CN109608284A - A kind of preparation and application of the humic acid complex fertilizer containing active microorganism - Google Patents
A kind of preparation and application of the humic acid complex fertilizer containing active microorganism Download PDFInfo
- Publication number
- CN109608284A CN109608284A CN201811622987.5A CN201811622987A CN109608284A CN 109608284 A CN109608284 A CN 109608284A CN 201811622987 A CN201811622987 A CN 201811622987A CN 109608284 A CN109608284 A CN 109608284A
- Authority
- CN
- China
- Prior art keywords
- humic acid
- parts
- preparation
- fertilizer
- containing active
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B1/00—Superphosphates, i.e. fertilisers produced by reacting rock or bone phosphates with sulfuric or phosphoric acid in such amounts and concentrations as to yield solid products directly
- C05B1/02—Superphosphates
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pest Control & Pesticides (AREA)
- Soil Sciences (AREA)
- Fertilizers (AREA)
Abstract
The invention discloses the preparations and application of a kind of humic acid complex fertilizer containing active microorganism, preparation method, it includes the following steps: step 1, the pretreatment of raw material；Step 2, the preparation of humic acid urea；Step 3, the preparation of functional microorganism bacterium powder；Step 4, fertilizer inorganic compounding compounds；Step 5, the preparation of the humic acid complex fertilizer containing active microorganism.The humic acid complex fertilizer containing active microorganism of preparation is applied in prophyiaxis and promoting growth, improvement soil biological fertilizer.Fertilizer of the invention integrates organic and inorganic, biological fertility, while improveing soil, nutrient needed for balanced crop, stimulate plant growth, enhancing crop degeneration-resistant, the application of such fertilizer can effectively reduce chemical fertilizer and applications of pesticide amount, the effect of reaching upgrading volume increase simultaneously belong to green, ecological new function fertilizer.
Description
Technical field
The present invention relates to the preparation of microbial manure field more particularly to a kind of humic acid complex fertilizer containing active microorganism and
Using.
Background technique
Humic acid is animals and plants remains, wherein the remains of mainly plant, by the decomposition and conversion of microorganism and ground
A series of processes of Geochemistry and a kind of organic substance for being formed and being accumulated.Humic acid organic nutrition element mainly include C,
H, O, N, S, humic acid have complexing, chelating and adsorption ability, can be reduced the loss of ammonium nitrogen；Increase phosphorus to move in the soil
Dynamic distance inhibits soil to water-soluble phosphorus fixation, invalidates phosphorus and be converted into available phosphorus, promotes absorption of the root system to phosphorus；It is yellow rotten
Storage potassium ion can be absorbed in acid, and the content for improving effective potassium is especially particularly evident to the synergy of potash fertilizer.
Humic acid is the basis of microbial growth, while being also the basis of soil fertility, and humic acid and microorganism are total
It is same to constitute the soil environment of plant grew well.Can effectively be activated humic acid using the method for chemical activation can be to for crop
State, wherein fulvic acid is the absorbable optimisation substance form utilized of crop, is based on this, exploitation humic acid containing active microorganism is compound
Fertilizer will play useful effect in terms of increasing crop yield, improving crop quality, enhancing crop anti-adversity, improvement, and be
The development of China's green ecological agricultural escorts, and is of great significance for the green ecological development of modern agriculture.
Summary of the invention
The purpose of the present invention is to solve the shortcomings of the prior art and providing a kind of humic acid complex fertilizer containing active microorganism
Preparation and application, the effective component in humic acid is made full use of, its maximum effect is played.By the humic acid compounding after activation
Different formulations fertilizer and functional microorganism are used for during composite heat transfer, to prepare with prophyiaxis and promoting growth, conditioned soil
The new bio-fertilizer of earth.
In order to achieve the above objectives, the present invention is achieved through the following technical solutions.
A kind of preparation method of the humic acid complex fertilizer containing active microorganism, it includes the following steps:
Step 1, the pretreatment of raw material: it is spare that lignite raw material be crushed into 40-60 mesh, take alkali activator: lignite=
Alkali activator is added to and crushes in lignite by the parts by weight of 3-10:100, is uniformly mixed, and stands 1-3 days, detects water-soluble rotten
Phytic acid content (mass percent) >=2.0%, total humic acid content (mass percent) >=40% complete the pre- place of raw material
Reason, the humic acid activated are spare；
Step 2, the preparation of humic acid urea: weighing 90 parts of urea of parts by weight and be added in 10 parts of water, adds at 120 DEG C
Heat keeps urea in a molten state, and step 1 step 1 that 1.5-2 times of weight of urea part is added after urea melts completely is located in advance
Humic acid after reason, temperature are controlled at 90-100 DEG C, add the potassium carbonate of humic acid parts by weight 2%-5%, are uniformly mixed, instead
Answering 15-20min, measurement pH is that 9-11 can be spare to get humic acid urea；
Step 3, the preparation of functional microorganism bacterium powder: taking microbial bacterial agent fermentation liquid, and bacterial sediment spore is collected after centrifugation
Bacterial sediment spore liquid is uniformly mixed by sub- liquid with absorption carrier 1:3 in mass ratio, at 30-40 DEG C, is dried in vacuo 5min,
Pulvis is made, pulvis mesh number >=80 mesh are spare to get microbial germ powder；
The absorption carrier includes organic absorption carrier and mineral absorption carrier by organic adsorption carrier weighs by weight
7-8 parts, mineral carrier weighs 2-3 parts by weight；
Step 4, fertilizer inorganic compounding compounds: in parts by weight, weighing 1.0-25.0 parts of monoammonium phosphate, ammonium sulfate
1.0-20.0 parts, 1.0-12.0 parts of calcium superphosphate, 1-5 parts of calcium magnesium phosphate, 6-9 parts of Diammonium phosphate (DAP), 13.0-19.0 parts of potassium sulfate,
1.0-6.0 parts of ammonium nitrate, 1.0-10.0 parts of potassium nitrate, 1.0-8.0 parts of potassium chloride, 3-6 parts of filler element powder, microelement 1.0-
5.0 parts, after evenly mixing, obtain inorganic fertilizer formula；
The microelement is borax, zinc sulfate, magnesium sulfate, and quality is than borax, zinc sulfate, magnesium sulfate 1:2:2；
Step 5, the preparation of the humic acid complex fertilizer containing active microorganism: 30-40 parts of humic acid urea, nothing are weighed by weight
59.5-69 parts of machine fertilizer formula, 0.5-1.0 parts of microbial germ powder are uniformly mixed, and can be obtained with disk or rotary drum prilling process production
Microorganism humic acid complex fertilizer.
Further, the humic acid content (mass percent) >=40.0% in the lignite in the step 1.
Further, the activator in the step 1 is sodium hydroxide, potassium hydroxide, potassium carbonate, one in ammonium hydrogen carbonate
Kind or the quality such as a variety of it is compound.
Further, the microorganism in the step 3 is colloid bacillus cereus (Bacillus
Amyloliquefaciens), bacillus subtilis (Bacillus Subtillis), bacillus amyloliquefaciens (Bacillus
The quality such as one of amyloliquefaciens) or a variety of are compound；
The preservation registration number of the colloid bacillus cereus is CGMCC No.15851；The preservation of the bacillus subtilis is stepped on
Mark is CGMCCNo.15847；The preservation registration number of the bacillus amyloliquefaciens is CGMCC No.15848.
Further, the organic adsorption carrier in the step 3 is turf, biomass charcoal powder, rice bran, one in seawood meal
Kind or the quality such as a variety of it is compound, the mineral absorption carrier be concave convex rod, bentonite, diatomite, montmorillonite, in polyacrylamide
The quality such as one or more it is compound.
Further, in the step 2 humic acid urea obtained the content of organic matter >=50%, total humic acid content >=
25%, soluble humic acid >=1.5%.
Further, living bacteria count >=0.2 hundred million in microorganism humic acid complex fertilizer made from the step 5.
A kind of humic acid complex fertilizer containing active microorganism of the preparation method preparation of the humic acid complex fertilizer containing active microorganism,
Application in prophyiaxis and promoting growth, improvement soil biological fertilizer.
Fertilizer of the invention integrates organic and inorganic, biological fertility, while improveing soil, needed for balanced crop
Nutrient, stimulation plant growth, enhancing crop are degeneration-resistant, and the application of such fertilizer can effectively reduce chemical fertilizer and applications of pesticide amount,
The effect of reaching upgrading volume increase simultaneously belong to green, ecological new function fertilizer.
Detailed description of the invention
Fig. 1 is preparation process flow structural schematic diagram of the invention；
Specific embodiment
Below with reference to embodiment, the present invention will be further described, but is not limited to the content on specification.
A kind of preparation method of the humic acid complex fertilizer containing active microorganism, includes the following steps:
Step 1, the pretreatment of raw material: it is spare to crushed 40-60 mesh for lignite raw material, then according to alkali activator:
Alkali activator is added to crush in lignite and be uniformly mixed by lignite=3-10:100 parts by weight, stands 1-3 days, to lignite and
Alkali activator is sufficiently reacted, i.e. detection fulvo acid content up to 2.0% or more, total humic acid content up to 40% or more,
Complete the pretreatment of raw material.
Step 2, the preparation of humic acid urea: weighing 90 parts of urea of parts by weight and be added in 10 parts of aqueous solutions, and heating makes to urinate
Element is in a molten state, and temperature is controlled at 120 DEG C, and it is pre- that 1.5-2 times of weight of urea part step 1 is added after urea melts completely
Treated humic acid, temperature, which is controlled, to be added the potassium carbonate of humic acid parts by weight 2%-5% at 90-100 DEG C and is uniformly mixed,
And the reaction was continued 15-20min, measure pH value.
Step 3, the preparation of functional microorganism bacterium powder: microbial bacterial agent fermentation liquid is chosen, through bacterial sediment is collected after centrifugation
Spore liquid, absorption carrier are made of in proportion organic adsorption carrier and mineral absorption carrier, and organic adsorption carrier claims by weight
7-8 parts are taken, 2-3 parts of mineral carrier, aseptically, bacterial sediment spore liquid and absorption carrier 1:3 in mass ratio are mixed
It closes uniformly and dries 5min at 30-40 DEG C, the pulvis that 80 mesh of granularity or more is made is spare, and above procedure is in sterile room
It completes.
Step 4, fertilizer formula compounds: in parts by weight, the humic acid urea of organic components selecting step 2, inorganic
Fertilizer compounds corresponding formula on demand.Weigh 1.0-25.0 parts of monoammonium phosphate, 1.0-20.0 parts of ammonium sulfate, calcium superphosphate 1.0-
12.0 parts, 1-5 parts of calcium magnesium phosphate, 6-9 parts of Diammonium phosphate (DAP), 13.0-19.0 parts of potassium sulfate, 1.0-6.0 parts of ammonium nitrate, potassium nitrate
1.0-10.0 parts, 1.0-8.0 parts of potassium chloride, 3-6 parts of filler element powder, 1.0-5.0 parts of microelement, after evenly mixing, obtain
Inorganic fertilizer formula.Microelement is borax, zinc sulfate, magnesium sulfate, is weighed by 1:2:2 parts by weight.
Filler element powder can be montmorillonite powder, cross 80 meshes.
Step 5, the preparation of the humic acid complex fertilizer containing active microorganism: accordingly matched using disk or rotary drum prilling process production
Square fertilizer, raw material compounding press humic acid urea 30-40 parts, inorganic fertilizer formula 59.5-69 parts, solid microbial 0.5-1.0
Part.Wherein functional microorganism is added in the form of film coating after the completion of granulation of fertilizer.
In step 1, the lignite raw material is lignite of the total humic acid content 40.0% or more.
Activator described in step 1 includes one or more of sodium hydroxide, potassium hydroxide, potassium carbonate, ammonium hydrogen carbonate.
The pH of humic acid urea is maintained between 9-11 in step 2.
Functional microorganism, which is chosen, in step 3 has diseases prevention, growth promotion, Soluble phosphorus, potassium decomposing, the bacillus of fixed nitrogen function thin
One or more of bacterium carries out compound.Functional microorganism is mentioned by Fermentation Research Center Yunnan Co., Ltd.
For numbering respectively with the colloid bacillus cereus (Bacillus amyloliquefaciens) of Soluble phosphorus potassium decomposing function:
WSWFJ-11, preservation registration number CGMCC No.15851, the bacillus subtilis (Bacillus with growth promotion function
Subtillis), number: WSWFJ-7, preservation registration number CGMCCNo.15847, the Xie Dian with the black sick function of prevention and treatment tobacco two
Afnyloliquefaciens (Bacillus amyloliquefaciens), number: WSWFJ-8, preservation registration number CGMCC
No.15848)。
Organic adsorption carrier described in step 3 is one of turf, biomass charcoal powder, rice bran, seawood meal or several, mine
Object absorption carrier is one of concave convex rod, bentonite, diatomite, montmorillonite, polyacrylamide or several.Vacuum is selected in drying
Drying mode, temperature are controlled at 40-50 DEG C.
The content of organic matter >=50% of humic acid urea in step 4, total humic acid content >=25%, soluble humic acid >=
1.5%.
Living bacteria count >=0.2 hundred million/g of the humic acid complex fertilizer containing active microorganism made of step 5.
Illustrated below with specific embodiment.
A kind of active microorganism humic acid complex fertilizer preparation method of embodiment 1
A kind of preparation method of the humic acid complex fertilizer containing active microorganism, includes the following steps:
Step 1, the activation of humic acid: it is spare to crushed 60 meshes for lignite raw material, then according to sodium hydroxide: lignite=
Alkaline chemical is added to crush in lignite and be uniformly mixed by the parts by weight of 4:100,3 days is stood, to lignite and alkali electroless
Substance sufficiently reacts the pretreatment for completing raw material.
Step 2, the preparation of humic acid urea: weighing 90 parts of urea of parts by weight and being added to 10 parts of heated in water solution makes urea
In a molten state, temperature is controlled at 120 DEG C, and the activation humic acid of 2 times of weight of urea parts is added after urea melts completely,
Temperature control at this time is at 95 DEG C, and the potassium carbonate for adding humic acid parts by weight 3% is uniformly mixed, and the reaction was continued 20min, measurement
PH value.
Step 3, the preparation of functional microorganism bacterium powder: the microbial bacterial agent fermentation liquid with specific function is chosen, through being centrifuged
Bacterial sediment-spore liquid is collected afterwards, and absorption carrier is made of in proportion organic adsorption carrier and mineral absorption carrier, organic adsorption
Carrier weighs 7 parts by weight, 3 parts of mineral carrier, will aseptically be centrifuged spore liquid and absorption carrier in mass ratio
1:3 is uniformly mixed and low temperature drying, and it is spare that pulvis is made.
Step 4, fertilizer formula compounds: in parts by weight, it is on-demand that organic components choose humic acid urea, inorganic fertilizer
Seek the corresponding formula of compounding.Weigh 40 parts of humic acid urea, 25 parts of monoammonium phosphate, 1 part of ammonium sulfate, 1 part of calcium superphosphate, calcium magnesium phosphate
4.0 parts, 9 parts of Diammonium phosphate (DAP), 13 parts of potassium sulfate, 1 part of ammonium nitrate, 1 part of potassium nitrate, 5.0 parts of potassium chloride, 4.2 parts of filler element powder,
1 part of microelement, after evenly mixing, obtain inorganic fertilizer formula.
Step 5, step 4 material the preparation of the humic acid complex fertilizer containing active microorganism: is used into disk or drum granulating work
Skill produces granular fertilizers, and the ratio that the additive amount of solid functional microorganism microbial inoculum accounts for fertilizer quality is 0.7 ‰, and in coating rank
Function bacterium powder is sprayed at fertilizer surface with dusting powders by section, while spraying anticaking agent.The N-P of the fertilizer2O5-K2O=16-
6-8, organic matter >=20%, humic acid >=10%, living bacteria count >=0.2 hundred million.
A kind of active microorganism humic acid complex fertilizer preparation method of embodiment 2
A kind of preparation method of the humic acid complex fertilizer containing active microorganism, includes the following steps:
Step 1, the activation of humic acid: it is spare to crushed 60 meshes for lignite raw material, then according to sodium hydroxide: lignite=
Alkaline chemical is added to crush in lignite and be uniformly mixed by the parts by weight of 3:100,3 days is stood, to lignite and alkali electroless
Substance sufficiently reacts the pretreatment for completing raw material.
Step 2, the preparation of humic acid urea: weighing 90 parts of urea of parts by weight and being added to 10 parts of heated in water solution makes urea
In a molten state, temperature controls the activation corruption plant that 1.5 times of weight of urea parts are added after urea melts completely at 120 DEG C
Acid, temperature control at this time is at 90 DEG C, and the potassium carbonate for adding humic acid parts by weight 2% is uniformly mixed, and the reaction was continued 15min,
Measure pH value.
Step 3, the preparation of functional microorganism bacterium powder: the microbial bacterial agent fermentation liquid with specific function is chosen, through being centrifuged
Bacterial sediment-spore liquid is collected afterwards, and absorption carrier is made of in proportion organic adsorption carrier and mineral absorption carrier, organic adsorption
Carrier weighs 8 parts by weight, 2 parts of mineral carrier, will aseptically be centrifuged spore liquid and absorption carrier in mass ratio
1:3 is uniformly mixed and low temperature drying, and it is spare that pulvis is made.
Step 4, fertilizer formula compounds: in parts by weight, it is on-demand that organic components choose humic acid urea, inorganic fertilizer
Seek the corresponding formula of compounding.Weigh 30 parts of humic acid urea, 1 part of monoammonium phosphate, 20 parts of ammonium sulfate, 12 parts of calcium superphosphate, calcium and magnesium phosphorus
Fertile 1 part, 6 parts of Diammonium phosphate (DAP), 19 parts of potassium sulfate, it is 6 parts of ammonium nitrate, 10 parts of potassium nitrate, 1 part of potassium chloride, 3 parts of filler element powder, micro-
5 parts of secondary element, after evenly mixing, obtain inorganic fertilizer formula.
Step 5, step 4 material the preparation of the humic acid complex fertilizer containing active microorganism: is used into disk or drum granulating work
Skill produces granular fertilizers, and function bacterium powder is sprayed at fertilizer surface with dusting powders in the coating stage, while spraying anti-caking
Block agent.Organic matter >=20% of the fertilizer, humic acid >=10%, living bacteria count >=0.2 hundred million.
A kind of active microorganism humic acid complex fertilizer preparation method of embodiment 3
A kind of preparation method of the humic acid complex fertilizer containing active microorganism, includes the following steps:
Step 1, the activation of humic acid: it is spare to crushed 50 meshes for lignite raw material, then according to sodium hydroxide: lignite=
Alkaline chemical is added to crush in lignite and be uniformly mixed by the parts by weight of 10:100,2 days is stood, to lignite and alkali electroless
Substance sufficiently reacts the pretreatment for completing raw material.
Step 2, the preparation of humic acid urea: weighing 90 parts of urea of parts by weight and being added to 10 parts of heated in water solution makes urea
In a molten state, temperature controls the activation corruption plant that 1.8 times of weight of urea parts are added after urea melts completely at 120 DEG C
Acid, temperature control at this time is at 100 DEG C, and the potassium carbonate for adding humic acid parts by weight 5% is uniformly mixed, and the reaction was continued 18min,
Measure pH value.
Step 3, the preparation of functional microorganism bacterium powder: the microbial bacterial agent fermentation liquid with specific function is chosen, through being centrifuged
Bacterial sediment-spore liquid is collected afterwards, and absorption carrier is made of in proportion organic adsorption carrier and mineral absorption carrier, organic adsorption
Carrier weighs 7.5 parts by weight, 2.5 parts of mineral carrier, aseptically will be centrifuged spore liquid and absorption carrier presses matter
Amount is uniformly mixed than 1:3 and low temperature drying, and it is spare that pulvis is made.
Step 4, fertilizer formula compounds: in parts by weight, it is on-demand that organic components choose humic acid urea, inorganic fertilizer
Seek the corresponding formula of compounding.Weigh 35 parts of humic acid urea, 13 parts of monoammonium phosphate, 10 parts of ammonium sulfate, 6 parts of calcium superphosphate, calcium and magnesium phosphorus
Fertile 3 parts, 7 parts of Diammonium phosphate (DAP), 16 parts of potassium sulfate, it is 4 parts of ammonium nitrate, 6 parts of potassium nitrate, 8 parts of potassium chloride, 6 parts of filler element powder, micro
3 parts of element, after evenly mixing, obtain inorganic fertilizer formula.
Step 5, step 4 material the preparation of the humic acid complex fertilizer containing active microorganism: is used into disk or drum granulating work
Skill produces granular fertilizers, and function bacterium powder is sprayed at fertilizer surface with dusting powders in the coating stage, while spraying anti-caking
Block agent.Organic matter >=20% of the fertilizer, humic acid >=10%, living bacteria count >=0.2 hundred million.
A kind of application effect of the 16-6-8 of humic acid complex fertilizer containing active microorganism of embodiment 4 on cucumber
1. test material and method
1.1 experimental field overviews
Test site: the Songming County street Song Yang rice seedling bed dam is glutinous loam, content of organic matter 39.89g.kg for examination soil-1,
PH5.9, alkaline hydrolysis nitrogen content 203.5mg.kg-1, available phosphorus content 93.47mg.kg-1, quick-acting potassium content 491.68mg.kg-1。
1.2 test material
It is potassium sulfate type biology-organic-inorganic composite fertilizer that Yunnan Yunye Fertilizer Co., Ltd. provides for examination fertilizer
(N-P2O5-K2O content 16-6-8, organic components be our company's oil cake organic fertilizer, organic matter machine matter >=20%, humic acid >=
10%) (the N-P of humic acid complex fertilizer containing active microorganism2O5-K2O content 16-6-8, machine matter >=20%, humic acid >=10% have
Imitate viable count >=0.2 hundred million), functional microorganism composite bacteria agent selects the bacillus amyloliquefaciens and activated soil with growth promotion function
The colloid bacillus cereus of earth nutrient, living bacteria count >=20,000,000,000/g) it is limited by Yunnan Province microbial fermentation engineering research center
Company provides, and is " original flavor 1 " for examination cucumber variety.
1.3 experimental design
Test in 24 to 2017 years Mays in 2017 on September 3, in area be 240m2Heliogreenhouse carry out, test in 2017
Nursery on April 17, transplanting on May 24 were received to August 17th by cell list June 27, and when harvest is 15 plants of cell random searching every
Economical character.Test sets 4 processing, 3 repetitions of each processing.Test sets 2 processing, check plot: in local conventional base manure
On the basis of base apply biology-organic-inorganic composite fertilizer 30kg (N-P2O5-K2O content 16-6-8, organic components are that our company's oil cake has
Machine fertilizer), demonstration area: the local routine base manure+30kg of humic acid complex fertilizer containing active microorganism (N-P2O5-K2O content 16-6-8, machine
Matter >=20%, humic acid >=10%, living bacteria count >=0.2 hundred million), plot area 40m2, local routine base manure application is decomposed
Chicken manure 500kg/667m2+ top dressing 15-5-25 compound fertilizer 50kg/667m2, during which water and fertilizer management measure accomplishes unanimously.
2. result and analysis
Influence of 2.1 different fertilizations to cucumber breeding time
As shown in Table 1: with the growth of cucumber, melon phase demonstration area beginning shifts to an earlier date 1 day compared with check plot, contains the melon phase and shifts to an earlier date
3 days, containing the melon phase shifted to an earlier date 6 days, in general, application containing humic acid complex fertilizer more conventional organic-inorganic composite fertilizer breeding time
In advance.
Influence of 1 different fertilization of table to cucumber breeding time
| Processing | Take out the climing phase/moon day | Melon phase beginning/moon day | Contain the melon phase/moon day | Contain the melon later period/moon |
| Control | 6.2-6.26 | 6.26-7.16 | 7.23-9.18 | 9.18- day 10.4 |
| Demonstration | 6.2-6.26 | 6.26-7.15 | 7.24-9.15 | 9.15-9.28 |
Influence of 2.2 different fertilizations to cucumber economical character
As shown in Table 2: the more conventional composite organic-inorganic fertilizer processing of the processing of application humic acid biological compound fertilizer, strain
High, fruiting number and fruit shape are more excellent, and plant height increases by 0.59%, and stem thickness increases by 1.07%, and female flower number increases by 2.0%, and fruit is long to be increased
9.4%, fruit slightly increases by 3.2%.
Influence of 2 different fertilization of table to cucumber economical character
Influence of 2.3 different fertilizations to cucumber economic benefit and the output value
As shown in Table 3: application humic acid complex fertilizer containing active microorganism is compared with standard biologic organic-inorganic composite fertilizer
Yield enhancing rate is 3.6%.
Influence of 3 different fertilization of table to cucumber economic benefit and the output value
Conclusion: in general, application humic acid complex fertilizer containing active microorganism exists compared with standard biologic organic-inorganic composite fertilizer
There is certain effect in terms of promoting plant growth and yield, yield, the output value can be improved up to 3.6%, illustrate that humic acid has promotion crop
Growth promotes crop yield and the effect of quality, can scale in the production practices of cucumber.
Field information of 5 humic acid complex fertilizer containing active microorganism of embodiment on tobacco
1. place of demonstrating
The own clothing township of exemplary arrangement carries out, and plot soil fertility is medium, and fertility is evenly distributed, and illumination and irrigation condition are good.
2. exemplary materials:
Experimental cultivar: K326
For trying fertilizer are as follows: special base fertilizer for tobacco (N-P2O5-K2O=15-15-18), humic acid complex fertilizer containing active microorganism
(organic matter >=20%, humic acid >=10%, N-P2O5-K2O=15-15-18) dedicated top dressing (the N-P of tobacco2O5-K2O=12.5-
0-33.5)。
3. exemplary design
In Wuding County base Cha Dian, 2000 mu of demonstration area is respectively arranged in unit.Demonstration kind is K326.Base manure is applied in demonstration area
With humic acid complex fertilizer containing active microorganism.Plot in flakes with conventional fertilizer application local around demonstration area is control.
The method of administration of humic acid complex fertilizer containing active microorganism are as follows: application is mixed thoroughly with base manure when transplanting, it is not mixed with fungicide
With.
The fertilizer application mode of own clothing conventional fertilizer application are as follows: apply special base fertilizer for tobacco 30kg, the dedicated top dressing 20kg of tobacco per acre.
4. primary growth stage is recorded
Breeding time progress investigation statistics the results are shown in Table 4.The demonstration group phase than late 2 days of control, demonstrates prosperous as can be seen from the table
8 days are advanced by for a long time, squaring period is advanced by 3 days, and the phase of binding is advanced by 2 days, and just the roasting phase is advanced by 2 days, and entire breeding time shifts to an earlier date
6 days.
4 breeding time of table progress investigation statistics table
5. field growing way appearance is investigated
Field growing way appearance investigation statistics the results are shown in Table 5.It demonstrated as can be seen from the table in plant type, leaf color, master pulse thickness, moved
After cultivation 25d and 50d growth potential with compare no significant difference, demonstration 75 days growing ways, Mature properties etc. after plant uniformity, transplanting
Aspect is better than compareing.
The investigation of 5 field growing way appearance of table
6. prosperous growth phase economical character
Prosperous growth phase economical character statistical result is shown in Table 6.Demonstration and to impinging upon prosperous growth phase economical character as can be seen from the table
It has nothing in common with each other.Stem girth, the single plant number of sheets, upper leaf maximum leaf area are all that demonstration behaves oneself best；Plant height, middle leaf maximum leaf area
It puts up the best performance for the cigarette strain of control.
6 prosperous growth phase of table economical character statistical form
7. bind phase economical character
The phase economical character statistical result that binds is shown in Table 7.Demonstration and to impinging upon the phase economical character that binds as can be seen from the table
It has nothing in common with each other.Plant height, stem girth, pitch are all that control behaves oneself best；The number of blade, middle and upper part leaf maximum leaf area are the cigarette strain of demonstration
It puts up the best performance.
Table 7 binds phase economical character statistical form
8. disease a situation arises investigation
Disease a situation arises investigation result is by being shown in Table 8.The ground mainly has climacteric spot disease, root black as can be seen from the table
Maize ear rot, tomato spotted wilt, mosaic disease occur.The disease incidence of demonstration is far below control.
8 disease of table a situation arises investigation statistics table
| Processing | Climacteric spot disease | Root black rot | Tomato spotted wilt | Mosaic disease |
| Demonstration | 0.98% | 0.78% | 0.20% | 5.70% |
| Control | 4.72% | 1.40% | 2.80% | 18.80% |
9. economic characters
The statistical result of economic characters is shown in Table 9.As can be seen from the table, the per mu yield of demonstration area, per mu yield value, average price, on
Equal cigarettes ratio and better-than-average cigarette ratio improve 1.83%, 10.38%, 8.41%, 2.58% and 3.08% than control respectively.
9 economic characters statistical form of table
In summary: humic acid complex fertilizer containing active microorganism increases production compared with common fertilizer with upgrading, prevents and treats pest and disease damage
Biological and ecological methods to prevent plant disease, pests, and erosion effect is suitable for tobacco planting.
Obviously, above embodiment of the invention be only to clearly illustrate example of the present invention, and not be
Restriction to embodiments of the present invention.For those of ordinary skill in the art, on the basis of the above description also
It can make other variations or changes in different ways.Here all embodiments can not be exhaustive.It is all to belong to this
The obvious changes or variations that the technical solution of invention is extended out are still in the scope of protection of the present invention.
Claims (8)
1. a kind of preparation method of humic acid complex fertilizer containing active microorganism, it is characterised in that: it includes the following steps:
Step 1, the pretreatment of raw material: it is spare that lignite raw material be crushed into 40-60 mesh, take alkali activator: lignite=3-10:
Alkali activator is added to and crushes in lignite by 100 parts by weight, is uniformly mixed, and stands 1-3 days, detects fulvo acid
Content (mass percent) >=2.0%, total humic acid content (mass percent) >=40% are completed the pretreatment of raw material, are obtained
It is spare to the humic acid of activation；
Step 2, the preparation of humic acid urea: 90 parts of urea of parts by weight are weighed and are added in 10 parts of water, heats, makes at 120 DEG C
Urea is in a molten state, and the pretreated rotten plant of step 1 of 1.5-2 times of weight of urea part is added after urea melts completely
Acid, temperature are controlled at 90-100 DEG C, add the potassium carbonate of humic acid parts by weight 2%-5%, are uniformly mixed, and 15- is reacted
20min, measurement pH are that 9-11 can be spare to get humic acid urea；
Step 3, the preparation of functional microorganism bacterium powder: taking microbial bacterial agent fermentation liquid, and bacterial sediment spore liquid is collected after centrifugation,
Bacterial sediment spore liquid is uniformly mixed with absorption carrier 1:3 in mass ratio, at 30-40 DEG C, 5min is dried in vacuo, powder is made
Agent, pulvis mesh number >=80 mesh are spare to get microbial germ powder；
The absorption carrier includes organic absorption carrier and mineral absorption carrier, and organic adsorption carrier weighs 7-8 parts by weight,
Mineral carrier weighs 2-3 parts by weight；
Step 4, the inorganic compounding compounding of fertilizer: in parts by weight, 1.0-25.0 parts of monoammonium phosphate, ammonium sulfate 1.0- are weighed
20.0 parts, 1.0-12.0 parts of calcium superphosphate, 1-5 parts of calcium magnesium phosphate, 6-9 parts of Diammonium phosphate (DAP), 13.0-19.0 parts of potassium sulfate, nitric acid
1.0-6.0 parts of ammonium, 1.0-10.0 parts of potassium nitrate, 1.0-8.0 parts of potassium chloride, 3-6 parts of filler element powder, microelement 1.0-5.0
Part, after evenly mixing, obtain inorganic fertilizer formula；
The microelement be borax, zinc sulfate, magnesium sulfate, borax, zinc sulfate, magnesium sulfate mass ratio be 1:2:2；
Step 5, the preparation of the humic acid complex fertilizer containing active microorganism: 30-40 parts of humic acid urea, inorganic fertilizer are weighed by weight
59.5-69 parts, 0.5-1.0 parts of microbial germ powder are formulated, are uniformly mixed, micro- life can be obtained with disk or rotary drum prilling process production
Object humic acid complex fertilizer.
2. a kind of preparation method of humic acid complex fertilizer containing active microorganism according to claim 1, it is characterised in that: institute
State the humic acid content (mass percent) >=40.0% in the lignite in step 1.
3. a kind of preparation method of humic acid complex fertilizer containing active microorganism according to claim 1, it is characterised in that: institute
Stating activator in step 1 is that one of sodium hydroxide, potassium hydroxide, potassium carbonate, ammonium hydrogen carbonate or the quality such as a variety of are compound.
4. a kind of preparation method of humic acid complex fertilizer containing active microorganism according to claim 1, it is characterised in that: institute
Stating the microorganism in step 3 is colloid bacillus cereus (Bacillus amyloliquefaciens), bacillus subtilis
One of (Bacillus Subtillis), bacillus amyloliquefaciens (Bacillus amyloliquefaciens) are a variety of
Etc. quality compounding；
The preservation registration number of the colloid bacillus cereus is CGMCC No.15851；The preservation registration number of the bacillus subtilis
For CGMCCNo.15847；The preservation registration number of the bacillus amyloliquefaciens is CGMCC No.15848.
5. a kind of preparation method of humic acid complex fertilizer containing active microorganism according to claim 1, it is characterised in that: institute
Stating organic adsorption carrier in step 3 is one of turf, biomass charcoal powder, rice bran, seawood meal or the quality compounding such as a variety of,
The mineral absorption carrier is one of concave convex rod, bentonite, diatomite, montmorillonite, polyacrylamide or the quality such as a variety of
Compounding.
6. a kind of preparation method of humic acid complex fertilizer containing active microorganism according to claim 1, it is characterised in that: institute
State the content of organic matter >=50% of humic acid urea obtained in step 2, total humic acid content >=25%, soluble humic acid >=
1.5%.
7. a kind of preparation method of humic acid complex fertilizer containing active microorganism according to claim 1, it is characterised in that: institute
State living bacteria count >=0.2 hundred million in microorganism humic acid complex fertilizer made from step 5.
8. a kind of preparation method of humic acid complex fertilizer containing active microorganism according to claim 1 is prepared micro- containing activity
Biological humic compound fertilizer, the application in prophyiaxis and promoting growth, improvement soil biological fertilizer.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811622987.5A CN109608284A (en) | 2018-12-28 | 2018-12-28 | A kind of preparation and application of the humic acid complex fertilizer containing active microorganism |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811622987.5A CN109608284A (en) | 2018-12-28 | 2018-12-28 | A kind of preparation and application of the humic acid complex fertilizer containing active microorganism |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109608284A true CN109608284A (en) | 2019-04-12 |
Family
ID=66011949
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811622987.5A Pending CN109608284A (en) | 2018-12-28 | 2018-12-28 | A kind of preparation and application of the humic acid complex fertilizer containing active microorganism |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109608284A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110759787A (en) * | 2019-12-17 | 2020-02-07 | 中向旭曜科技有限公司 | Preparation method of soil conditioner rich in humate |
| CN111233573A (en) * | 2020-01-19 | 2020-06-05 | 浙江丰瑜生态科技股份有限公司 | Newly-reclaimed rice field soil improvement humic acid compound fertilizer and preparation method thereof |
| CN111662118A (en) * | 2020-06-03 | 2020-09-15 | 贵州西洋实业有限公司 | Humic acid compound fertilizer and preparation method thereof |
| CN111848244A (en) * | 2019-11-03 | 2020-10-30 | 黑龙江丰富农业科技发展有限公司 | Fulvic acid type special fertilizer for industrial hemp |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102173945A (en) * | 2011-02-17 | 2011-09-07 | 山东省农业科学院农业资源与环境研究所 | Water-soluble fertilizer containing urea humate and preparation method thereof |
| CN102584498A (en) * | 2012-03-28 | 2012-07-18 | 中国农业科学院农业资源与农业区划研究所 | Humic acid urea and preparing method thereof |
| CN103058735A (en) * | 2012-12-24 | 2013-04-24 | 德邦华源（北京）有机农业荒漠化治理技术发展有限公司 | Humus acid urea fertilizer and anhydrous preparation method thereof |
| CN106146178A (en) * | 2016-08-10 | 2016-11-23 | 云南尚呈生物科技有限公司 | A kind of preparation method of mineral sources humic acid urea |
| CN108218615A (en) * | 2017-12-25 | 2018-06-29 | 云南云叶化肥股份有限公司 | A kind of organic and inorganic humic acid fertilizer containing active microorganism and preparation method thereof |
-
2018
- 2018-12-28 CN CN201811622987.5A patent/CN109608284A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102173945A (en) * | 2011-02-17 | 2011-09-07 | 山东省农业科学院农业资源与环境研究所 | Water-soluble fertilizer containing urea humate and preparation method thereof |
| CN102584498A (en) * | 2012-03-28 | 2012-07-18 | 中国农业科学院农业资源与农业区划研究所 | Humic acid urea and preparing method thereof |
| CN103058735A (en) * | 2012-12-24 | 2013-04-24 | 德邦华源（北京）有机农业荒漠化治理技术发展有限公司 | Humus acid urea fertilizer and anhydrous preparation method thereof |
| CN106146178A (en) * | 2016-08-10 | 2016-11-23 | 云南尚呈生物科技有限公司 | A kind of preparation method of mineral sources humic acid urea |
| CN108218615A (en) * | 2017-12-25 | 2018-06-29 | 云南云叶化肥股份有限公司 | A kind of organic and inorganic humic acid fertilizer containing active microorganism and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 王玉堂: "《有益微生物制剂及其在水产养殖中的应用》", 30 September 2018, 海洋出版社 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111848244A (en) * | 2019-11-03 | 2020-10-30 | 黑龙江丰富农业科技发展有限公司 | Fulvic acid type special fertilizer for industrial hemp |
| CN110759787A (en) * | 2019-12-17 | 2020-02-07 | 中向旭曜科技有限公司 | Preparation method of soil conditioner rich in humate |
| CN111233573A (en) * | 2020-01-19 | 2020-06-05 | 浙江丰瑜生态科技股份有限公司 | Newly-reclaimed rice field soil improvement humic acid compound fertilizer and preparation method thereof |
| CN111233573B (en) * | 2020-01-19 | 2021-11-30 | 浙江丰瑜生态科技股份有限公司 | Newly-reclaimed rice field soil improvement humic acid compound fertilizer and preparation method thereof |
| CN111662118A (en) * | 2020-06-03 | 2020-09-15 | 贵州西洋实业有限公司 | Humic acid compound fertilizer and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103833445B (en) | The preparation method of a kind of Organic farming charcoal composite fertilizer | |
| CN102816005B (en) | Peanut special microbial fertilizer and production method thereof | |
| CN109608284A (en) | A kind of preparation and application of the humic acid complex fertilizer containing active microorganism | |
| CN103113143A (en) | Efficient biological organic fertilizer made from yellow mealworm fecula sand | |
| CN103044146A (en) | Complex control type long-acting controlled-release organic and inorganic biological fertilizer | |
| CN101817702A (en) | Special bio-organic fertilizer for peaches and preparation method thereof | |
| CN101130465A (en) | Grain type humic acid compound biological fertilizer and manufacturing method therefor | |
| CN103232289B (en) | Special carbon-vinegar slow-release biological fertilizer for tobaccos and preparation method thereof | |
| CN105884510B (en) | High-activity particle type biological organic fertilizer and its preparation method and application | |
| CN106518529A (en) | Compound biochar-based slow-release fertilizer and application method thereof | |
| CN107266249A (en) | A kind of prevention and control vegetable insect disease type double membrane slow release fertilizer and preparation method thereof | |
| CN102040434B (en) | Method for producing compound microbial fertilizer by microbial inoculum packing method | |
| CN103232304A (en) | Special carbon-vinegar slow-release biological fertilizer for potatoes and preparation method thereof | |
| CN106966834A (en) | A kind of complex microorganism granular fertilizer and preparation method thereof | |
| CN102442846B (en) | Method for producing bio-organic fertilizer by performing spraying granulation | |
| CN103232290B (en) | Carbon-vinegar slow-release biological fertilizer and application thereof | |
| CN109485524A (en) | A kind of dedicated organic base fertilizer of rice and preparation method thereof | |
| CN107382496A (en) | A kind of artificial soil for strengthening crop anti-adversity and the method for strengthening crop anti-adversity | |
| CN102040430B (en) | Method for producing compound microbial fertilizer with insecticidal effect | |
| CN109220647B (en) | Planting method of rice with high trace elements and high enzyme activity | |
| CN117658740A (en) | Biological organic fertilizer for improving alkaline sandy soil and preparation method and application thereof | |
| CN102910979B (en) | Biological organic fertilizer and organic-inorganic compound fertilizer prepared from amino acid multi-element chelate by utilizing ricin and preparation method of biological organic fertilizer and organic-inorganic compound fertilizer | |
| CN1746138A (en) | Production of long-effective ammonium bicarbonate composite fertilizer of vegetable | |
| CN107759307A (en) | Humic acid organic fertilizer | |
| CN110015936A (en) | A kind of functional organic fertilizer and preparation method thereof for improveing salt-soda soil |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20190412 |
|
| RJ01 | Rejection of invention patent application after publication |