CN104277586A - High-temperature-resistant anti-corrosion printing ink and preparation method thereof - Google Patents
High-temperature-resistant anti-corrosion printing ink and preparation method thereof Download PDFInfo
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- CN104277586A CN104277586A CN201410630386.4A CN201410630386A CN104277586A CN 104277586 A CN104277586 A CN 104277586A CN 201410630386 A CN201410630386 A CN 201410630386A CN 104277586 A CN104277586 A CN 104277586A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/106—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
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- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses a high-temperature-resistant anti-corrosion printing ink. The high-temperature-resistant anti-corrosion printing ink is characterized by being prepared from the following raw materials in parts by weight: 27-30 parts of EVA resin, 2-4 parts of glycol monostearate, 7-10 parts of ethyl acetate 12-14 parts of carbon tetrachloride, 1-3 parts of zinc oxide, 2-3 parts of high-purity beryllium oxide powder, 1-2 parts of vermiculite, 2-3 parts of polytetrafluoroethylene micropowder, 1.2-3 parts of asphalt, 3-4 parts of wheat gluten flour, 0.5-0.9 part of zinc naphthenate, 4-6 parts of corn oil, 2.1-4.3 parts of cane sugar, 3-5 parts of organic pigment, 5-7 parts of auxiliaries and a proper amount of water. The high temperature-resistant anti-corrosion printing ink is simple to prepare and simple and convenient to operate; such components as asphalt and zinc naphthenate are added so that various performance indexes of the printing ink are improved; the obtained printing ink has the advantages of high temperature resistance, anti-corrosion, high drying speed and the like; patterns printed by use of the printing ink are clear, smooth and secure, and also resistant to a high temperature like 1000 DEG C without discoloring.
Description
Technical field
The present invention relates to printing material technical field, be specifically related to a kind of fire resistant anticorrosive printing-ink and preparation method thereof.
Background technology
Ink is the material for the formation of graph text information in printing process, by chromoplastid (as pigment, dyestuff etc.), low-melting ink vehicle, fill out the uniform mixture with the pulpous state adherent of certain degree of mobilization that the materials such as (filling) expects, additional material form, can print, and dry in printed body.Therefore ink should have chromatic colour, good printing adaptability, suitable rate of drying.In addition, the application indexes of the aspects such as certain solvent resistant, acid, alkali, water, light, heat, wear-resisting, fungus and mildew resistance should also be had.Along with printing, paper and other requirement etc. are more and more higher, the printing-ink that prior art is produced cannot meet the demand of Printing industry and goods completely.
For overcoming the deficiencies in the prior art, be necessary to be improved existing printing-ink production technology, thus produce the printing-ink with functions such as cost is low, function diversification, high temperature resistant, hardness is high, wear-resisting, chemically burn into rate of drying is fast, printing adaptability is good.
Summary of the invention
Object of the present invention is just to provide a kind of fire resistant anticorrosive printing-ink and preparation method thereof, to overcome the deficiencies in the prior art.
The object of the present invention is achieved like this:
A kind of fire resistant anticorrosive printing-ink, it is characterized in that, be made up of the raw material of following weight part: EVA resin 27-30, ethylene glycol monostearate 2-4, ethyl acetate 7-10, tetracol phenixin 12-14, zinc oxide 1-3, high-purity beryllium oxide powder 2-3, vermiculite 1-2, ptfe micropowder 2-3, pitch 1.2-3.2, wheat flour strength flour 3-4, zinc naphthenate 0.5-0.9, Semen Maydis oil 4-6, sucrose 2.1-4.3, pigment dyestuff 3-5, auxiliary agent 5-7, suitable quantity of water.
Described auxiliary agent is made up of following raw materials in part by weight: organobentonite 4-7, hollow glass micro-ball 1-2, Rutile type Titanium Dioxide 1-3, white vaseline 3-5, Propenoic acid, 2-methyl, isobutyl ester 6-9, polymethacrylate 6-8, butanethiol tin 0.2-0.5, stannous sulfate 0.3-0.6, triethyl aluminum 2-3, red drying oil 1-4, dimethyl silicone oil 3-5, Oleum Verniciae fordii 2.1-3.5, ethylene glycol 4-6, Vltra tears 0.4-0.8, its preparation method first the hydrochloric acid soln of organobentonite 5-10% is soaked 5-7 hour, deionized water wash 4-5 time, 5-6 hour is soaked again with the sodium hydroxide solution of 6-11%, deionization washing is for several times to being neutrality, dry, secondly Propenoic acid, 2-methyl, isobutyl ester is added in organobentonite after the treatment, ethylene glycol, red drying oil, dimethyl silicone oil, stannous sulfate heated and stirred 2-3 hour, oven dry grinds to form ultra-fine micropowder, finally add other remaining component ultrasonic grindings again 30-40 minute and get final product.
The preparation method of described a kind of fire resistant anticorrosive printing-ink, is characterized in that comprising the following steps:
(1) sucrose is added water to be stirred to dissolve completely, add wheat flour strength flour heated and stirred to boiling, add high-purity beryllium oxide powder ultrasonic grinding 30-40 minute, spraying dry;
(2) vermiculite is put into calcining furnace and process 40-50 minute at 630-770 DEG C, add ptfe micropowder, pitch, zinc oxide grinding 30-50 minute while hot;
(3) by ethyl acetate, tetracol phenixin stirring and evenly mixing, be heated to 70-95 DEG C and add EVA resin, ethylene glycol monostearate, zinc naphthenate stirring 1-2 hour, be cooled to 45-60 DEG C, add step (1), (2) reaction mass and other remaining component agitation grindings 2-3 hour, be dispersed to granularity suction filtration below 30 μm, discharging.
The present invention has following beneficial effect: the present invention prepares simple, easy and simple to handle, add the composition such as pitch, zinc naphthenate, improve the property indices of printing-ink, the printing-ink utilizing the present invention to obtain has the advantages such as fire resistant anticorrosive, wear-resisting, rate of drying is fast, the pattern using the present invention to print off is not only clear, smooth, firm, and the high temperature nondiscoloration of ability 1000 DEG C.
Embodiment
Described a kind of fire resistant anticorrosive printing-ink, it is characterized in that, be made up of the raw material of following weight part: EVA resin 28, ethylene glycol monostearate 3, ethyl acetate 7, tetracol phenixin 13, zinc oxide 3, high-purity beryllium oxide powder 2, vermiculite 2, ptfe micropowder 3, pitch 3.2, wheat flour strength flour 4, zinc naphthenate 0.7, Semen Maydis oil 4, sucrose 2.7, pigment dyestuff 5, auxiliary agent 7, suitable quantity of water.
Described auxiliary agent is made up of following raw materials in part by weight: organobentonite 5, hollow glass micro-ball 1, Rutile type Titanium Dioxide 2, white vaseline 4, Propenoic acid, 2-methyl, isobutyl ester 8, polymethacrylate 7, butanethiol tin 0.4, stannous sulfate 0.3, triethyl aluminum 2, red drying oil 1, dimethyl silicone oil 3, Oleum Verniciae fordii 2.8, ethylene glycol 4, Vltra tears 0.7, its preparation method first the hydrochloric acid soln of organobentonite 5-10% is soaked 5-7 hour, deionized water wash 4-5 time, 5-6 hour is soaked again with the sodium hydroxide solution of 6-11%, deionization washing is for several times to being neutrality, dry, secondly Propenoic acid, 2-methyl, isobutyl ester is added in organobentonite after the treatment, ethylene glycol, red drying oil, dimethyl silicone oil, stannous sulfate heated and stirred 2-3 hour, oven dry grinds to form ultra-fine micropowder, finally add other remaining component ultrasonic grindings again 30-40 minute and get final product.
Making method comprises the following steps:
(1) sucrose is added water to be stirred to dissolve completely, add wheat flour strength flour heated and stirred to boiling, add high-purity beryllium oxide powder ultrasonic grinding 30-40 minute, spraying dry;
(2) vermiculite is put into calcining furnace and process 40-50 minute at 630-770 DEG C, add ptfe micropowder, pitch, zinc oxide grinding 30-50 minute while hot;
(3) by ethyl acetate, tetracol phenixin stirring and evenly mixing, be heated to 70-95 DEG C and add EVA resin, ethylene glycol monostearate, zinc naphthenate stirring 1-2 hour, be cooled to 45-60 DEG C, add step (1), (2) reaction mass and other remaining component agitation grindings 2-3 hour, be dispersed to granularity suction filtration below 30 μm, discharging.
The technical parameter index of the printing-ink using the present invention to produce is as follows:
(1) wear-resisting, use cross-hatching ox-hide tape stripping, draw compartment apart from 1mm, 99.6% attachment;
(2) viscosity (S): 53.7;
(3) gloss (%) (60 DEG C): 89.9;
(4) first dryness (mm): 31.
Claims (2)
1. a fire resistant anticorrosive printing-ink, it is characterized in that, be made up of the raw material of following weight part: EVA resin 27-30, ethylene glycol monostearate 2-4, ethyl acetate 7-10, tetracol phenixin 12-14, zinc oxide 1-3, high-purity beryllium oxide powder 2-3, vermiculite 1-2, ptfe micropowder 2-3, pitch 1.2-3.2, wheat flour strength flour 3-4, zinc naphthenate 0.5-0.9, Semen Maydis oil 4-6, sucrose 2.1-4.3, pigment dyestuff 3-5, auxiliary agent 5-7, suitable quantity of water, described auxiliary agent is made up of following raw materials in part by weight: organobentonite 4-7, hollow glass micro-ball 1-2, Rutile type Titanium Dioxide 1-3, white vaseline 3-5, Propenoic acid, 2-methyl, isobutyl ester 6-9, polymethacrylate 6-8, butanethiol tin 0.2-0.5, stannous sulfate 0.3-0.6, triethyl aluminum 2-3, red drying oil 1-4, dimethyl silicone oil 3-5, Oleum Verniciae fordii 2.1-3.5, ethylene glycol 4-6, Vltra tears 0.4-0.8, its preparation method first the hydrochloric acid soln of organobentonite 5-10% is soaked 5-7 hour, deionized water wash 4-5 time, 5-6 hour is soaked again with the sodium hydroxide solution of 6-11%, deionization washing is for several times to being neutrality, dry, secondly Propenoic acid, 2-methyl, isobutyl ester is added in organobentonite after the treatment, ethylene glycol, red drying oil, dimethyl silicone oil, stannous sulfate heated and stirred 2-3 hour, oven dry grinds to form ultra-fine micropowder, finally add other remaining component ultrasonic grindings again 30-40 minute and get final product.
2. the making method of a kind of fire resistant anticorrosive printing-ink according to claim 1, is characterized in that comprising the following steps:
(1) sucrose is added water to be stirred to dissolve completely, add wheat flour strength flour heated and stirred to boiling, add high-purity beryllium oxide powder ultrasonic grinding 30-40 minute, spraying dry;
(2) vermiculite is put into calcining furnace and process 40-50 minute at 630-770 DEG C, add ptfe micropowder, pitch, zinc oxide grinding 30-50 minute while hot;
(3) by ethyl acetate, tetracol phenixin stirring and evenly mixing, be heated to 70-95 DEG C and add EVA resin, ethylene glycol monostearate, zinc naphthenate stirring 1-2 hour, be cooled to 45-60 DEG C, add step (1), (2) reaction mass and other remaining component agitation grindings 2-3 hour, be dispersed to granularity suction filtration below 30 μm, discharging.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410630386.4A CN104277586A (en) | 2014-11-11 | 2014-11-11 | High-temperature-resistant anti-corrosion printing ink and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410630386.4A CN104277586A (en) | 2014-11-11 | 2014-11-11 | High-temperature-resistant anti-corrosion printing ink and preparation method thereof |
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| Publication Number | Publication Date |
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| CN104277586A true CN104277586A (en) | 2015-01-14 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201410630386.4A Pending CN104277586A (en) | 2014-11-11 | 2014-11-11 | High-temperature-resistant anti-corrosion printing ink and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113797803A (en) * | 2021-09-23 | 2021-12-17 | 深圳宝峰印刷有限公司 | Environment-friendly printing ink not prone to oxidative discoloration, and preparation method and device thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS63248878A (en) * | 1987-04-01 | 1988-10-17 | Seiko Epson Corp | Heat transfer ink |
| US7169219B1 (en) * | 2002-03-06 | 2007-01-30 | Wynne John H | Peelable stenciling ink and method of using |
| CN102604477A (en) * | 2012-03-25 | 2012-07-25 | 重庆宏图油墨有限公司 | Benzene-free environmentally friendly composite ink and preparation method thereof |
| CN103265840A (en) * | 2013-05-31 | 2013-08-28 | 苏州凹凸彩印厂 | Bright red gravure printing ink and preparation method thereof |
| CN103881475A (en) * | 2014-04-08 | 2014-06-25 | 董奇爱 | Printing ink |
-
2014
- 2014-11-11 CN CN201410630386.4A patent/CN104277586A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS63248878A (en) * | 1987-04-01 | 1988-10-17 | Seiko Epson Corp | Heat transfer ink |
| US7169219B1 (en) * | 2002-03-06 | 2007-01-30 | Wynne John H | Peelable stenciling ink and method of using |
| CN102604477A (en) * | 2012-03-25 | 2012-07-25 | 重庆宏图油墨有限公司 | Benzene-free environmentally friendly composite ink and preparation method thereof |
| CN103265840A (en) * | 2013-05-31 | 2013-08-28 | 苏州凹凸彩印厂 | Bright red gravure printing ink and preparation method thereof |
| CN103881475A (en) * | 2014-04-08 | 2014-06-25 | 董奇爱 | Printing ink |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113797803A (en) * | 2021-09-23 | 2021-12-17 | 深圳宝峰印刷有限公司 | Environment-friendly printing ink not prone to oxidative discoloration, and preparation method and device thereof |
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Application publication date: 20150114 |
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