CN109695088A - A kind of production technology of cotton fiber four sides stretch yarn dyed fabric - Google Patents
A kind of production technology of cotton fiber four sides stretch yarn dyed fabric Download PDFInfo
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- CN109695088A CN109695088A CN201811610278.5A CN201811610278A CN109695088A CN 109695088 A CN109695088 A CN 109695088A CN 201811610278 A CN201811610278 A CN 201811610278A CN 109695088 A CN109695088 A CN 109695088A
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- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
- D03D15/50—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the properties of the yarns or threads
- D03D15/54—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the properties of the yarns or threads coloured
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- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D13/00—Woven fabrics characterised by the special disposition of the warp or weft threads, e.g. with curved weft threads, with discontinuous warp threads, with diagonal warp or weft
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- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
- D03D15/50—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the properties of the yarns or threads
- D03D15/533—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the properties of the yarns or threads antistatic; electrically conductive
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- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
- D03D15/50—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the properties of the yarns or threads
- D03D15/56—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the properties of the yarns or threads elastic
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B3/00—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating
- D06B3/04—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of yarns, threads or filaments
- D06B3/09—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of yarns, threads or filaments as packages, e.g. cheeses
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- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2201/00—Cellulose-based fibres, e.g. vegetable fibres
- D10B2201/01—Natural vegetable fibres
- D10B2201/02—Cotton
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- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2201/00—Cellulose-based fibres, e.g. vegetable fibres
- D10B2201/20—Cellulose-derived artificial fibres
- D10B2201/22—Cellulose-derived artificial fibres made from cellulose solutions
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2331/00—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products
- D10B2331/10—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products polyurethanes
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2401/00—Physical properties
- D10B2401/06—Load-responsive characteristics
- D10B2401/062—Load-responsive characteristics stiff, shape retention
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2401/00—Physical properties
- D10B2401/13—Physical properties anti-allergenic or anti-bacterial
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2401/00—Physical properties
- D10B2401/16—Physical properties antistatic; conductive
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2403/00—Details of fabric structure established in the fabric forming process
- D10B2403/01—Surface features
- D10B2403/011—Dissimilar front and back faces
- D10B2403/0114—Dissimilar front and back faces with one or more yarns appearing predominantly on one face, e.g. plated or paralleled yarns
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Abstract
The invention discloses a kind of production technologies of cotton fiber four sides stretch yarn dyed fabric, include the following steps: the preparation of step S1 yarn, the dyeing of step S2 warp thread, the dyeing of step S3 weft yarn, step S4 warp end preparing, step S5 weaving, step S6 final finishing.A kind of production technology of cotton fiber four sides stretch yarn dyed fabric according to the present invention, warp thread uses the terylene covered yarn by cheese yarn dyeing, weft yarn uses the tencel fiber and Coolmax fabric core-spun yarn by cheese yarn dyeing, and use satin weave, so that the one side of fabric is that cotton fiber is presented, another and blended tencel and Coolmax fiber is presented, tencel and Coolmax fiber and a mask of skin contact can effectively improve the moisture absorption hydrofuge function and anti-static function of fabric, improve the comfort of fabric.Warp thread and weft yarn are first impregnation aids and are stood using cheese yarn dyeing, enable warp and weft to be easier to paint in dyeing, color fastness is high.
Description
Technical field
The present invention relates to textile fabric production technical field, especially a kind of production work of cotton fiber four sides stretch yarn dyed fabric
Skill.
Background technique
Four-side elasticity fabric requires soft, comfortable, good hygroscopicity as leisure trousering, and color saturation is high, pure, while again
It is required that wear-resisting, strength height, phozy pilling.Although traditional linen-cotton natural fabric material has the characteristics that soft, comfortable moisture absorption,
Dark color system, especially black will appear whiten, the problem that depth is inadequate, sensitive color is for example dark blue, wine is red, black, dark-grey etc. exists
Phenomena such as fast light sweat poor color fastness, coloured light changes after solarization;Traditional cotton ammonia cladded yarn as warp thread weaving when, due to steel
The friction of reed is easy to cause de- cotton and reveals core.And the hygroscopicity of cotton ammonia four-side elasticity fabric and its performance such as antistatic have into
The space that one step improves.
Tencel fiber has the characteristics that soft pendency, sense of touch uniqueness, elegant innervation, air-moisture-permeable, plain gloss, gives
Meet, safety, the feeling generous full of texture, noble quality.It is comfortable that nanometer tencel is used high-count pure cotton fabric filling tencel fiber
It is ventilative, it is anti-mite antistatic and meanwhile have many advantages, such as again durability by force, elasticity is good, it is not wrinkled, convenient for arranging washing.
Coolmax fiber is a kind of four pipeline ahermatypic polyester fibers, is profiled fibre, cross section in cross,
So the surface of fiber is formed four grooves, meanwhile, fiber surface area also increases, can be by body surface using the siphon of groove
Moisture content siphon away, while vaporing away as soon as possible.So can be by physical activity when generated sweat drain into the steaming of clothes surface layer rapidly
Hair keeps skin salubrious, activity is enabled to feel more comfortable.It has good wet guilding, and the knitting fabric to interweave with cotton fiber has
It is good to lead wet effect.
Tencel fiber and Coolmax fiber are the moisture absorption hydrofuge effect and anti-static function that inner layer can effectively improve fabric.
Summary of the invention
The object of the present invention is to provide a kind of production technologies of cotton fiber four sides stretch yarn dyed fabric, so that four sides produced
Stretch yarn dyed fabric not only has many advantages, such as good stability of the dimension, good hygroscopicity, also has and has been not easy electrostatic and antibacterial, moisture absorption
Property is further promoted.
In order to solve the above technical problems, the object of the present invention is achieved like this:
A kind of production technology of cotton fiber four sides stretch yarn dyed fabric according to the present invention, includes the following steps:
Step S1, the preparation of yarn: warp thread is using cotton ammonia cladded yarn and Quality Pure Cotton Yarn Production plying institute at the cotton ammonia cored
For yarn using cotton fiber as clad, spandex as heart yarn, the content of spandex is 6%;The fineness of the Quality Pure Cotton Yarn Production is 21-40s;
Weft yarn uses Modal and Coolmax fiber as clad, spandex for the covering yarn of heart yarn;The fineness of used spandex is
20D, 40D or 70D;Clad in weft yarn is 21S-40S, and the content of Coolmax fiber is in 50-65%;
Step S2, the dyeing of warp thread: using the staining method of cylinder yarn, including warp thread metal, warp thread pre-treatment, through yarn-dyed
Color, warp thread are soaped;
The warp thread metal is the oiling device that warp thread is used to slack winder, uniformly goes up auxiliary agent to warp thread, simultaneously
Network stands setting time at loose formula cylinder yarn required for dyeing;The density for being formed by loose formula cylinder yarn is 0.3-0.35g/
cm3, the weight of single only loose formula cylinder yarn is 0.6-0.7kg;Overfeeding is used when winder, using stainless steel wire helical Bourdon tube, before dye
Want chamfering;Used auxiliary agent is the aqueous solution of scouring agent, penetrating agent JFC, degreaser, isopropanolamine;Scouring agent be added
Concentration is 50-60g/L, the concentration of degreaser is 40-50g/L, the concentration of penetrating agent JFC is 10-20g/L, isopropanolamine 10-
15g/L;Time of repose is 12-16 hours;
Warp thread pre-treatment is in the warp thread pine formula cylinder yarn merging dye vat cylinder after standing, is 1:10-15 addition according to bath raio
Pretreatment liquid, the scouring agent containing 2-3g/L in the pretreatment liquid, 5-10g/L stabilizer BS, 1-2g/L dispersion chela
Mixture is warming up to 85-90 DEG C from room temperature according to the rate of 0.7-1 DEG C/min, and constant temperature operates 30-40min, after liquid is discharged,
10-15min is washed using the clear water of 60-65 DEG C of temperature, then the acetum for the use of pH value being 5.5-6 under the conditions of 45-50 DEG C
Pickling 8-10min is carried out, is discharged after acetum under room temperature again and washes 10-20min using clear water;
Warp dyeing is that the warp thread pine formula cylinder yarn Jing Guo pre-treatment is placed in dye liquor to dye;After pre-treatment,
Clear water is added and arrives bath raio 1:6-10, under the conditions of 40 DEG C, addition anhydrous sodium sulphate, bleeding agent AI BAFIJOW UNI, spandex promotor
ERIONAL ELA, diffusant UNIVADINF DFM, and the use of vinegar acid for adjusting pH value is 4.4-5.5,5-10min is run, is added
The Megafix reactive dye of 0.5-1%o.w.f operate the dye of positive ion of addition 0.2-0.5%o.w.f after 3-5min, according to
Constant temperature operates 30-50min, the cooling washing 5-10min of overflow later, row after the rate of 0.7-1 DEG C/min is warming up to 100-110 DEG C
Dye liquor out;
Warp thread is soaped, and refers to again plus clear water reaches bath raio 1:6-10, acid soap is added according to the ratio of 3-5g/L under room temperature
The ratio anion syntannin class color fixing agent of lotion, 1-2g/L is warming up to 90-100 DEG C after operating 8-15min, operates 10-
Drain is washed after 20min, the warp thread after being dyed;
Step S3, the dyeing of weft yarn: using the staining method of cylinder yarn, including weft yarn metal, weft yarn pre-treatment, weft yarn dye
Color, weft yarn are soaped;
The weft yarn metal refers to the oiling device that weft yarn is used to slack winder, uniformly goes up auxiliary agent to weft yarn, together
Loose formula cylinder yarn required for Shi Luocheng dyeing, and stand setting time;The density for being formed by loose formula cylinder yarn is 0.25-0.3g/
cm3, the weight of single only loose formula cylinder yarn is 0.5-0.6kg;Overfeeding is used when winder, color plastic straighttube wants chamfering before dye;Made
Auxiliary agent is the aqueous solution of scouring agent, chelated dispersants and bleeding agent;And adjusting pH value using soda ash is 10-11;When standing
Between be 12-16 hours;
The weft yarn pre-treatment is in the weft yarn pine formula cylinder yarn merging dye vat cylinder after standing, and adding water to bath raio is 1:
8-10, operate 8-15min, according still further to 1-2g/L ratio be added scouring agent, the caustic soda of 4-8g/L, 6-10g/L hydrogen peroxide, according to
The rate of 0.7-1 DEG C/min is warming up to 80-90 DEG C, and constant temperature operates 20-30min, after liquid is discharged, uses 60-65 DEG C of temperature
Clear water wash 10-15min, then under the conditions of 45-50 DEG C using pH value be 5.5-6 acetum carry out pickling 8-10min,
It is discharged after acetum under room temperature again and washes 10-20min using clear water;
The weft yarn dyeing is that the weft yarn after pre-treatment is added water to bath raio for 1:10-15, under the conditions of 40 DEG C, then
According to the levelling agent of the ratio addition 1-2g/L of 1-2g/L, penetrating agent JFC, the 1-2g/L of defoaming agent AF, 3-5g/L of 2-3g/L
Spandex promotor ERIONAL ELA operate 10-15min and using vinegar acid for adjusting pH value in 4.5-5;According still further to 2-3g/L's
Dyeing accelerant NP is added in ratio, and the Maxion type dye of 0.2-0.5%o.w.f operates 5-10min, according still further to 0.3-0.6%o.w.f
Ratio be added Nylosan N-type dyestuff, after being warming up to 65-70 DEG C according to the rate of 1-2 DEG C/min, according still further to 0.5-0.7 DEG C/
The rate of min is warming up to 100-105 DEG C, and constant temperature operates 60-90min, is cooled to 60-65 DEG C according still further to the rate of 2-3 DEG C/min,
And after liquid is discharged, washed twice using the clear water of 60-65 DEG C of temperature;
The weft yarn is soaped, and refers to again plus clear water reaches bath raio 1:6-10, be added under room temperature according to the ratio of 3-5g/L
After hydrogen peroxide operates 8-15min, it is warming up to the 45-55 DEG C of ratio according to 1-2g/L and soaping agent, anion syntannin class is added
Color fixing agent is warming up to 90-100 DEG C according to the rate of 1-2 DEG C/min, drain is washed after operating 10-20min, after being dyed
Weft yarn;
Step S4, warp end preparing: the warp thread after dyeing is being knitted according to technique setting warping using elastomeric yarn warping machine
On axis;
Step S5, it weaves: being weaved according to the technique of setting, the grammes per square metre of weaved fabric is 80-120g/m2;Fabric
Tissue uses satin weave;
Step S6, final finishing: the woven fabric of previous step institute is singed, is washed, is preshrunk, high-temperature shaping, non-ironing
Processing and drying.
As a further illustration of the above scheme, the anhydrous sodium sulphate being added is 1-2g/L, bleeding agent in warp dyeing step
AI BAFIJOW UNI is 1-2g/L, spandex promotor ERIONAL ELA is 2-3g/L, diffusant UNIVADINF DFM is 1-
2g/L。
As a further illustration of the above scheme, the content of used scouring agent is 10-15g/L in weft yarn metal step,
The content of chelated dispersants is 15-20g/L and the content of bleeding agent is 20-30g/L.
As a further illustration of the above scheme, in step S6 final finishing,
Singing is using natural gas gassing frame, speed 100-120m/min, and burner number is 2, and pressure of singing is 13mbra, is burnt
Hair series is 3-4;
Washing, is washed, using feed preparation unit roller active drive technology, straight displacement elastic devices tension is using 80-85 DEG C of condition
0.1Mpa, padding machine pressure are 0.1Mpa;Used rinsing solution contains softening agent;
Overfeeding 20-25% when preshrunk;
High-temperature shaping, overfeeding 20-25% straight in 160-170 DEG C of condition of temperature, cropping overfeeding 4-5%;
Noniron finish is mixed using being made of resin FEL, strong protecting agent HDP, softening agent SF48, penetrating agent JFC and water
Liquid is closed fabric is carried out to pad processing;Wherein, resin FEL is 50-60g/L, and strong protecting agent HDP is 10-20g/L, softening agent
SF48 is 15-20g/L, penetrating agent JFC 5-10g/L;
Drying is under the conditions of 110 DEG C.
The beneficial effects of the present invention are: a kind of production technology of cotton fiber four sides stretch yarn dyed fabric according to the present invention,
Warp thread uses the terylene covered yarn by cheese yarn dyeing, and weft yarn uses the tencel fiber and Coolmax fiber by cheese yarn dyeing
Covering yarn, and use satin weave, it is another and that blended tencel and Coolmax is presented is fine so that the one side of fabric is that cotton fiber is presented
One mask of dimension, tencel and Coolmax fiber and skin contact can effectively improve fabric moisture absorption hydrofuge function and antistatic function
Can, improve the comfort of fabric.Warp thread and weft yarn are first impregnation aids and are stood using cheese yarn dyeing, so that warp and weft is contaminating
It can be easier to paint when color, color fastness is high.
Specific embodiment
The present invention is further described combined with specific embodiments below.
Embodiment one
A kind of production technology of cotton fiber four sides stretch yarn dyed fabric, includes the following steps: step involved in the present embodiment
The preparation of S1 yarn, the dyeing of step S2 warp thread, the dyeing of step S3 weft yarn, step S4 warp end preparing, step S5 weaving, step
S6 final finishing.Wherein, warp thread dyeing use cylinder yarn staining method, including warp thread metal, warp thread pre-treatment, warp dyeing,
Warp thread is soaped.The dyeing of weft yarn also uses the staining method of cylinder yarn, including weft yarn metal, weft yarn pre-treatment, weft yarn dyeing, weft yarn
It soaps.
In the preparation of step S1 yarn, warp thread is using cotton ammonia cladded yarn and Quality Pure Cotton Yarn Production plying institute at the cotton ammonia
For covering yarn using cotton fiber as clad, spandex as heart yarn, the content of spandex is 6%.The fineness of used spandex is
20D。
Weft yarn uses Modal and Coolmax fiber as clad, spandex for the covering yarn of heart yarn;Used spandex
Fineness be 40D;Clad in weft yarn is 21S, and the content of Coolmax fiber is 50%.
In the dyeing of step S2 warp thread, using the staining method of cylinder yarn.Dyeing include warp thread metal, warp thread pre-treatment,
Warp dyeing, warp thread are soaped.
Warp thread metal is the oiling device that warp thread is used to slack winder, uniformly goes up auxiliary agent to warp thread, while network is at dye
Pine formula cylinder yarn required for color, and stand setting time;The density for being formed by loose formula cylinder yarn is 0.3g/cm3, single only loose formula cylinder
The weight of yarn is 0.6kg.Chamfering is wanted before dye using stainless steel wire helical Bourdon tube using overfeeding when winder.It needs strictly to accomplish
Thread density is uniform, in the same size.It prevents not of uniform size, elastic different, causes dyeing flower and inside and outside color difference.Standing setting may make
Auxiliary agent preferably infiltrates into yarn interior, can preferably remove Yarn oiling agent and impurity, improve the stainability of yarn.
In warp thread metal step, used auxiliary agent be scouring agent, penetrating agent JFC, degreaser, isopropanolamine it is water-soluble
Liquid;The concentration of scouring agent be added is 50g/L, the concentration of degreaser is 40g/L, the concentration of penetrating agent JFC is 10g/L, isopropyl
Hydramine is 10g/L;Time of repose is 12 hours.
It is in the warp thread pine formula cylinder yarn merging dye vat cylinder after standing, is that pretreatment liquid is added in 1:10 according to bath raio, it is described
Pretreatment liquid in the scouring agent containing 2g/L, 5g/L stabilizer BS, 1g/L dispersion chelating agent, from room temperature according to 0.7 DEG C/
The rate of min is warming up to 85 DEG C, and constant temperature operates 30min, after liquid is discharged, washes 10min using the clear water of 60 DEG C of temperature, then
Pickling 8min is carried out using the acetum that pH value is 5.5 under the conditions of 45 DEG C, is discharged after acetum under room temperature again using clear
Water washes 10min.
Warp dyeing is that the warp thread pine formula cylinder yarn Jing Guo pre-treatment is placed in dye liquor to dye;After pre-treatment,
Clear water is added and arrives bath raio 1:6, under the conditions of 40 DEG C, addition anhydrous sodium sulphate, bleeding agent AI BAFIJOW UNI, spandex promotor
ERIONAL ELA, diffusant UNIVADINF DFM, and the use of vinegar acid for adjusting pH value is 4.4,5-10min is run, is added 0.5%
The Megafix reactive dye of o.w.f operate the dye of positive ion of addition 0.2%o.w.f after 3-5min, according to 0.7 DEG C/min's
Constant temperature operates 30-50min after rate is warming up to 100 DEG C, and dye liquor is discharged in the cooling washing 5min of overflow later.
In warp dyeing step, the anhydrous sodium sulphate being added is 1g/L, bleeding agent AI BAFIJOW UNI is 1g/L, spandex promotees
Into agent ERIONAL ELA be 2g/L, diffusant UNIVADINF DFM is 1g/L.The Megafix reactive dye being added are blue
Or yellow.
Warp thread is soaped, and refers to again plus clear water reaches bath raio 1:6, under room temperature according to the ratio of 3g/L be added acid scouring agent,
The ratio anion syntannin class color fixing agent of 1-2g/L is warming up to 90 DEG C after operating 8min, washes drain after operating 10min,
Warp thread after being dyed.
In the dyeing of step S3 weft yarn, using the staining method of cylinder yarn, including weft yarn metal, weft yarn pre-treatment, weft yarn
Dyeing, weft yarn are soaped.
Weft yarn metal refers to the oiling device that weft yarn is used to slack winder, to the uniform upper auxiliary agent of weft yarn, while network at
Loose formula cylinder yarn required for dyeing, and stand setting time;The density for being formed by loose formula cylinder yarn is 0.25g/cm3, single only pine
The weight of formula cylinder yarn is 0.5kg;Overfeeding is used when winder, color plastic straighttube wants chamfering before dye;Used auxiliary agent is concise
Agent, chelated dispersants and bleeding agent aqueous solution;And adjusting pH value using soda ash is 10;Time of repose is 12 hours.
Weft yarn pre-treatment is in the weft yarn pine formula cylinder yarn merging dye vat cylinder after standing, and adding water to bath raio is 1:8, operating
Scouring agent, the caustic soda of 4g/L is added according still further to the ratio of 1g/L in 8min, and 6g/L hydrogen peroxide heats up according to the rate of 0.7 DEG C/min
To 80 DEG C, constant temperature operates 20min, after liquid is discharged, washes 10min using the clear water of 60 DEG C of temperature, then under the conditions of 45 DEG C
Pickling 8min is carried out using the acetum that pH value is 5.5, is discharged after acetum under room temperature again and washes 10min using clear water.
Weft yarn dyeing is that the weft yarn after pre-treatment is added water to bath raio for 1:10, under the conditions of 40 DEG C, according still further to 1g/L's
Ratio be added the levelling agent of 1g/L, 2g/L defoaming agent AF, 3g/L penetrating agent JFC, and using vinegar acid for adjusting pH value 4.5,
Operate 10min;Dyeing accelerant NP is added according still further to the ratio of 2g/L, the Maxion type dye of 0.2%o.w.f operates 5min, then presses
NylosanN type dye is added according to the ratio of 0.3%o.w.f, after being warming up to 65 DEG C according to the rate of 1 DEG C/min, according still further to 0.5
DEG C/rate of min is warming up to 100 DEG C, constant temperature operates 60min, is cooled to 60 DEG C according still further to the rate of 2 DEG C/min, and by liquid
After discharge, washed twice using the clear water of 60 DEG C of temperature.The color for the Maxion dyestuff being added is blue, with warp dyeing institute
It is identical to contaminate color.
Weft yarn is soaped, and refers to again plus clear water reaches bath raio 1:6, hydrogen peroxide is added according to the ratio of 3g/L under room temperature and operates
After 8min, it is warming up to 45 DEG C of ratios according to 1g/L and soaping agent, anion syntannin class color fixing agent is added, according to 1 DEG C/min
Rate be warming up to 90 DEG C, wash drain after operating 10min, the weft yarn after being dyed.
In step S4 warp end preparing, the warp thread after dyeing is existed according to technique setting warping using elastomeric yarn warping machine
On beam of a loom.Warping is will be through being evenly arranged on beam of a loom according to design requirement.Warping is without particular/special requirement in the present embodiment, and normal
The technique for advising warp end preparing when elastic fabric weaving is identical.
It in step S5 weaving, is weaved according to the technique of setting, the grammes per square metre of weaved fabric is 80-120g/m2.Satin
Line includes Warp Satin and satin.The front of Warp Satin, which is presented, is floated long line, and reverse side is presented latitude and floats long line.Satin
Front present latitude float long line, return existing presentation and floated long line.Either Warp Satin or satin can be achieved the one of fabric
Warp thread is presented in face, and weft yarn is presented on one side.
Fabric tissue uses Warp Satin in the present embodiment.The fabric tissue may make the front of fabric that nylon cored is presented
Mixed tencel and Coolmax fiber is presented in yarn, reverse side.Nylon can increase the wear resistance of fabric, mixed tencel and Coolmax
The skin-friendly of fabric can be improved in fiber, improve fabric penetrability and can be by physical activity when generated sweat drain into clothes rapidly
Surface layer evaporation is filled, keeps skin salubrious, activity is enabled to feel more comfortable.It has good wet guilding, the knitting to interweave with cotton fiber
Fabric leads wet effect with good.8 pieces of satin weaves or 10 pieces of satin weaves are used in the present embodiment.
In step S6 final finishing, the woven fabric of previous step institute is singed, washed, preshrunk, high-temperature shaping, is exempted from
Scald processing and drying.
Singing is using natural gas gassing frame, speed 100m/min, and burner number is 2, and pressure of singing is 13mbra, grade of singing
Number is 3-4.
Washing, is washed using 80 DEG C of conditions, and using feed preparation unit roller active drive technology, straight displacement elastic devices tension is 0.1Mpa,
Padding machine pressure is 0.1Mpa;Used rinsing solution contains softening agent.
The overfeeding 20% in preshrunk.
High-temperature shaping, overfeeding 20% straight in 160 DEG C of conditions of temperature, cropping overfeeding 4%.
Noniron finish is mixed using being made of resin FEL, strong protecting agent HDP, softening agent SF48, penetrating agent JFC and water
Liquid is closed fabric is carried out to pad processing;Wherein, resin FEL is 50g/L, and strong protecting agent HDP is 10g/L, and softening agent SF48 is
15g/L, penetrating agent JFC 5g/L.
Drying is under the conditions of 110 DEG C.
Embodiment two
A kind of production technology of cotton fiber four sides stretch yarn dyed fabric, includes the following steps: step involved in the present embodiment
The preparation of S1 yarn, the dyeing of step S2 warp thread, the dyeing of step S3 weft yarn, step S4 warp end preparing, step S5 weaving, step
S6 final finishing.Wherein, warp thread dyeing use cylinder yarn staining method, including warp thread metal, warp thread pre-treatment, warp dyeing,
Warp thread is soaped.The dyeing of weft yarn also uses the staining method of cylinder yarn, including weft yarn metal, weft yarn pre-treatment, weft yarn dyeing, weft yarn
It soaps.
In the preparation of step S1 yarn, warp thread is using cotton ammonia cladded yarn and Quality Pure Cotton Yarn Production plying institute at the cotton ammonia
For covering yarn using cotton fiber as clad, spandex as heart yarn, the content of spandex is 6%.The fineness of used spandex is
40D。
Weft yarn uses Modal and Coolmax fiber as clad, spandex for the covering yarn of heart yarn;Used spandex
Fineness be 70D;Clad in weft yarn is 21S-40S, and the content of Coolmax fiber is 65%.
In the dyeing of step S2 warp thread, using the staining method of cylinder yarn.Dyeing include warp thread metal, warp thread pre-treatment,
Warp dyeing, warp thread are soaped.
Warp thread metal is the oiling device that warp thread is used to slack winder, uniformly goes up auxiliary agent to warp thread, while network is at dye
Pine formula cylinder yarn required for color, and stand setting time;The density for being formed by loose formula cylinder yarn is 0.35g/cm3, single only loose formula
The weight of cylinder yarn is 0.7kg.Chamfering is wanted before dye using stainless steel wire helical Bourdon tube using overfeeding when winder.It needs strictly to do
It is uniform to thread density, it is in the same size.It prevents not of uniform size, elastic different, causes dyeing flower and inside and outside color difference.Standing setting can make
It obtains auxiliary agent and preferably infiltrates into yarn interior, can preferably remove Yarn oiling agent and impurity, improve the stainability of yarn.
In warp thread metal step, used auxiliary agent be scouring agent, penetrating agent JFC, degreaser, isopropanolamine it is water-soluble
Liquid;The concentration of scouring agent be added is 60g/L, the concentration of degreaser is 50g/L, the concentration of penetrating agent JFC is 20g/L, isopropyl
Hydramine is 15g/L;Time of repose is 16 hours.
It is in the warp thread pine formula cylinder yarn merging dye vat cylinder after standing, is that pretreatment liquid is added in 1:15 according to bath raio, it is described
Pretreatment liquid in the scouring agent containing 3g/L, 10g/L stabilizer BS, 2g/L dispersion chelating agent, from room temperature according to 1 DEG C/
The rate of min is warming up to 90 DEG C, and constant temperature operates 40min, after liquid is discharged, washes 15min using the clear water of 65 DEG C of temperature, then
Pickling 10min is carried out using the acetum that pH value is 6 under the conditions of 50 DEG C, is discharged after acetum under room temperature again and uses clear water
Wash 20min.
Warp dyeing is that the warp thread pine formula cylinder yarn Jing Guo pre-treatment is placed in dye liquor to dye;After pre-treatment,
Clear water is added and arrives bath raio 1:10, under the conditions of 40 DEG C, addition anhydrous sodium sulphate, bleeding agent AI BAFIJOW UNI, spandex promotor
ERIONAL ELA, diffusant UNIVADINF DFM, and the use of vinegar acid for adjusting pH value is 5.5,10min is run, is added 1%
The Megafix reactive dye of o.w.f operate the dye of positive ion of addition 0.5%o.w.f after 3-5min, according to the speed of 1 DEG C/min
Constant temperature operates 30-50min after rate is warming up to 110 DEG C, and dye liquor is discharged in the cooling washing 5-10min of overflow later.
In warp dyeing step, the anhydrous sodium sulphate being added is 1-2g/L, bleeding agent AI BAFIJOW UNI is 2g/L, spandex
Promotor ERIONAL ELA is 3g/L, diffusant UNIVADINF DFM is 2g/L.The Megafix reactive dye being added are indigo plant
Color or yellow.
Warp thread is soaped, and refers to again plus clear water reaches bath raio 1:10, under room temperature according to the ratio of 5g/L be added acid scouring agent,
The ratio anion syntannin class color fixing agent of 2g/L is warming up to 100 DEG C after operating 15min, washes drain after operating 20min,
Warp thread after being dyed.
In the dyeing of step S3 weft yarn, using the staining method of cylinder yarn, including weft yarn metal, weft yarn pre-treatment, weft yarn
Dyeing, weft yarn are soaped.
Weft yarn metal refers to the oiling device that weft yarn is used to slack winder, to the uniform upper auxiliary agent of weft yarn, while network at
Loose formula cylinder yarn required for dyeing, and stand setting time;The density for being formed by loose formula cylinder yarn is 0.3g/cm3, single only loose formula
The weight of cylinder yarn is 0.6kg;Overfeeding is used when winder, color plastic straighttube wants chamfering before dye;Used auxiliary agent is concise
Agent, chelated dispersants and bleeding agent aqueous solution;And adjusting pH value using soda ash is 11;Time of repose is 16 hours.
Weft yarn pre-treatment is in the weft yarn pine formula cylinder yarn merging dye vat cylinder after standing, and adding water to bath raio is 1:10, operating
Scouring agent, the caustic soda of 8g/L is added according still further to the ratio of 2g/L in 15min, and 10g/L hydrogen peroxide heats up according to the rate of 1 DEG C/min
To 90 DEG C, constant temperature operates 30min, after liquid is discharged, washes 15min using the clear water of 65 DEG C of temperature, then under the conditions of 50 DEG C
Pickling 10min is carried out using the acetum that pH value is 6, is discharged after acetum under room temperature again and washes 20min using clear water.
Weft yarn dyeing is that the weft yarn after pre-treatment is added water to bath raio for 1:15, under the conditions of 40 DEG C, according still further to 2g/L's
Ratio be added the levelling agent of 2g/L, 3g/L defoaming agent AF, 5g/L penetrating agent JFC, and adjust ph value 5 using acetic acid, fortune
Turn 15min;Dyeing accelerant NP is added according still further to the ratio of 3g/L, the Maxion type dye of 0.5%o.w.f operates 10min, according still further to
NylosanN type dye is added in the ratio of 0.6%o.w.f, after being warming up to 70 DEG C according to the rate of 2 DEG C/min, according still further to 0.7 DEG C/
The rate of min is warming up to 105 DEG C, and constant temperature operates 90min, is cooled to 65 DEG C according still further to the rate of 3 DEG C/min, and liquid is discharged
Afterwards, twice using the clear water washing of 65 DEG C of temperature.The Maxion type dye being added is pink colour, the color contaminated with warp thread not phase
Together.
Weft yarn is soaped, and refers to again plus clear water reaches bath raio 1:10, hydrogen peroxide is added according to the ratio of 5g/L under room temperature and operates
After 15min, it is warming up to 55 DEG C of ratios according to 2g/L and soaping agent, anion syntannin class color fixing agent is added, according to 2 DEG C/min
Rate be warming up to 100 DEG C, wash drain after operating 20min, the weft yarn after being dyed.
In step S4 warp end preparing, the warp thread after dyeing is existed according to technique setting warping using elastomeric yarn warping machine
On beam of a loom.Warping is will be through being evenly arranged on beam of a loom according to design requirement.Warping is without particular/special requirement in the present embodiment, and normal
The technique for advising warp end preparing when elastic fabric weaving is identical.
It in step S5 weaving, is weaved according to the technique of setting, the grammes per square metre of weaved fabric is 260-300g/m2。
Satin weave includes Warp Satin and satin.The front of Warp Satin, which is presented, is floated long line, and reverse side is presented latitude and floats long line.Filling satin
The front of line is presented latitude and floats long line, returns existing presentation and is floated long line.Either fabric can be achieved in Warp Satin or satin
Warp thread is presented on one side, weft yarn is presented on one side.
Fabric tissue uses satin in the present embodiment.The fabric tissue may make the front of fabric that mixed day is presented
Nylon covering yarn is presented in silk and Coolmax fiber, reverse side.Nylon can increase the wear resistance of fabric, mixed tencel and Coolmax
The skin-friendly of fabric can be improved in fiber, improve fabric penetrability and can be by physical activity when generated sweat drain into clothes rapidly
Surface layer evaporation is filled, keeps skin salubrious, activity is enabled to feel more comfortable.It has good wet guilding, the knitting to interweave with cotton fiber
Fabric leads wet effect with good.8 pieces of satin weaves or 10 pieces of satin weaves are used in the present embodiment.
In step S6 final finishing, the woven fabric of previous step institute is singed, washed, preshrunk, high-temperature shaping, is exempted from
Scald processing and drying.
Singing is using natural gas gassing frame, speed 120m/min, and burner number is 2, and pressure of singing is 13mbra, grade of singing
Number is 3-4.
Washing, is washed using 85 DEG C of conditions, and using feed preparation unit roller active drive technology, straight displacement elastic devices tension is 0.1Mpa,
Padding machine pressure is 0.1Mpa;Used rinsing solution contains softening agent.
The overfeeding 25% in preshrunk.
High-temperature shaping, overfeeding 25% straight in 170 DEG C of conditions of temperature, cropping overfeeding 5%.
Noniron finish is mixed using being made of resin FEL, strong protecting agent HDP, softening agent SF48, penetrating agent JFC and water
Liquid is closed fabric is carried out to pad processing;Wherein, resin FEL is 60g/L, and strong protecting agent HDP is 20g/L, and softening agent SF48 is
20g/L, penetrating agent JFC 10g/L.
Drying is under the conditions of 110 DEG C.
Fabric prepared by embodiment one and embodiment two is subjected to color fastness test according to respective standard.And with conventional city
The cotton ammonia cladded yarn four sides elastic fabric bought on field compares.
Using GB/T 8630-2002 " measurement of change in size after textile washing and drying " measurement.Dyefastness: it presses
GB/T 3921-2008 " textile color stability test fastness to soaping ", GB/T 3920-2008 " textile color stability test
Colour fastness to rubbing ", GB/T 3922-2013 " textile color stability test colour fastness to perspiration " standard is measured.
As can be seen from the above table, fabric fastness to soaping prepared by embodiment one and embodiment two, rub resistance color jail
The indexs such as degree, colour fastness to perspiration are better than comparative example.
It is high that wicking is carried out to fabric prepared by embodiment one and embodiment two and conventional cotton ammonia cored four-side elasticity fabric
Degree is compared with water evaporation rate.As a result it see the table below.
Project | Embodiment one | Embodiment two | Comparative example |
Measure wicking height/cm | 15.5-16.5 | 14.1-14.8 | 7.1-7.9 |
Water evaporation rate/% | 30.2-35.2 | 29.8-32.6 | 20.1-21.1 |
As can be seen from the above table, the fabric for applying tencel and Coolmax fiber has better measure wicking height and moisture
Evaporation rate, then embodiment one and the two woven fabric of institute of embodiment have better moisture absorption hydrofuge effect.
The preferred embodiment of the present invention has been described in detail above.It should be appreciated that those skilled in the art without
It needs creative work according to the present invention can conceive and makes many modifications and variations.Therefore, all technologies in the art
Personnel are available by logical analysis, reasoning, or a limited experiment on the basis of existing technology under this invention's idea
Technical solution, all should be within the scope of protection determined by the claims.
Claims (4)
1. a kind of production technology of cotton fiber four sides stretch yarn dyed fabric, which comprises the steps of:
Step S1, the preparation of yarn: warp thread using cotton ammonia cladded yarn and Quality Pure Cotton Yarn Production plying at, the cotton ammonia cladded yarn with
For cotton fiber as clad, spandex as heart yarn, the content of spandex is 6%;The fineness of the Quality Pure Cotton Yarn Production is 21-40s;Weft yarn
Use Modal and Coolmax fiber as clad, spandex for the covering yarn of heart yarn;The fineness of used spandex be 20D,
40D or 70D;Clad in weft yarn is 21S-40S, and the content of Coolmax fiber is in 50-65%;
Step S2, the dyeing of warp thread: using the staining method of cylinder yarn, including warp thread metal, warp thread pre-treatment, warp dyeing, warp
Yarn is soaped;
The warp thread metal is the oiling device that warp thread is used to slack winder, to the uniform upper auxiliary agent of warp thread, while network at
Loose formula cylinder yarn required for dyeing, and stand setting time;The density for being formed by loose formula cylinder yarn is 0.3-0.35g/cm3, single
Only the weight of loose formula cylinder yarn is 0.6-0.7kg;Chamfering is wanted before dye using stainless steel wire helical Bourdon tube using overfeeding when winder;
Used auxiliary agent is the aqueous solution of scouring agent, penetrating agent JFC, degreaser, isopropanolamine;The concentration of scouring agent be added is
50-60g/L, degreaser concentration be 40-50g/L, the concentration of penetrating agent JFC is 10-20g/L, isopropanolamine 10-15g/L;
Time of repose is 12-16 hours;
Warp thread pre-treatment is in the warp thread pine formula cylinder yarn merging dye vat cylinder after standing, is place before 1:10-15 is added according to bath raio
Manage liquid, the scouring agent containing 2-3g/L in the pretreatment liquid, 5-10g/L stabilizer BS, 1-2g/L dispersion chelating agent,
It is warming up to 85-90 DEG C from room temperature according to the rate of 0.7-1 DEG C/min, constant temperature operates 30-40min, after liquid is discharged, uses
The clear water of 60-65 DEG C of temperature washes 10-15min, then is carried out under the conditions of 45-50 DEG C using the acetum that pH value is 5.5-6
Pickling 8-10min is discharged after acetum under room temperature again and washes 10-20min using clear water;
Warp dyeing is that the warp thread pine formula cylinder yarn Jing Guo pre-treatment is placed in dye liquor to dye;After pre-treatment, it is added
Clear water is to bath raio 1:6-10, and under the conditions of 40 DEG C, anhydrous sodium sulphate, bleeding agent AI BAFIJOW UNI, spandex promotor ERIONAL is added
ELA, diffusant UNIVADINF DFM, and the use of vinegar acid for adjusting pH value is 4.4-5.5,5-10min is run, 0.5-1% is added
The Megafix reactive dye of o.w.f operate the dye of positive ion of addition 0.2-0.5%o.w.f after 3-5min, according to 0.7-1
DEG C/rate of min be warming up to 100-110 DEG C after constant temperature operating 30-50min, the cooling washing 5-10min of overflow later, discharge dye
Liquid;
Warp thread is soaped, and refers to again plus clear water reaches bath raio 1:6-10, under room temperature according to the ratio of 3-5g/L be added acid scouring agent,
The ratio anion syntannin class color fixing agent of 1-2g/L is warming up to 90-100 DEG C after operating 8-15min, after operating 10-20min
Wash drain, the warp thread after being dyed;
Step S3, the dyeing of weft yarn: using the staining method of cylinder yarn, including weft yarn metal, weft yarn pre-treatment, weft yarn dyeing, latitude
Yarn is soaped;
The weft yarn metal refers to the oiling device that weft yarn is used to slack winder, to weft yarn uniformly upper auxiliary agent, while network
At loose formula cylinder yarn required for dyeing, and stand setting time;The density for being formed by loose formula cylinder yarn is 0.25-0.3g/cm3,
The weight of single only loose formula cylinder yarn is 0.5-0.6kg;Overfeeding is used when winder, color plastic straighttube wants chamfering before dye;It is used
Auxiliary agent is the aqueous solution of scouring agent, chelated dispersants and bleeding agent;And adjusting pH value using soda ash is 10-11;Time of repose is
12-16 hours;
The weft yarn pre-treatment is in the weft yarn pine formula cylinder yarn merging dye vat cylinder after standing, and adding water to bath raio is 1:8-10,
8-15min is operated, scouring agent, the caustic soda of 4-8g/L, 6-10g/L hydrogen peroxide, according to 0.7-1 is added according still further to the ratio of 1-2g/L
DEG C/rate of min is warming up to 80-90 DEG C, constant temperature operates 20-30min, after liquid is discharged, uses the clear water of 60-65 DEG C of temperature
10-15min is washed, then carries out pickling 8-10min using the acetum that pH value is 5.5-6 under the conditions of 45-50 DEG C, vinegar is discharged
10-20min is washed using clear water under room temperature again after acid solution;
The weft yarn dyeing is that the weft yarn after pre-treatment is added water to bath raio for 1:10-15, under the conditions of 40 DEG C, according still further to
The ammonia of the levelling agent of 1-2g/L, the penetrating agent JFC of defoaming agent AF, 3-5g/L of 2-3g/L, 1-2g/L is added in the ratio of 1-2g/L
Synthetic fibre promotor ERIONAL ELA, and 10-15min is operated in 4.5-5 using vinegar acid for adjusting pH value;According still further to the ratio of 2-3g/L
Dyeing accelerant NP is added, the Maxion type dye of 0.2-0.5%o.w.f operates 5-10min, according still further to the ratio of 0.3-0.6%o.w.f
Nylosan N-type dyestuff is added in example, after being warming up to 65-70 DEG C according to the rate of 1-2 DEG C/min, according still further to 0.5-0.7 DEG C/min
Rate be warming up to 100-105 DEG C, constant temperature operates 60-90min, be cooled to 60-65 DEG C according still further to the rate of 2-3 DEG C/min, and
After liquid is discharged, washed twice using the clear water of 60-65 DEG C of temperature;
The weft yarn is soaped, and refers to again plus clear water reaches bath raio 1:6-10, dioxygen is added according to the ratio of 3-5g/L under room temperature
After water transport turns 8-15min, it is warming up to the 45-55 DEG C of ratio according to 1-2g/L and soaping agent, anion syntannin class fixation is added
Agent is warming up to 90-100 DEG C according to the rate of 1-2 DEG C/min, washes drain after operating 10-20min, the weft yarn after being dyed;
Step S4, the warp thread after dyeing warp end preparing: is arranged on beam of a loom according to technique by warping using elastomeric yarn warping machine;
Step S5, it weaves: being weaved according to the technique of setting, the grammes per square metre of weaved fabric is 80-120g/m2;Fabric tissue is adopted
Use satin weave;
Step S6, final finishing: the woven fabric of previous step institute is singed, is washed, preshrunk, high-temperature shaping, non-ironing processing
And drying.
2. the production technology of cotton fiber four sides as described in claim 1 stretch yarn dyed fabric, which is characterized in that warp dyeing step
In, the anhydrous sodium sulphate being added is 1-2g/L, bleeding agent AI BAFIJOWUNI is 1-2g/L, spandex promotor ERIONAL ELA is
2-3g/L, diffusant UNIVADINF DFM are 1-2g/L.
3. the production technology of cotton fiber four sides as described in claim 1 stretch yarn dyed fabric, which is characterized in that weft yarn metal step
In, the content of used scouring agent is 10-15g/L, and the content of chelated dispersants is 15-20g/L and the content of bleeding agent is 20-
30g/L。
4. the production technology of cotton fiber four sides as described in claim 1 stretch yarn dyed fabric, which is characterized in that step S6 final finishing
In,
Singing is using natural gas gassing frame, speed 100-120m/min, and burner number is 2, and pressure of singing is 13mbra, grade of singing
Number is 3-4;
Washing, is washed using 80-85 DEG C of condition, and using feed preparation unit roller active drive technology, straight displacement elastic devices tension is 0.1Mpa, is rolled
Vehicle pressure is 0.1Mpa;Used rinsing solution contains softening agent;
Overfeeding 20-25% when preshrunk;
High-temperature shaping, overfeeding 20-25% straight in 160-170 DEG C of condition of temperature, cropping overfeeding 4-5%;
Noniron finish is to form mixed liquor using by resin FEL, strong protecting agent HDP, softening agent SF48, penetrating agent JFC and water
Fabric is carried out to pad processing;Wherein, resin FEL is 50-60g/L, and strong protecting agent HDP is 10-20g/L, softening agent SF48
For 15-20g/L, penetrating agent JFC 5-10g/L;
Drying is under the conditions of 110 DEG C.
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CN112609290A (en) * | 2020-12-04 | 2021-04-06 | 张家港市金陵纺织有限公司 | Production process of comfortable cotton-polyester interwoven double-layer cloth color woven fabric |
CN112878060A (en) * | 2021-01-14 | 2021-06-01 | 湖州倍亨纺织有限公司 | Preparation method and preparation device of degradable tencel trademark tape |
CN113122995A (en) * | 2021-05-26 | 2021-07-16 | 重庆财衡巨纺织有限公司 | Lyocell-based fabric and production process |
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Application publication date: 20190430 |
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