cloth are soaked with, the wet tissue liquid is prepared by following weight parts raw material: 10-20 parts of propylene glycol, 2-15 parts of Phenoxyethanols, 1-8 parts of methylparabens, 9-17 parts of propylbens, 5-10 parts of methylisothiazolinones, 80-90 parts of pure water, 1-3 portions of emollients, 1-3 parts of auxiliary agents, 20-30 parts of essence and 10-15 parts of disinfection antibacterial agents；The wet tissue liquid is prepared by following step: pure water being added into the stirred autoclave of 500mL, essence is then added, is stirred 30-35 minutes；Disinfection antibacterial agent, emollient are sequentially added into stirred autoclave again, is stirred 30-35 minutes；There is good anti-microbial property to have good moisturizing effect simultaneously for the invention.
Description
Technical field
The present invention relates to floor wet tissue technical fields, and in particular to a kind of stain removal bactericidal floor wet tissue and its preparation process.
Background technique
With the raising of people 's material life level, floor tile class is decorated throughout all kinds of places, on the market for them
All kinds of cleaning products of exploitation also come into being, but some tastes of all kinds of detergents are pungent, some are difficult to rinse, and corrode floor porcelain
Brick, residual chemicals can even have an adverse effect to people's health, and use at high cost.Floor wet tissue is to be with non-woven fabrics
Primary raw material addition wet tissue liquid is prepared；
The wet tissue liquid anti-microbial property of existing technique preparation is poor, while not having emollient, although being added to moisturizing
Agent, but the antioxygenic property of emollient is poor, service life is low.
Summary of the invention
In order to overcome above-mentioned technical problem, the purpose of the present invention is to provide a kind of stain removal bactericidal floor wet tissue and its systems
Standby technique, the wet tissue liquid anti-microbial property for solving existing technique preparation is poor, while not having emollient, although being added to profit
Skin agent, but the technical problems such as the antioxygenic property of emollient is poor, and service life is low.
The purpose of the present invention can be achieved through the following technical solutions:
A kind of stain removal bactericidal floor wet tissue, it is described wet including the wet tissue liquid that spunlace non-woven cloth and spunlace non-woven cloth are soaked with
Towel liquid is prepared by following weight parts raw material: 10-20 parts of propylene glycol, 2-15 parts of Phenoxyethanols, 1-8 parts of methylparabens, 9-
17 parts of propylbens, 5-10 parts of methylisothiazolinones, 80-90 parts of pure water, 1-3 portions of emollients, 1-3 parts of auxiliary agents, 20-30
Part essence and 10-15 parts of disinfection antibacterial agents；
The wet tissue liquid is prepared by following step:
1) pure water is added into the stirred autoclave of 500mL, essence is then added, is stirred 30-35 minutes；
2) disinfection antibacterial agent, emollient are sequentially added into stirred autoclave again, is stirred 30-35 minutes；
3) it is eventually adding propylene glycol, Phenoxyethanol, methylparaben, propylben, methylisothiazolinone and auxiliary agent,
Stirring 25-30 minutes, the pH value for adjusting solution in stirred autoclave is acidity, and mixed liquor is filtered, and wet tissue liquid both can be obtained；
Wherein, the disinfection antibacterial agent is prepared by following step:
10-15 parts of bentonites are put into conical flask, the dilute sulfuric acid of 220mL is then added, is heated in 95 DEG C of water-baths
And 3h is stirred with the revolving speed of 2000r/min, above-mentioned mixed liquor is separated in centrifuge, is washed with deionized water bentonite, directly
To pH close to 7；Above-mentioned bentonite is put into conical flask, 200mL deionized water is added, is slowly stirred in 55 DEG C of water-baths
Then 100mL neopelex is added in 10min, adjusting pH value after 30min is 6.5-7, and the AgNO of 100mL is added3,
Adjusting speed of agitator is 800r/min, stirs 2h, takes upper layer turbid solution to be centrifugated, is washed with deionized to no silver ion,
Dispersed with dehydrated alcohol and dried in 60 DEG C of baking ovens, 400 meshes are crossed after grinding, obtains carrying silver-colored bentonite, put it into another
In beaker, 30mL dehydrated alcohol is added, and dispersed 5 minutes with ultrasonic cleaner；1mLKH-560 coupling agent is added, continues point
It dissipates 5 minutes, disinfection antibacterial agent can be obtained.
A kind of preparation process of stain removal bactericidal floor wet tissue, the preparation process are prepared by following step:
Step 1: choose one of cotton pulp, wood pulp or staple fibre, through drying, compresses or vacuumize wet tissue original is made
Material unit body, is stored in the tank of manufacturing device, in case disinfection treatment；
Step 2: preparation wet tissue liquid, by propylene glycol, Phenoxyethanol, methylparaben, propylben, methyl-isothiazol
Quinoline ketone, pure water, emollient, auxiliary agent, essence and disinfection antibacterial agent are added sequentially in stirred autoclave, are mixed, and are adjusted
The pH value of solution is acidity in stirred autoclave, and mixed liquor is filtered, and wet tissue liquid can be obtained；
Step 3: taking wet tissue material unit body, cut, the fritter of cutting is put into wet tissue liquid immersion treatment, time
For 30min, sealed package later.
As a further solution of the present invention: the concentration of the dilute sulfuric acid is 1.5mol/L, the AgNO3Concentration be
0.02moL/L。
As a further solution of the present invention: the auxiliary agent is at least one of lactic acid, citric acid.
As a further solution of the present invention: the emollient is prepared by following step:
In the dry four-hole bottle of 250mL for being passed through mouth with thermometer, condenser, blender and nitrogen, addition C8 alkene,
Solvent toluene and platinum catalyst solution are passed through nitrogen, 75-80 DEG C of activation 30-40 minutes are heated under stirring, then in nitrogen
According to 2 DEG C per minute heatings, the reaction was continued under the protection of gas, then instills trisiloxanes, and reaction temperature is kept to stablize, and controls temperature
At 95 DEG C, after reaction 1-2 hours, after reaction mixture becomes clear, fully reacting is determined by gas method, is finally depressurized
Distillation removal solvent toluene, obtains clear liquid, and antioxidant is then added and is stirred 5-10 minutes to get moisturizing is arrived
Agent.
As a further solution of the present invention: the emollient is prepared by following weight parts raw material: 30-55 parts of C8Alkene
Hydrocarbon, 20-50 part toluene, 1-5 parts of platinum catalysts, 15-30 parts of trisiloxanes and 10-20 parts of antioxidant agent.
As a further solution of the present invention: the wet tissue liquid is prepared by following weight parts raw material: 15 parts of propylene glycol,
10 parts of Phenoxyethanols, 5 parts of methylparabens, 10 parts of propylbens, 8 parts of methylisothiazolinones, 85 parts of pure water, 2 parts of profits
Skin agent, 2 parts of auxiliary agents, 10 parts of essence and 12 parts of disinfection antibacterial agents.
Beneficial effects of the present invention:
1, wet tissue liquid has good anti-microbial property, is to use dodecane because bentonite is after the pre- modification of persulfuric acid
Base benzene sulfonic acid sodium salt carries out ion-exchange reactions and adsorption reaction as dispersing agent and silver nitrate, is combined with each other with silver ion, makes
It is standby to go out to carry silver-colored bentonite, there is good anti-microbial property, while being modified to spunlace non-woven cloth using silver-colored bentonite is carried, makes it
With good durable antibiotic performance, antibiotic rate joined active material Phenoxyethanol 97% or more, Phenoxyethanol tool
Toxic low, nonirritant and without damageability, performance is mild, is suitable as daily life sanitary disinfecting articles；
2, the emollient being prepared into, which is added in annex solution, can not only inhibit the greasy of product, while can increase skin
Salubrious and comfort level, do not influence other functional components play under the action of, can also contribute to the dispersion of various composition,
So that the annex solution of preparation has superior spreadability and smoothness, while by addition antioxidant, so that emollient
With good antioxidation.
Specific embodiment
Below in conjunction with the embodiment of the present invention, technical scheme in the embodiment of the invention is clearly and completely described,
Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based in the present invention
Embodiment, all other embodiment obtained by those of ordinary skill in the art without making creative efforts, all
Belong to the scope of protection of the invention.
Embodiment 1
A kind of stain removal bactericidal floor wet tissue, it is described wet including the wet tissue liquid that spunlace non-woven cloth and spunlace non-woven cloth are soaked with
Towel liquid is prepared by following weight parts raw material: 15 parts of propylene glycol, 10 parts of Phenoxyethanols, 5 parts of methylparabens, 10 parts of nipalgins
Propyl ester, 8 parts of methylisothiazolinones, 85 parts of pure water, 2 portions of emollients, 2 parts of auxiliary agents, 10 parts of essence and 12 parts of disinfection antibacterial agents；
The wet tissue liquid is prepared by following step:
1) pure water is added into the stirred autoclave of 500mL, essence is then added, is stirred 32 minutes；
2) disinfection antibacterial agent, emollient are sequentially added into stirred autoclave again, is stirred 33 minutes；
3) it is eventually adding propylene glycol, Phenoxyethanol, methylparaben, propylben, methylisothiazolinone and auxiliary agent,
Stirring 26 minutes, the pH value for adjusting solution in stirred autoclave is acidity, and mixed liquor is filtered, and wet tissue liquid both can be obtained；
Wherein, the disinfection antibacterial agent is prepared by following step:
13 parts of bentonites are put into conical flask, then be added 220mL dilute sulfuric acid, in 95 DEG C of water-baths heating and with
The revolving speed of 2000r/min stirs 3h, and above-mentioned mixed liquor is separated in centrifuge, is washed with deionized water bentonite, until pH
Close to 7；Above-mentioned bentonite is put into conical flask, 200mL deionized water is added, is slowly stirred 10min in 55 DEG C of water-baths,
Then 100mL neopelex is added, it is 6.8 that pH value is adjusted after 30min, and the AgNO of 100mL is added3, adjust stirring
Revolving speed is 800r/min, stirs 2h, takes upper layer turbid solution to be centrifugated, is washed with deionized to no silver ion, with anhydrous second
Alcohol disperses and dries in 60 DEG C of baking ovens, and 400 meshes are crossed after grinding, obtains carrying silver-colored bentonite, puts it into another beaker, add
Enter 30mL dehydrated alcohol, and is dispersed 5 minutes with ultrasonic cleaner；1mLKH-560 coupling agent is added, continues dispersion 5 minutes, i.e.,
Disinfection antibacterial agent can be obtained.
A kind of preparation process of stain removal bactericidal floor wet tissue, the preparation process are prepared by following step:
Step 1: choose one of cotton pulp, wood pulp or staple fibre, through drying, compresses or vacuumize wet tissue original is made
Material unit body, is stored in the tank of manufacturing device, in case disinfection treatment；
Step 2: preparation wet tissue liquid, by propylene glycol, Phenoxyethanol, methylparaben, propylben, methyl-isothiazol
Quinoline ketone, pure water, emollient, auxiliary agent, essence and disinfection antibacterial agent are added sequentially in stirred autoclave, are mixed, and are adjusted
The pH value of solution is acidity in stirred autoclave, and mixed liquor is filtered, and wet tissue liquid can be obtained；
Step 3: taking wet tissue material unit body, cut, the fritter of cutting is put into wet tissue liquid immersion treatment, time
For 30min, sealed package later.
Wherein, the concentration of the dilute sulfuric acid is 1.5mol/L, the AgNO3Concentration be 0.02moL/L；The auxiliary agent is
In citric acid；The emollient is prepared by following weight parts raw material: 40 parts of C8Alkene, 30 parts of toluene, 3 parts of platinum catalysts,
25 parts of trisiloxanes and 15 parts of antioxidant agent；
The emollient is prepared by following step:
In the dry four-hole bottle of 250mL for being passed through mouth with thermometer, condenser, blender and nitrogen, addition C8 alkene,
Solvent toluene and platinum catalyst solution are passed through nitrogen, and 78 DEG C are heated under stirring and is activated 35 minutes, then in the guarantor of nitrogen
According to 2 DEG C per minute heatings, the reaction was continued under shield, then instills trisiloxanes, and reaction temperature is kept to stablize, and controls temperature at 95 DEG C,
After reaction 1.5 hours, after reaction mixture becomes clear, fully reacting is determined by gas method, finally vacuum distillation is gone
Except solvent toluene, clear liquid is obtained, antioxidant is then added and is stirred 8 minutes to get emollient is arrived.
Embodiment 2
A kind of stain removal bactericidal floor wet tissue, it is described wet including the wet tissue liquid that spunlace non-woven cloth and spunlace non-woven cloth are soaked with
Towel liquid is prepared by following weight parts raw material: 10 parts of propylene glycol, 2 parts of Phenoxyethanols, 1 part of methylparaben, 9 parts of nipalgins third
Ester, 5 parts of methylisothiazolinones, 80 parts of pure water, 1 portion of emollient, 1 part of auxiliary agent, 20 parts of essence and 10 parts of disinfection antibacterial agents；
The wet tissue liquid is prepared by following step:
1) pure water is added into the stirred autoclave of 500mL, essence is then added, is stirred 30 minutes；
2) disinfection antibacterial agent, emollient are sequentially added into stirred autoclave again, is stirred 30 minutes；
3) it is eventually adding propylene glycol, Phenoxyethanol, methylparaben, propylben, methylisothiazolinone and auxiliary agent,
Stirring 25 minutes, the pH value for adjusting solution in stirred autoclave is acidity, and mixed liquor is filtered, and wet tissue liquid both can be obtained；
Wherein, the disinfection antibacterial agent is prepared by following step:
10 parts of bentonites are put into conical flask, then be added 220mL dilute sulfuric acid, in 95 DEG C of water-baths heating and with
The revolving speed of 2000r/min stirs 3h, and above-mentioned mixed liquor is separated in centrifuge, is washed with deionized water bentonite, until pH
Close to 7；Above-mentioned bentonite is put into conical flask, 200mL deionized water is added, is slowly stirred 10min in 55 DEG C of water-baths,
Then 100mL neopelex is added, it is 6.5 that pH value is adjusted after 30min, and the AgNO of 100mL is added3, adjust stirring
Revolving speed is 800r/min, stirs 2h, takes upper layer turbid solution to be centrifugated, is washed with deionized to no silver ion, with anhydrous second
Alcohol disperses and dries in 60 DEG C of baking ovens, and 400 meshes are crossed after grinding, obtains carrying silver-colored bentonite, puts it into another beaker, add
Enter 30mL dehydrated alcohol, and is dispersed 5 minutes with ultrasonic cleaner；1mLKH-560 coupling agent is added, continues dispersion 5 minutes, i.e.,
Disinfection antibacterial agent can be obtained.
A kind of preparation process of stain removal bactericidal floor wet tissue, the preparation process are prepared by following step:
Step 1: choose one of cotton pulp, wood pulp or staple fibre, through drying, compresses or vacuumize wet tissue original is made
Material unit body, is stored in the tank of manufacturing device, in case disinfection treatment；
Step 2: preparation wet tissue liquid, by propylene glycol, Phenoxyethanol, methylparaben, propylben, methyl-isothiazol
Quinoline ketone, pure water, emollient, auxiliary agent, essence and disinfection antibacterial agent are added sequentially in stirred autoclave, are mixed, and are adjusted
The pH value of solution is acidity in stirred autoclave, and mixed liquor is filtered, and wet tissue liquid can be obtained；
Step 3: taking wet tissue material unit body, cut, the fritter of cutting is put into wet tissue liquid immersion treatment, time
For 30min, sealed package later.
Wherein, the concentration of the dilute sulfuric acid is 1.5mol/L, the AgNO3Concentration be 0.02moL/L；The auxiliary agent is
In citric acid；The emollient is prepared by following weight parts raw material: 30 parts of C8Alkene, 20 parts of toluene, 1 part of platinum catalyst,
15 parts of trisiloxanes and 10 parts of antioxidant agent；
The emollient is prepared by following step:
In the dry four-hole bottle of 250mL for being passed through mouth with thermometer, condenser, blender and nitrogen, addition C8 alkene,
Solvent toluene and platinum catalyst solution are passed through nitrogen, and 75 DEG C are heated under stirring and is activated 30 minutes, then in the guarantor of nitrogen
According to 2 DEG C per minute heatings, the reaction was continued under shield, then instills trisiloxanes, and reaction temperature is kept to stablize, and controls temperature at 95 DEG C,
After reaction 1 hour, after reaction mixture becomes clear, fully reacting is determined by gas method, finally vacuum distillation removal
Solvent toluene obtains clear liquid, and antioxidant is then added and is stirred 5 minutes to get emollient is arrived.
Embodiment 3
A kind of stain removal bactericidal floor wet tissue, it is described wet including the wet tissue liquid that spunlace non-woven cloth and spunlace non-woven cloth are soaked with
Towel liquid is prepared by following weight parts raw material: 20 parts of propylene glycol, 15 parts of Phenoxyethanols, 8 parts of methylparabens, 17 parts of nipalgins
Propyl ester, 10 parts of methylisothiazolinones, 90 parts of pure water, 3 portions of emollients, 3 parts of auxiliary agents, 30 parts of essence and 15 parts of disinfecting, antimicrobials
Agent；
The wet tissue liquid is prepared by following step:
1) pure water is added into the stirred autoclave of 500mL, essence is then added, is stirred 35 minutes；
2) disinfection antibacterial agent, emollient are sequentially added into stirred autoclave again, is stirred 35 minutes；
3) it is eventually adding propylene glycol, Phenoxyethanol, methylparaben, propylben, methylisothiazolinone and auxiliary agent,
Stirring 30 minutes, the pH value for adjusting solution in stirred autoclave is acidity, and mixed liquor is filtered, and wet tissue liquid both can be obtained；
Wherein, the disinfection antibacterial agent is prepared by following step:
15 parts of bentonites are put into conical flask, then be added 220mL dilute sulfuric acid, in 95 DEG C of water-baths heating and with
The revolving speed of 2000r/min stirs 3h, and above-mentioned mixed liquor is separated in centrifuge, is washed with deionized water bentonite, until pH
Close to 7；Above-mentioned bentonite is put into conical flask, 200mL deionized water is added, is slowly stirred 10min in 55 DEG C of water-baths,
Then 100mL neopelex is added, it is 7 that pH value is adjusted after 30min, and the AgNO of 100mL is added3, adjust stirring and turn
Speed is 800r/min, stirs 2h, takes upper layer turbid solution to be centrifugated, is washed with deionized to no silver ion, uses dehydrated alcohol
Disperse and dried in 60 DEG C of baking ovens, 400 meshes are crossed after grinding, obtains carrying silver-colored bentonite, put it into another beaker, is added
30mL dehydrated alcohol, and dispersed 5 minutes with ultrasonic cleaner；1mLKH-560 coupling agent is added, continues dispersion 5 minutes
Obtain disinfection antibacterial agent.
A kind of preparation process of stain removal bactericidal floor wet tissue, the preparation process are prepared by following step:
Step 1: choose one of cotton pulp, wood pulp or staple fibre, through drying, compresses or vacuumize wet tissue original is made
Material unit body, is stored in the tank of manufacturing device, in case disinfection treatment；
Step 2: preparation wet tissue liquid, by propylene glycol, Phenoxyethanol, methylparaben, propylben, methyl-isothiazol
Quinoline ketone, pure water, emollient, auxiliary agent, essence and disinfection antibacterial agent are added sequentially in stirred autoclave, are mixed, and are adjusted
The pH value of solution is acidity in stirred autoclave, and mixed liquor is filtered, and wet tissue liquid can be obtained；
Step 3: taking wet tissue material unit body, cut, the fritter of cutting is put into wet tissue liquid immersion treatment, time
For 30min, sealed package later.
Wherein, the concentration of the dilute sulfuric acid is 1.5mol/L, the AgNO3Concentration be 0.02moL/L；The auxiliary agent is
In citric acid；The emollient is prepared by following weight parts raw material: 55 parts of C8Alkene, 50 parts of toluene, 5 parts of platinum catalysts,
30 parts of trisiloxanes and 20 parts of antioxidant agent；
The emollient is prepared by following step:
In the dry four-hole bottle of 250mL for being passed through mouth with thermometer, condenser, blender and nitrogen, addition C8 alkene,
Solvent toluene and platinum catalyst solution are passed through nitrogen, and 80 DEG C are heated under stirring and is activated 40 minutes, then in the guarantor of nitrogen
According to 2 DEG C per minute heatings, the reaction was continued under shield, then instills trisiloxanes, and reaction temperature is kept to stablize, and controls temperature at 95 DEG C,
After reaction 2 hours, after reaction mixture becomes clear, fully reacting is determined by gas method, finally vacuum distillation removal
Solvent toluene obtains clear liquid, and antioxidant is then added and is stirred 10 minutes to get emollient is arrived.
The working principle of the invention:
1, wet tissue liquid has good anti-microbial property, is to use dodecane because bentonite is after the pre- modification of persulfuric acid
Base benzene sulfonic acid sodium salt carries out ion-exchange reactions and adsorption reaction as dispersing agent and silver nitrate, is combined with each other with silver ion, makes
It is standby to go out to carry silver-colored bentonite, there is good anti-microbial property, while being modified to spunlace non-woven cloth using silver-colored bentonite is carried, makes it
With good durable antibiotic performance, antibiotic rate is 97% or more, while Phenoxyethanol has toxicity low, nonirritant and lossless
Bad property, performance is mild, is suitable as daily life sanitary disinfecting articles；
2, the emollient being prepared into, which is added in annex solution, can not only inhibit the greasy of product, while can increase skin
Salubrious and comfort level, do not influence other functional components play under the action of, can also contribute to the dispersion of various composition,
So that the annex solution of preparation has superior spreadability and smoothness, while by addition antioxidant, so that emollient
With good antioxidation.
In the description of this specification, the description of reference term " one embodiment ", " example ", " specific example " etc. means
Particular features, structures, materials, or characteristics described in conjunction with this embodiment or example are contained at least one implementation of the invention
In example or example.In the present specification, schematic expression of the above terms may not refer to the same embodiment or example.
Moreover, particular features, structures, materials, or characteristics described can be in any one or more of the embodiments or examples to close
Suitable mode combines.
Above content is only citing made for the present invention and explanation, affiliated those skilled in the art are to being retouched
The specific embodiment stated does various modifications or additions or is substituted in a similar manner, and without departing from invention or surpasses
More range defined in the claims, is within the scope of protection of the invention.
Claims (7)
1. a kind of stain removal bactericidal floor wet tissue, which is characterized in that the wet tissue being soaked with including spunlace non-woven cloth and spunlace non-woven cloth
Liquid, the wet tissue liquid are prepared by following weight parts raw material: 10-20 parts of propylene glycol, 2-15 parts of Phenoxyethanols, 1-8 parts of Ni Bo
Tortoise beetle ester, 9-17 part propylben, 5-10 parts of methylisothiazolinones, 80-90 parts of pure water, 1-3 portions of emollients, 1-3 parts
Auxiliary agent, 20-30 part essence and 10-15 parts of disinfection antibacterial agents；
The wet tissue liquid is prepared by following step:
1) pure water is added into the stirred autoclave of 500mL, essence is then added, is stirred 30-35 minutes；
2) disinfection antibacterial agent, emollient are sequentially added into stirred autoclave again, is stirred 30-35 minutes；
3) it is eventually adding propylene glycol, Phenoxyethanol, methylparaben, propylben, methylisothiazolinone and auxiliary agent, is stirred
25-30 minutes, the pH value for adjusting solution in stirred autoclave was acidity, and mixed liquor is filtered, and wet tissue liquid both can be obtained；
Wherein, the disinfection antibacterial agent is prepared by following step:
10-15 parts of bentonites are put into conical flask, then be added 220mL dilute sulfuric acid, in 95 DEG C of water-baths heating and with
The revolving speed of 2000r/min stirs 3h, and above-mentioned mixed liquor is separated in centrifuge, is washed with deionized water bentonite, until pH
Close to 7；Above-mentioned bentonite is put into conical flask, 200mL deionized water is added, is slowly stirred 10min in 55 DEG C of water-baths,
Then 100mL neopelex is added, adjusting pH value after 30min is 6.5-7, and the AgNO of 100mL is added3, adjusting stirs
Mixing revolving speed is 800r/min, stirs 2h, takes upper layer turbid solution to be centrifugated, is washed with deionized to no silver ion, use is anhydrous
Ethyl alcohol disperses and dries in 60 DEG C of baking ovens, and 400 meshes are crossed after grinding, obtains carrying silver-colored bentonite, put it into another beaker,
30mL dehydrated alcohol is added, and is dispersed 5 minutes with ultrasonic cleaner；1mLKH-560 coupling agent is added, continues dispersion 5 minutes,
Disinfection antibacterial agent can be obtained.
2. a kind of preparation process of stain removal bactericidal floor wet tissue, which is characterized in that the preparation process is prepared by following step
It arrives:
Step 1: choose one of cotton pulp, wood pulp or staple fibre, through drying, compresses or vacuumize wet tissue raw material list is made
First body, is stored in the tank of manufacturing device, in case disinfection treatment；
Step 2: preparation wet tissue liquid, by propylene glycol, Phenoxyethanol, methylparaben, propylben, methylisothiazolinone,
Pure water, emollient, auxiliary agent, essence and disinfection antibacterial agent are added sequentially in stirred autoclave, are mixed, and it is anti-to adjust stirring
It answers the pH value of solution in kettle for acidity, and mixed liquor is filtered, wet tissue liquid can be obtained；
Step 3: taking wet tissue material unit body, cut, the fritter of cutting is put into wet tissue liquid immersion treatment, the time is
30min, later sealed package.
3. a kind of stain removal bactericidal floor wet tissue according to claim 1, which is characterized in that the concentration of the dilute sulfuric acid is
1.5mol/L, the AgNO3Concentration be 0.02moL/L.
4. a kind of stain removal bactericidal floor wet tissue according to claim 1, which is characterized in that the auxiliary agent is lactic acid, lemon
At least one of acid.
5. a kind of stain removal bactericidal floor wet tissue according to claim 1, which is characterized in that the emollient passes through following steps
Suddenly it is prepared:
In the dry four-hole bottle of 250mL for being passed through mouth with thermometer, condenser, blender and nitrogen, C8 alkene, solvent is added
Toluene and platinum catalyst solution are passed through nitrogen, 75-80 DEG C of activation 30-40 minutes are heated under stirring, then in nitrogen
According to 2 DEG C per minute heatings, the reaction was continued under protection, then instills trisiloxanes, and reaction temperature is kept to stablize, and controls temperature 95
DEG C, after reaction 1-2 hours, after reaction mixture becomes clear, fully reacting is determined by gas method, is finally evaporated under reduced pressure
Solvent toluene is removed, clear liquid is obtained, antioxidant is then added and is stirred 5-10 minutes to get emollient is arrived.
6. a kind of stain removal bactericidal floor wet tissue according to claim 5, which is characterized in that the emollient is by following weight
Part raw material is prepared: 30-55 parts of C8Alkene, 20-50 part toluene, 1-5 parts of platinum catalysts, 15-30 parts of trisiloxanes and 10-20
Part antioxidant agent.
7. a kind of stain removal bactericidal floor wet tissue according to claim 1, which is characterized in that the wet tissue liquid is by following weight
Part raw material is prepared: 15 parts of propylene glycol, 10 parts of Phenoxyethanols, 5 parts of methylparabens, 10 parts of propylbens, 8 parts of methyl are different
Thiazolinone, 85 parts of pure water, 2 portions of emollients, 2 parts of auxiliary agents, 10 parts of essence and 12 parts of disinfection antibacterial agents.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910033463.0A CN109758059A (en) | 2019-01-14 | 2019-01-14 | A kind of stain removal bactericidal floor wet tissue and its preparation process |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910033463.0A CN109758059A (en) | 2019-01-14 | 2019-01-14 | A kind of stain removal bactericidal floor wet tissue and its preparation process |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109758059A true CN109758059A (en) | 2019-05-17 |
Family
ID=66453806
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910033463.0A Pending CN109758059A (en) | 2019-01-14 | 2019-01-14 | A kind of stain removal bactericidal floor wet tissue and its preparation process |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109758059A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110881916A (en) * | 2019-11-27 | 2020-03-17 | 铜陵麟安生物科技有限公司 | Degreasing wet tissue special for kitchen and preparation method thereof |
| CN115975445A (en) * | 2022-12-29 | 2023-04-18 | 绍兴百立杰环保科技有限公司 | Preparation method of mildew-proof antibacterial formaldehyde-removing diaphragm |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103876675A (en) * | 2012-12-23 | 2014-06-25 | 吕艳 | Production method of health wet wipe |
| CN105078795A (en) * | 2014-05-05 | 2015-11-25 | 金红叶纸业集团有限公司 | Skin moisturizing emulsion and skin moisturizing wet tissue |
| WO2016100118A1 (en) * | 2014-12-16 | 2016-06-23 | Momentive Performance Materials Inc. | Cosmetic composition and method of preparation |
| CN105725901A (en) * | 2016-02-01 | 2016-07-06 | 上海渊泉集币收藏品有限公司 | Wet tissue and preparation method thereof |
| CN105851015A (en) * | 2016-04-18 | 2016-08-17 | 句容东发生活用品有限公司 | Decontaminating disinfectant wet tissue for floor |
| CN107412090A (en) * | 2017-04-26 | 2017-12-01 | 烟台新时代健康产业日化有限公司 | A kind of long-acting bacteriostatic composition and its preparation method and application |
-
2019
- 2019-01-14 CN CN201910033463.0A patent/CN109758059A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103876675A (en) * | 2012-12-23 | 2014-06-25 | 吕艳 | Production method of health wet wipe |
| CN105078795A (en) * | 2014-05-05 | 2015-11-25 | 金红叶纸业集团有限公司 | Skin moisturizing emulsion and skin moisturizing wet tissue |
| WO2016100118A1 (en) * | 2014-12-16 | 2016-06-23 | Momentive Performance Materials Inc. | Cosmetic composition and method of preparation |
| CN105725901A (en) * | 2016-02-01 | 2016-07-06 | 上海渊泉集币收藏品有限公司 | Wet tissue and preparation method thereof |
| CN105851015A (en) * | 2016-04-18 | 2016-08-17 | 句容东发生活用品有限公司 | Decontaminating disinfectant wet tissue for floor |
| CN107412090A (en) * | 2017-04-26 | 2017-12-01 | 烟台新时代健康产业日化有限公司 | A kind of long-acting bacteriostatic composition and its preparation method and application |
Non-Patent Citations (2)
| Title |
|---|
| 朱岳 等: "膨润土抗菌剂的制备及在粘胶纤维中的应用", 《天津工业大学学报》 * |
| 罗儒显 等: "C8烯烃改性三硅氧烷润肤剂的合成研究", 《化工新型材料》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110881916A (en) * | 2019-11-27 | 2020-03-17 | 铜陵麟安生物科技有限公司 | Degreasing wet tissue special for kitchen and preparation method thereof |
| CN115975445A (en) * | 2022-12-29 | 2023-04-18 | 绍兴百立杰环保科技有限公司 | Preparation method of mildew-proof antibacterial formaldehyde-removing diaphragm |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| GB2354168A (en) | Antimicrobial agents | |
| US20090035339A1 (en) | Methods of Inactivating Viruses | |
| US2295505A (en) | Composition of matter | |
| DE202010018137U1 (en) | Cleaning agent containing carbamide and / or at least one derivative thereof | |
| JP2021524847A (en) | Antimicrobial composition | |
| CN109758059A (en) | A kind of stain removal bactericidal floor wet tissue and its preparation process | |
| CN111518635A (en) | Composite long-acting disinfection and bacteriostasis cleaning agent for medical textiles and preparation method thereof | |
| CN112137913A (en) | Washing-free disinfection gel and preparation method thereof | |
| CN110511826A (en) | It is a kind of to sterilize nontoxic machine dishwasher detergent and preparation method thereof | |
| WO2015124943A1 (en) | Cleaning composition | |
| CN103740491B (en) | A kind of Antibacterial laundry detergent and processing technology thereof | |
| JP6739772B2 (en) | Antibacterial/antiviral composition, aqueous solution, soap, hygiene product, household detergent, kitchen detergent, laundry detergent, residential antibacterial/antiviral agent, kitchen antibacterial/antiviral agent, clothing antibacterial/antiviral agent , Cosmetics, wet tissues and hand towels | |
| WO2018007805A1 (en) | Hygiene products | |
| CN101912358A (en) | Washing-free hand disinfectant and preparation method | |
| CN106520403A (en) | Silver carboxymethyl chitosan anti-microbial brightening laundry detergent and preparation method thereof | |
| DE10163650A1 (en) | Chlorine-free sanitary cleansing agent, e.g. for use in toilets, contains a component acting as a disinfectant when in aqueous solution at pH 1-4, a strong acid, a surfactant and optionally a Lewis acid or foaming agent | |
| US3251733A (en) | Antimicrobic compositions and process for protection of organic materials therewith | |
| KR101646606B1 (en) | Detergent composition of spray type and cleaning method using the same | |
| WO2005011385A1 (en) | Food-grade sanitizing composition | |
| CN109135939A (en) | A kind of dish washing liquid and preparation method thereof | |
| JPH0453531B2 (en) | ||
| JP4558934B2 (en) | Antibacterial agent | |
| CN106544178A (en) | A kind of silver carboxymethyl chitosan antibacterial softening laundry liquid and preparation method thereof | |
| CN106544177A (en) | A kind of silver carboxymethyl chitosan antimicrobial laundry liquid and preparation method thereof | |
| CN106135274A (en) | A kind of medicated clothing skin degerming agent composition containing iodine and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20190517 |