CN109721430A - The production method of moderate-element water-soluble fertilizer - Google Patents
The production method of moderate-element water-soluble fertilizer Download PDFInfo
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- CN109721430A CN109721430A CN201910179649.7A CN201910179649A CN109721430A CN 109721430 A CN109721430 A CN 109721430A CN 201910179649 A CN201910179649 A CN 201910179649A CN 109721430 A CN109721430 A CN 109721430A
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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Abstract
The invention discloses the production method of moderate-element water-soluble fertilizer, 1) water-soluble calcareous fertilizer, water-soluble fertiliser containing magnesium, water-soluble boron fertilizer are added to the water to obtain moderate-element solution；2) ion exchange resin and hydrochloric acid is added in weathering coal dust, obtains fulvic acid solution；3) fruit tree boiling is centrifuged, obtains filtrate and waste residue；4) by Radix Glycyrrhizae, honeysuckle and peppermint tanning, medical fluid and the dregs of a decoction are obtained；5) by 1) moderate-element solution, 2) fulvic acid solution, 3) filtrate and 4) medical fluid is uniformly mixed, are added urea, Diammonium phosphate (DAP), zymocyte liquid；6) plant ash, maize flour, 3) waste residue, 4) dregs of a decoction mixing is added in stalk, animal argol, 5) mixed liquor is added, fermentation；It is separated by solid-liquid separation, obtains fertilizer.The production technology of fertilizer of the present invention greatly enriches the nutrition of fertilizer, and passes through the combination of mineral resources fulvic acid and biochemical fulvic acid, and Yellow humic acid fertilizer obtained is also stabilized under solid forms, improves antibacterial, the bacteriostasis of soil.
Description
Technical field
The present invention relates to a kind of fertilizer production methods, and in particular to the production method of moderate-element water-soluble fertilizer.
Background technique
Nutrient necessary to plant growth includes 17 kinds, and according to nutrient required in growing process
Number, be divided into a great number of elements, moderate-element, microelement, wherein a great number of elements is C, H, O, N, P, K, and moderate-element is
Ca, Mg, S, microelement Fe, B, Mn, Cu, Zn, Mo, Cl, Ni.Existing moderate-element is concentrated mainly on nitric acid calcareous fertilisers, nitre
Sour magnesium, water etc. carry out being mixed with according to a certain percentage, this makes the nutrition of moderate-element Water soluble fertilizer excessively single, product
Matter is poor, and cost of material is higher.Fulvic acid is component part most active in humic acid, its molecular weight is smaller, readily soluble
Yu Shui, flocculation resistance can be good, are used widely in fertilizer field.Fulvic acid is both a kind of soil conditioner and a plant
Object growth regulator, while the still synergist of inorganic fertilizer, sustained release agent.It is reported that fulvic acid can significantly improve crop to nitrogen,
The absorption rate of phosphorus, potassium.Phosphate fertilizer utilization efficiency is set to improve 8.4%~44.1%；Potassium utilization rate is set to improve 17.7%；With ammonium bicarbonate
It is used in mixed way with ammonium hydroxide, 3.37 times and 11.80 times are respectively increased in utilization rate.There are mainly two types of fulvic acid sources, and one is straw
Stalk etc. extracts after biofermentation, referred to as biochemical fulvic acid；One is being extracted in minerals, referred to as mineral resources fulvic acid.It is existing
Yellow humic acid fertilizer be all made of single biochemical fulvic acid or mineral resources fulvic acid, and biochemical fulvic acid finished product is easy in air
Water suction deliquesces, therefore is only applicable to liquid form, and transport uses very inconvenient.Mineral resources fulvic acid is due to being applicable in intolerant to hard water
Range is extremely restricted, and production method makes fulvic acid conversion recovery rate low.
Summary of the invention
Problem to be solved by this invention is that existing moderate-element water-soluble fertilizer yin-yang is single, while Yellow humic acid fertilizer is equal
Using single biochemical fulvic acid or mineral resources fulvic acid, and biochemical fulvic acid finished product hygroscopic deliquescence in air, therefore
It is only applicable to liquid form, transport uses very inconvenient.Mineral resources fulvic acid is since intolerant to hard water, the scope of application is greatly limited
System, and production method makes fulvic acid conversion recovery rate low, and it is an object of the present invention to provide a kind of production of moderate-element water-soluble fertilizer
Method greatly enriches the nutrition of fertilizer by the combination of moderate-element and fulvic acid, and passes through mineral resources fulvic acid and life
The combination for changing fulvic acid, enables Yellow humic acid fertilizer obtained to be also stabilized under solid forms, and preparation process is significantly
The conversion ratio for improving fulvic acid, fertilizer obtained be capable of it is good promote phosphorus nitrogen absorption, improve soil antibacterial,
Bacteriostasis.
The technical solution adopted by the invention is as follows:
The production method of moderate-element water-soluble fertilizer, Yellow humic acid fertilizer include the raw material of following mass component: water-soluble calcium
10-12 parts fertile, water-soluble 12-15 parts of fertiliser containing magnesium, 2-3 parts of water-soluble boron fertilizer, 8-10 parts of weathering coal dust, ion exchange resin 30-35
Part, 6-8 parts of hydrochloric acid, 100-110 parts of tree branch, 15-20 parts of stalk, 5-10 parts of animal argol, 8-10 parts of plant ash, maize flour
5-8 parts, 3-5 parts of Radix Glycyrrhizae, 4-7 parts of honeysuckle, 1-2 parts of peppermint, 2-3 parts of ammonium sulfate, 1-4 parts of urea, 3-6 parts of ammonium hydrogen carbonate, phosphorus
Sour diammonium 1-3 parts, 30-35 parts of zymocyte liquid；1) production technology includes the following steps: water-soluble calcareous fertilizer, water-soluble fertiliser containing magnesium, water
Dissolubility boron fertilizer, which is mixed to join in suitable quantity of water, stirs evenly to obtain moderate-element solution；2) weathered coal powder is milled down to 100 mesh hereinafter,
And ion exchange resin and hydrochloric acid is added, after the reaction was completed, coal dust slag and resin are settled, and be centrifuged to obtain water of the top containing fulvic acid
Solution；3) tree branch is crushed, crosses 80-100 mesh, ammonium sulfate and suitable quantity of water is added, at a temperature of 100 DEG C -105 DEG C, steamed
2-3h is boiled, ammonium hydrogen carbonate is then added and stirs evenly, centrifugation is squeezed after 3-5h, is filtered to get filtrate and waste residue；4) by Radix Glycyrrhizae, gold and silver
Colored and peppermint is put into suitable quantity of water after mashing, and boils 1.5-2h at a temperature of being heated to 95-100 DEG C, filters to obtain medical fluid and the dregs of a decoction；5)
Will by the moderate-element solution in step 1), 2) in the medical fluid of fulvic acid solution, the filtrate of step 3) and step 4) be uniformly mixed,
And urea is added, and Diammonium phosphate (DAP), zymocyte liquid mixing；6) stalk, animal argol are crushed and are added plant ash, maize flour, step
It is rapid 3) in waste residue, the dregs of a decoction in step 4) uniformly mix, be put into fermentation vat, then add mixed liquor obtained in step 5)
Enter wherein, closed fermenting tank is sufficiently fermented；7) after sufficiently fermenting, fermentation material is heated, and persistently leads into fermentation vat
Enter steam 25-30min, wherein heating temperature is 78-80 DEG C；8) finally fermentation material is separated by solid-liquid separation, filtrate is taken to be made
Grain obtains moderate-element water-soluble fertilizer.
The production technology of fertilizer of the present invention greatly enriches the battalion of fertilizer by the combination of moderate-element and fulvic acid
It supports, and passes through the combination of mineral resources fulvic acid and biochemical fulvic acid, enable Yellow humic acid fertilizer obtained under solid forms
Also it is stabilized, and preparation process greatly improves the conversion ratio of fulvic acid, fertilizer obtained being capable of good promotion phosphorus nitrogen
The absorption of element improves antibacterial, the bacteriostasis of soil.Under the premise of using a small amount of moderate-element water-soluble fertilizer, pass through
It in conjunction with fulvic acid, had both solved the problems, such as that moderate-element nutrition was single, and had reduced cost of material, and overcome two kinds of not homologous Huangs
The limitation of rotten acid.Wherein the aqueous solution with fulvic acid is made by ion-exchange using coal dust first in the preparation of fulvic acid,
Then the biochemical fulvic acid in tree branch is extracted, is mixed with mineral resources fulvic acid obtained in weathering coal dust, finally
It is mixed and ferments with components such as fruit tree tree slag, stalk, animal argol, maize flour, plant ash, Chinese medicine dregs, can make
It obtains coal dust adequately to be extracted with the fulvic acid in fruit tree, while making the full of nutrition of fertilizer obtained, in animal argol
Nutrition not only enrich and environmental protection, be free of chemical industry additive, wherein after sufficiently fermenting, heat to fermentation material, and to fermentation
Steam 25-30min is continually fed into pond, wherein heating temperature is 78-80 DEG C, is passed through the material after fermentation by steam, can
Make sufficiently to adhere between biochemical fulvic acid and solid material, changing biochemical fulvic acid can only be with limitation existing for liquid form；Using
Radix Glycyrrhizae, honeysuckle, peppermint have good antibacterial, bacteriostasis, and fertilizer of the invention is mixed by the extracting solution and the dregs of a decoction of three
It is fermented together with fruit tree tree slag above-mentioned etc., so that fertilizer has good antibacterial ability.
The fermentation vat includes the fermentation pond body of tapered doleiform shape, the neck mouth outer wall and fermentation pond body pond body of pond body of fermenting
Circumferentially it is sequentially connected with arc-shaped liquid-in pipe between outer wall, the both ends of the liquid-in pipe phase between neck mouth and pond body respectively
It is connected to, is arranged with open-topped drainage box at pond body neck mouth of fermenting, multiple liquid-entering holes are offered on the side wall of drainage box, enter liquid
The position in hole corresponds and is connected to liquid-in pipe bottle mouth position apical position；Fermentation offers the discharging with valve on pond body bottom surface
Hole, it further includes open-topped outer pond that the upper surface of discharge hole, which is covered with dismountable sealing strainer, and fermentation pond body is placed on
In outer pond, Wai Chizhong is provided with heating device.
Fermentation vat of the invention when in use first removes drainage box from the bottleneck of fermentation pond body, then will be all
Solid material is put into pond, and drainage box is fastened on bottle mouth position and rotating is aligned its liquid-entering hole with liquid-in pipe, will be mixed
Zymocyte liquid, medical fluid, filtrate mixed liquor pour into drainage box, and then liquid is split even into every liquid-in pipe, then by
Liquid-in pipe enters in fermentation pond body from fermentation vat body sidewall surrounding is evenly dispersed, uniformly mixes with solid material, significantly
The mixing uniformity improved between liquid and solid material；Wherein, fermentation is placed on Wai Chizhong, and Wai Chizhong is provided with heating dress
It sets, after fermentation, the intracorporal fertilizer of fermentation vat can be heated by heating device, finally need to discharge and solid-liquid divides
From when, will fermentation pond body proposed from outer pond, valve is then opened, so that water-soluble fertilizer liquid is drained into from discharge hole
In outer pond, and expect admittedly, stays in fermentation pond body, play preliminary separation of solid and liquid.
The production method of moderate-element water-soluble fertilizer, Yellow humic acid fertilizer include the raw material of following mass component: weathering coal dust 8
Part, 30 parts of ion exchange resin, 6 parts of hydrochloric acid, 100 parts of tree branch, 15 parts of stalk, 5 parts of animal argol, 8 parts of plant ash, corn
5 parts of face, 3 parts of Radix Glycyrrhizae, 4 parts of honeysuckle, 1 part of peppermint, 2 parts of ammonium sulfate, 1 part of urea, 3 parts of ammonium hydrogen carbonate, 1 part of Diammonium phosphate (DAP), hair
30 parts of yeast-like fungi liquid.
The production method of moderate-element water-soluble fertilizer, Yellow humic acid fertilizer include the raw material of following mass component: weathering coal dust
10 parts, 35 parts of ion exchange resin, 8 parts of hydrochloric acid, 110 parts of tree branch, 20 parts of stalk, 10 parts of animal argol, 10 parts of plant ash,
8 parts of maize flour, 5 parts of Radix Glycyrrhizae, 7 parts of honeysuckle, 2 parts of peppermint, 3 parts of ammonium sulfate, 4 parts of urea, 6 parts of ammonium hydrogen carbonate, Diammonium phosphate (DAP) 3
Part, 35 parts of zymocyte liquid.
The production method of moderate-element water-soluble fertilizer, Yellow humic acid fertilizer include the raw material of following mass component: weathering coal dust 9
Part, 33 parts of ion exchange resin, 7 parts of hydrochloric acid, 105 parts of tree branch, 18 parts of stalk, 8 parts of animal argol, 9 parts of plant ash, corn
7 parts of face, 4 parts of Radix Glycyrrhizae, 6 parts of honeysuckle, 1 part of peppermint, 2 parts of ammonium sulfate, 3 parts of urea, 4 parts of ammonium hydrogen carbonate, 2 parts of Diammonium phosphate (DAP), hair
32 parts of yeast-like fungi liquid.
It is connected with rubber hose at the drainage outer box wall liquid-entering hole, in the bottle mouth position that drainage box is placed on to fermentation pond body
When, by every rubber hose alignment liquid-in pipe and be inserted first, such solution when being flowed into liquid-in pipe from liquid-entering hole,
It can be avoided solution between drainage box and bottleneck by rubber hose to leak.
The side wall in the outer pond and bottom surface are interconnected hollow structure, and inlet tube is connected on the side wall in outer pond and is gone out
Liquid pipe can be passed through cooling fluid into a set of cups hollow structure when in use, so that fertilizer temperature in fermentation pond body be made uniformly to decline.
In conclusion by adopting the above-described technical solution, the beneficial effects of the present invention are:
1. the production method of moderate-element water-soluble fertilizer of the present invention, passes through the knot of mineral resources fulvic acid and biochemical fulvic acid
It closes, Yellow humic acid fertilizer obtained is also stabilized under solid forms, and preparation process greatly improves yellow corruption
The conversion ratio of acid, fertilizer obtained are capable of the absorption of good promotion phosphorus nitrogen, improve antibacterial, the bacteriostasis of soil；
2. the production method of moderate-element water-soluble fertilizer of the present invention, the fermentation vat of use can make liquid and solid material
It is uniformly mixed in pan feeding, greatly improves the mixing uniformity between liquid and solid material, improve the quality of fermentation.
Detailed description of the invention
In order to illustrate the technical solution of the embodiments of the present invention more clearly, below will be to needed in the embodiment attached
Figure is briefly described, it should be understood that the following drawings illustrates only certain embodiments of the present invention, therefore is not construed as pair
The restriction of range for those of ordinary skill in the art without creative efforts, can also be according to this
A little attached drawings obtain other relevant attached drawings, in which:
Fig. 1 is schematic structural view of the invention；
The pond body marked in the figure: 1- ferments, 2- liquid-in pipe, 3- drainage box, 4- liquid inlet, the outer pond 5-.
Specific embodiment
In order to make the objectives, technical solutions, and advantages of the present invention clearer, with reference to the accompanying drawings and embodiments, right
The present invention is further elaborated.It should be appreciated that described herein, specific examples are only used to explain the present invention, not
For limiting the present invention, i.e., described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is logical
The component for the embodiment of the present invention being often described and illustrated herein in the accompanying drawings can be arranged and be designed with a variety of different configurations.
Therefore, the detailed description of the embodiment of the present invention provided in the accompanying drawings is not intended to limit below claimed
The scope of the present invention, but be merely representative of selected embodiment of the invention.Based on the embodiment of the present invention, those skilled in the art
Member's every other embodiment obtained without making creative work, shall fall within the protection scope of the present invention.
It should be noted that the relational terms of term " first " and " second " or the like be used merely to an entity or
Operation is distinguished with another entity or operation, and without necessarily requiring or implying between these entities or operation, there are any
This actual relationship or sequence.Moreover, the terms "include", "comprise" or its any other variant be intended to it is non-exclusive
Property include so that include a series of elements process, method, article or equipment not only include those elements, but also
Further include other elements that are not explicitly listed, or further include for this process, method, article or equipment it is intrinsic
Element.In the absence of more restrictions, the element limited by sentence "including a ...", it is not excluded that including described
There is also other identical elements in the process, method, article or equipment of element.
Feature and performance of the invention are described in further detail below with reference to embodiment.
Embodiment one
One kind that present pre-ferred embodiments provide, the production method of moderate-element water-soluble fertilizer, Yellow humic acid fertilizer include
The raw material of following mass component: 10 parts of water-soluble calcareous fertilizer, water-soluble 12 parts of fertiliser containing magnesium, 2 parts of water-soluble boron fertilizer, 8 parts of weathering coal dust, from
30 parts of sub-exchange resin, 6 parts of hydrochloric acid, 100 parts of tree branch, 15 parts of stalk, 5 parts of animal argol, 8 parts of plant ash, maize flour 5
Part, 3 parts of Radix Glycyrrhizae, 4 parts of honeysuckle, 1 part of peppermint, 2 parts of ammonium sulfate, 1 part of urea, 3 parts of ammonium hydrogen carbonate, 1 part of Diammonium phosphate (DAP), zymophyte
30 parts of liquid.Production technology includes the following steps: 1) to be mixed to join water-soluble calcareous fertilizer, water-soluble fertiliser containing magnesium, water-soluble boron fertilizer suitable
Moderate-element solution is stirred evenly to obtain in amount water；2) weathered coal powder is milled down to 100 mesh hereinafter, and be added ion exchange resin and
Hydrochloric acid settles coal dust slag and resin, and be centrifuged to obtain aqueous solution of the top containing fulvic acid after the reaction was completed；3) by tree branch powder
It is broken, 80 meshes are crossed, ammonium sulfate and suitable quantity of water is added, at a temperature of 100 DEG C, then boiling 2h is added ammonium hydrogen carbonate and stirs evenly,
Centrifugation is squeezed after 3h, is filtered to get filtrate and waste residue；4) by Radix Glycyrrhizae, honeysuckle and peppermint are put into suitable quantity of water after mashing, and are heated to
1.5h is boiled at a temperature of 95 DEG C, filters to obtain medical fluid and the dregs of a decoction；5) will by the moderate-element solution in step 1), 2) in fulvic acid it is molten
The medical fluid of liquid, the filtrate of step 3) and step 4) is uniformly mixed, and urea is added, Diammonium phosphate (DAP), zymocyte liquid mixing；6) by straw
Stalk, animal argol are crushed and are added plant ash, maize flour, the waste residue in step 3), the dregs of a decoction in step 4) and uniformly mix, and are put into
In fermentation vat, then mixed liquor obtained in step 5) is added thereto, closed fermenting tank is sufficiently fermented；7) to sufficiently send out
After ferment, fermentation material is heated, and steam 25min is continually fed into fermentation vat, wherein heating temperature is 78 DEG C；It 8) finally will hair
Ferment material is separated by solid-liquid separation, and filtrate is taken to carry out being granulated to obtain moderate-element water-soluble fertilizer.
Embodiment two
One kind that present pre-ferred embodiments provide, the production method of moderate-element water-soluble fertilizer, Yellow humic acid fertilizer include
The raw material of following mass component: 12 parts of water-soluble calcareous fertilizer, water-soluble 15 parts of fertiliser containing magnesium, 3 parts of water-soluble boron fertilizer, 10 parts of weathering coal dust,
35 parts of ion exchange resin, 8 parts of hydrochloric acid, 110 parts of tree branch, 20 parts of stalk, 10 parts of animal argol, 10 parts of plant ash, corn
8 parts of face, 5 parts of Radix Glycyrrhizae, 7 parts of honeysuckle, 2 parts of peppermint, 3 parts of ammonium sulfate, 4 parts of urea, 6 parts of ammonium hydrogen carbonate, 3 parts of Diammonium phosphate (DAP), hair
35 parts of yeast-like fungi liquid.Production technology includes the following steps: that 1) water-soluble calcareous fertilizer, water-soluble fertiliser containing magnesium, water-soluble boron fertilizer are mixed and be added
Moderate-element solution is stirred evenly to obtain into suitable quantity of water；2) weathered coal powder is milled down to 100 mesh hereinafter, and amberlite is added
Rouge and hydrochloric acid settle coal dust slag and resin, and be centrifuged to obtain aqueous solution of the top containing fulvic acid after the reaction was completed；3) by fruit tree tree
Branch crushes, and sieves with 100 mesh sieve, and ammonium sulfate and suitable quantity of water is added, and at a temperature of 105 DEG C, then ammonium hydrogen carbonate stirring is added in boiling 3h
Uniformly, centrifugation is squeezed after 5h, is filtered to get filtrate and waste residue；4) by Radix Glycyrrhizae, honeysuckle and peppermint are put into suitable quantity of water after mashing, and add
Heat filters to obtain medical fluid and the dregs of a decoction to 2h is boiled at a temperature of 100 DEG C；5) will by the moderate-element solution in step 1), 2) in it is yellow rotten
The medical fluid of acid solution, the filtrate of step 3) and step 4) is uniformly mixed, and urea is added, Diammonium phosphate (DAP), zymocyte liquid mixing；6)
Plant ash, maize flour, the waste residue in step 3), the dregs of a decoction in step 4) are crushed and are added by stalk, animal argol uniformly to mix,
It is put into fermentation vat, is then added thereto mixed liquor obtained in step 5), closed fermenting tank is sufficiently fermented；7) wait fill
After distributing ferment, fermentation material is heated, and steam 30min is continually fed into fermentation vat, wherein heating temperature is 80 DEG C；8) last
Fermentation material is separated by solid-liquid separation, filtrate is taken to carry out being granulated to obtain moderate-element water-soluble fertilizer.
Embodiment three
One kind that present pre-ferred embodiments provide, the production method of moderate-element water-soluble fertilizer, Yellow humic acid fertilizer include
The raw material of following mass component: 11 parts of water-soluble calcareous fertilizer, water-soluble 13 parts of fertiliser containing magnesium, 3 parts of water-soluble boron fertilizer, 9 parts of weathering coal dust, from
33 parts of sub-exchange resin, 7 parts of hydrochloric acid, 105 parts of tree branch, 18 parts of stalk, 8 parts of animal argol, 9 parts of plant ash, maize flour 7
Part, 4 parts of Radix Glycyrrhizae, 6 parts of honeysuckle, 1 part of peppermint, 2 parts of ammonium sulfate, 3 parts of urea, 4 parts of ammonium hydrogen carbonate, 2 parts of Diammonium phosphate (DAP), zymophyte
32 parts of liquid.Production technology includes the following steps: 1) to be mixed to join water-soluble calcareous fertilizer, water-soluble fertiliser containing magnesium, water-soluble boron fertilizer suitable
Moderate-element solution is stirred evenly to obtain in amount water；2) weathered coal powder is milled down to 100 mesh hereinafter, and be added ion exchange resin and
Hydrochloric acid settles coal dust slag and resin, and be centrifuged to obtain aqueous solution of the top containing fulvic acid after the reaction was completed；3) by tree branch powder
It is broken, 90 meshes are crossed, ammonium sulfate and suitable quantity of water is added, at a temperature of 100 DEG C, then boiling 2h is added ammonium hydrogen carbonate and stirs evenly,
Centrifugation is squeezed after 4, is filtered to get filtrate and waste residue；4) by Radix Glycyrrhizae, honeysuckle and peppermint are put into suitable quantity of water after mashing, and are heated to
2h is boiled at a temperature of 100 DEG C, filters to obtain medical fluid and the dregs of a decoction；5) will by the moderate-element solution in step 1), 2) in fulvic acid it is molten
The medical fluid of liquid, the filtrate of step 3) and step 4) is uniformly mixed, and urea is added, Diammonium phosphate (DAP), zymocyte liquid mixing；6) by straw
Stalk, animal argol are crushed and are added plant ash, maize flour, the waste residue in step 3), the dregs of a decoction in step 4) and uniformly mix, and are put into
In fermentation vat, then mixed liquor obtained in step 5) is added thereto, closed fermenting tank is sufficiently fermented；7) to sufficiently send out
After ferment, fermentation material is heated, and steam 30min is continually fed into fermentation vat, wherein heating temperature is 80 DEG C；It 8) finally will hair
Ferment material is separated by solid-liquid separation, and filtrate is taken to carry out being granulated to obtain moderate-element water-soluble fertilizer.
The production technology of fertilizer of the present invention greatly enriches the battalion of fertilizer by the combination of moderate-element and fulvic acid
It supports, and passes through the combination of mineral resources fulvic acid and biochemical fulvic acid, enable Yellow humic acid fertilizer obtained under solid forms
Also it is stabilized, and preparation process greatly improves the conversion ratio of fulvic acid, fertilizer obtained being capable of good promotion phosphorus nitrogen
The absorption of element improves antibacterial, the bacteriostasis of soil.Under the premise of using a small amount of moderate-element water-soluble fertilizer, pass through
It in conjunction with fulvic acid, had both solved the problems, such as that moderate-element nutrition was single, and had reduced cost of material, and overcome two kinds of not homologous Huangs
The limitation of rotten acid.Wherein the aqueous solution with fulvic acid is made by ion-exchange using coal dust first in the preparation of fulvic acid,
Then the biochemical fulvic acid in tree branch is extracted, is mixed with mineral resources fulvic acid obtained in weathering coal dust, finally
It is mixed and ferments with components such as fruit tree tree slag, stalk, animal argol, maize flour, plant ash, Chinese medicine dregs, can make
It obtains coal dust adequately to be extracted with the fulvic acid in fruit tree, while making the full of nutrition of fertilizer obtained, in animal argol
Nutrition not only enrich and environmental protection, be free of chemical industry additive, wherein after sufficiently fermenting, heat to fermentation material, and to fermentation
Steam 25-30min is continually fed into pond, wherein heating temperature is 78-80 DEG C, is passed through the material after fermentation by steam, can
Make sufficiently to adhere between biochemical fulvic acid and solid material, changing biochemical fulvic acid can only be with limitation existing for liquid form；Using
Radix Glycyrrhizae, honeysuckle, peppermint have good antibacterial, bacteriostasis, and fertilizer of the invention is mixed by the extracting solution and the dregs of a decoction of three
It is fermented together with fruit tree tree slag above-mentioned etc., so that fertilizer has good antibacterial ability.
Preferably, as shown in Figure 1, the fermentation vat includes the fermentation pond body 1 of tapered doleiform shape, the neck mouth for pond body of fermenting
Arc-shaped liquid-in pipe 2, the both ends point of liquid-in pipe are circumferentially sequentially connected between outer wall and fermentation pond body pond body outer wall
It is not connected between neck mouth and pond body, is arranged with open-topped drainage box 3 at pond body neck mouth of fermenting, on the side wall of drainage box
Multiple liquid-entering holes 4 are offered, the position of liquid-entering hole corresponds and is connected to liquid-in pipe bottle mouth position apical position；Fermentation pond body bottom
The discharge hole with valve is offered on face, it further includes top opening that the upper surface of discharge port, which is covered with dismountable sealing strainer,
Outer pond 5, fermentation pond body be placed on Wai Chizhong, Wai Chizhong is provided with heating device.
Fermentation vat of the invention when in use first removes drainage box from the bottleneck of fermentation pond body, then will be all
Solid material is put into pond, and drainage box is fastened on bottle mouth position and rotating is aligned its liquid-entering hole with liquid-in pipe, will be mixed
Zymocyte liquid, medical fluid, filtrate mixed liquor pour into drainage box, and then liquid is split even into every liquid-in pipe, then by
Liquid-in pipe enters in fermentation pond body from fermentation vat body sidewall surrounding is evenly dispersed, uniformly mixes with solid material, significantly
The mixing uniformity improved between liquid and solid material；Wherein, fermentation is placed on Wai Chizhong, and Wai Chizhong is provided with heating dress
It sets, after fermentation, the intracorporal fertilizer of fermentation vat can be heated by heating device, finally need to discharge and solid-liquid divides
From when, will fermentation pond body proposed from outer pond, valve is then opened, so that water-soluble fertilizer liquid is drained into from discharge hole
In outer pond, and expect admittedly, stays in fermentation pond body, play preliminary separation of solid and liquid.
Preferably, it is connected with rubber hose at the drainage outer box wall liquid-entering hole, drainage box is being placed on fermentation pond body
When bottle mouth position, every rubber hose is aligned liquid-in pipe first and is inserted, such solution is flowed into from liquid-entering hole into liquid
When in pipe, solution can be avoided between drainage box and bottleneck by rubber hose and leak.
Preferably, the side wall in the outer pond and bottom surface are interconnected hollow structure, be connected on the side wall in outer pond into
Liquid pipe and outlet tube can be passed through cooling fluid into a set of cups hollow structure when in use, to make fertilizer temperature in fermentation pond body
Uniformly decline.
The foregoing is merely illustrative of the preferred embodiments of the present invention, the protection scope being not intended to limit the invention, any
Those skilled in the art within the spirit and principles in the present invention made by any modifications, equivalent replacements, and improvements etc.,
It should all be included in the protection scope of the present invention.
Claims (7)
1. the production method of moderate-element water-soluble fertilizer, which is characterized in that Yellow humic acid fertilizer includes the raw material of following mass component:
10-12 parts of water-soluble calcareous fertilizer, water-soluble 12-15 parts of fertiliser containing magnesium, 2-3 parts of water-soluble boron fertilizer, 8-10 parts of weathering coal dust, amberlite
30-35 parts of rouge, 6-8 parts of hydrochloric acid, 100-110 parts of tree branch, 15-20 parts of stalk, 5-10 parts of animal argol, plant ash 8-10
Part, 5-8 parts of maize flour, 3-5 parts of Radix Glycyrrhizae, 4-7 parts of honeysuckle, 1-2 parts of peppermint, 2-3 parts of ammonium sulfate, 1-4 parts of urea, ammonium hydrogen carbonate
3-6 parts, 1-3 parts of Diammonium phosphate (DAP), 30-35 parts of zymocyte liquid；1) production technology includes the following steps: water-soluble calcareous fertilizer, water-soluble
Property fertiliser containing magnesium, water-soluble boron fertilizer are mixed to join in suitable quantity of water and stir evenly to obtain moderate-element solution；2) weathered coal powder is milled down to
100 mesh hereinafter, and ion exchange resin and hydrochloric acid is added, after the reaction was completed, settle coal dust slag and resin, and be centrifuged top contains
The aqueous solution of fulvic acid；3) tree branch is crushed, crosses 80-100 mesh, ammonium sulfate and suitable quantity of water is added, in 100 DEG C -105 DEG C
At a temperature of, then boiling 2-3h is added ammonium hydrogen carbonate and stirs evenly, centrifugation is squeezed after 3-5h, is filtered to get filtrate and waste residue；4) will
Radix Glycyrrhizae, honeysuckle and peppermint are put into suitable quantity of water after mashing, and boil 1.5-2h at a temperature of being heated to 95-100 DEG C, filter to obtain medical fluid
And the dregs of a decoction；5) will by the moderate-element solution in step 1), 2) in fulvic acid solution, the filtrate of step 3) and step 4) medical fluid
It is uniformly mixed, and urea is added, Diammonium phosphate (DAP), zymocyte liquid mixing；6) by stalk, animal argol be crushed and be added plant ash,
The dregs of a decoction in waste residue, step 4) in maize flour, step 3) uniformly mix, and are put into fermentation vat, then will obtain in step 5)
Mixed liquor be added thereto, closed fermenting tank is sufficiently fermented；7) after sufficiently fermenting, fermentation material is heated, and to fermentation
Steam 25-30min is continually fed into pond, wherein heating temperature is 78-80 DEG C；8) finally fermentation material is separated by solid-liquid separation, is taken
Filtrate carries out being granulated to obtain moderate-element water-soluble fertilizer.
2. the production method of moderate-element water-soluble fertilizer according to claim 1, which is characterized in that the fermentation vat includes
The fermentation pond body (1) of tapered doleiform shape, ferment pond body (1) neck mouth outer wall with ferment pond body (1) pond body outer wall between along
Circumferencial direction is sequentially connected with arc-shaped liquid-in pipe (2), and the both ends of liquid-in pipe (2) are connected between neck mouth and pond body respectively,
It is arranged with open-topped drainage box (3) at fermentation pond body (1) neck mouth, offers multiple liquid-entering holes on the side wall of drainage box (3)
(4), the position of liquid-entering hole (4) corresponds and is connected to liquid-in pipe (2) bottle mouth position apical position；It ferments on pond body (1) bottom surface
The discharge hole with valve is offered, it further includes open-topped outer that the upper surface of discharge hole, which is covered with dismountable sealing strainer,
Pond (5), fermentation pond body (1) are placed in outer pond (5), are provided with heating device in outer pond (5).
3. the production method of moderate-element water-soluble fertilizer according to claim 1, which is characterized in that Yellow humic acid fertilizer includes
The raw material of following mass component: 10 parts of water-soluble calcareous fertilizer, water-soluble 12 parts of fertiliser containing magnesium, 2 parts of water-soluble boron fertilizer, 8 parts of weathering coal dust, from
30 parts of sub-exchange resin, 6 parts of hydrochloric acid, 100 parts of tree branch, 15 parts of stalk, 5 parts of animal argol, 8 parts of plant ash, maize flour 5
Part, 3 parts of Radix Glycyrrhizae, 4 parts of honeysuckle, 1 part of peppermint, 2 parts of ammonium sulfate, 1 part of urea, 3 parts of ammonium hydrogen carbonate, 1 part of Diammonium phosphate (DAP), zymophyte
30 parts of liquid.
4. the production method of moderate-element water-soluble fertilizer according to claim 1, which is characterized in that Yellow humic acid fertilizer includes
The raw material of following mass component: 12 parts of water-soluble calcareous fertilizer, water-soluble 15 parts of fertiliser containing magnesium, 3 parts of water-soluble boron fertilizer, 10 parts of weathering coal dust,
35 parts of ion exchange resin, 8 parts of hydrochloric acid, 110 parts of tree branch, 20 parts of stalk, 10 parts of animal argol, 10 parts of plant ash, corn
8 parts of face, 5 parts of Radix Glycyrrhizae, 7 parts of honeysuckle, 2 parts of peppermint, 3 parts of ammonium sulfate, 4 parts of urea, 6 parts of ammonium hydrogen carbonate, 3 parts of Diammonium phosphate (DAP), hair
35 parts of yeast-like fungi liquid.
5. the production method of moderate-element water-soluble fertilizer according to claim 1, which is characterized in that Yellow humic acid fertilizer includes
The raw material of following mass component: 11 parts of water-soluble calcareous fertilizer, water-soluble 13 parts of fertiliser containing magnesium, 3 parts of water-soluble boron fertilizer, 9 parts of weathering coal dust, from
33 parts of sub-exchange resin, 7 parts of hydrochloric acid, 105 parts of tree branch, 18 parts of stalk, 8 parts of animal argol, 9 parts of plant ash, maize flour 7
Part, 4 parts of Radix Glycyrrhizae, 6 parts of honeysuckle, 1 part of peppermint, 2 parts of ammonium sulfate, 3 parts of urea, 4 parts of ammonium hydrogen carbonate, 2 parts of Diammonium phosphate (DAP), zymophyte
32 parts of liquid.
6. the production method of moderate-element water-soluble fertilizer according to claim 2, which is characterized in that the drainage box (3)
Outer wall liquid-entering hole is connected with rubber hose at (4).
7. the production method of moderate-element water-soluble fertilizer according to claim 2, which is characterized in that the outer pond (6)
Side wall and bottom surface are interconnected hollow structure, are connected with inlet tube and outlet tube on the side wall of outer pond (6).
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| CN101450955A (en) * | 2007-12-05 | 2009-06-10 | 山东泉林纸业有限责任公司 | Method for producing yellow humic acid from grass type stalk |
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| CN107176869A (en) * | 2016-03-09 | 2017-09-19 | 高云 | A kind of Synergistic composite fertilizer and preparation method thereof |
| CN206635343U (en) * | 2017-04-12 | 2017-11-14 | 中国农业科学院麻类研究所 | A kind of high solid installation for fermenting |
| CN109180248A (en) * | 2018-11-02 | 2019-01-11 | 孙同娟 | A kind of municipal administration gardens nutritious fertilizer and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101450955A (en) * | 2007-12-05 | 2009-06-10 | 山东泉林纸业有限责任公司 | Method for producing yellow humic acid from grass type stalk |
| CN104945080A (en) * | 2015-04-11 | 2015-09-30 | 杨金佑 | Efficient fertilizer for land recycling ecological treatment of urban refuses |
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| CN107176869A (en) * | 2016-03-09 | 2017-09-19 | 高云 | A kind of Synergistic composite fertilizer and preparation method thereof |
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