CN109673685A - A kind of drug and preparation method thereof for uncinula necator - Google Patents

A kind of drug and preparation method thereof for uncinula necator Download PDF

Info

Publication number
CN109673685A
CN109673685A CN201810846737.3A CN201810846737A CN109673685A CN 109673685 A CN109673685 A CN 109673685A CN 201810846737 A CN201810846737 A CN 201810846737A CN 109673685 A CN109673685 A CN 109673685A
Authority
CN
China
Prior art keywords
drug
uncinula necator
compound
vitamins
extracted solution
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810846737.3A
Other languages
Chinese (zh)
Inventor
章伟贵
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Puding Lusheng Garden Ecological Agriculture Co Ltd
Original Assignee
Puding Lusheng Garden Ecological Agriculture Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Puding Lusheng Garden Ecological Agriculture Co Ltd filed Critical Puding Lusheng Garden Ecological Agriculture Co Ltd
Priority to CN201810846737.3A priority Critical patent/CN109673685A/en
Publication of CN109673685A publication Critical patent/CN109673685A/en
Pending legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01GHORTICULTURE; CULTIVATION OF VEGETABLES, FLOWERS, RICE, FRUIT, VINES, HOPS OR SEAWEED; FORESTRY; WATERING
    • A01G13/00Protecting plants
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01GHORTICULTURE; CULTIVATION OF VEGETABLES, FLOWERS, RICE, FRUIT, VINES, HOPS OR SEAWEED; FORESTRY; WATERING
    • A01G17/00Cultivation of hops, vines, fruit trees, or like trees
    • A01G17/02Cultivation of hops or vines
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/44Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a nitrogen atom attached to the same carbon skeleton by a single or double bond, this nitrogen atom not being a member of a derivative or of a thio analogue of a carboxylic group, e.g. amino-carboxylic acids
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/02Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
    • A01N43/04Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
    • A01N43/14Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
    • A01N43/16Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/34Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
    • A01N43/36Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom five-membered rings
    • A01N43/38Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom five-membered rings condensed with carbocyclic rings
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/72Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms
    • A01N43/74Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms five-membered rings with one nitrogen atom and either one oxygen atom or one sulfur atom in positions 1,3
    • A01N43/781,3-Thiazoles; Hydrogenated 1,3-thiazoles
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N45/00Biocides, pest repellants or attractants, or plant growth regulators, containing compounds having three or more carbocyclic rings condensed among themselves, at least one ring not being a six-membered ring
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/34Rosaceae [Rose family], e.g. strawberry, hawthorn, plum, cherry, peach, apricot or almond
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40Liliopsida [monocotyledons]
    • A01N65/42Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental Sciences (AREA)
  • Zoology (AREA)
  • Plant Pathology (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Agronomy & Crop Science (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Pest Control & Pesticides (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Botany (AREA)
  • Toxicology (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The present invention relates to pesticide field, in particular to a kind of drug for uncinula necator;It is made of following raw material by weight: compound extracted solution 30-50, compound amino acid 3-12, multi-vitamins 1-10;The combination drug for uncinula necator of the application preparation, effectively inhibit the growth of pathogen, during spraying, drug of the present invention will not damage grape itself, simultaneously, play the role of to greatest extent to uncinula necator again good for the disease incidence control of the powdery mildew of grape 2% or so, to the total effective rate of the uncinula necator fallen ill 95% or more.

Description

A kind of drug and preparation method thereof for uncinula necator
Technical field
The present invention relates to pesticide field, in particular to a kind of drug and preparation method thereof for uncinula necator.
Background technique
Grape is not only delicious and tasty, but also nutritive value is very high.Grape sugar content is up to 10%- in mature berry 30%, based on glucose.A variety of tartaric acid in grape help to digest, and suitably eat a little grapes more, can be good for Pi stomach function regulating.In grape Containing mineral calcium, potassium, phosphorus, iron and multivitamin B1, vitamin B2, vitamin B6, vitamin C and citrin etc., also It is of great advantage to neurasthenia, excessive fatigue containing grape there are many amino acid of needed by human body, is often eaten, wherein Vitis davidii Foex (scientific name: It Vitisdavidiivar.davidii is) mutation under Vitaceae Vitis, fruit is most in amur grape for Vitis davidii Foex It greatly, is the valuable materials of vertical greening and Grape Breeding.As a kind of amur grape resource, Vitis davidii Foex has high disease-resistant Property, moisture-proof and resistance.General grape variety needs weekly spraying pesticide, needs a large amount of chemical fertilizer, and wild Vitis davidii Foex does not have to Spraying pesticide only needs a small amount of organic fertilizer, is entirely the black fruit of green non-pollution.According to surveying and determination, Vitis davidii Foex berry is except aqueous Exceptionally, also contain about 15%-25% carbohydrate (mainly glucose, fructose), various organic acids (malic acid, tartaric acid and few Citric acid, succinic acid, gallic acid, oxalic acid, salicylic acid of amount etc.) and minerals and various vitamins, amino acid, albumen Matter, carbohydrate, crude fibre, calcium, phosphorus, iron, zinc, selenium, carrotene, thiamine, riboflavin, ascorbic acid etc..Modern times doctor It learns it is also found that: the antioxidant resveratrol contained in wild Vitis davidii Foex skin and grape pip is high, has actively to cardiovascular and cerebrovascular diseases Preventive and therapeutic action, Vitis davidii Foex is amur grape, it inherits the trophism of other grape varieties, it have very high battalion Value is supported, multivitamin and microelement are rich in, often eat softening blood vessel and raises body, it being capable of certain journey The prevention of arterial of degree hardens, it is also powerful antioxidant, therefore has good pre- anti-aging and whitening function.
In view of grape nutritive value abundant and medical value, thus with it is high can implanting, therefore it is each in China There is plantation in province, and most important wine-growing is that disease is used for, and easily occurs multiple diseases in wine-growing, if powdery mildew is grape Major Diseases, fruit, blade and the green portions such as new school is climing can be aggrieved, and maximum with fruit damage loss.Fruit is aggrieved, first On fruit surface, one layer of grayish white powdery of generation is mould, wipes white powder, and brown decorative pattern is presented in epidermis, and last epidermal cell becomes dun Color.Blade is aggrieved, mould in leaf surface one layer of canescence silty of generation, gradually spreads to entire blade, the contracting of disease leaf roll is withered when serious It withers.New branches and tendrils are aggrieved, and canescence stigma is just presented, and rear extension sprawling makes complete climing morbidity, and disease is climing to become dark gray by canescence, most Black afterwards.Cause of disease Pseudomonas ascomycetes Uncinula.Asexual generation belongs to Fungi Imperfecti powder spore category.Pathogen is with mycelium killed Overwintering in tissue or perula piece, next spring generates mitogenetic robe, travels to host surfaces by means of wind-force;Suction is generated on mycelia Device is directly protruding into host cell and draws nutrition, and mycelia then spreads in host surfaces, and fruit face, branches and tendrils and blade face are in crineous, Mainly influenced by haustorium.Disease is generally on July, the middle ten days occurs to 9-10 is monthly, uses sending out for powdery mildew at present 1 3-5 Baume degrees lime sulfur should be sprayed before bud, and 500 times of 0.2-0.5 Baume degrees lime sulfur or 50% thiophanate are sprayed after germination The targeted agents such as 1000 times of liquid of liquid or 70% thiophanate methyl or 25% 1000 times of liquid of trazodone wettable powder are used In, but spraying for traditional medicament, there is medicament residue, cause harm to the human body, disease is not significant a series of for effect Problem, harm is larger, so, improving to the prevention and treatment of traditional uncinula necator is the emphasis studied at present.
Summary of the invention
The present invention is in order to solve the above technical problems, provide a kind of drug and preparation method thereof for uncinula necator.
It is realized particular by following technical scheme:
A kind of drug for uncinula necator is made of following raw material by weight: compound extracted solution 30-50, Compound amino acid 3-12, multi-vitamins 1-10.
It is made of following raw material by weight: compound extracted solution 40, compound amino acid 8, multi-vitamins 5.
The compound extracted solution is to mix Chinese parasol tree bark, flowering peach, onion by the mass ratio of 1:0.8-1.2:0.1-0.3 It closes, adds water infusion 30-40min, filter, filter residue is added again water repeat infusion twice, resulting filtrate mixing will be filtered three times, It is concentrated into the ethyl alcohol for 5 times of amounts that the 1/3. of volume is added concentrate quality, constant temperature reflux, vacuum distillation recycling ethyl alcohol obtains compound Extracting solution.
The constant temperature reflux, temperature are 55-65 DEG C.
The compound amino acid is the mass ratio by cystine, tryptophan and alanine by 0.1-0.3:1:0.6-0.8 It is mixed to prepare.
The multi-vitamins are by VB1, VD and VE mix by the mass ratio of 0.3-0.6:0.2-0.4:0.1-0.5 It is made.
The drug for uncinula necator, when use spray grape complete stool, in the first ten-day period of the March to May The last ten-days period spray twice respectively, and each mu amount of spraying is 20-40kg, and the first tenday period of a month in June to late October spray 5 times respectively, each mu spray The amount of applying is 55-75kg.
The preparation method of the drug for uncinula necator is by compound amino acid and multi-vitamins by formula It after weighing, is added in compound extracted solution, under the frequency of 30-40KHz, is ultrasonically treated 12-18min, stands 3-5h, bottling is It can.
Being described further for effect to the drug for uncinula necator of preparation below:
1, with randomly selecting several mu of wine-growings, 3 groups are randomly divided into, is managed using daily management mode, it is different Place is that first group in wine-growing, sprays twice respectively in the first ten-day period of the March to late May, and each mu amount of spraying is 20-40kg, second group is used for referring to first group, and the drug for being commercially available for uncinula necator, the mu amount of spraying are sprayed to grape Identical, third group does not spray any drug, and test period is the entire wine-growing phase, respectively to the disease incidence of uncinula necator into Row statistics, the results are shown in Table 1:
Table 1
Project Disease incidence %
First group 2.21
Second group 4.32
Third group 13.6
2,2 groups with randomly selecting several mu of wine-growings, are randomly divided into, similar degree has occurred in every group of plantation grape Powdery mildew disease is managed using daily management mode, the difference is that, the first tenday period of a month in June to late October spray 5 respectively Secondary, each mu amount of spraying is 55-75kg, and second group is used for referring to first group, sprays to grape and is commercially available for grape white powder The drug of disease, the mu amount of spraying is identical, is indicated to uncinula necator with total effective rate for situation, wherein total effective rate generation Table be restored to before the onset of state and the state of an illness be eased, need the summation of the two situation of further medication observation, as a result such as Shown in table 2:
Table 2
Project Total effective rate %
First group 95.6
Second group 88.4
In conclusion the beneficial effects of the present invention are: the combination drug for uncinula necator of the application preparation has Effect inhibits the growth of pathogen, and during spraying, drug of the present invention will not damage grape itself, meanwhile, and most Playing the role of to uncinula necator for limits is good for right to the disease incidence control of the powdery mildew of grape 2% or so The total effective rate for the uncinula necator fallen ill is used for significant effect, effectively contains and killed cause of disease 95% or more Bacterium reduces the infringement of powdery mildew pathogenic bacteria and other pests pair, effectively avoids the growth of pathogen, the safety that ensure that.
Compound extracted solution prepared by the present invention has the effect of stronger antibacterial bacteriostatic, can effectively play inhibition and killing The effect of pathogen, thus achieve the effect that it is anti-, control and have both, meanwhile, also added in formula improve plant resistance, enhancing The multi-vitamins and compound amino acid of immunity can effectively improve the resistance of plant and the resistance to disease and insect, can increase Strong buffering power of soil is retained moisturizing, enhances crop drought resistance, cold-resistant, waterlogging-resistant ability;Blade protection film can also be strengthened simultaneously, supported Anti-microbial pathogen infects, disease-resistant, pest-resistant, and the disease incidence of uncinula necator is effectively reduced.
Specific embodiment
Specific embodiments of the present invention will be described in further detail below, but the invention is not limited to these realities Mode is applied, it is claimed to still fall within the claims in the present invention for any improvement or replacement on the present embodiment essence spirit Range.
Embodiment 1
A kind of drug for uncinula necator is made of following raw material by weight: compound extracted solution 30, compound Amino acid 3, multi-vitamins 1;The compound amino acid is the matter by cystine, tryptophan and alanine by 0.1:1:0.6 Amount ratio is mixed to prepare;The multi-vitamins are by VB1, VD and VE be mixed to prepare by the mass ratio of 0.3:0.2:0.1;Institute The compound extracted solution stated is to mix Chinese parasol tree bark, flowering peach, onion by the mass ratio of 1:0.8:0.1, adds water infusion 30min, mistake Filter adds filter residue water to repeat infusion twice again, will filter resulting filtrate mixing three times, and 1/3. addition for being concentrated into volume is dense The ethyl alcohol of 5 times of amounts of contracting liquid quality, the constant temperature reflux 1h at 55 DEG C, vacuum distillation recycling ethyl alcohol obtain compound extracted solution.
The preparation method of the drug for uncinula necator is by compound amino acid and multi-vitamins by formula It after weighing, is added in compound extracted solution, under the frequency of 30KHz, is ultrasonically treated 12min, stands 3-5h, bottling.
Embodiment 2
A kind of drug for uncinula necator is made of following raw material by weight: compound extracted solution 50, compound Amino acid 12, multi-vitamins 10;The compound amino acid is by cystine, tryptophan and alanine by 0.3:1:0.8 Mass ratio is mixed to prepare;The multi-vitamins are by VB1, VD and VE be mixed to prepare by the mass ratio of 0.6:0.4:-0.5; The compound extracted solution is to mix Chinese parasol tree bark, flowering peach, onion by the mass ratio of 1:1.2:0.3, adds water infusion 30min, Filtering adds filter residue water to repeat infusion twice again, will filter resulting filtrate mixing three times, and be concentrated into volume 1/3. is added The ethyl alcohol of 5 times of amounts of concentrate quality, the constant temperature reflux 1h at 65 DEG C, vacuum distillation recycling ethyl alcohol obtain compound extracted solution.
The preparation method of the drug for uncinula necator is by compound amino acid and multi-vitamins by formula It after weighing, is added in compound extracted solution, under the frequency of 40KHz, is ultrasonically treated 18min, stands 3-5h, bottling.
Embodiment 3
A kind of drug for uncinula necator is made of following raw material by weight: compound extracted solution 40, compound Amino acid 8, multi-vitamins 5;The compound amino acid is the matter by cystine, tryptophan and alanine by 0.2:1:0.7 Amount ratio is mixed to prepare;The multi-vitamins are by VB1, VD and VE be mixed to prepare by the mass ratio of 0.5:0.3:0.3;Institute The compound extracted solution stated is to mix Chinese parasol tree bark, flowering peach, onion by the mass ratio of 1:1:0.2, adds water infusion 35min, mistake Filter adds filter residue water to repeat infusion twice again, will filter resulting filtrate mixing three times, and 1/3. addition for being concentrated into volume is dense The ethyl alcohol of 5 times of amounts of contracting liquid quality, the constant temperature reflux 1h at 60 DEG C, vacuum distillation recycling ethyl alcohol obtain compound extracted solution.
The preparation method of the drug for uncinula necator is by compound amino acid and multi-vitamins by formula It after weighing, is added in compound extracted solution, under the frequency of 35KHz, is ultrasonically treated 15min, stands 3-5h, bottling.
Embodiment 4
A kind of drug for uncinula necator is made of following raw material by weight: compound extracted solution 30, compound Amino acid 12, multi-vitamins 1;The compound amino acid is by cystine, tryptophan and alanine by 0.1:1:0.8 Mass ratio is mixed to prepare;The multi-vitamins are by VB1, VD and VE be mixed to prepare by the mass ratio of 0.3:0.4:0.1; The compound extracted solution is to mix Chinese parasol tree bark, flowering peach, onion by the mass ratio of 1:0.8:0.3, adds water infusion 30min, Filtering adds filter residue water to repeat infusion twice again, will filter resulting filtrate mixing three times, and be concentrated into volume 1/3. is added The ethyl alcohol of 5 times of amounts of concentrate quality, the constant temperature reflux 1h at 55 DEG C, vacuum distillation recycling ethyl alcohol obtain compound extracted solution.
The preparation method of the drug for uncinula necator is by compound amino acid and multi-vitamins by formula It after weighing, is added in compound extracted solution, under the frequency of 30KHz, is ultrasonically treated 18min, stands 3h, bottling.
Embodiment 5
A kind of drug for uncinula necator is made of following raw material by weight: compound extracted solution 50, compound Amino acid 3, multi-vitamins 10;The compound amino acid is by cystine, tryptophan and alanine by 0.1:1:0.8 Mass ratio is mixed to prepare;The multi-vitamins are by VB1, VD and VE be mixed to prepare by the mass ratio of 0.3:0.4:0.1; The compound extracted solution is to mix Chinese parasol tree bark, flowering peach, onion by the mass ratio of 1:0.8:0.3, adds water infusion 40min, Filtering adds filter residue water to repeat infusion twice again, will filter resulting filtrate mixing three times, and be concentrated into volume 1/3. is added The ethyl alcohol of 5 times of amounts of concentrate quality, the constant temperature reflux 1h at 65 DEG C, vacuum distillation recycling ethyl alcohol obtain compound extracted solution.
The preparation method of the drug for uncinula necator is by compound amino acid and multi-vitamins by formula It after weighing, is added in compound extracted solution, under the frequency of 40KHz, is ultrasonically treated 12min, stands 5h, bottling.

Claims (8)

1. a kind of drug for uncinula necator, which is characterized in that be made of following raw material by weight: compound collecting Liquid 30-50, compound amino acid 3-12, multi-vitamins 1-10.
2. being used for the drug of uncinula necator as described in claim 1, which is characterized in that by following raw material by weight Composition: compound extracted solution 40, compound amino acid 8, multi-vitamins 5.
3. being used for the drug of uncinula necator as claimed in claim 1 or 2, which is characterized in that the compound extracted solution is Chinese parasol tree bark, flowering peach, onion are mixed by the mass ratio of 1:0.8-1.2:0.1-0.3, adds water infusion 30-40min, filters, it will Filter residue adds water to repeat infusion twice again, will filter resulting filtrate mixing three times, and concentrate is added in be concentrated into volume 1/3. The ethyl alcohol of 5 times of amounts of quality, constant temperature reflux, vacuum distillation recycling ethyl alcohol obtain compound extracted solution.
4. being used for the drug of uncinula necator as claimed in claim 3, which is characterized in that the constant temperature reflux, temperature are 55-65℃。
5. being used for the drug of uncinula necator as claimed in claim 1 or 2, which is characterized in that the compound amino acid is Cystine, tryptophan and alanine are mixed to prepare by the mass ratio of 0.1-0.3:1:0.6-0.8.
6. being used for the drug of uncinula necator as claimed in claim 1 or 2, which is characterized in that the multi-vitamins are By VB1, VD and VE be mixed to prepare by the mass ratio of 0.3-0.6:0.2-0.4:0.1-0.5.
7. being used for the drug of uncinula necator as described in claim 1, which is characterized in that sprayed when use to grape complete stool It applies, is sprayed respectively twice in the first ten-day period of the March to late May, each mu amount of spraying is 20-40kg, the first tenday period of a month in June to late October It sprays respectively 5 times, each mu amount of spraying is 55-75kg.
8. the preparation method for the drug of uncinula necator as described in claim 1, which is characterized in that be by compounded amino It after acid and multi-vitamins are weighed by formula, is added in compound extracted solution, under the frequency of 30-40KHz, is ultrasonically treated 12- 18min stands 3-5h, bottling.
CN201810846737.3A 2018-07-27 2018-07-27 A kind of drug and preparation method thereof for uncinula necator Pending CN109673685A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810846737.3A CN109673685A (en) 2018-07-27 2018-07-27 A kind of drug and preparation method thereof for uncinula necator

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810846737.3A CN109673685A (en) 2018-07-27 2018-07-27 A kind of drug and preparation method thereof for uncinula necator

Publications (1)

Publication Number Publication Date
CN109673685A true CN109673685A (en) 2019-04-26

Family

ID=66185479

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201810846737.3A Pending CN109673685A (en) 2018-07-27 2018-07-27 A kind of drug and preparation method thereof for uncinula necator

Country Status (1)

Country Link
CN (1) CN109673685A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114009433A (en) * 2021-12-13 2022-02-08 云南硕农农业科技有限公司 Composition capable of preventing and treating plant powdery mildew and application thereof

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101156606A (en) * 2007-11-20 2008-04-09 史建生 A plants antiseptic as well as preparing method and application
CN104705356A (en) * 2015-04-06 2015-06-17 于澎 Composition for preventing and treating Yangshan peach rhizopus
CN106259548A (en) * 2016-08-04 2017-01-04 金寨县万紫千红农业科技开发有限公司 Tea place organic composite Chinese medicine anthelmintic medicated bag and preparation method
CN106359465A (en) * 2016-08-18 2017-02-01 滁州嘉实农业科技有限公司 Botanical composition for treating grape powdery mildew and preparation method thereof
CN106490071A (en) * 2016-10-31 2017-03-15 郑州思辩科技有限公司 A kind of agricultural chemicals of preventing and treating uncinula necator and preparation method thereof
CN107691502A (en) * 2017-10-31 2018-02-16 银学庆 A kind of composition for preventing and treating wild cabbage virosis and preparation method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101156606A (en) * 2007-11-20 2008-04-09 史建生 A plants antiseptic as well as preparing method and application
CN104705356A (en) * 2015-04-06 2015-06-17 于澎 Composition for preventing and treating Yangshan peach rhizopus
CN106259548A (en) * 2016-08-04 2017-01-04 金寨县万紫千红农业科技开发有限公司 Tea place organic composite Chinese medicine anthelmintic medicated bag and preparation method
CN106359465A (en) * 2016-08-18 2017-02-01 滁州嘉实农业科技有限公司 Botanical composition for treating grape powdery mildew and preparation method thereof
CN106490071A (en) * 2016-10-31 2017-03-15 郑州思辩科技有限公司 A kind of agricultural chemicals of preventing and treating uncinula necator and preparation method thereof
CN107691502A (en) * 2017-10-31 2018-02-16 银学庆 A kind of composition for preventing and treating wild cabbage virosis and preparation method thereof

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
杨洪强等: "《有机园艺》", 31 July 2005, 中国农业出版社 *
郑跟娣: "《环渤海污染压力和海上响应的统筹调控研究》", 31 January 2016, 海洋出版社 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114009433A (en) * 2021-12-13 2022-02-08 云南硕农农业科技有限公司 Composition capable of preventing and treating plant powdery mildew and application thereof

Similar Documents

Publication Publication Date Title
CN110074113B (en) Application of stropharia rugoso-annulata polysaccharide, plant immunity inducer and application
CN105028528B (en) A kind of agricultural chemicals for preventing and treating cotton anthracnose
CN109548791A (en) A kind of bactericidal composition
CN106109261A (en) Whitening skin lightening breast and preparation method thereof
KR101230003B1 (en) Method for preparing natural soap composite using fermented wild vegetable juice
CN106508567A (en) Zizyphus maurtiana planting method
CN109673685A (en) A kind of drug and preparation method thereof for uncinula necator
CN102204575B (en) Silktree-albizia-extract-based preparation for controlling tetranychus cinnabarinus, and preparation and application thereof
CN107125273A (en) A kind of composition for preventing and treating grape grey mould and preparation method thereof
KR102330277B1 (en) Cosmetics composition comprising centella asiatica extracts
CN107173123A (en) A kind of prevention and controls of Vitis davidii Foex mildew
CN1035225A (en) A kind of novel plant bactericide and preparation method thereof
CN107771811B (en) Bitter gourd seed treating agent and method for treating bitter gourd seeds by using same
KR20170014494A (en) Water tissue comprising extracts of graviola and water tissue thereby
CN106983691B (en) Lotus polyphenol-containing anti-oxidation pore-shrinking sleeping mask and preparation method thereof
CN106942284B (en) It is a kind of prevent and treat grape disease complex biological bactericide and its application
CN104855186A (en) Pomegranate sooty mould control method
CN105028411B (en) Composition containing TrinexAN_SNacethyl and chitosan oligosaccharide or chitosan
CN105104389B (en) Composition and application containing Acibenzolar and chitosan oligosaccharide
CN106490048A (en) A kind of environment friendly agricultural of preventing and treating brassicaceous vegetable pest and disease damage and preparation method thereof
CN110226607B (en) Medicament composition for preventing and treating cucumber aphid and cucumber bacterial angular leaf spot
CN106259341A (en) A kind of Citrus fresh preservation with branches agent containing amino-oligosaccharide and cinnamic acid
CN107333537A (en) Carnation implantation methods
CN105394072A (en) Sterilization composition containing meptyldinocap and flusilazole and application thereof
CN106495862A (en) A kind of composite pesticide for apple tree cultivation and preparation method thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20190426