CN109608924A - A kind of flame-proof antibiotic paint preparation method for wooden equipment - Google Patents
A kind of flame-proof antibiotic paint preparation method for wooden equipment Download PDFInfo
- Publication number
- CN109608924A CN109608924A CN201811524120.6A CN201811524120A CN109608924A CN 109608924 A CN109608924 A CN 109608924A CN 201811524120 A CN201811524120 A CN 201811524120A CN 109608924 A CN109608924 A CN 109608924A
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- flame
- retardant
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Plant Pathology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention belongs to paint technology field, tool is disclosed and a kind of flame-proof antibiotic for wooden equipment paints preparation method；Using dispersibility of the titanate coupling agent modified titanium dioxide carrying silver antimicrobials in paint, titanium dioxide carrying silver antimicrobials dispersion effect is best；The present invention uses mesoporous silicon oxide composite flame-retardant agent, and preparation method is simple, and the design feature for combining mesoporous silicon oxide enhances the stability of fire retardant, improves the flame retardant property of paint；The present invention uses titanium dioxide carrying silver antimicrobials, and the titanium dioxide and silver generate antibacterial synergistic effect, and antibacterial effect is preferable；The present invention uses composite flame-retardant agent, effectively reduces cost, and improves flame retardant effect；The present invention loads fire retardant using mesoporous silicon oxide, has preferable stability, while producing fire-retardant synergistic effect, flame retardant effect is more preferably.
Description
Technical field
The invention belongs to paint technology fields, and in particular to a kind of flame-proof antibiotic paint preparation side for wooden equipment
Method.
Background technique
Paint be it is a kind of can securely be covered on body surface, the chemistry for playing protection, decoration, mark and other specific uses is mixed
Close object coating.More authoritative " coating process " book of Chinese paint industry is defined such that " coating is a kind of material, this
Material can be coated in object surface with different construction technologies, and it is secured, thin with some strength, continuous solid-state to form adherency
Film.The film common name film formed in this way, also known as paint film or coating.
Paint is the coating made of the raw materials such as iron oxide or resin to decorate and protect article.It is viscous oily
Pigment, it is inflammable in not dry situation, insoluble in fire, be slightly soluble in fat, dissolve in alcohol, aldehyde, ether, benzene, alkane, be soluble in gasoline, kerosene,
Diesel oil.It paints in place of Shortcomings existing market: such as without flameproof effect, being lost encountering fire etc. and causing to be difficult to make up etc., and
And paint production cost of material is higher, is unable to satisfy user's economic benefit.Simultaneously with environmental protection problem become increasingly conspicuous with
And pursuit of the people to health environment, antibacterium paint is as a kind of environmental-friendly new function material.
Summary of the invention
The present invention provides a kind of flame-proof antibiotics for wooden equipment to paint preparation method, is changed by titanate coupling agent
Dispersibility of the property titanium dioxide carrying silver antimicrobials in alkyd paint, is prepared the uniform antibacterium paint of performance；By fire-retardant
Composite flame-retardant agent is prepared in agent and the compound of mesoporous silicon oxide, to improve the flame retardant property of paint.
Specific technical solution of the present invention is as follows:
A kind of flame-proof antibiotic paint preparation method for wooden equipment, it is characterised in that: comprise the steps of:
(1) titanate coupling agent modified titanium dioxide carrying silver antimicrobials are used, modified antibacterial agent is prepared；
(2) aluminium hydroxide and antimony oxide are prepared into solution according to certain mass ratio, is then added vacuum drying mesoporous two
Composite flame-retardant agent is prepared in silica；
(3) it after mixing the modified antibacterial agent and the composite flame-retardant agent, is added in paint preparation process, by high-speed stirring
It mixes and flame-proof antibiotic paint is prepared.
Preferably, step (1) the modified antibacterial agent is specific the preparation method comprises the following steps: titanate coupling agent has been added to
It is stirred evenly in solvent, titanium dioxide carrying silver antimicrobials is then added and are stirred, in 45-65 DEG C of temperature, 350-400r/
Modified 1-3h under conditions of min revolving speed；It filters, wash, modified antibacterial agent is prepared after drying.
Preferably, step (2) described composite flame-retardant agent is specific the preparation method comprises the following steps: aluminium hydroxide and antimony oxide are pressed
It is uniformly mixed according to the ratio of 3:5, after addition distilled water is formulated as solution, vacuum drying mesoporous silicon dioxide powder is added,
1-3h is stirred at 65-80 DEG C, grinding obtains nanoscale complex antimicrobials in the ball mill after vacuum drying.
Preferably, the revolving speed of step (3) described high-speed stirred is 800 ~ 1200r/min.
The invention has the advantages that:
The present invention uses dispersibility of the titanate coupling agent modified titanium dioxide carrying silver antimicrobials in paint, TiO 2 carrying silver
Antibacterial agent dispersion effect is best；The present invention uses mesoporous silicon oxide composite flame-retardant agent, and preparation method is simple, and combines mesoporous
The design feature of silica enhances the stability of fire retardant, improves the flame retardant property of paint；The present invention uses titanium dioxide
Titanium carrying silver antimicrobials, the titanium dioxide and silver generate antibacterial synergistic effect, and antibacterial effect is preferable；The present invention uses composite flame-proof
Agent effectively reduces cost, and improves flame retardant effect；The present invention loads fire retardant using mesoporous silicon oxide, has preferable stablize
Property, while fire-retardant synergistic effect is produced, flame retardant effect is more preferably.
Specific embodiment
Technical solution of the present invention is further illustrated below by specific embodiment.
Embodiment 1
A kind of flame-proof antibiotic paint preparation method for wooden equipment comprises the steps of:
(1) titanate coupling agent modified titanium dioxide carrying silver antimicrobials are used, modified antibacterial agent is prepared；
The specific of modified antibacterial agent stirs evenly the preparation method comprises the following steps: titanate coupling agent is added in organic solvent,
Then titanium dioxide carrying silver antimicrobials are added to be stirred, modified 3h under conditions of 45 DEG C of temperature, 350r/min revolving speed；It takes out
Modified antibacterial agent is prepared after filter, washing, drying；
(2) aluminium hydroxide and antimony oxide are prepared into solution according to certain mass ratio, is then added vacuum drying mesoporous two
Composite flame-retardant agent is prepared in silica；
The composite flame-retardant agent specific is the preparation method comprises the following steps: aluminium hydroxide and antimony oxide are mixed according to the ratio of 3:5 equal
It is even, after addition distilled water is formulated as solution, vacuum drying mesoporous silicon dioxide powder is added, 3h, vacuum are stirred at 65 DEG C
Grinding obtains nanoscale complex antimicrobials in the ball mill after drying；
(3) it after mixing the modified antibacterial agent and the composite flame-retardant agent, is added in paint preparation process, by 800r/
Flame-proof antibiotic paint is prepared in the high-speed stirred of min.
Embodiment 2
A kind of flame-proof antibiotic paint preparation method for wooden equipment comprising the steps of:
(1) titanate coupling agent modified titanium dioxide carrying silver antimicrobials are used, modified antibacterial agent is prepared；
The specific of modified antibacterial agent stirs evenly the preparation method comprises the following steps: titanate coupling agent is added in organic solvent,
Then titanium dioxide carrying silver antimicrobials are added to be stirred, modified 1h under conditions of 65 DEG C of temperature, 400r/min revolving speed；It takes out
Modified antibacterial agent is prepared after filter, washing, drying
(2) aluminium hydroxide and antimony oxide are prepared into solution according to certain mass ratio, is then added vacuum drying mesoporous two
Composite flame-retardant agent is prepared in silica；
The composite flame-retardant agent specific is the preparation method comprises the following steps: aluminium hydroxide and antimony oxide are mixed according to the ratio of 3:5 equal
It is even, after addition distilled water is formulated as solution, vacuum drying mesoporous silicon dioxide powder is added, 1h, vacuum are stirred at 80 DEG C
Grinding obtains nanoscale complex antimicrobials in the ball mill after drying；
(3) it after mixing the modified antibacterial agent and the composite flame-retardant agent, is added in paint preparation process, by 1200r/
Flame-proof antibiotic paint is prepared in the high-speed stirred of min.
Embodiment 3
A kind of flame-proof antibiotic paint preparation method for wooden equipment comprising the steps of:
(1) titanate coupling agent modified titanium dioxide carrying silver antimicrobials are used, modified antibacterial agent is prepared；
The specific of modified antibacterial agent stirs evenly the preparation method comprises the following steps: titanate coupling agent is added in organic solvent,
Then titanium dioxide carrying silver antimicrobials are added to be stirred, modified 2h under conditions of 50 DEG C of temperature, 380r/min revolving speed；It takes out
Modified antibacterial agent is prepared after filter, washing, drying；
(2) aluminium hydroxide and antimony oxide are prepared into solution according to certain mass ratio, is then added vacuum drying mesoporous two
Composite flame-retardant agent is prepared in silica；
The composite flame-retardant agent specific is the preparation method comprises the following steps: aluminium hydroxide and antimony oxide are mixed according to the ratio of 3:5 equal
It is even, after addition distilled water is formulated as solution, vacuum drying mesoporous silicon dioxide powder is added, 2h, vacuum are stirred at 75 DEG C
Grinding obtains nanoscale complex antimicrobials in the ball mill after drying；
(3) it after mixing the modified antibacterial agent and the composite flame-retardant agent, is added in paint preparation process, by 1000r/
Flame-proof antibiotic paint is prepared in min high-speed stirred.
Claims (4)
1. a kind of flame-proof antibiotic for wooden equipment paints preparation method, it is characterised in that: comprise the steps of:
(1) titanate coupling agent modified titanium dioxide carrying silver antimicrobials are used, modified antibacterial agent is prepared；
(2) aluminium hydroxide and antimony oxide are prepared into solution according to certain mass ratio, is then added vacuum drying mesoporous two
Composite flame-retardant agent is prepared in silica；
(3) it after mixing the modified antibacterial agent and the composite flame-retardant agent, is added in paint preparation process, by high-speed stirring
It mixes and flame-proof antibiotic paint is prepared.
2. painting preparation method for the flame-proof antibiotic of wooden equipment according to claim 1, it is characterised in that: step (1)
The specific of modified antibacterial agent stirs evenly the preparation method comprises the following steps: titanate coupling agent is added in organic solvent, then
Titanium dioxide carrying silver antimicrobials are added to be stirred, modified 1- under conditions of 45-65 DEG C of temperature, 350-400r/min revolving speed
3h；It filters, wash, modified antibacterial agent is prepared after drying.
3. painting preparation method for the flame-proof antibiotic of wooden equipment according to claim 1, it is characterised in that: step (2)
The composite flame-retardant agent specific adds the preparation method comprises the following steps: aluminium hydroxide and antimony oxide are uniformly mixed according to the ratio of 3:5
Enter after distilled water is formulated as solution, vacuum drying mesoporous silicon dioxide powder is added, 1-3h, vacuum are stirred at 65-80 DEG C
Grinding obtains nanoscale complex antimicrobials in the ball mill after drying.
4. painting preparation method for the flame-proof antibiotic of wooden equipment according to claim 1, it is characterised in that: step (3)
The revolving speed of the high-speed stirred is 800 ~ 1200r/min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811524120.6A CN109608924A (en) | 2018-12-13 | 2018-12-13 | A kind of flame-proof antibiotic paint preparation method for wooden equipment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811524120.6A CN109608924A (en) | 2018-12-13 | 2018-12-13 | A kind of flame-proof antibiotic paint preparation method for wooden equipment |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109608924A true CN109608924A (en) | 2019-04-12 |
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ID=66008097
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811524120.6A Pending CN109608924A (en) | 2018-12-13 | 2018-12-13 | A kind of flame-proof antibiotic paint preparation method for wooden equipment |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109608924A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115558252A (en) * | 2022-10-14 | 2023-01-03 | 江西省萍乡市轩品塑胶制品有限公司 | Biodegradable master batch for injection molding knife, fork and spoon and preparation method thereof |
-
2018
- 2018-12-13 CN CN201811524120.6A patent/CN109608924A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115558252A (en) * | 2022-10-14 | 2023-01-03 | 江西省萍乡市轩品塑胶制品有限公司 | Biodegradable master batch for injection molding knife, fork and spoon and preparation method thereof |
| CN115558252B (en) * | 2022-10-14 | 2023-09-19 | 江西轩品新材料有限公司 | Biodegradable injection molding cutter, fork and spoon master batch and preparation method thereof |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20190412 |