CN109736105A - A kind of multi-color spectrum ecological health colouring method of dyestuff - Google Patents
A kind of multi-color spectrum ecological health colouring method of dyestuff Download PDFInfo
- Publication number
- CN109736105A CN109736105A CN201910205650.2A CN201910205650A CN109736105A CN 109736105 A CN109736105 A CN 109736105A CN 201910205650 A CN201910205650 A CN 201910205650A CN 109736105 A CN109736105 A CN 109736105A
- Authority
- CN
- China
- Prior art keywords
- indigo naturalis
- indigo
- fabric
- dyeing
- lemon
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Abstract
The invention discloses a kind of multi-color spectrum ecological health colouring methods of dyestuff, including Chinese medicine indigo naturalis to the non-reduced dyeing of polyester fiber, spun polyester thread, dacron or terylene non-woven fabric and Chinese medicine indigo naturalis to the non-reduced of blend polyester fiber, blend polyester yarn, blend polyester intertexture or non-woven fabrics and reduction one one bath two-step dyeing.The present invention controllably completes the non-reduced directly upper dye of indigo in Chinese medicine indigo naturalis and two kinds of ingredients of indigo red individually or collectively completions, obtains blue, purple and bluish violet series chromatography；With healthcare function.
Description
Technical field
The present invention relates to a kind of multi-color spectrum ecological health colouring methods of dyestuff.
Background technique
With the improvement of living standards, increasingly pay attention to for clothing health, environmental protection, comfortable etc., natural dye also by
The concern of people.What natural dye was mainly obtained from plant, animal or mineral resources, biological degradability is good, with environment phase
Capacitive is good, non-toxic to humans, the little or no dyestuff by chemical process.Wherein vegetable colour is mostly Chinese medicine,
In dyeing course, drug and flavor component are absorbed together with pigment by fabric, and the fabric after making dye has special health care to human body
Function.
Indigo naturalis is dicotyledon medicine acanthaceous vegetable acanthaceous indigo, dicotyledon medicine leguminous plant wood indigo plant, dicotyledon
Drying pigment in medicine cruciferae isatis, careless smalt or polygonaceae plant indigo plant leaf.As the raw medicine for having pharmacological action,
It is widely used in warm disease excess heat, macula, snakebite and bugbite etc..It has recently been demonstrated that the indigo red in Chinese medicine indigo naturalis also have it is anti-
The function of the tumours such as leukaemia.
Chinese medicine indigo naturalis can be used as natural dye, be using the indigo ingredient in indigo naturalis, due to indigo not soluble in water, naturally
Cellulose fibre (cotton, fiber crops, viscose glue) and protein fibre (silk, hair) dyeing Shi Yaoyong reducing agent are reduced into hidden under alkaline condition
The sodium salt of colour solid contaminates in ability；Due to indigo leuco compound sodium salt to polyester fiber without affinity, indigo naturalis shows dyeing terylene
Technology is to be dyed the indigo reduction in indigo naturalis again at vat acid with reducing agent.
Problems and disadvantages of the existing technology:
(1) prior art Chinese medicine indigo naturalis can be used as natural dye to textile dyeing, be using the indigo ingredient in indigo naturalis,
Fiber is above contaminated after leuco compound sodium salt or vat acid need to be reduced by indigo naturalis, process is complicated；
(2) dyeing of existing Chinese medicine indigo naturalis utilizes the indigo ingredient in indigo naturalis, so, Shade of Dyed Textiles is blue, chromatography
It is single；
(3) because only that indigo upper dye therein, the indigo red with healthcare functions such as anti-leukocythemias are unutilized.
Summary of the invention
The purpose of the present invention is to provide a kind of methods, and easy, product dyestuff with health care function multi-color spectrum ecology is protected
Strong colouring method.
The technical solution of the invention is as follows:
A kind of multi-color spectrum ecological health colouring method of dyestuff, it is characterized in that: including Chinese medicine indigo naturalis to polyester fiber, spun polyester thread
Or dacron non-reduced dyeing and Chinese medicine indigo naturalis it is non-to blend polyester fiber, blend polyester yarn or blend polyester intertexture
Reduction and reduction one one bath two-step dyeing；
(1) non-reduced dyeing of the Chinese medicine indigo naturalis to polyester fiber, spun polyester thread or dacron, terylene non-woven fabric, including it is following
Step:
Indigo naturalis 10-50%o.w.f, first plus on a small quantity lemon extract or plant ash extracting solution grind 20-30min in indigo naturalis, so
Afterwards, by bath raio 1:10-1:50, remaining extracting solution is added, dyes 30-60min at 100-120 DEG C；
The lemon extract or plant ash extracting solution are to extract to obtain with extractant by lemon or plant ash, and extractant is second
Alcohol: water quality ratio=2:8-1:9 extracts 30-60 minutes；The mass volume ratio of lemon or plant ash and extractant is 10-100g/
L；
(2) Chinese medicine indigo naturalis to the non-reduced of blend polyester fiber, blend polyester yarn, blend polyester intertexture or non-woven fabrics and is gone back
Former one bath two-step dyeing, including the following steps:
Step 1: indigo naturalis 10-50%o.w.f, is added lemon extract 100g/L, first plus on a small quantity lemon extract is ground in indigo naturalis
Then mill 20-30min is added remaining lemon extract by bath raio 1:10-1:50, dyes 30- at 100-120 DEG C
60min；
The lemon extract is to extract to obtain with extractant by lemon, and extractant is ethyl alcohol: water quality ratio=2:8-1:9, leaching
It mentions 30-60 minutes；The mass volume ratio of lemon and extractant is 100g/L；
Step 2: adding 50 g/L of glucose or one of tyrosine or tea polyphenols in the above raffinate, add 100 g/L of plant ash,
The cloth that the first step contaminates is put into, 60-120 min is dyed at 40-60 DEG C；Dye finishes, washing, and air is ventilative.
First add described in method (1) and grind 20-30min in indigo naturalis on a small quantity, refers to and first add lemon extract or plant ash
20-30min is ground in indigo naturalis in the 10 ~ 30% of extracting solution total amount.
Grind first plus in indigo naturalis 20-30min on a small quantity described in method (2), refer to first plus lemon extract total amount 10 ~
30% grinds 20-30min in indigo naturalis.
In method (1):
(1) the indigo naturalis dyed fabric of lemon extract is to contaminate in indigo red, and fabric is aubergine, with the increase of indigo naturalis dosage,
Aubergine is more obvious, and when indigo naturalis 50% o.w.f of dosage, fabric is purplish red colour-stable；
(2) the indigo naturalis dyed fabric of plant ash extracting solution be indigo upper dye, with the raising of temperature, indigo red be converted into it is indigo,
Fabric is blue；
(3) as indigo naturalis 50%o.w.f, the indigo naturalis dyed textiles of lemon extract are aubergine, this dyeing residual liquid can continue weight
Counterstain, and the dyed fabric of blue color effect is obtained, residual liquid rate 100%；
It (4), can be in fabric to dacron high temperature tie dyeing as indigo naturalis 50%o.w.f with the indigo naturalis dye liquor of lemon extract
It is upper to obtain outside white ground, purple and blue two kinds of colors can also be obtained；
(5) the resistance to fastness of fading of soaping of the non-reduced dyed fabric of dacron indigo naturalis is 4-5 grades, and cotton, to wash staining fastness be 5 grades.
A kind of dyestuff-Chinese medicine indigo naturalis multi-color spectrum health care staining technique the present invention relates to full terylene and containing polyester fabric.
The directly upper dyeing and weaving object of the non-reduced method of Chinese medicine indigo naturalis has been invented, process flow has been simplified；Indigo naturalis need to be passed through by solving the prior art
Fiber, the problem of process complexity are above contaminated after being reduced into leuco compound sodium salt or vat acid.
It is non-reduced straight that the present invention controllably completes indigo in Chinese medicine indigo naturalis and two kinds of ingredients of indigo red individually or collectively completions
Dye is connected, blue, purple and bluish violet series chromatography is obtained；Purple textile is that indigo red dyes to obtain, and there is anti-leukocythemia etc. to protect
Health-care function.
The dyeing of existing Chinese medicine indigo naturalis is solved using the indigo ingredient in indigo naturalis, Shade of Dyed Textiles is blue, color
Compose the unutilized problem of indigo reds single, with healthcare functions such as anti-leukocythemias.
Using the method for raffinate dual-staining, the purple dyed fabric for arriving blue color effect, residual liquid rate 100% can be obtained.Clearly
Clean environmental protection.
It, can be in fabric to dacron high temperature tie dyeing as indigo naturalis 50%o.w.f with the indigo naturalis dye liquor of lemon extract
It is upper to obtain outside white ground, purple and blue two kinds of colors can also be obtained.
Dacron indigo naturalis dyed fabric is resistance to, and soap fastness of fading is 4-5 grades, and cotton, to wash staining fastness be 5 grades.
Detailed description of the invention
Present invention will be further explained below with reference to the attached drawings and examples.
Fig. 1 is lemon extract, ethanol/water, Chinese medicine indigo naturalis dye bath multi-color spectrum is added for plant ash extracting solution and color is joined
Number.
Fig. 2 is the multiple dyed color parameter of Chinese medicine indigo naturalis dyeing residual liquid and chromatography.
Illustrate: when a positive value, the inclined feux rouges of sample, positive value is bigger, and feux rouges is more.When b negative value, the inclined blue light of sample, negative value is got over
Greatly, blue light light is more.
The extracting solution of the ethanol/water of lemon and plant ash is colorless and transparent.
Specific embodiment
Embodiment 1:
Non-reduced dyeing using Chinese medicine indigo naturalis to polyester fiber, spun polyester thread or dacron, non-woven fabrics, including following step
It is rapid:
Indigo naturalis 10-50%o.w.f, first plus on a small quantity lemon extract or plant ash extracting solution (10% or so) grind 20- in indigo naturalis
Then 30min is added remaining extracting solution by bath raio 1:10-1:50, dyes 30-60min at 100-120 DEG C；
The lemon extract or plant ash extracting solution are to extract to obtain with extractant by lemon or plant ash, and extractant is second
Alcohol: water quality ratio=2:8-1:9 extracts 30-60 minutes；The mass volume ratio of lemon or plant ash and extractant is 10-100g/
L.The extracting solution of the ethanol/water of lemon and plant ash is colorless and transparent.
The dyeing effect and advantage of generation:
(1) the indigo naturalis dyed fabric of lemon extract is to contaminate in indigo red, and fabric is aubergine, with the increase of indigo naturalis dosage,
Aubergine is more obvious, and when indigo naturalis 50% o.w.f of dosage, fabric aubergine is basicly stable.
(2) the indigo naturalis dyed fabric of plant ash extracting solution is indigo upper dye, and with the raising of temperature, indigo red is converted into indigo
Indigo plant, fabric are blue.
(3) as indigo naturalis 50%o.w.f, the indigo naturalis dyed textiles of lemon extract are aubergine, this dyeing residual liquid can be after
Continuous dual-staining, and the dyed fabric of blue color effect is obtained, residual liquid rate 100%.Clean and environmental protection.
(4) the indigo naturalis dye liquor for using lemon extract, as indigo naturalis 50%o.w.f, to dacron high temperature tie dyeing, Ke Yi
It is obtained on fabric outside white ground, purple and blue two kinds of colors can also be obtained.
(5) dacron indigo naturalis dispersion dyeing fabric it is resistance to soap fade fastness be 4-5 grades, being stained with (cotton is washed) color fastness is 5
Grade.
Embodiment 2:
Using Chinese medicine indigo naturalis to blend polyester fiber, blend polyester yarn or blend polyester intertexture, non-woven fabrics it is non-reduced with also
Former one bath two-step dyeing, including the following steps:
Step 1: indigo naturalis 10-50%o.w.f, first plus on a small quantity lemon extract (10% or so) grinds 20-30min in indigo naturalis,
Then, remaining extracting solution is added by bath raio 1:10-1:50, dyes 30-60min at 100-120 DEG C；
The lemon extract is to extract to obtain with extractant by lemon, and extractant is ethyl alcohol: water quality ratio=2:8-1:9, leaching
It mentions 30-60 minutes；The mass volume ratio of lemon and extractant is 100g/L；
Step 2: adding 50 g/L of glucose or one of tyrosine or tea polyphenols in the above raffinate, add 100 g/L of plant ash,
The cloth that the first step contaminates is put into, 60-120 min is dyed at 40-60 DEG C；Dye finishes, washing, and air is ventilative.
Dyed by an above one bath two-step, make terylene purple, with other fibers of blend polyester (cotton, fiber crops, silk,
Wool etc.) it is fiber, yarn, fabric that blue obtains purple and blue color blending effect.
Claims (4)
1. the multi-color spectrum ecological health colouring method of a kind of dyestuff, it is characterized in that: including Chinese medicine indigo naturalis to polyester fiber, Polyester Yarns
The non-reduced dyeing of line or dacron, terylene non-woven fabric；Chinese medicine indigo naturalis is to blend polyester fiber, blend polyester Sha Xian terylene
The non-reduced and reduction one one bath two-step dyeing of blended fabric or non-woven fabrics；
(1) non-reduced dyeing of the Chinese medicine indigo naturalis to polyester fiber, spun polyester thread or dacron, terylene non-woven fabric, including it is following
Step:
Indigo naturalis 10-50%o.w.f, first plus on a small quantity lemon extract or plant ash extracting solution grind 20-30min in indigo naturalis, so
Afterwards, by bath raio 1:10-1:50, remaining extracting solution is added, dyes 30-60min at 100-120 DEG C；
The lemon extract or plant ash extracting solution are to extract to obtain with extractant by lemon or plant ash, and extractant is second
Alcohol: water quality ratio=2:8-1:9 extracts 30-60 minutes；The mass volume ratio of lemon or plant ash and extractant is 10-100g/
L；
(2) Chinese medicine indigo naturalis to the non-reduced of blend polyester fiber, blend polyester yarn, blend polyester intertexture or non-woven fabrics and is gone back
Former one bath two-step dyeing, including the following steps:
Step 1: indigo naturalis 10-50%o.w.f, first plus on a small quantity lemon extract grinds 20-30min in indigo naturalis, then, by bath
Remaining lemon extract is added than 1:10-1:50, dyes 30-60min at 100-120 DEG C；
The lemon extract is to extract to obtain with extractant by lemon, and extractant is ethyl alcohol: water quality ratio=2:8-1:9, leaching
It mentions 30-60 minutes；The mass volume ratio of lemon and extractant is 100g/L；
Step 2: adding 50 g/L of glucose or one of tyrosine or tea polyphenols in the above raffinate, add 100 g/L of plant ash,
The cloth that the first step contaminates is put into, 60-120 min is dyed at 40-60 DEG C；Dye finishes, washing, and air is ventilative.
2. the multi-color spectrum ecological health colouring method of a kind of dyestuff according to claim 1, it is characterized in that: in method (1)
It is described to grind first plus in indigo naturalis 20-30min on a small quantity, refer to first plus lemon extract or plant ash extracting solution total amount 10 ~ 30%
20-30min is ground in indigo naturalis.
3. the multi-color spectrum ecological health colouring method of a kind of dyestuff according to claim 1, it is characterized in that: in method (2)
It is described to grind first plus in indigo naturalis 20-30min on a small quantity, refer to first plus lemon extract total amount 10 ~ 30% is ground in indigo naturalis
20-30min。
4. a kind of multi-color spectrum ecological health colouring method of dyestuff according to claim 1, it is characterized in that: in method (1):
(1) the indigo naturalis dyed fabric of lemon extract is to contaminate in indigo red, and fabric is aubergine, with the increase of indigo naturalis dosage,
Aubergine is more obvious, and when indigo naturalis 50% o.w.f of dosage, fabric is purplish red colour-stable；
(2) the indigo naturalis dyed fabric of plant ash extracting solution be indigo upper dye, with the raising of temperature, indigo red be converted into it is indigo,
Fabric is blue；
(3) as indigo naturalis 50%o.w.f, the indigo naturalis dyed textiles of lemon extract are aubergine, this dyeing residual liquid can continue weight
Counterstain, and the dyed fabric of blue color effect is obtained, residual liquid rate 100%；
It (4), can be in fabric to dacron high temperature tie dyeing as indigo naturalis 50%o.w.f with the indigo naturalis dye liquor of lemon extract
It is upper to obtain outside white ground, purple and blue two kinds of colors can also be obtained；
(5) the resistance to fastness of fading of soaping of dacron indigo naturalis dispersion dyeing fabric is 4-5 grades, and cotton, to wash staining fastness be 5 grades.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910205650.2A CN109736105B (en) | 2019-03-19 | 2019-03-19 | Multi-color spectrum ecological health-care dyeing method of dye |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910205650.2A CN109736105B (en) | 2019-03-19 | 2019-03-19 | Multi-color spectrum ecological health-care dyeing method of dye |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109736105A true CN109736105A (en) | 2019-05-10 |
| CN109736105B CN109736105B (en) | 2021-07-09 |
Family
ID=66370837
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910205650.2A Active CN109736105B (en) | 2019-03-19 | 2019-03-19 | Multi-color spectrum ecological health-care dyeing method of dye |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109736105B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115679718A (en) * | 2022-11-07 | 2023-02-03 | 东华大学 | Method for dyeing cotton yarn by indigo non-reduction dye-penetration method |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2009024310A (en) * | 2007-07-19 | 2009-02-05 | Kanehisa:Kk | Quick dyeing and deep dyeing method with natural indigo and indigo dye |
| CN101696553A (en) * | 2009-10-30 | 2010-04-21 | 五邑大学 | Method for dying fabrics by color combination of vegetable dyes |
| CN104088173A (en) * | 2014-06-10 | 2014-10-08 | 河南工程学院 | Union dyeing method of polyester-cotton fabric with indigo dye |
| CN106906674A (en) * | 2017-03-14 | 2017-06-30 | 无锡城市职业技术学院 | A kind of method that natural botanical extraction liquid dyes mohair yarn fiber |
-
2019
- 2019-03-19 CN CN201910205650.2A patent/CN109736105B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2009024310A (en) * | 2007-07-19 | 2009-02-05 | Kanehisa:Kk | Quick dyeing and deep dyeing method with natural indigo and indigo dye |
| CN101696553A (en) * | 2009-10-30 | 2010-04-21 | 五邑大学 | Method for dying fabrics by color combination of vegetable dyes |
| CN104088173A (en) * | 2014-06-10 | 2014-10-08 | 河南工程学院 | Union dyeing method of polyester-cotton fabric with indigo dye |
| CN106906674A (en) * | 2017-03-14 | 2017-06-30 | 无锡城市职业技术学院 | A kind of method that natural botanical extraction liquid dyes mohair yarn fiber |
Non-Patent Citations (6)
| Title |
|---|
| 张瑞萍 等: "珊瑚绒面料的中药青黛染色", 《印染》 * |
| 张艳 等: "青黛在涤纶织物上染色性能的研究", 《染料与染色》 * |
| 汪大骆 等: "中药青黛对水刺涤纶无纺布的还原染色工艺研究", 《印染助剂》 * |
| 郑微微 等: "《不同细度聚酯纤维对靛蓝染料的吸附性能》", 《广西轻工业》 * |
| 郝龙云 等: "涤纶织物靛蓝染色", 《印染》 * |
| 韦苏娟 等: "涤纶纤维的青黛染色工艺", 《南通大学学报（自然科学版）》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115679718A (en) * | 2022-11-07 | 2023-02-03 | 东华大学 | Method for dyeing cotton yarn by indigo non-reduction dye-penetration method |
| CN115679718B (en) * | 2022-11-07 | 2024-04-09 | 东华大学 | Method for dyeing cotton yarn by indigo non-reduction dyeing method |
Also Published As
| Publication number | Publication date |
|---|---|
| CN109736105B (en) | 2021-07-09 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN100549102C (en) | The preparation method of spatholobus stem natural dye | |
| CN101349020A (en) | Method for dyeing modified cellulose fiber fabric on rhubarb and curcuma longa dyes | |
| CN102587153A (en) | Method for dyeing silk broadcloth by using plant dye solution extracted from lily | |
| CN106087476A (en) | Dyeing technique on a kind of colorant match based on vegetable colour | |
| CN100462501C (en) | Yellow (red) native mordant agent of natural plant dye and its using method | |
| CN109162117A (en) | Using natural pigment to the method for cotton fabric green colouring | |
| CN101307571A (en) | Dyeing method of lotus in natural fiber | |
| CN105970697A (en) | Color fixing process method for natural dyeing of textiles | |
| CN104047099A (en) | Manufacturing technology of health-care type blended knitted fabric | |
| CN106906674A (en) | A kind of method that natural botanical extraction liquid dyes mohair yarn fiber | |
| CN106012589A (en) | Edible dye-dyed cashmere and method for preparing yarns | |
| CN104233860A (en) | Process for ferric salt after-mordanting of real silk fabric by using henna pigment | |
| CN109736105A (en) | A kind of multi-color spectrum ecological health colouring method of dyestuff | |
| CN102965978B (en) | Dyeing method for hybrid loose fibers | |
| CN106192460B (en) | A kind of Phellinus pigment dyeing method of silk fabric | |
| CN109181351A (en) | A kind of natural textile dyestuff for bamboo fibre | |
| CN108948781A (en) | The preparation method of spun gold emperor's chrysanthemum natural dye and the natural dye and colouring method prepared by this method | |
| CN107130446A (en) | Red pigments extracts and its to the method for textile dyeing in a kind of cape jasmine fruit | |
| CN108252119B (en) | Polygonum multiflorum dye solution, preparation method and application thereof, and fabric dyeing method | |
| CN102924965A (en) | Tea tree fruit reddish brown pigment and its preparation method and use | |
| CN106638027B (en) | A method of being derived from the natural dye dyeing wool fabric of Testa sojae atricolor | |
| CN104233862A (en) | Process for aluminum salt pre-mordanting and after-dyeing for real silk fabric by using henna pigment | |
| CN103741506A (en) | Dyeing method for underwear fabric | |
| CN114182542A (en) | Method for dyeing green by vegetable dye one-bath process | |
| KR101554433B1 (en) | Natural dying method using zizania latifolia |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |