CN104277579A - Waterproof low-odor environment-friendly printing ink and preparation method thereof - Google Patents

Waterproof low-odor environment-friendly printing ink and preparation method thereof Download PDF

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Publication number
CN104277579A
CN104277579A CN201410630454.7A CN201410630454A CN104277579A CN 104277579 A CN104277579 A CN 104277579A CN 201410630454 A CN201410630454 A CN 201410630454A CN 104277579 A CN104277579 A CN 104277579A
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parts
printing ink
water
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minute
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CN201410630454.7A
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CN104277579B (en
Inventor
朱江玲
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Shantou Shun Rong Printing Technology Co., Ltd.
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HEFEI WANWEI ELECTRICAL EQUIPMENT ENGINEERING Co Ltd
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/02—Printing inks
    • C09D11/10—Printing inks based on artificial resins
    • C09D11/106—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C09D11/107—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds from unsaturated acids or derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/02—Printing inks
    • C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/02—Printing inks
    • C09D11/10—Printing inks based on artificial resins
    • C09D11/106—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/02—Printing inks
    • C09D11/14—Printing inks based on carbohydrates
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Inks, Pencil-Leads, Or Crayons (AREA)

Abstract

The invention discloses waterproof low-odor environment-friendly printing ink which is characterized by being prepared from the following raw materials in parts by weight: 20-25 parts of water-soluble acrylic resin, 7-9 parts of isopropyl lanolate, 12-15 parts of tributyl phosphate, 10-12 parts of decabromodiphenyl ether, 3-6 parts of polyvinyl alcohol, 1.2-3.5 parts of cellulose acetate butyrate, 4-7 parts of calamus oil, 2-4 parts of quartz sand, 3-5 parts of oxidized starch, 0.4-0.8 part of magnesium hydroxide, 0.3-0.7 part of magnesium silicate, 0.2-0.5 part of sodium diacetate, 0.1-0.3 part of polyphenylmethylsiloxane, 4-6 parts of organic pigment, 5-7 parts of an additive and a proper amount of water. The waterproof low-odor environment-friendly printing ink is reasonable in formula, simple in process and relatively excellent in property and has the advantages of small fineness, water resistance, rapid drying, corrosion resistance and the like, a product printed by using the ink disclosed by the invention is not only not gelatinized, but also rapid to dry after being soaked in water, and is also high in glossiness and low in odor after being soaked in glue, and the waterproof low-odor environment-friendly printing ink is energy-saving and environment-friendly and wide in application prospect.

Description

Low odor profiles environmental printing ink of a kind of waterproof and preparation method thereof
Technical field
The present invention relates to printing material technical field, be specifically related to low odor profiles environmental printing ink of a kind of waterproof and preparation method thereof.
Background technology
Ink is the material for the formation of graph text information in printing process, by chromoplastid (as pigment, dyestuff etc.), low-melting ink vehicle, fill out the uniform mixture with the pulpous state adherent of certain degree of mobilization that the materials such as (filling) expects, additional material form, can print, and dry in printed body.Therefore ink should have chromatic colour, good printing adaptability, suitable rate of drying.In addition, the application indexes of the aspects such as certain solvent resistant, acid, alkali, water, light, heat, wear-resisting, fungus and mildew resistance should also be had.Along with printing, paper and other requirement etc. are more and more higher, the printing-ink that prior art is produced cannot meet the demand of Printing industry and goods completely.
For overcoming the deficiencies in the prior art, be necessary to be improved existing printing-ink production technology, thus produce the printing-ink with functions such as cost is low, function diversification, high temperature resistant, hardness is high, wear-resisting, chemically burn into rate of drying is fast, printing adaptability is good.
Summary of the invention
Object of the present invention is just to provide low odor profiles environmental printing ink of a kind of waterproof and preparation method thereof, to overcome the deficiencies in the prior art.
The object of the present invention is achieved like this:
The low odor profiles environmental printing ink of a kind of waterproof, it is characterized in that, be made up of the raw material of following weight part: water soluble acrylic resin 20-25, lanolin fatty acid isopropyl ester 7-9, tributyl phosphate 12-15, decabromodiphynly oxide 10-12, polyvinyl alcohol 3-6, cellulose acetate butyrate 1.2-3.5, oil of Rhizoma Acori Graminei 4-7, quartz sand 2-4, Sumstar 190 3-5, magnesium hydroxide 0.4-0.8, Magnesium Silicate q-agent 0.3-0.7, sodium Diacetate 0.2-0.5, PSI 0.1-0.3, pigment dyestuff 4-6, auxiliary agent 5-7, suitable quantity of water.
Described auxiliary agent is made up of following raw materials in part by weight: organobentonite 4-7, hollow glass micro-ball 1-2, Rutile type Titanium Dioxide 1-3, white vaseline 3-5, Propenoic acid, 2-methyl, isobutyl ester 6-9, polymethacrylate 6-8, butanethiol tin 0.2-0.5, stannous sulfate 0.3-0.6, triethyl aluminum 2-3, red drying oil 1-4, dimethyl silicone oil 3-5, Oleum Verniciae fordii 2.1-3.5, ethylene glycol 4-6, Vltra tears 0.4-0.8, its preparation method first the hydrochloric acid soln of organobentonite 5-10% is soaked 5-7 hour, deionized water wash 4-5 time, 5-6 hour is soaked again with the sodium hydroxide solution of 6-11%, deionization washing is for several times to being neutrality, dry, secondly Propenoic acid, 2-methyl, isobutyl ester is added in organobentonite after the treatment, ethylene glycol, red drying oil, dimethyl silicone oil, stannous sulfate heated and stirred 2-3 hour, oven dry grinds to form ultra-fine micropowder, finally add other remaining component ultrasonic grindings again 30-40 minute and get final product.
The preparation method of the low odor profiles environmental printing ink of described a kind of waterproof, is characterized in that comprising the following steps:
(1) polyvinyl alcohol being added hot water stirs to dissolving completely, adding Sumstar 190, sodium Diacetate, oil of Rhizoma Acori Graminei ultrasonic grinding 30-40 minute, spraying dry;
(2) quartz sand is put into calcining furnace and process 40-50 minute at 630-770 DEG C, cooling adds magnesium hydroxide, Magnesium Silicate q-agent, lanolin fatty acid isopropyl ester grinding 30-50 minute;
(3) by tributyl phosphate, decabromodiphynly oxide stirring and evenly mixing, be heated to 76-95 DEG C and add water soluble acrylic resin, cellulose acetate butyrate, PSI stirring 1-2 hour, be cooled to 45-60 DEG C, add step (1), (2) reaction mass and other remaining component agitation grindings 2-3 hour, be dispersed to granularity suction filtration below 30 μm, discharging.
The present invention has following beneficial effect: the present invention fills a prescription reasonable and technique is simple, the performance of the printing-ink each side of preparation is all more excellent, have that fineness is little, water resisting property, fast drying, the advantage such as corrosion-resistant, with the product of ink printing of the present invention not only soak not gelatinization but also fast drying, printing product impregnation after glossiness high, smell is low, energy-conserving and environment-protective, have a extensive future.
Embodiment
The low odor profiles environmental printing ink of described a kind of waterproof, it is characterized in that, be made up of the raw material of following weight part: water soluble acrylic resin 23, lanolin fatty acid isopropyl ester 8, tributyl phosphate 14, decabromodiphynly oxide 11, polyvinyl alcohol 4, cellulose acetate butyrate 2.5, oil of Rhizoma Acori Graminei 6, quartz sand 3, Sumstar 190 5, magnesium hydroxide 0.7, Magnesium Silicate q-agent 0.5, sodium Diacetate 0.3, PSI 0.1, pigment dyestuff 4, auxiliary agent 7, suitable quantity of water.
Described auxiliary agent is made up of following raw materials in part by weight: organobentonite 5, hollow glass micro-ball 1, Rutile type Titanium Dioxide 2, white vaseline 4, Propenoic acid, 2-methyl, isobutyl ester 8, polymethacrylate 7, butanethiol tin 0.4, stannous sulfate 0.3, triethyl aluminum 2, red drying oil 1, dimethyl silicone oil 3, Oleum Verniciae fordii 2.8, ethylene glycol 4, Vltra tears 0.7, its preparation method first the hydrochloric acid soln of organobentonite 5-10% is soaked 5-7 hour, deionized water wash 4-5 time, 5-6 hour is soaked again with the sodium hydroxide solution of 6-11%, deionization washing is for several times to being neutrality, dry, secondly Propenoic acid, 2-methyl, isobutyl ester is added in organobentonite after the treatment, ethylene glycol, red drying oil, dimethyl silicone oil, stannous sulfate heated and stirred 2-3 hour, oven dry grinds to form ultra-fine micropowder, finally add other remaining component ultrasonic grindings again 30-40 minute and get final product.
Making method comprises the following steps:
(1) polyvinyl alcohol being added hot water stirs to dissolving completely, adding Sumstar 190, sodium Diacetate, oil of Rhizoma Acori Graminei ultrasonic grinding 30-40 minute, spraying dry;
(2) quartz sand is put into calcining furnace and process 40-50 minute at 630-770 DEG C, cooling adds magnesium hydroxide, Magnesium Silicate q-agent, lanolin fatty acid isopropyl ester grinding 30-50 minute;
(3) by tributyl phosphate, decabromodiphynly oxide stirring and evenly mixing, be heated to 76-95 DEG C and add water soluble acrylic resin, cellulose acetate butyrate, PSI stirring 1-2 hour, be cooled to 45-60 DEG C, add step (1), (2) reaction mass and other remaining component agitation grindings 2-3 hour, be dispersed to granularity suction filtration below 30 μm, discharging.
The technical parameter index of the printing-ink using the present invention to produce is as follows:
(1) wear-resisting, use cross-hatching ox-hide tape stripping, draw compartment apart from 1mm, 100% attachment;
(2) viscosity (S): 35;
(3) gloss (%) (60 DEG C): 81;
(4) first dryness (mm): 34;
(5) water tolerance is good, uses the cotton balls being soaked with salt solution, and 300 grams of pressure wipings 50 times, are as good as shape.

Claims (2)

1. the low odor profiles environmental printing ink of waterproof, it is characterized in that, be made up of the raw material of following weight part: water soluble acrylic resin 20-25, lanolin fatty acid isopropyl ester 7-9, tributyl phosphate 12-15, decabromodiphynly oxide 10-12, polyvinyl alcohol 3-6, cellulose acetate butyrate 1.2-3.5, oil of Rhizoma Acori Graminei 4-7, quartz sand 2-4, Sumstar 190 3-5, magnesium hydroxide 0.4-0.8, Magnesium Silicate q-agent 0.3-0.7, sodium Diacetate 0.2-0.5, PSI 0.1-0.3, pigment dyestuff 4-6, auxiliary agent 5-7, suitable quantity of water, described auxiliary agent is made up of following raw materials in part by weight: organobentonite 4-7, hollow glass micro-ball 1-2, Rutile type Titanium Dioxide 1-3, white vaseline 3-5, Propenoic acid, 2-methyl, isobutyl ester 6-9, polymethacrylate 6-8, butanethiol tin 0.2-0.5, stannous sulfate 0.3-0.6, triethyl aluminum 2-3, red drying oil 1-4, dimethyl silicone oil 3-5, Oleum Verniciae fordii 2.1-3.5, ethylene glycol 4-6, Vltra tears 0.4-0.8, its preparation method first the hydrochloric acid soln of organobentonite 5-10% is soaked 5-7 hour, deionized water wash 4-5 time, 5-6 hour is soaked again with the sodium hydroxide solution of 6-11%, deionization washing is for several times to being neutrality, dry, secondly Propenoic acid, 2-methyl, isobutyl ester is added in organobentonite after the treatment, ethylene glycol, red drying oil, dimethyl silicone oil, stannous sulfate heated and stirred 2-3 hour, oven dry grinds to form ultra-fine micropowder, finally add other remaining component ultrasonic grindings again 30-40 minute and get final product.
2. the making method of the low odor profiles environmental printing ink of a kind of waterproof according to claim 1, is characterized in that comprising the following steps:
(1) polyvinyl alcohol being added hot water stirs to dissolving completely, adding Sumstar 190, sodium Diacetate, oil of Rhizoma Acori Graminei ultrasonic grinding 30-40 minute, spraying dry;
(2) quartz sand is put into calcining furnace and process 40-50 minute at 630-770 DEG C, cooling adds magnesium hydroxide, Magnesium Silicate q-agent, lanolin fatty acid isopropyl ester grinding 30-50 minute;
(3) by tributyl phosphate, decabromodiphynly oxide stirring and evenly mixing, be heated to 76-95 DEG C and add water soluble acrylic resin, cellulose acetate butyrate, PSI stirring 1-2 hour, be cooled to 45-60 DEG C, add step (1), (2) reaction mass and other remaining component agitation grindings 2-3 hour, be dispersed to granularity suction filtration below 30 μm, discharging.
CN201410630454.7A 2014-11-11 2014-11-11 The low smell environmental printing of a kind of waterproof ink and preparation method thereof Active CN104277579B (en)

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104610807A (en) * 2015-01-15 2015-05-13 长兴艾飞特塑料科技有限公司 Water-based ink compounded by modified nano sepiolite and water-based acrylic resin and preparation method of water-based ink
CN104761949A (en) * 2015-03-26 2015-07-08 安徽雅美油墨有限公司 Antioxidation durably-bright environment-friendly water-based ink
CN105315765A (en) * 2015-11-16 2016-02-10 贾崇丰 Printing ink and preparation method thereof
CN106011977A (en) * 2016-06-30 2016-10-12 九牧厨卫股份有限公司 Method for forming punctate pattern on surface of metal
CN109021685A (en) * 2018-09-21 2018-12-18 楼乐超 A kind of hydrophobicity fixation ink and its preparation process
CN110117437A (en) * 2018-02-06 2019-08-13 陕西奥华油墨科技有限公司 The molten high temperature surface printing series ink of BC830 alcohol ester

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0351328A1 (en) * 1988-07-11 1990-01-17 Eastman Kodak Company Curable ink compositions
JP2004323798A (en) * 2003-04-28 2004-11-18 Canon Finetech Inc Water-based ink for inkjet printer
CN1916091A (en) * 2006-09-06 2007-02-21 深圳市永仁包装印刷材料有限公司 Water-soluble gold and silver inks, and preparation method
CN103627247A (en) * 2013-12-11 2014-03-12 苏州谊恒印务有限公司 Alcohol-soluble lithographic ink

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0351328A1 (en) * 1988-07-11 1990-01-17 Eastman Kodak Company Curable ink compositions
JP2004323798A (en) * 2003-04-28 2004-11-18 Canon Finetech Inc Water-based ink for inkjet printer
CN1916091A (en) * 2006-09-06 2007-02-21 深圳市永仁包装印刷材料有限公司 Water-soluble gold and silver inks, and preparation method
CN103627247A (en) * 2013-12-11 2014-03-12 苏州谊恒印务有限公司 Alcohol-soluble lithographic ink

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104610807A (en) * 2015-01-15 2015-05-13 长兴艾飞特塑料科技有限公司 Water-based ink compounded by modified nano sepiolite and water-based acrylic resin and preparation method of water-based ink
CN104761949A (en) * 2015-03-26 2015-07-08 安徽雅美油墨有限公司 Antioxidation durably-bright environment-friendly water-based ink
CN105315765A (en) * 2015-11-16 2016-02-10 贾崇丰 Printing ink and preparation method thereof
CN105315765B (en) * 2015-11-16 2020-11-13 贾崇丰 Printing ink
CN106011977A (en) * 2016-06-30 2016-10-12 九牧厨卫股份有限公司 Method for forming punctate pattern on surface of metal
CN106011977B (en) * 2016-06-30 2018-07-17 九牧厨卫股份有限公司 A kind of method that metal surface forms dot pattern
CN110117437A (en) * 2018-02-06 2019-08-13 陕西奥华油墨科技有限公司 The molten high temperature surface printing series ink of BC830 alcohol ester
CN109021685A (en) * 2018-09-21 2018-12-18 楼乐超 A kind of hydrophobicity fixation ink and its preparation process

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Inventor after: Zeng Dongsheng

Inventor before: Zhu Jiangling

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Effective date of registration: 20170425

Address after: 515000 Guangdong, Shantou District, north of the Yangtze River Road, Longhu

Patentee after: Shantou Shun Rong Printing Technology Co., Ltd.

Address before: 230001 Anhui City, Hefei Province, Tunxi Road, No. 193, No. 3 Ningguo Road, building Electronics

Patentee before: HEFEI WANWEI ELECTRICAL EQUIPMENT ENGINEERING CO., LTD.

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