CN109594330A - The preparation method and moisturizing non-woven fabrics of a kind of moisturizing type non-woven fabrics and application - Google Patents
The preparation method and moisturizing non-woven fabrics of a kind of moisturizing type non-woven fabrics and application Download PDFInfo
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- CN109594330A CN109594330A CN201811528689.XA CN201811528689A CN109594330A CN 109594330 A CN109594330 A CN 109594330A CN 201811528689 A CN201811528689 A CN 201811528689A CN 109594330 A CN109594330 A CN 109594330A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P29/00—Non-central analgesic, antipyretic or antiinflammatory agents, e.g. antirheumatic agents; Non-steroidal antiinflammatory drugs [NSAID]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/42—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
- D04H1/425—Cellulose series
- D04H1/4258—Regenerated cellulose series
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/42—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
- D04H1/4266—Natural fibres not provided for in group D04H1/425
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/42—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
- D04H1/4382—Stretched reticular film fibres; Composite fibres; Mixed fibres; Ultrafine fibres; Fibres for artificial leather
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/44—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling
- D04H1/46—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling by needling or like operations to cause entanglement of fibres
- D04H1/492—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling by needling or like operations to cause entanglement of fibres by fluid jet
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with hydrogen peroxide or peroxides of metals; with persulfuric, permanganic, pernitric, percarbonic acids or their salts
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
Abstract
The invention discloses a kind of preparation method of moisturizing type non-woven fabrics and moisturizing non-woven fabrics and application, which is tangled two kinds of fiber flexibilities by water jet process, is not influenced the original characteristic of fiber, will not be damaged fiber；Using spunlace non-woven cloth as substrate, the further micro emulsion atomization process of the present invention, which uniformly seeps pure natural prescription Essence, to be attached in substrate, is avoided the loss of prescription Essence, be ensure that skin effect；It seeps attached process simultaneously and will not influence the skin-friendly of non-woven fabrics, the still soft comfortable of non-woven fabrics after treatment, the moisturizing type nonwoven thickness of preparation is uniform, elongation is high.
Description
Technical field
The present invention relates to field of nonwoven fabric technology, more particularly, to the preparation method and profit of a kind of moisturizing type non-woven fabrics
Skin non-woven fabrics and application.
Background technique
Non-woven fabrics is a kind of fabric for not needing spinning and weaving and being formed, and only carries out textile staple or long filament
Orientation or random alignment form fibre net structure, are then reinforced using the methods of mechanical, hot sticky or chemical.It is directly utilized
High polymer slice, staple fiber or long filament have soft, ventilative peace by what various web forming methods and concretion technology were formed
The tencel product of face structure.Sheet-like nonwoven cloth material production skincare product is generallyd use currently on the market, based on white,
It is functional not prominent enough.Its skin-care effect mainly by nonwoven surface spray liquid skin treatments or attachment powder skin conditioner come
It realizes, but both modes all have corresponding technological deficiency in actual production.Powder skin conditioner adding technology is complicated,
In effect ingredient stripping property it is bad；And liquid skin treatments will appear the lower infiltration loss of effective component during sprinkling, shield
It remains little on skin articles, to influence the skin effect of product.
Butter fruit is a kind of very high fruit of nutritive value, contains multivitamin, fatty acid abundant and protein and height
The elements such as sodium, potassium, magnesium, the calcium of content, nutritive value can match in excellence or beauty with cream, or even have the laudatory title of " forest cream ", generally as
Fruit is edible, can also be made as dish and can.Galam butter in butter fruit can be moisturized the skin effectively, keep skin water
Point, it is frequently used in skin-protection product.Since galam butter can not resist the hot gas of distillation, can be destroyed in extraction process smart matter at
Point.The extraction of galam butter at present is extracted mainly by cold press technique, and extraction efficiency is not high, and the utilization rate of galam butter is low.
Summary of the invention
Limited the technical problem to be solved by the present invention is to be directed to the skin effect of skin care non-woven fabrics in the prior art, color is general
Logical deficiency provides a kind of preparation method of moisturizing type non-woven fabrics, which pre-processes butter fruit fiber, makes ox
Oily fruit fiber can retain fiber true qualities and have preferably soft skin fitness；After two kinds of fibers are mixed and made into spunlace non-woven cloth,
Then skin care drug will uniformly be seeped by micro emulsion atomization process and will be attached on non-woven fabrics, and make moisturizing type non-woven fabrics that there is antibacterial kill
Bacterium, the effect for cleaning skin.
Another technical problem to be solved by the present invention is that the moisturizing non-woven fabrics that the preparation method is prepared is provided, the profit
Skin type non-woven fabrics is combined with the medicine essence of skin care whitening using butter fruit fiber and viscose rayon as raw material, has and moistens skin
The effect of skin, restraining and sterilizing bacteria.
The present invention also technical problems to be solved are to provide the application of the moisturizing type non-woven fabrics.
The purpose of the present invention is achieved through the following technical solutions:
A kind of moisturizing type non-woven fabrics, the moisturizing type non-woven fabrics is using butter fruit fiber, viscose rayon as main raw material(s), warp
Following steps are prepared:
S1. it pre-processes: butter fruit fiber and viscose rayon is pre-processed respectively；
S2. raw material mixes: butter fruit fiber pretreated in step S1 and viscose rayon are mixed；
S3. non-woven fabrics is prepared: hydrophilic treated, shredding, combing, auxiliary net, drawing-off, water by the composite fibre in step S2
After thorn, drying, spunlace non-woven cloth is obtained；
S4. skim the cream off milk liquid: being decocted after each component in prescription is mixed with distilled water, prescription solution is obtained after filtering, to group
Square solution distilation obtains the prescription Essence of high-purity；
S5. micro emulsion is atomized: using spunlace non-woven cloth obtained in step S3 as carrier, the addition of prescription Essence being had for 4~8 times
By high pressure nozzle jet atomization after solvent dilution, the prescription Essence after atomization is under the high pressure draught effect of upper and lower convection current
It is evenly distributed on natural fiber spunlace non-woven cloth.
S6. sterile drying: obtaining spunlace non-woven cloth after handling in step S5 and carry out drying and processing in aseptic space,
Obtain moisturizing type non-woven fabrics；
Wherein to the pretreating process of butter fruit fiber in step S1 are as follows: butter fruit fiber is put into aqueous slkali and is impregnated；
To the pretreating process of viscose rayon are as follows: mix to be put into overflow dyeing machine with emulsifier by viscose rayon and be heat-treated.
Further, in butter fruit fiber preprocessing process in step S1, the alkaline concentration is 1~3g/L, temperature
Degree is 40~80 DEG C, and soaking time is 40~80min, and bath raio is 1:8~10.
Further, the aqueous slkali is NaOH solution.
Preferably, the NaOH solution concentration is 1g/L, and temperature is 60 DEG C, soaking time 50min, bath raio 1:10.
Further, in viscose rayon preprocessing process in step S1, the emulsifier and viscose rayon mass ratio are 1
~3:100, the heat treatment temperature are 60~100 DEG C, and the time is 20~50min.:
Preferably, the emulsifier and viscose rayon mass ratio are 1:100, and the heat treatment temperature is 80 DEG C, and the time is
30min。
The present invention carries out immersion treatment to butter fruit fiber using aqueous slkali, has softened butter fruit fiber, has improved butter
The cohesive force of fruit fiber and viscose rayon, and the butter fruit fiber after aqueous slkali soaking has better skin-friendly.
Further, the mass ratio of butter fruit fiber and viscose rayon is 5~10:90~95 in step S2.
Preferably, the mass ratio of butter fruit fiber and viscose rayon is 5:95.
Further, hydrophilic process described in step S3 are as follows: carry out the composite fibre in step S2 with hydrogen peroxide and water
Processing, treatment temperature are 60 DEG C, and the processing time is 12 hours, and wherein the mass ratio of hydrogen peroxide, water and fiber is 1:4:5.
Shredding, carding step: successively carrying out thick shredding and smart shredding, after by various fibers after more storehouse mixing machines mix,
Using sending cotton blower to be sent to double cylinder and double doffer carding machine for composite fibre is uniform and stable, combed using double cylinder and double doffer
Fibrous raw material is processed into the thin net being made of single fiber by reason machine, through cross lapping and drawing-off, to manufacture centainly quantitative three-dimensional
The fibre web of disordered arrangements.
Lapping process: by the way of cross lapping；Set the quantification of 35g/m of fibre web2, the quantitative difference of two layers of fiber
For 18g/m2, the actual quantification of fibre web is 36g/m2。
Drafting process: using roller type drafting machine, will originally be in transversely arranged fibre web to longitudinal arrangement, and was formed preferable
Vertically and horizontally strength requires, to meet using upper strength requirement, drafting multiple 2.1.
Further, the processing of spun lacing described in step S3 is walked in rotary drum spun-laced machine, rotary drum spun-laced machine including 4 spun lacings
Suddenly, in the 4 spun lacing step, the 1st to the 4th spun lacing pressure is successively are as follows: 16~22kg, 15~18kg, 30~35kg, 15~
18kg。
Preferably, the 1st to the 4th spun lacing pressure is successively are as follows: 18kg, 17kg, 32kg, 17kg.
Water jet process keeps fiber entangled to each other together on the fine water flow jet to web of high pressure in the present invention, from
And web is enable to reinforce, have certain mechanical strength.Pass through the breaking strength to butter fruit fiber and viscose rayon, resurgence
Influence of the factors such as rate, oil content, fiber number, length to spunlace non-woven cloth performance, determine blended spun lacing spun lacing pressure be 12~
30kg, spun lacing pressure is bigger, and water needle energy is higher, and the non-woven fabrics intensity that spun lacing goes out is also higher, but excessively high hydraulic pressure can be made
At fibrous fracture and fiber loss, causes non-woven fabrics intensity to decline or the fiber in web is directly made to generate displacement and influence nothing
The quality of woven fabric；The surface of hypotony, web cannot consolidate well.
The present invention is reinforced, and use according to the performance and content of butter fruit fiber and viscose rayon using 4 water jet processes
The pressure distribution reduced again from low to high, pressure are respectively as follows: 16~22kg, 15~18kg, 30~35kg, 15~18kg.The
The hypertonia of one of spun lacing can reduce non-woven fabrics quality, be lost fibrous fracture, aggravate the burden of water circulation system, cause
Two, the snagging of three water jet processes is serious.Two spun lacing pressure are too small, and web is reinforced loosely, loosely organized, butter fruit
Fiber and viscose rayon cannot combine closely, and non-woven fabrics is made to form coarse surface, and the uniformity of nonwoven cloth cover is caused to decline, and rise
Hair is serious, influences the feel of product；Two spun lacing pressure are excessive, make that fiber alignment is mixed and disorderly, the decline of entanglement degree, to make strong in length and breadth
Power ratio increases, and causes fibre damage.Three spun lacing high pressures reinforce web, reach butter fruit fiber and viscose rayon
Good mechanical property.The main function of four spun lacings is the modification that positive and negative are carried out to nonwoven cloth cover, is not reached to entanglement degree
Fiber to saturation further punctures, it is made to reach saturation as far as possible, this just determines that spun lacing pressure cannot be too low；Meanwhile four
Spun lacing carries out certain reparation to the surface of non-woven fabrics, this just determines that spun lacing pressure cannot be excessively high.It is further preferred that the ox
By four spun lacing steps, spun lacing pressure is respectively 18kg, 17kg, 32kg, 17kg for oily fruit fiber and viscose rayon.
Further, each group is divided into Asian puccoon, the fleece-flower root, ganoderma lucidum, Radix Angelicae Sinensis, Rhizoma Chuanxiong, asarum, Hu in prescription described in step S4
The one or more of fiber crops.
Asian puccoon major function is cool blood, activating microcirculation and removing stasis medicinal, removing toxic substances promoting eruption, has the effect of significant ground anti-acne and anti-inflammatory.
The fleece-flower root has the function of expanding blood vessel, Skin Cell can be made to obtain enough blood volumes, can promote to have rosy cheeks to have
Gloss.
Polysaccharide component contained by ganoderma lucidum can eliminate interior free yl, delaying cell aging, street cleaner of the ganoderma lucidum as blood, energy
Melanin, the brown pigment in blood are eliminated, the formation of freckle, senile plaque is controlled.
Contain various trace elements in Radix Angelicae Sinensis, to skin nutrition, prevent it is coarse play an important role, may act on acne,
The treatment of freckle.
Rhizoma Chuanxiong has the function of vital energy regualting and blood circulation-promoting, wind-expelling pain-stopping, has stronger restraint to the activity of pathogenic dermatophyte.
Volatile oil and vitamin A in asarum play the role of maintaining elasticity of skin, improve microcirculation and anti-inflammatory antibacterial.
Further, decocting time is 2~4 hours in step S4.
Further, distilation technological parameter is as follows in step S4: temperature is 120~140 DEG C, and the time is 2~4 small
When.
Further, micro emulsion atomization process described in step S5 is as follows: atomization temperature is 18~24 DEG C, and atomizing pressure is
0.6~0.8MPa, air column jet air pressure are 0.6~0.9MPa.
Further, high pressure draught described in step S5 is one kind of nitrogen or carbon dioxide.
Further, organic solvent described in step S5 is mixed with prescription Essence 4~6:1 in mass ratio, it is preferable that institute
Organic solvent is stated to mix with prescription Essence 4:1 in mass ratio.
Further, organic solvent described in step S5 is one of ethyl alcohol, glycerol, propylene glycol, benzyl alcohol, polyethylene glycol
Or it is several.
Further, drying temperature described in step S6 is 60~80 DEG C, and the time is 10~15S.
Present invention simultaneously provides application of the above-mentioned moisturizing type non-woven fabrics in the manufacture soft towel of cotton.
Compared with prior art, the beneficial effects of the present invention are:
The present invention is by pre-processing butter fruit fiber, so that butter fiber sufficiently softens, improves butter fruit fibre
The cohesive force of dimension and viscose rayon, and the butter fruit fiber after softening has better skin-friendly.It is prepared with butter fruit fiber
At non-woven fabrics, be in aqua in color, rich in there is galam butter in butter fruit fiber, have good treatment to skin is repaired
Effect, can moisten, softening skin.By butter fruit fiber directly as the raw material of non-woven fabrics, the step of cold press technique extraction is eliminated
Suddenly, the galam butter in butter fruit fiber can be fully used, and the moisturizing type non-woven fabrics soothing effect of preparation is good.
Prescription Essence used in the present invention is pure plant prescription, has and moisturizes the skin, delays senescence, anti-inflammatory suppression
The effect of bacterium.It after moisturizing type non-woven fabrics with prescription Essence is contacted with human skin, is carried out clearly to skin surface first
Clean, the effective component in subsequent prescription Essence enters skin histology by pore, reaches and inhibits bacterium, diminish inflammation, moisten
The effect of skin.
The present invention by micro emulsion atomization process by prescription Essence by uniformly being seeped and being attached to using spunlace non-woven cloth as substrate
In substrate, the loss of prescription Essence is avoided, ensure that skin effect；Micro emulsion atomization process will not influence non-woven fabrics simultaneously
Skin-friendly, the still soft comfortable of non-woven fabrics after treatment.
Specific embodiment
To facilitate the understanding of the present invention, present invention work more comprehensively, is meticulously described below in conjunction with embodiment, but this hair
Bright protection scope is not limited to embodiment in detail below.
Unless otherwise defined, all technical terms used hereinafter and the normally understood meaning of those skilled in the art
It is identical.Technical term used herein is intended merely to the purpose of description specific embodiment, it is no intended to limit of the invention
Protection scope.
Unless otherwise specified, various raw material, reagent, the instrument and equipment etc. used in the present invention can pass through city
Field is commercially available or can be prepared by existing method.
It is as follows to the hydrophilic treated of composite fibre, shredding, combing, lapping, drafting step:
Hydrophilic process: the composite fibre in step S2 is handled with hydrogen peroxide and water, and treatment temperature is 60 DEG C, processing
Time is 12 hours, and wherein the mass ratio of hydrogen peroxide, water and fiber is 1:4:5.
Shredding, carding step: successively carrying out thick shredding and smart shredding, after by various fibers after more storehouse mixing machines mix,
Using sending cotton blower to be sent to double cylinder and double doffer carding machine for composite fibre is uniform and stable, combed using double cylinder and double doffer
Fibrous raw material is processed into the thin net being made of single fiber by reason machine, through cross lapping and drawing-off, to manufacture centainly quantitative three-dimensional
The fibre web of disordered arrangements.
Lapping process: by the way of cross lapping；Set the quantification of 35g/m of fibre web2, the quantitative difference of two layers of fiber
For 18g/m2, the actual quantification of fibre web is 36g/m2。
Drafting process: using roller type drafting machine, will originally be in transversely arranged fibre web to longitudinal arrangement, and was formed preferable
Vertically and horizontally strength requires, to meet using upper strength requirement, drafting multiple 2.1.
Although a kind of above-mentioned specific embodiment for being only exemplified by above-mentioned processing step, those skilled in the art can manage
Solution, other extracting methods (method especially in the limited range of the present invention) for being not limited to ad hoc fashion are also the same
Essentially identical extraction effect may be implemented, can be used for realizing the present invention, this is no longer particularly limited.
Embodiment 1
The present embodiment provides a kind of preparation methods of moisturizing type non-woven fabrics, and its step are as follows:
S1. butter fruit fiber is put into concentration is 1g/L, is impregnated in the NaOH solution that temperature is 60 DEG C, soaking time is
50min, bath raio 1:10；Emulsifier and viscose rayon after 1:100 is mixed in mass ratio, are put into overflow dyeing machine at heat
Reason, heat treatment temperature are 80 DEG C, time 30min；
S2. butter fruit fiber and viscose rayon is obtained after handling in step S1 to mix according to mass fraction 5:95；
S3. composite fibre obtained in step S2 is put into rotary drum after hydrophilic treated, shredding, combing, auxiliary net, drawing-off
Formula spun-laced machine carries out spun lacing, including 4 water jets；Using 4 water jet processes, wherein first to the 4th spun lacing pressure is successively
Are as follows: 18kg, 17kg, 32kg, 17kg；
S4. 10 parts of Asian puccoon, 5 parts of the fleece-flower root, 20 parts of ganoderma lucidum, 30 parts of Radix Angelicae Sinensis, 5 parts of Rhizoma Chuanxiong are weighed, with distillation decocting after mixing
It takes 4 hours, is distilled 4 hours under the conditions of 120 DEG C after filtering, obtain high-purity prescription Essence；
S5. using spunlace non-woven cloth obtained in step S3 as carrier, after 4 times of ethanol solution dilutions are added in prescription Essence
By high pressure nozzle jet atomization, the prescription Essence after atomization is evenly distributed on day under the high pressure draught effect of upper and lower convection current
On right fiber spun-laced non-woven fabrics, 20 DEG C of atomization temperature, atomizing pressure 0.8MPa, air column jet air pressure 0.8MPa；
S6. non-woven fabrics is obtained after handling in step S5 and dries 10S under the conditions of 80 DEG C, obtains moisturizing type non-woven fabrics.
Embodiment 2
The present embodiment provides a kind of preparation method of moisturizing type non-woven fabrics, difference from Example 1 referring to embodiment 1
It is: step S1 are as follows: it is 3g/L that butter fruit fiber, which is put into concentration, is impregnated in the NaOH solution that temperature is 60 DEG C, soaking time
For 50min, bath raio 1:10；Emulsifier and viscose rayon after 3:100 is mixed in mass ratio, are put into overflow dyeing machine at heat
Reason, heat treatment temperature are 80 DEG C, time 30min.
Embodiment 3
The present embodiment provides a kind of preparation method of moisturizing type non-woven fabrics, difference from Example 1 referring to embodiment 1
It is: step S1 are as follows: it is 1g/L that butter fruit fiber, which is put into concentration, is impregnated in the NaOH solution that temperature is 40 DEG C, soaking time
For 40min, bath raio 1:8；Emulsifier and viscose rayon after 1:100 is mixed in mass ratio, are put into overflow dyeing machine at heat
Reason, heat treatment temperature are 80 DEG C, time 30min.
Embodiment 4
The present embodiment provides a kind of preparation method of moisturizing type non-woven fabrics, difference from Example 1 referring to embodiment 1
It is: step S1 are as follows: it is 1g/L that butter fruit fiber, which is put into concentration, is impregnated in the NaOH solution that temperature is 80 DEG C, soaking time
For 60min, bath raio 1:8；Emulsifier and viscose rayon after 1:100 is mixed in mass ratio, are put into overflow dyeing machine at heat
Reason, heat treatment temperature are 80 DEG C, time 30min.
Embodiment 5
The present embodiment provides a kind of preparation method of moisturizing type non-woven fabrics, difference from Example 1 referring to embodiment 1
It is: step S1 are as follows: it is 1g/L that butter fruit fiber, which is put into concentration, is impregnated in the NaOH solution that temperature is 60 DEG C, soaking time
For 50min, bath raio 1:10；Emulsifier and viscose rayon after 1:100 is mixed in mass ratio, are put into overflow dyeing machine at heat
Reason, heat treatment temperature are 60 DEG C, time 20min.
Embodiment 6
The present embodiment provides a kind of preparation method of moisturizing type non-woven fabrics, difference from Example 1 referring to embodiment 1
It is: step S1 are as follows: it is 1g/L that butter fruit fiber, which is put into concentration, is impregnated in the NaOH solution that temperature is 60 DEG C, soaking time
For 50min, bath raio 1:10；Emulsifier and viscose rayon after 1:100 is mixed in mass ratio, are put into overflow dyeing machine at heat
Reason, heat treatment temperature are 100 DEG C, time 50min.
Embodiment 7
The present embodiment provides a kind of preparation methods of moisturizing type non-woven fabrics, and its step are as follows:
S1. butter fruit fiber is put into concentration is 1g/L, is impregnated in the NaOH solution that temperature is 60 DEG C, soaking time is
50min, bath raio 1:10；Emulsifier and viscose rayon after 1:100 is mixed in mass ratio, are put into overflow dyeing machine at heat
Reason, heat treatment temperature are 80 DEG C, time 30min；
S2. butter fruit fiber and viscose rayon is obtained after handling in step S1 to mix according to mass fraction 6:94；
S3. composite fibre obtained in step S2 is put into rotary drum after hydrophilic treated, shredding, combing, auxiliary net, drawing-off
Formula spun-laced machine carries out spun lacing, including 4 water jets；Using 4 water jet processes, wherein first to the 4th spun lacing pressure is successively
Are as follows: 16kg, 18kg, 33kg, 18kg；
S4. 5 parts of Asian puccoon, 10 parts of the fleece-flower root, 20 parts of ganoderma lucidum, 20 parts of Rhizoma Chuanxiong, 5 parts of asarum, 10 parts of flax are weighed, is used after mixing
Distillation is decocted in water for oral dose 4 hours, distills 2 hours under the conditions of 140 DEG C after filtering, obtains high-purity prescription Essence；
S5. using spunlace non-woven cloth obtained in step S3 as carrier, 8 times of propylene glycol solution dilutions are added in prescription Essence
Afterwards by high pressure nozzle jet atomization, the prescription Essence after atomization is equal under the high-pressure carbon dioxide airflow function of upper and lower convection current
It is even to be distributed on natural fiber spunlace non-woven cloth, 18 DEG C of atomization temperature, atomizing pressure 0.6MPa, air column jet air pressure 0.6MPa；
S6. non-woven fabrics is obtained after handling in step S5 and dries 15S under the conditions of 70 DEG C, obtains moisturizing type non-woven fabrics.
Embodiment 8
The present embodiment provides a kind of preparation methods of moisturizing type non-woven fabrics, and its step are as follows:
S1. butter fruit fiber is put into concentration is 1g/L, is impregnated in the NaOH solution that temperature is 60 DEG C, soaking time is
50min, bath raio 1:10；Emulsifier and viscose rayon after 1:100 is mixed in mass ratio, are put into overflow dyeing machine at heat
Reason, heat treatment temperature are 80 DEG C, time 30min；
S2. butter fruit fiber and viscose rayon is obtained after handling in step S1 to mix according to mass fraction 8:92；
S3. composite fibre obtained in step S2 is put into rotary drum after hydrophilic treated, shredding, combing, auxiliary net, drawing-off
Formula spun-laced machine carries out spun lacing, including 4 water jets；Using 4 water jet processes, wherein first to the 4th spun lacing pressure is successively
Are as follows: 22kg, 18kg, 35kg, 15kg；
S4. 10 parts of Asian puccoon, 5 parts of the fleece-flower root, 20 parts of ganoderma lucidum, 30 parts of Radix Angelicae Sinensis, 5 parts of Rhizoma Chuanxiong are weighed, with distillation decocting after mixing
It takes 4 hours, is distilled 4 hours under the conditions of 140 DEG C after filtering, obtain high-purity prescription Essence；
S5. using spunlace non-woven cloth obtained in step S3 as carrier, 6 times of benzyl alcohol solution dilutions are added in prescription Essence
Afterwards by high pressure nozzle jet atomization, the prescription Essence after atomization uniformly divides under the high pressure nitrogen airflow function of upper and lower convection current
Cloth is on natural fiber spunlace non-woven cloth, and 24 DEG C of atomization temperature, atomizing pressure 0.8MPa, air column jet air pressure 0.9MPa；
S6. non-woven fabrics is obtained after handling in step S5 and dries 12S under the conditions of 60 DEG C, obtains moisturizing type non-woven fabrics.
Embodiment 9
The present embodiment provides a kind of preparation methods of moisturizing type non-woven fabrics, and its step are as follows:
S1. butter fruit fiber is put into concentration is 1g/L, is impregnated in the NaOH solution that temperature is 60 DEG C, soaking time is
50min, bath raio 1:10；Emulsifier and viscose rayon after 1:100 is mixed in mass ratio, are put into overflow dyeing machine at heat
Reason, heat treatment temperature are 80 DEG C, time 30min；
S2. butter fruit fiber and viscose rayon is obtained after handling in step S1 to mix according to mass fraction 5:95；
S3. composite fibre obtained in step S2 is put into rotary drum after hydrophilic treated, shredding, combing, auxiliary net, drawing-off
Formula spun-laced machine carries out spun lacing, including 4 water jets；Using 4 water jet processes, wherein first to the 4th spun lacing pressure is successively
Are as follows: 20kg, 15kg, 30kg, 18kg；
S4. 10 parts of Asian puccoon, 10 parts of the fleece-flower root, 15 parts of ganoderma lucidum, 20 parts of Radix Angelicae Sinensis, 15 parts of asarum are weighed, distilled water is used after mixing
Decoction 4 hours, distills 3 hours under the conditions of 130 DEG C after filtering, obtains high-purity prescription Essence；
S5. using spunlace non-woven cloth obtained in step S3 as carrier, it is dilute that 4 times of polyglycol solutions are added in prescription Essence
By high pressure nozzle jet atomization after releasing, the prescription Essence after atomization is uniform under the high pressure nitrogen airflow function of upper and lower convection current
It is distributed on natural fiber spunlace non-woven cloth, 22 DEG C of atomization temperature, atomizing pressure 0.7MPa, air column jet air pressure 0.9MPa；
S6. non-woven fabrics is obtained after handling in step S5 and dries 10S under the conditions of 60 DEG C, obtains moisturizing type non-woven fabrics.
Comparative example 1
This comparative example provides a kind of preparation method of moisturizing type non-woven fabrics, difference from Example 1 referring to embodiment 1
It is: butter fruit fiber is not pre-processed in step S1.
Comparative example 2
This comparative example provides a kind of preparation method of moisturizing type non-woven fabrics, difference from Example 1 referring to embodiment 1
Be: butter fruit fiber and viscose rayon mass fraction ratio are 15:85 in step S2.
Comparative example 3
This comparative example provides a kind of preparation method of moisturizing type non-woven fabrics, difference from Example 1 referring to embodiment 1
Be: first to the 4th spun lacing pressure is successively during step S3 spun lacing are as follows: 14kg, 12kg, 20kg, 12kg.
Comparative example 4
This comparative example provides a kind of preparation method of moisturizing type non-woven fabrics, difference from Example 1 referring to embodiment 1
Be: first to the 4th spun lacing pressure is successively during step S3 spun lacing are as follows: 20kg, 22kg, 45kg, 20kg.
Comparative example 5
This comparative example provides a kind of preparation method of moisturizing type non-woven fabrics, difference from Example 1 referring to embodiment 1
It is: not using micro emulsion atomization process in step S5, but spunlace non-woven cloth is dipped in prescription Essence.
The moisturizing type non-woven fabrics prepared below to Examples 1 to 9 and comparative example 1~5 carries out quality testing and skin irritatin
Property experiment and moisturizing experiment.
The experimental result of quality testing is shown in Table 1.
Table 1
Skin irritation test
By taking the tender sensitive skin of children as an example, observation moisturizing type non-woven fabrics is anti-to the irritation and anaphylaxis of skin for this experiment
It answers, provides reference to evaluate its skin-friendly.
(1) skin irritation test is carried out using young rat, is divided into experimental group and control group, by young rat before experiment first 24 hours
Hair shaves off, and the moisturizing type non-woven fabrics of Examples 1 to 9 preparation and the daily skin of young rat are kept in contact 4 hours, after continuous 5 days,
Observing skin, whether there is or not erythema, the allergic reactions such as oedema.
Experimental result are as follows:
In Examples 1 to 9, young rat epidermis has no erythema, the allergic reactions such as oedema.
Moisturizing performance test
5 volunteers are chosen in this experiment, and volunteer is in same working environment, relatively by the women that the age is 25~35
Humidity is 20%, in the environment that temperature is 25 DEG C.First using the moisture of skin of moisture of skin tester measurement volunteer's face
Value, the moisturizing type non-woven fabrics prepared using embodiment 1 and commercially available skin care cloth cleaning face, record is initial respectively, and 2 is small after cleaning
When, 4 hours volunteer's skin of face moisture values after cleaning, the results are shown in Table 2:
Table 2
Above-mentioned experimental result is analyzed it is found that the product that in the present invention prepared by Examples 1 to 9 is superior in quality
Comparative example 1~5, wherein best with the effect of embodiment 1.The thickness of fabric nonwoven cloth containing butter fruit provided by the invention is uniform, stretches
Long rate is good, soft suitable skin, and water absorption rate is high.
After the moisturizing type non-woven fabrics and young rat skin that in the present invention prepared by Examples 1 to 9 continuously contact with, do not occur red
Spot, the medium allergic reaction of water.This explanation, the product skin-friendly is good, non-stimulated to skin safe.
Moisturizing type non-woven fabrics prepared by the present invention can be moisturized the skin effectively, moisturizing water lock.2 hours after use, facial water
Divide almost free of losses, skin can effectively be made to keep water profit；Even in the lower environment of humidity, after 4 hours, facial skin
Skin water loss is less.The present invention can lock the moisture of skin with depth, and skin is made not dry water shortage because of the influence of environment,
The moisture content of skin is kept for a long time and moistens degree.
Obviously, above-described embodiment is only intended to clearly illustrate technical solution of the present invention example, and is not
Restriction to embodiments of the present invention.For those of ordinary skill in the art, on the basis of the above description also
It can make other variations or changes in different ways.There is no necessity and possibility to exhaust all the enbodiments.It is all
Made any modifications, equivalent replacements, and improvements etc. within the spirit and principles in the present invention should be included in right of the present invention and want
Within the protection scope asked.
Claims (10)
1. a kind of preparation method of moisturizing type non-woven fabrics, which is characterized in that the moisturizing type non-woven fabrics is with butter fruit fiber, viscose glue
Fiber is main raw material(s), is prepared through following steps:
S1. it pre-processes: butter fruit fiber and viscose rayon is pre-processed respectively；
S2. raw material mixes: butter fruit fiber pretreated in step S1 and viscose rayon are mixed；
S3. non-woven fabrics is prepared: the hydrophilic treated, shredding, combing, auxiliary net, drawing-off, spun lacing, dry by the composite fibre in step S2
After dry, spunlace non-woven cloth is obtained；
S4. skim the cream off milk liquid: it is decocted after each component in prescription is mixed with distilled water, prescription solution is obtained after filtering, it is molten to prescription
Liquid distilation obtains the prescription Essence of high-purity；
S5. micro emulsion is atomized: using spunlace non-woven cloth obtained in step S3 as carrier, 4 ~ 8 times of prescription Essence addition is organic molten
By high pressure nozzle jet atomization after dilution agent, the prescription Essence after atomization is uniform under the high pressure draught effect of upper and lower convection current
It is distributed on natural fiber spunlace non-woven cloth；
S6. sterile drying: spunlace non-woven cloth is obtained after handling in step S5 and carries out drying and processing in aseptic space, must be moistened
Skin type non-woven fabrics；
Wherein to the pretreating process of butter fruit fiber in step S1 are as follows: butter fruit fiber is put into aqueous slkali and is impregnated；To viscous
The pretreating process of glue fiber are as follows: mix to be put into overflow dyeing machine with emulsifier by viscose rayon and be heat-treated.
2. preparation method according to claim 1, which is characterized in that butter fruit fiber preprocessing process in step S1
In, the alkaline concentration is 1 ~ 3g/L, and temperature is 40 ~ 80 DEG C, and soaking time is 40 ~ 80min, and bath raio is 1:8 ~ 10.
3. preparation method according to claim 2, which is characterized in that the alkaline concentration is 1g/L, and temperature is 60 DEG C,
Soaking time is 50min, bath raio 1:10.
4. moisturizing type non-woven fabrics according to claim 1, which is characterized in that viscose rayon preprocessing process in step S1
In, the emulsifier and viscose rayon mass ratio are 1 ~ 3:100, and the heat treatment temperature is 60 ~ 100 DEG C, the time is 20 ~
50min。
5. the preparation method according to claim 4, which is characterized in that in viscose rayon preprocessing process in step S1,
The emulsifier and viscose rayon mass ratio are 1:100, and the heat treatment temperature is 80 DEG C, time 30min.
6. preparation method according to claim 1, which is characterized in that the matter of butter fruit fiber and viscose rayon in step S2
Amount is than being 5 ~ 10:90 ~ 95.
7. preparation method according to claim 1, which is characterized in that the processing of spun lacing described in step S3 is in rotary drum spun lacing
It is carried out in machine, rotary drum spun-laced machine includes 4 spun lacing steps, and in the 4 spun lacing step, the 1st to the 4th spun lacing pressure is successively
Are as follows: 16 ~ 22kg, 15 ~ 18kg, 30 ~ 35kg, 15 ~ 18kg.
8. preparation method according to claim 1, which is characterized in that micro emulsion atomization process described in step S5 is as follows: mist
Changing temperature is 18 ~ 24 DEG C, and atomizing pressure is 0.6 ~ 0.8MPa, and air column jet air pressure is 0.6 ~ 0.9MPa.
9. preparation method according to claim 1, which is characterized in that organic solvent described in step S5 and prescription Essence
The mixing of 4 ~ 6:1 in mass ratio, it is preferable that the organic solvent is mixed with prescription Essence 4:1 in mass ratio.
10. any one preparation method is prepared according to claim 1 ~ 9 moisturizing non-woven fabrics and its manufacturing the soft towel of cotton
In application.
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