CN109588756A - A kind of preparation method of moringa seeds base wrap bobbin - Google Patents
A kind of preparation method of moringa seeds base wrap bobbin Download PDFInfo
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- CN109588756A CN109588756A CN201910039474.XA CN201910039474A CN109588756A CN 109588756 A CN109588756 A CN 109588756A CN 201910039474 A CN201910039474 A CN 201910039474A CN 109588756 A CN109588756 A CN 109588756A
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- Prior art keywords
- moringa seeds
- moringa
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- preparation
- capsule
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/281—Treatment of tobacco products or tobacco substitutes by chemical substances the action of the chemical substances being delayed
- A24B15/283—Treatment of tobacco products or tobacco substitutes by chemical substances the action of the chemical substances being delayed by encapsulation of the chemical substances
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/301—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by aromatic compounds
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
- A24B15/303—Plant extracts other than tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/36—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances containing a heterocyclic ring
- A24B15/40—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances containing a heterocyclic ring having only oxygen or sulfur as hetero atoms
- A24B15/403—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances containing a heterocyclic ring having only oxygen or sulfur as hetero atoms having only oxygen as hetero atoms
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Botany (AREA)
- Cosmetics (AREA)
Abstract
The present invention provides a kind of preparation methods of moringa seeds base wrap bobbin, and steps are as follows: (1) crushing moringa seeds, be added in solvent, ultrasonic extraction obtains Moringa seed extract；(2) chitosan solution and guar gum solution are mixed, obtain encapsulating solution, the Moringa seed extract that step (1) obtains is added in encapsulating solution, mixed solution is slowly sprayed into calcium lactate solution with spray after stirring and is solidified, moringa seeds embedding capsule is obtained by filtration in washing；(3) the moringa seeds embedding capsule that step (2) obtains is added in the paper pulp for preparing cigarette paper, papermaking cuts to obtain cigarette paper.The present invention makes moringa seeds by oneself and embeds capsule, the nutrition of moringa seeds can be retained in capsule, simultaneously in cigarette aspiration procedure, volume capsule after heated gradually ruptures, the effective component that capsule is wrapped up after rupture is released, and the duct left in system after capsules break can be conducive to the sustained combustion of product as the channel of mass transfer and heat transfer.
Description
Technical field
The present invention relates to cigarette preparation fields, and in particular to a kind of preparation method of moringa seeds base wrap bobbin.
Background technique
Moringa (Moringa) is again a kind of tropical, subtropical zone multi-functional plant, because it has acid by title drumstick tree
Root and gain the name, be the general designation of Moringaceae (Moringaceae) Moringa platymiscium, originate in India.19th century, China introduced a fine variety so far
Moringa (Moringaoleifera), India's improvement kind Moringa (PKM1 and PKM2) and African Moringa are cultivated
(Moringastenopetala) 3 kinds, main plantation is in Guangdong, Guangxi, Hainan, Fujian, Yunnan, Sichuan and Chongqing
Etc. ground.Root, stem, leaf, flower, branch, seed and the bark of Moringa nutritional ingredient all rich in and medical active, are a kind of high
Fiber, high protein, homovitamin, low fat, low cholesterol plant, there is enhancing physical strength, adjust blood pressure, is control blood glucose, slow
Solution insomnia, inhibits the effect of germ at treatment anaemia.
Moringa seeds are spherical in shape, and diameter about lcm, quality is about 0.3 g, are rich in protein, grease, vitamin, mineral element
Etc. nutritional ingredients, have multiple biological activities.Contain natural plants phenols and polysaccharose substance in moringa seeds, has good anti-
Oxidation activity and stability are the good sources of the antioxidant for food industry.In recent years, unique edible in view of Moringa
Function and medical value, grinding to make internal disorder or usurp and at home and abroad cause many concerns as novel non-traditional food sources.However at present
Application of the Moringa in food focuses mostly in using leaf of Moringa as the food development of raw material, such as Moringa drink, Moringa flower cake, Moringa
Yoghourt etc., since moringa seeds are greater than the contribution to cigarette smell to the contribution of mouthfeel, the application in tobacco needs more
Research and development.
Patent 201310158174. 6 and 201310159094. 2 respectively describes the mixture by ethyl alcohol and oil ben
The application in cigarette shreds and cigarette filter rod is added as flavouring essence for tobacco.It is more that patent 201510002703. 2 discloses Moringa
The preparation method of hole particle and cigarette filter rod containing the Moringa porous particle.
Application in tobacco is also embodied on flavouring essence for tobacco, and invention 201810011289.5 discloses a kind of oil ben day
Right peppermint flavouring essence for tobacco, is added in tobacco, and taste, refrigerant throat-moistening are inhaled in correction in flue gas；Invention 201810012252.4 discloses
A kind of oil ben natural coffee flavouring essence for tobacco is added in tobacco and coordinates with tobacco, sets off cigarette perfume by contrast, improves and inhales taste, but essence
Class is added in cigarette to guarantee its lasting fragrance, usually adds some chemical substances；Patent 201510336852.2 is public
A kind of moringa seeds triacetyl glycerine extract and its application in cigarette are opened, by moringa seeds triacetyl glycerine extract
It after being configured to solution, is uniformly sprayed on filter stick tow and cigarette filter rod is made, then cigarette is made filter stick to contain moringa seeds effective
The cigarette of ingredient can significantly increase the sweet sense of flue gas, sweet taste is enable to be maintained for a long time in the oral cavity.
Moringa seeds are full of nutrition and balanced, have anti-oxidant, antibacterial, anticancer, reducing blood sugar and blood lipid, protect liver, protection skin etc.
Multiple biological activities are the potential sources of nourishing reinforced food.Tobacco is as a kind of special food, in the exploitation benefit of moringa seeds
In, it should more focus on the double grading of moringa seeds food medicine value, application of the Devoting Major Efforts To Developing moringa seeds in tobacco product improves
The novelty and diversity of its product, so that moringa seeds obtain more extensive, systematic difference in tobacco.
Summary of the invention
The invention proposes a kind of preparation methods of moringa seeds base wrap bobbin, solve existing moringa seeds in cigarette field
Application it is insufficient, the fragrance of Moringa seed extract and nutrition can be remained, not influence the suction performance of cigarette.
It realizes the technical scheme is that a kind of preparation method of moringa seeds base wrap bobbin, steps are as follows:
(1) moringa seeds are crushed, is added in solvent, ultrasonic extraction obtains Moringa seed extract；
(2) chitosan solution and guar gum solution are mixed, obtains encapsulating solution, the Moringa seed extract that step (1) is obtained
It is added in encapsulating solution, mixed solution is slowly sprayed into calcium lactate solution with spray after stirring and is solidified, washing is filtered
Capsule is embedded to moringa seeds；
(3) the moringa seeds embedding capsule that step (2) obtains is added in the paper pulp for preparing cigarette paper, papermaking cuts to obtain cigarette
Paper.
Moringa seeds are crushed to 40-70 mesh in the step (1), and solvent volume is than the mixing for ethyl alcohol, ethyl acetate and water
Solvent, the volume ratio of ethyl alcohol, ethyl acetate and water are (5-20): 1:(5-10), ultrasonic temperature is 55-70 DEG C, and ultrasonic time is
3-7h。
The mass concentration of chitosan solution and guar gum solution is 1-3% and 1-5% respectively in the step (2).
The volume ratio of Moringa seed extract and encapsulating solution is 1:(5-20 in the step (2)).
The concentration of calcium lactate solution is 0.05-0.5mol/L in the step (2).
The additive amount of moringa seeds embedding capsule is the 3-10% of pulp quality in the step (3).
The cigarette paper circumference is 42.2-24.5mm, length 84-84.2mm.
The cigarette paper circumference is 17.5-18mm, length 96-100mm.
The cigarette paper circumference is 20-20.5mm, length 84-85mm.
The beneficial effects of the present invention are:
(1) Moringa seed extract is added in cigarette paper preparation process by the present invention, can directly be covered cigarette paper in perfume (or spice) before suction
It is convenient and practical on cigarette；The taste of cigarette suction can be improved simultaneously；
(2) present invention self-control moringa seeds embed capsule, and the nutrition of moringa seeds can be retained in capsule, will not be with time flow
Die and be lost, while in cigarette aspiration procedure, it is heated after volume capsule gradually rupture, after rupture capsule wrap up it is effective at
Divide the duct for being released, and leaving in system after capsules break that can be conducive to product as the channel of mass transfer and heat transfer
Sustained combustion；
(3) for the first time wrap bobbin is made in moringa seeds by the present invention, is applied in the addition of whole branch cigarette, the moringa seeds base volume cigarette paper
Cylinder can be suitable for conventional cigarette in the market, ramuscule and on the various model Cigarettes such as branch, be that consumer improves one kind
Beneficial selection.
Specific embodiment
Below in conjunction with the embodiment of the present invention, technical solution of the present invention is clearly and completely described, it is clear that institute
The embodiment of description is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention,
Those of ordinary skill in the art's every other embodiment obtained under that premise of not paying creative labor, belongs to this hair
The range of bright protection.
Embodiment 1
A kind of preparation method of moringa seeds base wrap bobbin, steps are as follows:
(1) moringa seeds are crushed to 40 mesh, are added to the in the mixed solvent of ethyl alcohol, ethyl acetate and water, ethyl alcohol, ethyl acetate and
The volume ratio of water is 5:1:5, and ultrasound 3h extracts to obtain Moringa seed extract at 55 DEG C；
(2) 1% chitosan solution of mass concentration and 1% guar gum solution of mass concentration are mixed, encapsulating solution is obtained, by step
(1) the Moringa seed extract obtained is added in encapsulating solution, and the volume ratio of Moringa seed extract and encapsulating solution is 1:5, is stirred
Mixed solution is slowly sprayed into 0.05mol/L calcium lactate solution with spray after mixing and is solidified, moringa seeds packet is obtained by filtration in washing
Bury capsule；
(3) the moringa seeds embedding capsule that step (2) obtains is added in the paper pulp for preparing cigarette paper, papermaking cuts to obtain cigarette
Paper.
The present embodiment cigarette paper circumference is 42.2mm, length 84mm.
Embodiment 2
A kind of preparation method of moringa seeds base wrap bobbin, steps are as follows:
(1) moringa seeds are crushed to 60 mesh, are added to the in the mixed solvent of ethyl alcohol, ethyl acetate and water, ethyl alcohol, ethyl acetate and
The volume ratio of water is 10:1:10, and ultrasound 5h extracts to obtain Moringa seed extract at 65 DEG C；
(2) 2% chitosan solution of mass concentration and 3% guar gum solution of mass concentration are mixed, encapsulating solution is obtained, by step
(1) the Moringa seed extract obtained is added in encapsulating solution, and the volume ratio of Moringa seed extract and encapsulating solution is 1:10, is stirred
Mixed solution is slowly sprayed into 0.3mol/L calcium lactate solution with spray after mixing and is solidified, moringa seeds embedding is obtained by filtration in washing
Capsule；
(3) the moringa seeds embedding capsule that step (2) obtains is added in the paper pulp for preparing cigarette paper, papermaking cuts to obtain cigarette
Paper.
The present embodiment cigarette paper circumference is 17.5mm, length 96mm.
Embodiment 3
A kind of preparation method of moringa seeds base wrap bobbin, steps are as follows:
(1) moringa seeds are crushed to 70 mesh, are added to the in the mixed solvent of ethyl alcohol, ethyl acetate and water, ethyl alcohol, ethyl acetate and
The volume ratio of water is 20:1:10, and ultrasound 7h extracts to obtain Moringa seed extract at 70 DEG C；
(2) 3% chitosan solution of mass concentration and 5% guar gum solution of mass concentration are mixed, encapsulating solution is obtained, by step
(1) the Moringa seed extract obtained is added in encapsulating solution, and the volume ratio of Moringa seed extract and encapsulating solution is 1:20, is stirred
Mixed solution is slowly sprayed into 0.5mol/L calcium lactate solution with spray after mixing and is solidified, moringa seeds embedding is obtained by filtration in washing
Capsule；
(3) the moringa seeds embedding capsule that step (2) obtains is added in the paper pulp for preparing cigarette paper, papermaking cuts to obtain cigarette
Paper.
The present embodiment cigarette paper circumference is 20mm, length 84mm.
Embodiment 4
A kind of preparation method of moringa seeds base wrap bobbin, steps are as follows:
(1) moringa seeds are crushed to 70 mesh, are added to the in the mixed solvent of ethyl alcohol, ethyl acetate and water, ethyl alcohol, ethyl acetate and
The volume ratio of water is 15:1:8, and ultrasound 5h extracts to obtain Moringa seed extract at 70 DEG C；
(2) 3% chitosan solution of mass concentration and 3% guar gum solution of mass concentration are mixed, encapsulating solution is obtained, by step
(1) the Moringa seed extract obtained is added in encapsulating solution, and the volume ratio of Moringa seed extract and encapsulating solution is 1:15, is stirred
Mixed solution is slowly sprayed into 0.1mol/L calcium lactate solution with spray after mixing and is solidified, moringa seeds embedding is obtained by filtration in washing
Capsule；
(3) the moringa seeds embedding capsule that step (2) obtains is added in the paper pulp for preparing cigarette paper, papermaking cuts to obtain cigarette
Paper.
The present embodiment cigarette paper circumference is 20.5mm, length 85mm.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention
Within mind and principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.
Claims (9)
1. a kind of preparation method of moringa seeds base wrap bobbin, it is characterised in that steps are as follows:
(1) moringa seeds are crushed, is added in solvent, ultrasonic extraction obtains Moringa seed extract；
(2) chitosan solution and guar gum solution are mixed, obtains encapsulating solution, the Moringa seed extract that step (1) is obtained
It is added in encapsulating solution, mixed solution is slowly sprayed into calcium lactate solution with spray after stirring and is solidified, washing is filtered
Capsule is embedded to moringa seeds；
(3) the moringa seeds embedding capsule that step (2) obtains is added in the paper pulp for preparing cigarette paper, papermaking cuts to obtain cigarette
Paper.
2. the preparation method of moringa seeds base wrap bobbin according to claim 1, it is characterised in that: in the step (1)
Moringa seeds are crushed to 40-70 mesh, and solvent volume is than the mixed solvent for ethyl alcohol, ethyl acetate and water, ethyl alcohol, ethyl acetate and water
Volume ratio be (5-20): 1:(5-10), ultrasonic temperature be 55-70 DEG C, ultrasonic time 3-7h.
3. the preparation method of moringa seeds base wrap bobbin according to claim 1, it is characterised in that: in the step (2)
The mass concentration of chitosan solution and guar gum solution is 1-3% and 1-5% respectively.
4. the preparation method of moringa seeds base wrap bobbin according to claim 1, it is characterised in that: in the step (2)
The volume ratio of Moringa seed extract and encapsulating solution is 1:(5-20).
5. the preparation method of moringa seeds base wrap bobbin according to claim 1, it is characterised in that: in the step (2)
The concentration of calcium lactate solution is 0.05-0.5mol/L.
6. the preparation method of moringa seeds base wrap bobbin according to claim 1, it is characterised in that: in the step (3)
The additive amount that moringa seeds embed capsule is the 3-10% of pulp quality.
7. the preparation method of moringa seeds base wrap bobbin according to claim 1-6, it is characterised in that: the volume
Cigarette paper circumference is 42.2-24.5mm, length 84-84.2mm.
8. the preparation method of moringa seeds base wrap bobbin according to claim 1-6, it is characterised in that: the volume
Cigarette paper circumference is 17.5-18mm, length 96-100mm.
9. the preparation method of moringa seeds base wrap bobbin according to claim 1-6, it is characterised in that: the volume
Cigarette paper circumference is 20-20.5mm, length 84-85mm.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2018115257308 | 2018-12-13 | ||
| CN201811525730 | 2018-12-13 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109588756A true CN109588756A (en) | 2019-04-09 |
Family
ID=65965311
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| Application Number | Title | Priority Date | Filing Date |
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| CN201910039474.XA Pending CN109588756A (en) | 2018-12-13 | 2019-01-16 | A kind of preparation method of moringa seeds base wrap bobbin |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115005493A (en) * | 2022-06-08 | 2022-09-06 | 吉林烟草工业有限责任公司 | Bean-flavor characteristic extract, preparation method thereof and cigarette |
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| CN101925403A (en) * | 2008-01-25 | 2010-12-22 | R.J.雷诺兹烟草公司 | Process for manufacturing breakable capsules useful in tobacco products |
| CN102824887A (en) * | 2012-09-14 | 2012-12-19 | 云南烟草科学研究院 | Preparation method of controlled-release soft capsules for cigarettes |
| CN103881816A (en) * | 2014-03-28 | 2014-06-25 | 中国热带农业科学院农产品加工研究所 | Vanilla extract microcapsule as well as preparation method and application thereof |
| CN104005293A (en) * | 2014-05-30 | 2014-08-27 | 滁州卷烟材料厂 | Raw tipping paper capable of reducing injuries and resisting oxidization and preparation method thereof |
| CN105239462A (en) * | 2015-09-25 | 2016-01-13 | 云南中烟工业有限责任公司 | Flavoring lining paper for cigarettes |
| WO2018203340A1 (en) * | 2017-05-02 | 2018-11-08 | Pasupathi Kalyan | Healthy cigarette |
-
2019
- 2019-01-16 CN CN201910039474.XA patent/CN109588756A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101925403A (en) * | 2008-01-25 | 2010-12-22 | R.J.雷诺兹烟草公司 | Process for manufacturing breakable capsules useful in tobacco products |
| CN102824887A (en) * | 2012-09-14 | 2012-12-19 | 云南烟草科学研究院 | Preparation method of controlled-release soft capsules for cigarettes |
| CN103881816A (en) * | 2014-03-28 | 2014-06-25 | 中国热带农业科学院农产品加工研究所 | Vanilla extract microcapsule as well as preparation method and application thereof |
| CN104005293A (en) * | 2014-05-30 | 2014-08-27 | 滁州卷烟材料厂 | Raw tipping paper capable of reducing injuries and resisting oxidization and preparation method thereof |
| CN105239462A (en) * | 2015-09-25 | 2016-01-13 | 云南中烟工业有限责任公司 | Flavoring lining paper for cigarettes |
| WO2018203340A1 (en) * | 2017-05-02 | 2018-11-08 | Pasupathi Kalyan | Healthy cigarette |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115005493A (en) * | 2022-06-08 | 2022-09-06 | 吉林烟草工业有限责任公司 | Bean-flavor characteristic extract, preparation method thereof and cigarette |
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Application publication date: 20190409 |