CN109601665A - A kind of cynomorium songaricum Pu'er tea and preparation method thereof - Google Patents
A kind of cynomorium songaricum Pu'er tea and preparation method thereof Download PDFInfo
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- CN109601665A CN109601665A CN201910096410.3A CN201910096410A CN109601665A CN 109601665 A CN109601665 A CN 109601665A CN 201910096410 A CN201910096410 A CN 201910096410A CN 109601665 A CN109601665 A CN 109601665A
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- cynomorium songaricum
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- songaricum
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- 241000804384 Cynomorium songaricum Species 0.000 title claims abstract description 162
- 235000020339 pu-erh tea Nutrition 0.000 title claims abstract description 55
- 235000019224 Camellia sinensis var Qingmao Nutrition 0.000 title claims abstract description 52
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 229920001282 polysaccharide Polymers 0.000 claims abstract description 38
- 239000005017 polysaccharide Substances 0.000 claims abstract description 38
- 150000004676 glycans Chemical class 0.000 claims abstract description 37
- 150000008442 polyphenolic compounds Chemical class 0.000 claims abstract description 37
- 235000013824 polyphenols Nutrition 0.000 claims abstract description 37
- 235000013616 tea Nutrition 0.000 claims abstract description 35
- 241001122767 Theaceae Species 0.000 claims abstract description 33
- 239000002994 raw material Substances 0.000 claims abstract description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 64
- 235000019441 ethanol Nutrition 0.000 claims description 36
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 13
- 239000012528 membrane Substances 0.000 claims description 11
- 239000007788 liquid Substances 0.000 claims description 8
- 238000000605 extraction Methods 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 5
- 238000001035 drying Methods 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 4
- 230000000694 effects Effects 0.000 abstract description 14
- 210000002784 stomach Anatomy 0.000 abstract description 10
- 102000019197 Superoxide Dismutase Human genes 0.000 abstract description 6
- 108010012715 Superoxide dismutase Proteins 0.000 abstract description 6
- 210000004185 liver Anatomy 0.000 abstract description 6
- 150000003254 radicals Chemical class 0.000 abstract description 5
- 239000002207 metabolite Substances 0.000 abstract description 4
- 238000005516 engineering process Methods 0.000 abstract description 2
- 210000004051 gastric juice Anatomy 0.000 description 5
- 238000000748 compression moulding Methods 0.000 description 4
- 238000001694 spray drying Methods 0.000 description 4
- -1 Polysaccharides compound Chemical class 0.000 description 3
- 238000001514 detection method Methods 0.000 description 3
- 239000003814 drug Substances 0.000 description 3
- 230000006870 function Effects 0.000 description 3
- 210000004211 gastric acid Anatomy 0.000 description 3
- PFTAWBLQPZVEMU-DZGCQCFKSA-N (+)-catechin Chemical compound C1([C@H]2OC3=CC(O)=CC(O)=C3C[C@@H]2O)=CC=C(O)C(O)=C1 PFTAWBLQPZVEMU-DZGCQCFKSA-N 0.000 description 2
- SRBFZHDQGSBBOR-IOVATXLUSA-N D-xylopyranose Chemical compound O[C@@H]1COC(O)[C@H](O)[C@H]1O SRBFZHDQGSBBOR-IOVATXLUSA-N 0.000 description 2
- 102000004190 Enzymes Human genes 0.000 description 2
- 108090000790 Enzymes Proteins 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 238000012449 Kunming mouse Methods 0.000 description 2
- WSMYVTOQOOLQHP-UHFFFAOYSA-N Malondialdehyde Chemical compound O=CCC=O WSMYVTOQOOLQHP-UHFFFAOYSA-N 0.000 description 2
- 230000003078 antioxidant effect Effects 0.000 description 2
- 150000001720 carbohydrates Chemical class 0.000 description 2
- 235000005487 catechin Nutrition 0.000 description 2
- ADRVNXBAWSRFAJ-UHFFFAOYSA-N catechin Natural products OC1Cc2cc(O)cc(O)c2OC1c3ccc(O)c(O)c3 ADRVNXBAWSRFAJ-UHFFFAOYSA-N 0.000 description 2
- 229950001002 cianidanol Drugs 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 230000002255 enzymatic effect Effects 0.000 description 2
- 238000011049 filling Methods 0.000 description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 239000002574 poison Substances 0.000 description 2
- 231100000614 poison Toxicity 0.000 description 2
- 241000894007 species Species 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- ZFXYFBGIUFBOJW-UHFFFAOYSA-N theophylline Chemical compound O=C1N(C)C(=O)N(C)C2=C1NC=N2 ZFXYFBGIUFBOJW-UHFFFAOYSA-N 0.000 description 2
- 241000283690 Bos taurus Species 0.000 description 1
- HMFHBZSHGGEWLO-SOOFDHNKSA-N D-ribofuranose Chemical compound OC[C@H]1OC(O)[C@H](O)[C@@H]1O HMFHBZSHGGEWLO-SOOFDHNKSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- 238000004566 IR spectroscopy Methods 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 1
- 241001494479 Pecora Species 0.000 description 1
- 244000046052 Phaseolus vulgaris Species 0.000 description 1
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 1
- PYMYPHUHKUWMLA-LMVFSUKVSA-N Ribose Natural products OC[C@@H](O)[C@@H](O)[C@@H](O)C=O PYMYPHUHKUWMLA-LMVFSUKVSA-N 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- OUUQCZGPVNCOIJ-UHFFFAOYSA-M Superoxide Chemical class [O-][O] OUUQCZGPVNCOIJ-UHFFFAOYSA-M 0.000 description 1
- 244000273928 Zingiber officinale Species 0.000 description 1
- 235000006886 Zingiber officinale Nutrition 0.000 description 1
- 230000003213 activating effect Effects 0.000 description 1
- HMFHBZSHGGEWLO-UHFFFAOYSA-N alpha-D-Furanose-Ribose Natural products OCC1OC(O)C(O)C1O HMFHBZSHGGEWLO-UHFFFAOYSA-N 0.000 description 1
- 235000001014 amino acid Nutrition 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 230000003321 amplification Effects 0.000 description 1
- 229930014669 anthocyanidin Natural products 0.000 description 1
- 150000001452 anthocyanidin derivatives Chemical class 0.000 description 1
- 235000008758 anthocyanidins Nutrition 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
- PYMYPHUHKUWMLA-UHFFFAOYSA-N arabinose Natural products OCC(O)C(O)C(O)C=O PYMYPHUHKUWMLA-UHFFFAOYSA-N 0.000 description 1
- 238000005452 bending Methods 0.000 description 1
- SRBFZHDQGSBBOR-UHFFFAOYSA-N beta-D-Pyranose-Lyxose Natural products OC1COC(O)C(O)C1O SRBFZHDQGSBBOR-UHFFFAOYSA-N 0.000 description 1
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 1
- 230000035568 catharsis Effects 0.000 description 1
- 239000013065 commercial product Substances 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- 230000035622 drinking Effects 0.000 description 1
- 238000000855 fermentation Methods 0.000 description 1
- 230000004151 fermentation Effects 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 235000008397 ginger Nutrition 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 235000008216 herbs Nutrition 0.000 description 1
- 210000000936 intestine Anatomy 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 229910052748 manganese Inorganic materials 0.000 description 1
- 239000011572 manganese Substances 0.000 description 1
- 239000002398 materia medica Substances 0.000 description 1
- 230000007721 medicinal effect Effects 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 238000003199 nucleic acid amplification method Methods 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 229920001277 pectin Polymers 0.000 description 1
- 235000010987 pectin Nutrition 0.000 description 1
- 239000001814 pectin Substances 0.000 description 1
- 238000005502 peroxidation Methods 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 235000018102 proteins Nutrition 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 230000002000 scavenging effect Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 230000004206 stomach function Effects 0.000 description 1
- 239000002344 surface layer Substances 0.000 description 1
- 229960000278 theophylline Drugs 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
Classifications
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/06—Treating tea before extraction; Preparations produced thereby
- A23F3/14—Tea preparations, e.g. using additives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/82—Theaceae (Tea family), e.g. camellia
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P39/00—General protective or antinoxious agents
- A61P39/06—Free radical scavengers or antioxidants
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation or decoction
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/333—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using mixed solvents, e.g. 70% EtOH
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/39—Complex extraction schemes, e.g. fractionation or repeated extraction steps
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- Health & Medical Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Pharmacology & Pharmacy (AREA)
- Engineering & Computer Science (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Animal Behavior & Ethology (AREA)
- Biotechnology (AREA)
- Mycology (AREA)
- Epidemiology (AREA)
- Microbiology (AREA)
- Medical Informatics (AREA)
- Botany (AREA)
- Alternative & Traditional Medicine (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Biochemistry (AREA)
- Toxicology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Organic Chemistry (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The present invention provides a kind of cynomorium songaricum Pu'er tea and preparation method thereof, is related to tea making technology field, is prepared from raw materials including the following parts by weight: 1~5 part and 2~50 parts of Yunnan Pu'er cooked tea of Herba Cynomorii extract;Contain cynomorium songaricum polysaccharide and cynomorium songaricum polyphenol in the Herba Cynomorii extract.Refreshed oneself significant effect using cynomorium songaricum Pu'er tea provided by the invention, also there is warm stomach effect, mda content is effectively reduced, improved mouse liver superoxide dismutase activity, can effectively prevent the damage caused by body of free radical and its metabolite.
Description
Technical field
The present invention relates to tea making technology fields, and in particular to a kind of cynomorium songaricum Pu'er tea and preparation method thereof.
Background technique
The earliest function of tea be it is medicinal, Shennong's Herbal record, shennong went into the mountains collecting, tasting and testing different kinds of herbs to be used as medicine, day meet 72 poison, tea and solve it.
Tealeaves has good medical effect, and the Tang Dynasty is to have " tea medicine " word, in " mountain man is clear to supply " that Song Dynasty woods flood is write, also there is " tea, i.e. medicine
" judgement.
China be to the preparation of tea it is diversified, have smoked beans tea, fragrance tea, ginger salt tea etc..9 beginnings of the century, tealeaves at
Divide gradually clear.By the separation and identification of modern science, chemical component is contained in tealeaves up to more than 450 kinds, inorganic mineral is first
Element is up to more than 40 kinds.Chemical component has tea polyphenols, vegetable soda, protein, amino acid, vitamin, pectin element, organic acid, rouge
Polysaccharide, carbohydrate, enzyme, pigment etc..
Pu'er cooked tea, by ripe loose tea made of artificial rapid-result fermentation, there is warm stomach to protect stomach function with big-leaf species in yunnan sundrying tea
Effect, can detoxify, defaecation.Clear people's Zhao Xuemin's supplementary Amplifications of the Compendium of Materia Medica is recorded: " Pu'er tea bitter solves greasy cattle and sheep poison -- include intestines
Remove heat by catharsis ", have the function of helping digestion.Pu'er tea flavour it is warm-natured and, after the mellow Pu'er tea of sweet cunning enters human body stomach, protection can be formed
Film is attached to the surface layer of stomach, and long-term drinking Pu'er tea can play the role of nourishing the stomach, shield stomach.
Contain tea polyphenols, catechin, tea polysaccharide, theophylline, anthocyanidin etc. in Pu'er tea.Tea Polysaccharides compound is commonly referred to as
Tea polysaccharide is the mixture that the element of the first species is complicated and changes greatly, and tea polysaccharide is a kind of acidoglycoprotein, and saccharide portion is by Ah
Draw uncle's sugar, xylose, ribose, glucose and galactolipin to form, and be combined with a large amount of mineral matter element, main calcic, magnesium, iron,
Manganese and a small amount of microelement etc..Catechin is the peculiar composition of tealeaves, is that a kind of important non-enzymatic generated in plant resists
Oxidant is the main active of tea polyphenols, has sterilization, anti-oxidation efficacy, and major function is scavenging capacity oxygen radical,
Anti-lipid peroxidation and the endogenous enzyme activity for adjusting and activating internal oxygen radical.But do not disclose in the prior art as
What can further increase the antioxidant activity of Pu'er tea.
Summary of the invention
The purpose of the present invention is to provide a kind of cynomorium songaricum Pu'er tea and preparation method thereof is provided, using lock provided by the invention
Positive Pu'er tea improves the antioxidant activity of Pu'er tea.
The present invention provides a kind of cynomorium songaricum Pu'er teas, are prepared from raw materials including the following parts by weight: Herba Cynomorii extract 1
~5 parts and 2~50 parts of Yunnan Pu'er cooked tea;
Contain cynomorium songaricum polysaccharide and cynomorium songaricum polyphenol in the Herba Cynomorii extract.
Preferably, the mass percentage of the cynomorium songaricum polysaccharide in the cynomorium songaricum Pu'er tea is 10~15.7%.
Preferably, the mass percentage of the cynomorium songaricum polyphenol in the cynomorium songaricum Pu'er tea is 15~20.3%.
Preferably, the Herba Cynomorii extract preparation method the following steps are included:
1) it is soaked in after being sliced cynomorium songaricum in ethanol solution, 2~10h is extracted at 40~60 DEG C, extracted 3 times, merging mentions
After taking liquid, removing ethyl alcohol, the extracting solution for obtaining the polyphenol containing cynomorium songaricum and the cynomorium songaricum after alcohol extracting;
2) cynomorium songaricum after the alcohol extracting for obtaining the step 1) is dry, obtained drying cynomorium songaricum is soaked in water, 80
1~12h is extracted at~100 DEG C, and obtained extracting solution is filtered, the extracting solution containing cynomorium songaricum polysaccharide is obtained;
3) the mentioning containing cynomorium songaricum polysaccharide for obtaining the extracting solution for the polyphenol containing cynomorium songaricum that the step 1) obtains with step 2)
It takes liquid to mix, obtains cynomorium songaricum extracting solution, the cynomorium songaricum extracting solution is dry, obtain Herba Cynomorii extract.
Preferably, the concentration of the step 1) ethanol solution is 65~95%.
Preferably, the time that the step 1) is impregnated is 2~for 24 hours.
Preferably, the pH value of the step 2) water is 4~8.5.
Preferably, the time that the step 2) is impregnated is 2~for 24 hours.
Preferably, the extracting solution of step 3) polyphenol containing cynomorium songaricum also wraps after mixing with the extracting solution containing cynomorium songaricum polysaccharide
Include: the mixed liquor filter membrane that will be obtained, obtained mistake film liquid are cynomorium songaricum extracting solution;
The aperture of the filter membrane is 0.1~0.22 micron.
The present invention also provides the preparation methods of the cynomorium songaricum Pu'er tea described in above-mentioned technical proposal, comprising: by the cynomorium songaricum
Extract is mixed with Yunnan Pu'er cooked tea, obtains cynomorium songaricum Pu'er tea.
The present invention provides a kind of cynomorium songaricum Pu'er teas, are prepared from raw materials including the following parts by weight: Herba Cynomorii extract 1
~5 parts and 2~50 parts of Yunnan Pu'er cooked tea.In the present invention, the polysaccharide in the Herba Cynomorii extract and polyphenol and Pu'er cooked tea
Common allotment, significant effect of refreshing oneself have warm stomach effect, and mda content is effectively reduced, and improve mouse liver superoxides discrimination
Change enzymatic activity, can effectively prevent the damage caused by collective of free radical and its metabolite.
The embodiment of the present invention is as the result is shown: being refreshed oneself significant effect using cynomorium songaricum Pu'er tea provided by the invention, is had warm
Stomach effect, is effectively reduced mda content, improves mouse liver superoxide dismutase activity, can effectively prevent free radical and its
Metabolite is damaged caused by collective.
Detailed description of the invention
Fig. 1 is the infrared spectroscopy essential groups distribution map of cynomorium songaricum extracting solution.
Specific embodiment
The present invention provides a kind of cynomorium songaricum Pu'er teas, are prepared from raw materials including the following parts by weight: Herba Cynomorii extract 1
~5 parts and 2~50 parts of Yunnan Pu'er cooked tea;Contain cynomorium songaricum polysaccharide and cynomorium songaricum polyphenol in the Herba Cynomorii extract.
In the present invention, the cynomorium songaricum is preferably the cynomorium songaricum of Dulan cultivation.
In the present invention, the mass percentage of the cynomorium songaricum polysaccharide in the cynomorium songaricum Pu'er tea is preferably 10~15.7%.
In the present invention, the mass percentage of the cynomorium songaricum polyphenol in the cynomorium songaricum Pu'er tea is preferably 15~20.3%.
It is 1~5 part of Herba Cynomorii extract that cynomorium songaricum Pu'er tea provided by the invention, which includes parts by weight, preferably 2~4 parts.
In the present invention, cynomorium songaricum polysaccharide and cynomorium songaricum polyphenol are contained in the Herba Cynomorii extract.
In the present invention, the preparation method of the Herba Cynomorii extract preferably includes following steps:
1) it is soaked in after being sliced cynomorium songaricum in ethanol solution, 2~10h is extracted at 40~60 DEG C, extracted 3 times, merging mentions
After taking liquid, removing ethyl alcohol, the extracting solution for obtaining the polyphenol containing cynomorium songaricum and the cynomorium songaricum after alcohol extracting;
2) cynomorium songaricum after the alcohol extracting for obtaining the step 1) is dry, obtained drying cynomorium songaricum is soaked in water, 80
1~12h is extracted at~100 DEG C, and obtained extracting solution is filtered, the extracting solution containing cynomorium songaricum polysaccharide is obtained;
3) the mentioning containing cynomorium songaricum polysaccharide for obtaining the extracting solution for the polyphenol containing cynomorium songaricum that the step 1) obtains with step 2)
It takes liquid to mix, obtains cynomorium songaricum extracting solution, the cynomorium songaricum extracting solution is dry, obtain Herba Cynomorii extract.
The present invention is soaked in ethanol solution after being sliced cynomorium songaricum, and 2~10h is extracted at 40~60 DEG C, is extracted 3 times, is closed
And after extracting solution, removing ethyl alcohol, the extracting solution for obtaining the polyphenol containing cynomorium songaricum and the cynomorium songaricum after alcohol extracting.
The slice thickness and be not particularly limited using slice tool that the present invention is sliced the cynomorium songaricum be using conventional
Can, the slice tool is preferably the wooden knife.
In the present invention, the concentration of the ethanol solution is preferably 65~95%, and more preferably 70~90%, most preferably
75~85%.In the present invention, the time that the cynomorium songaricum after the slice is impregnated in ethanol solution is preferably 2~for 24 hours, more preferably
For 5~20h, most preferably 10~15h.
In the present invention, the temperature of the extraction is preferably 40~60 DEG C, and more preferably 50 DEG C;The time of the extraction is excellent
It is selected as 2~10h, more preferably 4~8h, most preferably 5~6h;The number of the extraction is preferably 3 times.
Cynomorium songaricum after the alcohol extracting that the present invention obtains is dry, obtained drying cynomorium songaricum is soaked in water, at 80~100 DEG C
1~12h is extracted, obtained extracting solution is filtered, the extracting solution containing cynomorium songaricum polysaccharide is obtained.
In the present invention, the dry cynomorium songaricum be soaked in the time in water be preferably 2~for 24 hours, more preferably 5~20h, most
Preferably 10~15h.In the present invention, the time of the extraction is preferably 1~12h, more preferably 4~10h, and most preferably 5
~8h;The temperature of the extraction is preferably 80~100 DEG C.In the present invention, the pH value of the water is preferably 4~8.5, more preferably
It is 5.8~7.0.
The present invention mixes the extracting solution of the obtained polyphenol containing cynomorium songaricum with the obtained extracting solution containing cynomorium songaricum polysaccharide, obtains
Cynomorium songaricum extracting solution, the cynomorium songaricum extracting solution is dry, obtain Herba Cynomorii extract.
In the present invention, the extracting solution of the polyphenol containing cynomorium songaricum preferably also wraps after mixing with the extracting solution containing cynomorium songaricum polysaccharide
Include: the mixed liquor filter membrane that will be obtained, obtained mistake film liquid are cynomorium songaricum extracting solution.In the present invention, the aperture of the filter membrane is
0.1~0.22 micron.In the present invention, the temperature when mixed liquor filter membrane is preferably 30~50 DEG C, more preferably 35~
45 DEG C, most preferably 40 DEG C.
It is 2~50 parts of Yunnan Pu'er cooked tea that cynomorium songaricum Pu'er tea provided by the invention, which includes parts by weight, preferably 10~
40 parts, more preferably 15~25 parts.The present invention is not particularly limited the source of the Yunnan Pu'er cooked tea, using conventional commercial
Product.
The present invention also provides the preparation methods of the cynomorium songaricum Pu'er tea described in above-mentioned technical proposal, comprising: by the cynomorium songaricum
Extract is mixed with Yunnan Pu'er cooked tea, obtains cynomorium songaricum Pu'er tea.
A kind of cynomorium songaricum Pu'er tea of the present invention and preparation method thereof is done further in detail combined with specific embodiments below
Thin introduction, technical solution of the present invention include but is not limited to following embodiment.
Embodiment 1
1) cynomorium songaricum that fresh Dulan is cultivated is cleaned up, the wooden knife slice, 65% ethyl alcohol impregnates 2 hours, 40
10h is extracted at DEG C, is extracted 3 times, after combined extract, removing ethyl alcohol, the extracting solution and the lock after alcohol extracting that obtain the polyphenol containing cynomorium songaricum
Sun.
2) cynomorium songaricum after alcohol extracting is dry, it is 6.8 that water, which is added, and adjusts pH value, impregnates 2 hours, it is small that 2.5 are extracted at 80 DEG C
When, obtained extracting solution is filtered, extracting solution containing cynomorium songaricum polysaccharide is obtained.
3) extracting solution containing cynomorium songaricum polysaccharide obtained by the above-mentioned extracting solution of polyphenol containing cynomorium songaricum 1) obtained and 2) merges, at 30 DEG C
Cross film, membrane aperture is 0.22 micron, obtains cynomorium songaricum extracting solution, measure content, polyphenol containing cynomorium songaricum 15.8%, contain cynomorium songaricum polysaccharide in
12.5%.Spray drying, obtains Herba Cynomorii extract.
4) 2 parts of Yunnan Pu'er cooked tea are weighed, 1 part of above-mentioned Herba Cynomorii extract is added, compression moulding obtains cynomorium songaricum Pu'er tea.
Embodiment 2
1) cynomorium songaricum that fresh Dulan is cultivated is cleaned up, the wooden knife slice, 95% ethyl alcohol impregnates 24 hours, 60
2h is extracted at DEG C, is extracted 3 times, after combined extract, removing ethyl alcohol, the extracting solution and the lock after alcohol extracting that obtain the polyphenol containing cynomorium songaricum
Sun.
2) cynomorium songaricum after alcohol extracting is dry, it is 5.5 that water, which is added, and adjusts pH value, impregnates 24 hours, it is small that 12 are extracted at 100 DEG C
When, obtained extracting solution is filtered, extracting solution containing cynomorium songaricum polysaccharide is obtained.
3) extracting solution containing cynomorium songaricum polysaccharide obtained by the above-mentioned extracting solution of polyphenol containing cynomorium songaricum 1) obtained and 2) merges, at 50 DEG C
Film is crossed, membrane aperture is 0.1 micron, obtains cynomorium songaricum extracting solution, measures content, and polyphenol containing cynomorium songaricum 20.2% contains cynomorium songaricum polysaccharide
14.9%.Spray drying, obtains Herba Cynomorii extract.
4) 50 parts of Yunnan Pu'er cooked tea are weighed, 5 parts of above-mentioned Herba Cynomorii extract is added, compression moulding obtains cynomorium songaricum Pu'er tea.
Embodiment 3
1) cynomorium songaricum that fresh Dulan is cultivated is cleaned up, the wooden knife slice, 85% ethyl alcohol impregnates 12 hours, 50
8h is extracted at DEG C, is extracted 3 times, after combined extract, removing ethyl alcohol, the extracting solution and the lock after alcohol extracting that obtain the polyphenol containing cynomorium songaricum
Sun.
2) cynomorium songaricum after alcohol extracting is dry, it is 4.0 that water, which is added, and adjusts pH value, impregnates 16 hours, it is small that 8 are extracted at 90 DEG C
When, obtained extracting solution is filtered, extracting solution containing cynomorium songaricum polysaccharide is obtained.
3) extracting solution of polyphenol containing cynomorium songaricum obtained by the above-mentioned extracting solution of polyphenol containing cynomorium songaricum 1) obtained and 2) merges, at 40 DEG C
Film is crossed, membrane aperture is 0.22 micron, obtains cynomorium songaricum extracting solution, measures content, and polyphenol containing cynomorium songaricum 18.7% contains cynomorium songaricum polysaccharide
15.0%.Spray drying, obtains Herba Cynomorii extract.
4) 25 parts of Yunnan Pu'er cooked tea are weighed, 2 parts of above-mentioned Herba Cynomorii extract is added, compression moulding obtains cynomorium songaricum Pu'er tea.
Embodiment 4
1) cynomorium songaricum that fresh Dulan is cultivated is cleaned up, the wooden knife slice, 75% ethyl alcohol impregnates 6 hours, 50
DEG C choosing extract 9h, extract 3 times, combined extract, remove ethyl alcohol after, the extracting solution and the lock after alcohol extracting that obtain the polyphenol containing cynomorium songaricum
Sun.
2) cynomorium songaricum after alcohol extracting is dry, it is 5.8 that water, which is added, and adjusts pH value, impregnates 8 hours, it is small that 12 are extracted at 85 DEG C
When, obtained extracting solution is filtered, extracting solution containing cynomorium songaricum polysaccharide is obtained.
3) extracting solution containing cynomorium songaricum polysaccharide obtained by the above-mentioned extracting solution of polyphenol containing cynomorium songaricum 1) obtained and 2) merges, at 45 DEG C
Film is crossed, membrane aperture is 0.1 micron, obtains cynomorium songaricum extracting solution, measures content, and polyphenol containing cynomorium songaricum 19.6% contains cynomorium songaricum polysaccharide
13.4%.Spray drying, obtains Herba Cynomorii extract.
4) 50 parts of Yunnan Pu'er cooked tea are weighed, 1 part of above-mentioned Herba Cynomorii extract is added, compression moulding obtains cynomorium songaricum Pu'er tea.
Embodiment 5
Cynomorium songaricum extracting solution prepared by embodiment 1 carries out infrared light detection, the result is shown in Figure 1.
As can be drawn from Figure 1, there is C-O stretching vibration at 1045, compound is polysaccharide;There is phenyl ring skeleton at 1604
Flexible amplitude or NH2 scissors bending vibration, compound are phenols.
Cynomorium songaricum extracting solution prepared by embodiment 1 carries out content detection, the results are shown in Table 1.
1 cynomorium songaricum film of table filters content detection
Cynomorium songaricum extracting solution | Cynomorium songaricum polyphenol | Cynomorium songaricum polysaccharide |
Content | 15.8% | 12.5% |
Embodiment 6
By healthy KM mouse 40,4 groups are randomly divided into, half male and half female gives prepared by embodiment 1 low dose of cynomorium songaricum Pu'er tea
Amount group and high dose group (5g/kg/d, 10g/kg/d), blank group press 0.2ml/10g stomach-filling pure water, give cynomorium songaricum Pu'er tea 30
It.The content for detecting malonaldehyde (MDA), superoxide dismutase (SOD), the results are shown in Table 2.
The influence of 2 cynomorium songaricum Pu'er tea mouse liver biochemical indicator of table
Compared with blank group: P < 0.05 *, P < 0.01 * *
By table 2, it can be concluded that, cynomorium songaricum Pu'er tea can improve mouse liver superoxide dismutase activity, reduce malonaldehyde and contain
Amount, can effectively prevent the damage caused by collective of free radical and its metabolite.
By healthy KM mouse 30,3 groups are randomly divided into, cynomorium songaricum Pu'er tea two of half male and half female, the preparation of embodiment 1 are administered
Group (low, high dose group dosage is respectively 5g/kg/d, 10g/kg/d), blank control group are administered seven days.Detect gastric juice amount, stomach
The content of sour (pH value), the results are shown in Table 3.
Influence after 3 cynomorium songaricum Pu'er tea stomach-filling of table 30 days to gastric juice index
Group | Dosage (g/kg) | Gastric juice amount (ml) | Gastric acid (pH value) |
Low dose group | 5 | 3.12±0.48* | 2.08±0.41** |
High dose group | 10 | 3.24±0.26** | 2.21±0.32** |
Blank group | —— | 2.35±0.30 | 3.54±0.50 |
Model group | —— | 3.77±0.54## | 1.86±0.29## |
Compared with blank group: #P < 0.05, ##P < 0.01;Compared with model group: P < 0.05 *, P < 0.01 * *
By table 3, it can be concluded that, compared with blank group, model group gastric juice amount obviously increases (P < 0.01).Compared with model group,
Two dosage group gastric juice amounts of cynomorium songaricum Pu'er tea significantly reduce.Compared with blank group, model group gastric acid (pH value) be substantially reduced (P <
0.01).Compared with model group, two dosage group gastric acids (pH value) of cynomorium songaricum Pu'er tea are significantly raised.
It can be concluded that, refreshed oneself significant effect using cynomorium songaricum Pu'er tea provided by the invention by above embodiments, there is warm stomach
Mda content is effectively reduced in effect, improves mouse liver superoxide dismutase activity, can effectively prevent free radical and its generation
Thank to product damage caused by collective.
The above is only a preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, various improvements and modifications may be made without departing from the principle of the present invention, these improvements and modifications are also answered
It is considered as protection scope of the present invention.
Claims (10)
1. a kind of cynomorium songaricum Pu'er tea, which is characterized in that be prepared from raw materials including the following parts by weight: Herba Cynomorii extract 1~5
Part and 2~50 parts of Yunnan Pu'er cooked tea;
Contain cynomorium songaricum polysaccharide and cynomorium songaricum polyphenol in the Herba Cynomorii extract.
2. cynomorium songaricum Pu'er tea according to claim 1, which is characterized in that the matter of the cynomorium songaricum polysaccharide in the cynomorium songaricum Pu'er tea
Measuring percentage composition is 10~15.7%.
3. cynomorium songaricum Pu'er tea according to claim 1, which is characterized in that the matter of the cynomorium songaricum polyphenol in the cynomorium songaricum Pu'er tea
Measuring percentage composition is 15~20.3%.
4. cynomorium songaricum Pu'er tea according to claim 1, which is characterized in that the preparation method of the Herba Cynomorii extract include with
Lower step:
1) it is soaked in after being sliced cynomorium songaricum in ethanol solution, 2~10h is extracted at 40~60 DEG C, extracted 3 times, combined extract,
After removing ethyl alcohol, the extracting solution for obtaining the polyphenol containing cynomorium songaricum and the cynomorium songaricum after alcohol extracting;
2) cynomorium songaricum after the alcohol extracting for obtaining the step 1) is dry, obtained drying cynomorium songaricum is soaked in water, 80~100
1~12h is extracted at DEG C, and obtained extracting solution is filtered, the extracting solution containing cynomorium songaricum polysaccharide is obtained;
3) extracting solution containing cynomorium songaricum polysaccharide for obtaining the extracting solution for the polyphenol containing cynomorium songaricum that the step 1) obtains and step 2)
Mixing, obtains cynomorium songaricum extracting solution, and the cynomorium songaricum extracting solution is dry, obtains Herba Cynomorii extract.
5. cynomorium songaricum Pu'er tea according to claim 4, which is characterized in that the concentration of the step 1) ethanol solution be 65~
95%.
6. cynomorium songaricum Pu'er tea according to claim 4, which is characterized in that the time that the step 1) is impregnated is 2~for 24 hours.
7. cynomorium songaricum Pu'er tea according to claim 4, which is characterized in that the pH value of the step 2) water is 4~8.5.
8. cynomorium songaricum Pu'er tea according to claim 4, which is characterized in that the time that the step 2) is impregnated is 2~for 24 hours.
9. cynomorium songaricum Pu'er tea according to claim 4, which is characterized in that the extracting solution of step 3) polyphenol containing cynomorium songaricum with
After extracting solution mixing containing cynomorium songaricum polysaccharide further include: the mixed liquor filter membrane that will be obtained, obtained mistake film liquid are cynomorium songaricum extraction
Liquid;
The aperture of the filter membrane is 0.1~0.22 micron.
10. the preparation method of cynomorium songaricum Pu'er tea according to any one of claims 1 to 9, comprising: by the Herba Cynomorii extract and cloud
Southern Pu'er cooked tea mixing, obtains cynomorium songaricum Pu'er tea.
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Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101103750A (en) * | 2007-08-08 | 2008-01-16 | 杨加龙 | Pseudo-ginseng health-care pu' er tea |
CN101218947A (en) * | 2008-01-22 | 2008-07-16 | 余锦洲 | Xinhui pericarpium citri reticulatae Pu ' er pressing tea and production method thereof |
CN101878844A (en) * | 2010-06-29 | 2010-11-10 | 瓜州亿得生物科技有限公司 | Cynomorium coffee |
CN102626156A (en) * | 2012-04-11 | 2012-08-08 | 徐州绿之野生物食品有限公司 | Ginkgo leaf extraction process and method for processing fermented ginkgo Pu'er tea |
CN103083374A (en) * | 2013-01-31 | 2013-05-08 | 孟令刚 | Tea cynomorium songaricum and preparation method thereof |
CN104663952A (en) * | 2015-03-18 | 2015-06-03 | 甘肃指南针生物工程中心(特殊普通合伙企业) | Anti-aging cynomorium songaricum tea and preparation method thereof |
CN105076571A (en) * | 2015-08-25 | 2015-11-25 | 云南省林业科学院 | Pu'er healthcare tea and method for manufacturing same |
CN107593986A (en) * | 2017-11-10 | 2018-01-19 | 荣成市熠欣海洋生物科技有限公司 | A kind of chrysanthemum tea and preparation method for preventing and treating kidney-yang deficiency |
-
2019
- 2019-01-31 CN CN201910096410.3A patent/CN109601665A/en active Pending
Patent Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101103750A (en) * | 2007-08-08 | 2008-01-16 | 杨加龙 | Pseudo-ginseng health-care pu' er tea |
CN101218947A (en) * | 2008-01-22 | 2008-07-16 | 余锦洲 | Xinhui pericarpium citri reticulatae Pu ' er pressing tea and production method thereof |
CN101878844A (en) * | 2010-06-29 | 2010-11-10 | 瓜州亿得生物科技有限公司 | Cynomorium coffee |
CN102626156A (en) * | 2012-04-11 | 2012-08-08 | 徐州绿之野生物食品有限公司 | Ginkgo leaf extraction process and method for processing fermented ginkgo Pu'er tea |
CN103083374A (en) * | 2013-01-31 | 2013-05-08 | 孟令刚 | Tea cynomorium songaricum and preparation method thereof |
CN104663952A (en) * | 2015-03-18 | 2015-06-03 | 甘肃指南针生物工程中心(特殊普通合伙企业) | Anti-aging cynomorium songaricum tea and preparation method thereof |
CN105076571A (en) * | 2015-08-25 | 2015-11-25 | 云南省林业科学院 | Pu'er healthcare tea and method for manufacturing same |
CN107593986A (en) * | 2017-11-10 | 2018-01-19 | 荣成市熠欣海洋生物科技有限公司 | A kind of chrysanthemum tea and preparation method for preventing and treating kidney-yang deficiency |
Non-Patent Citations (1)
Title |
---|
段园园等: "锁阳中粗多酚和粗多糖抗氧化活性的比较", 《中国现代中药》 * |
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