CN109717420A - A kind of dedicated glue formula of algal polysaccharides - Google Patents
A kind of dedicated glue formula of algal polysaccharides Download PDFInfo
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- CN109717420A CN109717420A CN201811579581.3A CN201811579581A CN109717420A CN 109717420 A CN109717420 A CN 109717420A CN 201811579581 A CN201811579581 A CN 201811579581A CN 109717420 A CN109717420 A CN 109717420A
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- algal polysaccharides
- brown alga
- sargassum fusifome
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Abstract
The present invention relates to a kind of dedicated glue formulas of algal polysaccharides, in parts by weight, including following material component: 40 ~ 70 parts of brown alga, 20 ~ 30 parts of kelp, 10 ~ 15 parts of sargassum fusifome, 1 ~ 5 part of plasticizer, 25 ~ 30 parts of water-retaining agent, 10 ~ 12 parts of dimethyl silicone polymer；The preparation process of the algal polysaccharides special glue includes the following steps: heating deionized water to 60 ~ 80 DEG C, sodium bicarbonate is added into deionized water, it is slowly added to brown alga, kelp, sargassum fusifome and is stirred continuously until forming clear solution, it is cooled to 40 ~ 60 DEG C to continue to stir, plasticizer, water-retaining agent and dimethyl silicone polymer is then added, is warming up to 70 ~ 90 DEG C, continue to stir, 30 ~ 50min is kept the temperature, filtering obtains algal polysaccharides special glue glue.The soft capsule shell that the dedicated glue formula of algal polysaccharides of the invention is prepared not only has good healthcare function, but also can also improve and be easy the problem of being sticked together existing for soft capsule.
Description
Technical field
The present invention relates to technical field of health care food more particularly to a kind of dedicated glue formulas of algal polysaccharides.
Background technique
Currently, the raw material for producing soft capsule is broadly divided into gelatin soft capsule and soft capsule, wherein soft-gelatin
The ingredient of capsule softgel shell is mainly gelatin, gelatin is using skin, bone of animal etc. be raw material pass through by classification, wash leaching, degreasing, in
With hydrolysis, filtering, concentration, gel, etc. animal protein colloid made of multiple tracks function sequence, have that high viscosity, high to freeze power, film forming tough
The features such as property is good, therefore often used by the softgel shell as soft capsule.But there is also many insufficient and some foods for gelatin itself
Product security risk influences medicine stability as being easy to react with some feed liquids in softgel shell；Water retention property is poor, is not easy long-term
Storage；Gelatin is easy to be influenced by religious taboo from the bone or fur of animal and the biography of the diseases such as similar rabid ox disease
It broadcasts.Therefore, it is had been obtained and is widely applied come replacing gelatin soft capsule using soft capsule.
Algae can be divided mainly into four class such as green alga, brown alga, red algae and cyanobacteria.Researches show that the seas extracted from seaweed for many
Polysaccharides can effectively inhibit virus, reduce cholesterol, hypoglycemic and reducing blood lipid and other effects.For example, fucoidin
It (Fucoidan) is a kind of iuntercellular polysaccharide being present in all brown algas.In recent years the study found that fucoidin have it is anti-
Oxidation, antitumor, antiviral, inhibition complement activation, inhibits sperm ovum binding, reducing blood lipid and absorbs the functions such as heavy metal anticoagulation,
For a kind of important functional health care material.
Summary of the invention
In view of the above-mentioned problems, the object of the present invention is to provide a kind of dedicated glue formula of algal polysaccharides, it is more using the seaweed
The soft capsule shell that the dedicated glue formula of sugar is prepared, not only has good healthcare function, but also can also improve plant flexible glue
The problem of being sticked together is easy existing for capsule.
In order to solve the above-mentioned technical problem, the dedicated glue formula of a kind of algal polysaccharides of the invention, including following material component:
40 ~ 70 parts of brown alga, 20 ~ 30 parts of kelp, 10 ~ 15 parts of sargassum fusifome, 1 ~ 5 part of plasticizer, 25 ~ 30 parts of water-retaining agent, polydimethylsiloxanes
10 ~ 12 parts of alkane；
The preparation process of the algal polysaccharides special glue includes the following steps:
Sodium bicarbonate is added into deionized water to 60 ~ 80 DEG C for heating deionized water, is slowly added to brown alga, kelp, sargassum fusifome simultaneously
It is stirred continuously up to forming clear solution, is cooled to 40 ~ 60 DEG C and continues to stir, plasticizer, water-retaining agent and poly- diformazan is then added
Radical siloxane is warming up to 70 ~ 90 DEG C, continues to stir, and keeps the temperature 30 ~ 50min, and filtering obtains algal polysaccharides special glue glue.
Specifically, by weight, including following raw material components: 55 parts of brown alga, 22 parts of kelp, 11 parts of sargassum fusifome, plasticising
2 parts of agent, 25 parts of water-retaining agent, 12 parts of dimethyl silicone polymer.
Further, the water-retaining agent includes one of glycerol, xylitol, mannitol, D-sorbite, maltitol
Or it is a variety of.
Further, the plasticizer includes polyethylene glycol and/or propylene glycol.
It further, further include pre-treatment step before brown alga, kelp, sargassum fusifome are added, the pre-treatment step
Include:
Clean the brown alga, kelp, sargassum fusifome；By the brown alga after cleaning, kelp, sargassum fusifome drying 1 ~ 2 at a temperature of 30 ~ 45 DEG C
Hour, brown alga, kelp, sargassum fusifome after then processing is dry at high temperature under high pressure, and by pressure by the way of moment pressure release
Release obtains brown alga, kelp, sargassum fusifome first product to normal pressure, by crushing obtain pretreated brown alga powder, kelp powder,
Sargassum fusifome powder.
Specifically, the temperature of the high temperature high pressure process is 150 ~ 200 DEG C, and pressure is 5 ~ 7MPa, and the processing time is 5 ~ 10
Second.
The dedicated glue formula of a kind of algal polysaccharides of the invention, has the following beneficial effects:
The dedicated glue formula of algal polysaccharides of the invention contains the effective component of the various health care functions such as algal polysaccharides, can be used to replace
Soft capsule shell is prepared for gelatin.Also, due to it can effectively prevent comprising dimethyl silicone polymer and water-retaining agent made of
Therefore the volatilization of the moisture content of soft capsule shell, the contact with moisture reduced between soft capsule and soft capsule can be very good to avoid soft
Capsule is bonded together, and improves the quality of soft capsule；
In addition, not only contribute to improve the dissolution rate of algal polysaccharides for the pre-treatment step of brown alga, kelp, sargassum fusifome, and
It can be economic and environment-friendly to avoid the use of organic solvent.
Specific embodiment
The following is a clear and complete description of the technical scheme in the embodiments of the invention, it is clear that described embodiment
Only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, the common skill in this field
Art personnel every other embodiment obtained without making creative work belongs to the model that the present invention protects
It encloses.
Embodiment 1
The present embodiment provides a kind of dedicated glue formula of algal polysaccharides, which can be used for suppressing soft capsule
Shell, specifically, include following material component: 55 parts of brown alga, 22 parts of kelp, 11 parts of sargassum fusifome, 2 parts of polyethylene glycol, xylitol and
12 parts of 25 parts of mixture, the dimethyl silicone polymer of mannitol.
The preparation process of the algal polysaccharides special glue of the present embodiment includes the following steps:
The pretreatment of brown alga, kelp, sargassum fusifome: cleaning 55 portions of brown algas, 22 portions of kelps, 11 parts sargassum fusifome 2 ~ 3 times；After cleaning
Brown alga, kelp, sargassum fusifome dry 2 hours at a temperature of 45 DEG C, brown alga, kelp after then processing is dry at high temperature under high pressure,
Sargassum fusifome, and discharged pressure to normal pressure by the way of moment pressure release, obtain brown alga, kelp, sargassum fusifome first product, first product warp
Crushing is crossed, is sieved with 100 mesh sieve, pretreated brown alga powder, kelp powder, sargassum fusifome powder are obtained.
Wherein, the temperature of high temperature high pressure process is 180 DEG C, pressure 7MPa, and the processing time is 8 seconds.
The preparation of algal polysaccharides special glue: 150 parts of deionized waters are added into melten gel tank, heating deionized water is to 60 DEG C, so
2 parts of sodium bicarbonates are added in deionized water after backward heating, are slow added into brown alga powder, Kelp Powder that pretreatment obtains
End, sargassum fusifome powder, and be stirred continuously up to forming clear solution, it is cooled to 50 DEG C and continues to stir, polyethylene glycol 2 is then added
Part, 12 parts of 25 parts of mixture, the dimethyl silicone polymer of xylitol and mannitol, be warming up to 80 DEG C, continue to stir, keep the temperature
40min, filtering, obtains algal polysaccharides special glue glue.
Embodiment 2
The present embodiment provides a kind of dedicated glue formula of algal polysaccharides, which can be used for suppressing soft capsule
Shell, specifically, including following material component: 40 parts of brown alga, 20 parts of kelp, 10 parts of sargassum fusifome, 1 part of propylene glycol, maltitol 28
Part, 10 parts of dimethyl silicone polymer.
The preparation process of the algal polysaccharides special glue of the present embodiment includes the following steps:
The pretreatment of brown alga, kelp, sargassum fusifome: cleaning 40 portions of brown algas, 20 portions of kelps, 10 parts sargassum fusifome 2 ~ 3 times；After cleaning
Brown alga, kelp, sargassum fusifome dry 2 hours at a temperature of 30 DEG C, brown alga, kelp after then processing is dry at high temperature under high pressure,
Sargassum fusifome, and discharged pressure to normal pressure by the way of moment pressure release, obtain brown alga, kelp, sargassum fusifome first product, first product warp
Crushing is crossed, is sieved with 100 mesh sieve, pretreated brown alga powder, kelp powder, sargassum fusifome powder are obtained.
Wherein, the temperature of high temperature high pressure process is 150 DEG C, pressure 7MPa, and the processing time is 10 seconds.
The preparation of algal polysaccharides special glue: 150 parts of deionized waters are added into melten gel tank, heating deionized water is to 80 DEG C, so
1 part of sodium bicarbonate is added in deionized water after backward heating, is slow added into brown alga powder, Kelp Powder that pretreatment obtains
End, sargassum fusifome powder, and be stirred continuously up to forming clear solution, it is cooled to 40 DEG C and continues to stir, propylene glycol 1 is then added
Part, 28 parts of maltitol, 10 parts of dimethyl silicone polymer, are warming up to 70 DEG C, continue to stir, and keep the temperature 50min, and filtering obtains sea
Polysaccharides special glue glue.
Embodiment 3
The present embodiment provides a kind of dedicated glue formula of algal polysaccharides, which can be used for suppressing soft capsule
Shell, specifically, including following material component: 70 parts of brown alga, 15 parts of sargassum fusifome, 5 parts of propylene glycol, 30 parts of glycerol, gathers 30 parts of kelp
11 parts of dimethyl siloxane.
The preparation process of the algal polysaccharides special glue of the present embodiment includes the following steps:
The pretreatment of brown alga, kelp, sargassum fusifome: cleaning 70 portions of brown algas, 30 portions of kelps, 15 parts sargassum fusifome 2 ~ 3 times；After cleaning
Brown alga, kelp, sargassum fusifome dry 1 hour at a temperature of 45 DEG C, brown alga, kelp after then processing is dry at high temperature under high pressure,
Sargassum fusifome, and discharged pressure to normal pressure by the way of moment pressure release, obtain brown alga, kelp, sargassum fusifome first product, first product warp
Crushing is crossed, is sieved with 100 mesh sieve, pretreated brown alga powder, kelp powder, sargassum fusifome powder are obtained.
Wherein, the temperature of high temperature high pressure process is 200 DEG C, pressure 5MPa, and the processing time is 5 seconds.
The preparation of algal polysaccharides special glue: 150 parts of deionized waters are added into melten gel tank, heating deionized water is to 70 DEG C, so
3 parts of sodium bicarbonates are added in deionized water after backward heating, are slow added into brown alga powder, Kelp Powder that pretreatment obtains
End, sargassum fusifome powder, and be stirred continuously up to forming clear solution, it is cooled to 60 DEG C and continues to stir, propylene glycol 5 is then added
Part, 30 parts of glycerol, 11 parts of dimethyl silicone polymer, are warming up to 90 DEG C, continue to stir, and keep the temperature 30min, and it is more to obtain seaweed for filtering
Sugared special glue glue.
To sum up, the dedicated glue formula of algal polysaccharides of the invention itself containing the various health care functions such as algal polysaccharides it is effective at
Point, replacing gelatin can be used to and prepare soft capsule shell.Also, due to including dimethyl silicone polymer and water-retaining agent, Ke Yiyou
The volatilization of the moisture content of soft capsule shell made of the prevention of effect, the contact with moisture reduced between soft capsule and soft capsule therefore can
To avoid soft capsule from being bonded together well, the quality of soft capsule is improved；
In addition, not only contribute to improve the dissolution rate of algal polysaccharides for the pre-treatment step of brown alga, kelp, sargassum fusifome, and
It can be economic and environment-friendly to avoid the use of organic solvent.
Above description sufficiently discloses a specific embodiment of the invention.It should be pointed out that being familiar with the field
Range of any change that technical staff does a specific embodiment of the invention all without departing from claims of the present invention.
Correspondingly, the scope of the claims of the invention is also not limited only to previous embodiment.
Claims (6)
1. a kind of dedicated glue formula of algal polysaccharides, which is characterized in that in parts by weight, including following material component: brown alga 40 ~
70 parts, 20 ~ 30 parts of kelp, 10 ~ 15 parts of sargassum fusifome, 1 ~ 5 part of plasticizer, 25 ~ 30 parts of water-retaining agent, dimethyl silicone polymer 10 ~ 12
Part；
The preparation process of the algal polysaccharides special glue includes the following steps:
Sodium bicarbonate is added into deionized water to 60 ~ 80 DEG C for heating deionized water, is slowly added to brown alga, kelp, sargassum fusifome simultaneously
It is stirred continuously up to forming clear solution, is cooled to 40 ~ 60 DEG C and continues to stir, plasticizer, water-retaining agent and poly- diformazan is then added
Radical siloxane is warming up to 70 ~ 90 DEG C, continues to stir, and keeps the temperature 30 ~ 50min, and filtering obtains algal polysaccharides special glue glue.
2. the dedicated glue formula of algal polysaccharides according to claim 1, which is characterized in that by weight, including following original
Expect component: 55 parts of brown alga, 22 parts of kelp, 11 parts of sargassum fusifome, 2 parts of plasticizer, 25 parts of water-retaining agent, 12 parts of dimethyl silicone polymer.
3. the dedicated glue formula of algal polysaccharides according to claim 1, which is characterized in that the water-retaining agent includes glycerol, wood
One or more of sugar alcohol, mannitol, D-sorbite, maltitol.
4. the dedicated glue formula of algal polysaccharides according to claim 1, which is characterized in that the plasticizer includes polyethylene glycol
And/or propylene glycol.
5. the dedicated glue formula of algal polysaccharides according to claim 1, which is characterized in that add by brown alga, kelp, sargassum fusifome
It further include pre-treatment step before entering, the pre-treatment step includes:
Clean the brown alga, kelp, sargassum fusifome；By the brown alga after cleaning, kelp, sargassum fusifome drying 1 ~ 2 at a temperature of 30 ~ 45 DEG C
Hour, brown alga, kelp, sargassum fusifome after then processing is dry at high temperature under high pressure, and by pressure by the way of moment pressure release
Release obtains brown alga, kelp, sargassum fusifome first product to normal pressure, by crushing obtain pretreated brown alga powder, kelp powder,
Sargassum fusifome powder.
6. the dedicated glue formula of algal polysaccharides according to claim 5, which is characterized in that the temperature of the high temperature high pressure process
It is 150 ~ 200 DEG C, pressure is 5 ~ 7MPa, and the processing time is 5 ~ 10 seconds.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201811579581.3A CN109717420A (en) | 2018-12-24 | 2018-12-24 | A kind of dedicated glue formula of algal polysaccharides |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201811579581.3A CN109717420A (en) | 2018-12-24 | 2018-12-24 | A kind of dedicated glue formula of algal polysaccharides |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111357875A (en) * | 2020-05-06 | 2020-07-03 | 天津市畜牧兽医研究所 | Cattle and sheep composite nutrition licking brick taking kelp paste as adhesive and preparation method and application thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102153669A (en) * | 2010-05-12 | 2011-08-17 | 北京雷力联合海洋生物科技有限公司 | Preparation method of low-molecule brown seaweed glucan |
| CN104000244A (en) * | 2014-06-16 | 2014-08-27 | 青岛银色世纪健康产业集团有限公司 | Euphausia superba oil soft capsule and preparing method thereof |
| CN104098711A (en) * | 2013-04-15 | 2014-10-15 | 黄俊勇 | Extraction method for algal polysaccharide |
| CN104489458A (en) * | 2014-11-29 | 2015-04-08 | 浙江宏辉胶丸有限公司 | Empty capsule adopting coral fungus polysaccharide |
-
2018
- 2018-12-24 CN CN201811579581.3A patent/CN109717420A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102153669A (en) * | 2010-05-12 | 2011-08-17 | 北京雷力联合海洋生物科技有限公司 | Preparation method of low-molecule brown seaweed glucan |
| CN104098711A (en) * | 2013-04-15 | 2014-10-15 | 黄俊勇 | Extraction method for algal polysaccharide |
| CN104000244A (en) * | 2014-06-16 | 2014-08-27 | 青岛银色世纪健康产业集团有限公司 | Euphausia superba oil soft capsule and preparing method thereof |
| CN104489458A (en) * | 2014-11-29 | 2015-04-08 | 浙江宏辉胶丸有限公司 | Empty capsule adopting coral fungus polysaccharide |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111357875A (en) * | 2020-05-06 | 2020-07-03 | 天津市畜牧兽医研究所 | Cattle and sheep composite nutrition licking brick taking kelp paste as adhesive and preparation method and application thereof |
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